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Information card for entry 4060140
Preview
| Coordinates | 4060140.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C31 H48 Li O P Si2 |
|---|---|
| Calculated formula | C31 H48 Li O P Si2 |
| Title of publication | eta5- Rh(I) Complexes of a lamba4-Phosphinine anion: Syntheses, X-ray Crystal Structures and Application in the Catalyzed Hydroformylation of Olefins |
| Authors of publication | A. Moores; N. Mezaiiles; L. Ricard; P. Le Floch |
| Journal of publication | Organometallics |
| Year of publication | 2005 |
| a | 10.101 ± 0.005 Å |
| b | 18.754 ± 0.005 Å |
| c | 34.757 ± 0.005 Å |
| α | 90 ± 0.005° |
| β | 94.11 ± 0.005° |
| γ | 90 ± 0.005° |
| Cell volume | 6567 ± 4 Å3 |
| Cell temperature | 150 ± 1 K |
| Ambient diffraction temperature | 150 ± 1 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0798 |
| Residual factor for significantly intense reflections | 0.0559 |
| Weighted residual factors for significantly intense reflections | 0.1468 |
| Weighted residual factors for all reflections included in the refinement | 0.1649 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.032 |
| Diffraction radiation wavelength | 0.71069 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
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Users of the data should acknowledge the original authors of the
structural data.