#------------------------------------------------------------------------------
#$Date: 2008-01-13 22:15:36 +0000 (Sun, 13 Jan 2008) $
#$Revision: 14 $
#$URL: svn://www.crystallography.net/cod/cif/4/4060498.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4060498
_journal_name_full  'Organometallics'
_journal_year       2005
_chemical_formula_moiety  'C42 H46 P2 Ru 2+, 2 F6 Sb -, C H2 Cl2'
_chemical_formula_sum 'C43 H48 Cl2 F12 P2 Ru Sb2'
_chemical_formula_weight  1270.22
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'C 2/c'
loop_
_symmetry_equiv_pos_as_xyz
 'x, y, z'
 '-x, y, -z+1/2'
 'x+1/2, y+1/2, z'
 '-x+1/2, y+1/2, -z+1/2'
 '-x, -y, -z'
 'x, -y, z-1/2'
 '-x+1/2, -y+1/2, -z'
 'x+1/2, -y+1/2, z-1/2'
_cell_length_a  24.3186(11)
_cell_length_b  29.7261(13)
_cell_length_c  16.5645(7)
_cell_angle_alpha  90.00
_cell_angle_beta  123.608(1)
_cell_angle_gamma  90.00
_cell_volume  9972.8(8)
_cell_formula_units_Z  8
_cell_measurement_temperature  150(2)
_exptl_crystal_density_diffrn  1.692
_diffrn_ambient_temperature  150(2)
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ru Ru 0.72174(3) 0.59663(2) 0.64187(4) 0.01985(17) Uani 1 1 d . . .
P1 P 0.63822(10) 0.64842(7) 0.59555(15) 0.0224(5) Uani 1 1 d . . .
P2 P 0.78748(10) 0.63104(7) 0.79151(15) 0.0247(5) Uani 1 1 d . . .
C1 C 0.6154(5) 0.5121(3) 0.6380(8) 0.051(3) Uani 1 1 d . . .
H1A H 0.6116 0.4793 0.6323 0.077 Uiso 1 1 calc R . .
H1B H 0.5740 0.5258 0.5859 0.077 Uiso 1 1 calc R . .
H1C H 0.6241 0.5213 0.7009 0.077 Uiso 1 1 calc R . .
C2 C 0.6708(5) 0.5273(3) 0.6302(7) 0.037(2) Uani 1 1 d . . .
C3 C 0.6605(4) 0.5398(3) 0.5411(7) 0.036(2) Uani 1 1 d . . .
H3 H 0.6166 0.5436 0.4866 0.043 Uiso 1 1 calc R . .
C4 C 0.7132(4) 0.5468(3) 0.5299(6) 0.029(2) Uani 1 1 d . . .
H4 H 0.7041 0.5546 0.4679 0.035 Uiso 1 1 calc R . .
C5 C 0.7788(4) 0.5426(3) 0.6086(6) 0.0244(18) Uani 1 1 d . . .
C6 C 0.7885(4) 0.5349(3) 0.7012(6) 0.029(2) Uani 1 1 d . . .
H6 H 0.8319 0.5342 0.7582 0.035 Uiso 1 1 calc R . .
C7 C 0.7331(4) 0.5283(3) 0.7074(7) 0.032(2) Uani 1 1 d . . .
H7 H 0.7407 0.5245 0.7697 0.039 Uiso 1 1 calc R . .
C8 C 0.8352(4) 0.5418(3) 0.5947(6) 0.033(2) Uani 1 1 d . . .
H8 H 0.8242 0.5635 0.5415 0.040 Uiso 1 1 calc R . .
C9 C 0.9020(4) 0.5544(4) 0.6813(7) 0.048(3) Uani 1 1 d . . .
H9A H 0.9346 0.5532 0.6640 0.072 Uiso 1 1 calc R . .
H9B H 0.9146 0.5333 0.7343 0.072 Uiso 1 1 calc R . .
H9C H 0.9004 0.5850 0.7019 0.072 Uiso 1 1 calc R . .
C10 C 0.8371(6) 0.4942(4) 0.5589(9) 0.066(3) Uani 1 1 d . . .
H10A H 0.8728 0.4926 0.5481 0.099 Uiso 1 1 calc R . .
H10B H 0.7949 0.4878 0.4981 0.099 Uiso 1 1 calc R . .
H10C H 0.8450 0.4720 0.6079 0.099 Uiso 1 1 calc R . .
C11 C 0.7911(4) 0.6899(3) 0.7672(6) 0.031(2) Uani 1 1 d . . .
C12 C 0.7724(4) 0.6975(3) 0.6774(6) 0.0251(19) Uani 1 1 d . . .
C13 C 0.7495(4) 0.6610(3) 0.6031(6) 0.0238(18) Uani 1 1 d . . .
C14 C 0.6803(4) 0.6519(3) 0.5347(6) 0.0263(19) Uani 1 1 d . . .
C15 C 0.8179(5) 0.7250(3) 0.8477(7) 0.052(3) Uani 1 1 d . . .
H15A H 0.8290 0.7104 0.9081 0.079 Uiso 1 1 calc R . .
H15B H 0.7843 0.7481 0.8297 0.079 Uiso 1 1 calc R . .
H15C H 0.8576 0.7389 0.8571 0.079 Uiso 1 1 calc R . .
C16 C 0.7736(4) 0.7442(3) 0.6401(7) 0.037(2) Uani 1 1 d . . .
H16A H 0.7567 0.7424 0.5711 0.055 Uiso 1 1 calc R . .
H16B H 0.8190 0.7555 0.6762 0.055 Uiso 1 1 calc R . .
H16C H 0.7458 0.7647 0.6492 0.055 Uiso 1 1 calc R . .
C17 C 0.7938(4) 0.6580(3) 0.5641(6) 0.033(2) Uani 1 1 d . . .
H17A H 0.8395 0.6649 0.6162 0.049 Uiso 1 1 calc R . .
H17B H 0.7786 0.6796 0.5111 0.049 Uiso 1 1 calc R . .
H17C H 0.7917 0.6275 0.5400 0.049 Uiso 1 1 calc R . .
C18 C 0.6478(4) 0.6438(3) 0.4285(6) 0.042(2) Uani 1 1 d . . .
H18A H 0.6006 0.6381 0.3985 0.063 Uiso 1 1 calc R . .
H18B H 0.6681 0.6176 0.4189 0.063 Uiso 1 1 calc R . .
H18C H 0.6534 0.6703 0.3986 0.063 Uiso 1 1 calc R . .
C19 C 0.6354(4) 0.7009(3) 0.6485(6) 0.0277(19) Uani 1 1 d . . .
C20 C 0.6410(5) 0.7056(3) 0.7349(7) 0.047(3) Uani 1 1 d . . .
H20 H 0.6515 0.6800 0.7754 0.057 Uiso 1 1 calc R . .
C21 C 0.6321(6) 0.7459(4) 0.7639(9) 0.066(3) Uani 1 1 d . . .
H21 H 0.6348 0.7479 0.8233 0.079 Uiso 1 1 calc R . .
C22 C 0.6193(6) 0.7833(4) 0.7104(9) 0.066(3) Uani 1 1 d . . .
H22 H 0.6159 0.8117 0.7334 0.079 Uiso 1 1 calc R . .
C23 C 0.6113(6) 0.7794(3) 0.6217(9) 0.063(3) Uani 1 1 d . . .
H23 H 0.5994 0.8052 0.5815 0.076 Uiso 1 1 calc R . .
C24 C 0.6204(5) 0.7389(3) 0.5901(8) 0.049(3) Uani 1 1 d . . .
H24 H 0.6165 0.7368 0.5299 0.058 Uiso 1 1 calc R . .
C25 C 0.5518(4) 0.6328(3) 0.5206(6) 0.033(2) Uani 1 1 d . . .
C26 C 0.5261(4) 0.6091(3) 0.5635(7) 0.042(2) Uani 1 1 d . . .
H26 H 0.5544 0.5992 0.6286 0.050 Uiso 1 1 calc R . .
C27 C 0.4601(5) 0.5997(4) 0.5134(10) 0.062(3) Uani 1 1 d . . .
H27 H 0.4429 0.5826 0.5430 0.075 Uiso 1 1 calc R . .
C28 C 0.4182(5) 0.6152(4) 0.4190(9) 0.063(3) Uani 1 1 d . . .
H28 H 0.3722 0.6094 0.3848 0.076 Uiso 1 1 calc R . .
C29 C 0.4429(5) 0.6386(4) 0.3755(8) 0.062(3) Uani 1 1 d . . .
H29 H 0.4139 0.6488 0.3108 0.075 Uiso 1 1 calc R . .
C30 C 0.5103(4) 0.6477(3) 0.4250(6) 0.043(2) Uani 1 1 d . . .
H30 H 0.5276 0.6637 0.3943 0.052 Uiso 1 1 calc R . .
C31 C 0.7603(4) 0.6233(3) 0.8749(6) 0.030(2) Uani 1 1 d . . .
C32 C 0.7999(5) 0.6403(4) 0.9691(7) 0.053(3) Uani 1 1 d . . .
H32 H 0.8399 0.6558 0.9897 0.064 Uiso 1 1 calc R . .
C33 C 0.7794(6) 0.6340(4) 1.0324(8) 0.068(3) Uani 1 1 d . . .
H33 H 0.8055 0.6452 1.0968 0.081 Uiso 1 1 calc R . .
C34 C 0.7221(6) 0.6118(5) 1.0014(9) 0.071(4) Uani 1 1 d . . .
H34 H 0.7090 0.6071 1.0452 0.085 Uiso 1 1 calc R . .
C35 C 0.6831(5) 0.5963(4) 0.9088(8) 0.051(3) Uani 1 1 d . . .
H35 H 0.6423 0.5819 0.8873 0.061 Uiso 1 1 calc R . .
C36 C 0.7032(4) 0.6016(3) 0.8480(6) 0.032(2) Uani 1 1 d . . .
H36 H 0.6766 0.5897 0.7842 0.039 Uiso 1 1 calc R . .
C37 C 0.8738(4) 0.6124(3) 0.8675(6) 0.031(2) Uani 1 1 d . . .
C38 C 0.8894(4) 0.5738(3) 0.9234(6) 0.040(2) Uani 1 1 d . . .
H38 H 0.8560 0.5577 0.9243 0.048 Uiso 1 1 calc R . .
C39 C 0.9541(4) 0.5590(4) 0.9778(7) 0.048(3) Uani 1 1 d . . .
H39 H 0.9652 0.5332 1.0176 0.058 Uiso 1 1 calc R . .
C40 C 1.0025(5) 0.5810(4) 0.9753(7) 0.051(3) Uani 1 1 d . . .
H40 H 1.0466 0.5701 1.0114 0.061 Uiso 1 1 calc R . .
C41 C 0.9864(4) 0.6187(3) 0.9205(7) 0.044(2) Uani 1 1 d . . .
H41 H 1.0204 0.6342 0.9202 0.053 Uiso 1 1 calc R . .
C42 C 0.9233(4) 0.6352(3) 0.8656(6) 0.035(2) Uani 1 1 d . . .
H42 H 0.9136 0.6615 0.8273 0.042 Uiso 1 1 calc R . .
Sb1 Sb 0.20895(3) 0.594514(19) 0.18510(4) 0.02720(16) Uani 1 1 d U . .
F1 F 0.2670(3) 0.5775(2) 0.1497(4) 0.0665(17) Uani 1 1 d U . .
F2 F 0.1508(3) 0.6100(2) 0.2205(4) 0.0583(16) Uani 1 1 d U . .
F3 F 0.2538(3) 0.64898(18) 0.2343(5) 0.0736(19) Uani 1 1 d U . .
F4 F 0.1525(2) 0.62024(18) 0.0623(3) 0.0422(13) Uani 1 1 d U . .
F5 F 0.1642(3) 0.53915(17) 0.1358(4) 0.0541(15) Uani 1 1 d U . .
F6 F 0.2665(2) 0.56746(15) 0.3067(3) 0.0390(12) Uani 1 1 d U . .
Sb2 Sb 0.5000 0.48885(3) 0.7500 0.0353(2) Uani 1 2 d SU . .
F7 F 0.5112(3) 0.4891(4) 0.8702(5) 0.127(4) Uani 1 1 d U A .
F8 F 0.5701(14) 0.4520(10) 0.7997(15) 0.121(12) Uani 0.39(2) 1 d PU A 1
F9 F 0.5597(13) 0.5356(10) 0.785(2) 0.137(11) Uani 0.39(2) 1 d PU A 1
F10 F 0.5909(6) 0.4925(8) 0.8138(9) 0.109(8) Uani 0.61(2) 1 d PU A 2
F11 F 0.5000 0.4301(7) 0.7500 0.153(9) Uani 0.61(2) 2 d SPU A 2
F12 F 0.5000 0.5474(8) 0.7500 0.208(12) Uani 0.61(2) 2 d SPU A 2
Sb3 Sb 0.5000 0.76521(3) 0.2500 0.0302(2) Uani 1 2 d SU . .
F13 F 0.5000 0.8269(3) 0.2500 0.134(5) Uani 1 2 d SU . .
F14 F 0.4206(3) 0.7628(3) 0.1314(5) 0.100(3) Uani 1 1 d U . .
F15 F 0.5438(3) 0.7644(2) 0.1859(5) 0.0664(17) Uani 1 1 d U . .
F16 F 0.5000 0.7032(3) 0.2500 0.078(3) Uani 1 2 d SU . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
Ru 0.0189(3) 0.0202(3) 0.0198(3) 0.0037(3) 0.0103(3) 0.0000(3)
P1 0.0215(11) 0.0221(11) 0.0234(11) 0.0011(9) 0.0123(9) 0.0006(9)
P2 0.0270(11) 0.0238(11) 0.0208(11) 0.0039(9) 0.0117(10) -0.0020(9)
C1 0.074(7) 0.023(5) 0.094(8) -0.012(5) 0.070(7) -0.018(5)
C2 0.053(6) 0.021(5) 0.053(6) 0.000(4) 0.039(6) 0.000(4)
C3 0.035(5) 0.023(5) 0.050(6) -0.007(4) 0.025(5) -0.004(4)
C4 0.038(5) 0.022(4) 0.031(5) -0.020(4) 0.021(4) -0.010(4)
C5 0.023(4) 0.020(4) 0.029(5) -0.004(4) 0.014(4) -0.004(3)
C6 0.029(5) 0.021(4) 0.045(6) 0.000(4) 0.025(4) 0.000(4)
C7 0.046(6) 0.021(5) 0.043(6) 0.009(4) 0.032(5) 0.000(4)
C8 0.043(5) 0.029(5) 0.042(5) 0.004(4) 0.033(5) 0.004(4)
C9 0.024(5) 0.068(7) 0.049(6) 0.005(5) 0.019(5) 0.007(5)
C10 0.075(8) 0.056(7) 0.090(9) -0.015(6) 0.059(8) 0.010(6)
C11 0.030(5) 0.030(5) 0.035(5) -0.004(4) 0.019(4) -0.003(4)
C12 0.023(4) 0.026(5) 0.035(5) 0.012(4) 0.021(4) 0.009(4)
C13 0.032(5) 0.021(4) 0.029(5) 0.014(4) 0.023(4) 0.011(4)
C14 0.029(5) 0.032(5) 0.023(4) 0.013(4) 0.017(4) 0.010(4)
C15 0.068(7) 0.044(6) 0.042(6) -0.024(5) 0.029(6) -0.028(5)
C16 0.037(5) 0.032(5) 0.043(6) 0.011(4) 0.024(5) 0.004(4)
C17 0.041(5) 0.027(5) 0.047(6) 0.014(4) 0.034(5) 0.006(4)
C18 0.039(5) 0.049(6) 0.040(6) 0.009(5) 0.023(5) 0.014(5)
C19 0.029(5) 0.021(4) 0.035(5) 0.004(4) 0.019(4) 0.008(4)
C20 0.068(7) 0.039(6) 0.055(7) -0.009(5) 0.047(6) -0.002(5)
C21 0.100(10) 0.038(7) 0.063(8) -0.012(6) 0.047(8) -0.008(6)
C22 0.078(9) 0.049(7) 0.085(9) -0.024(7) 0.054(8) 0.002(6)
C23 0.069(8) 0.020(5) 0.098(10) 0.008(6) 0.045(8) -0.004(5)
C24 0.050(6) 0.038(6) 0.065(7) -0.003(5) 0.036(6) 0.008(5)
C25 0.024(5) 0.030(5) 0.030(5) -0.001(4) 0.006(4) -0.006(4)
C26 0.028(5) 0.042(6) 0.051(6) 0.004(5) 0.020(5) -0.001(4)
C27 0.036(6) 0.062(8) 0.094(10) -0.001(7) 0.039(7) -0.002(6)
C28 0.027(6) 0.071(8) 0.073(9) -0.014(7) 0.016(6) -0.012(6)
C29 0.027(6) 0.099(10) 0.038(6) 0.005(6) 0.004(5) 0.013(6)
C30 0.026(5) 0.066(7) 0.033(5) 0.004(5) 0.013(4) -0.002(5)
C31 0.034(5) 0.038(5) 0.020(4) 0.004(4) 0.018(4) -0.003(4)
C32 0.059(7) 0.079(8) 0.032(6) -0.010(5) 0.031(5) -0.021(6)
C33 0.084(9) 0.100(10) 0.039(6) -0.019(6) 0.047(7) -0.014(8)
C34 0.077(9) 0.103(10) 0.054(8) 0.018(7) 0.050(7) -0.002(8)
C35 0.048(6) 0.074(8) 0.059(7) 0.019(6) 0.047(6) 0.009(6)
C36 0.038(5) 0.039(5) 0.029(5) 0.013(4) 0.025(4) 0.002(4)
C37 0.017(4) 0.045(5) 0.018(4) -0.002(4) 0.002(4) -0.003(4)
C38 0.028(5) 0.062(7) 0.034(5) 0.017(5) 0.019(4) 0.006(5)
C39 0.028(5) 0.063(7) 0.039(6) 0.025(5) 0.010(5) 0.015(5)
C40 0.032(6) 0.069(7) 0.044(6) 0.013(6) 0.016(5) 0.009(5)
C41 0.022(5) 0.056(6) 0.052(6) -0.004(5) 0.020(5) -0.015(5)
C42 0.029(5) 0.031(5) 0.041(5) -0.003(4) 0.017(4) -0.014(4)
Sb1 0.0240(3) 0.0259(3) 0.0287(3) 0.0034(2) 0.0127(3) 0.0025(2)
F1 0.046(3) 0.105(5) 0.063(4) 0.022(4) 0.039(3) 0.030(3)
F2 0.063(4) 0.066(4) 0.065(4) 0.014(3) 0.047(3) 0.026(3)
F3 0.070(4) 0.028(3) 0.081(4) 0.003(3) 0.016(4) -0.018(3)
F4 0.033(3) 0.050(3) 0.033(3) 0.026(2) 0.012(2) 0.013(2)
F5 0.039(3) 0.033(3) 0.049(3) -0.002(2) -0.001(3) -0.003(2)
F6 0.045(3) 0.029(3) 0.025(3) 0.004(2) 0.007(2) 0.004(2)
Sb2 0.0271(5) 0.0425(5) 0.0276(5) 0.000 0.0097(4) 0.000
F7 0.050(4) 0.290(11) 0.045(4) -0.011(5) 0.029(4) 0.045(6)
F8 0.13(2) 0.18(2) 0.052(13) 0.043(17) 0.051(16) 0.12(2)
F9 0.12(2) 0.135(16) 0.19(3) -0.114(17) 0.11(2) -0.091(16)
F10 0.027(5) 0.25(2) 0.039(7) 0.028(12) 0.014(5) -0.021(9)
F11 0.20(2) 0.055(7) 0.21(2) 0.000 0.11(2) 0.000
F12 0.21(3) 0.053(7) 0.23(3) 0.000 0.03(3) 0.000
Sb3 0.0323(5) 0.0266(4) 0.0322(5) 0.000 0.0183(4) 0.000
F13 0.318(16) 0.026(4) 0.155(10) 0.000 0.193(11) 0.000
F14 0.051(4) 0.174(8) 0.053(4) 0.001(4) 0.015(3) 0.036(4)
F15 0.092(5) 0.062(4) 0.086(5) -0.001(3) 0.074(4) -0.009(4)
F16 0.145(9) 0.025(4) 0.108(7) 0.000 0.098(7) 0.000
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ru P1 2.315(2) . ?
Ru P2 2.315(2) . ?
Ru C2 2.355(9) . ?
Ru C3 2.260(8) . ?
Ru C4 2.292(7) . ?
Ru C5 2.379(8) . ?
Ru C6 2.282(8) . ?
Ru C7 2.246(8) . ?
Ru C13 2.237(7) . ?
Ru C14 2.211(7) . ?
P1 C14 1.793(8) . ?
P1 C19 1.809(8) . ?
P1 C25 1.813(8) . ?
P2 C11 1.809(9) . ?
P2 C31 1.845(8) . ?
P2 C37 1.837(8) . ?
C1 H1A 0.980 . ?
C1 H1B 0.980 . ?
C1 H1C 0.980 . ?
C1 C2 1.494(12) . ?
C2 C3 1.402(12) . ?
C2 C7 1.337(12) . ?
C3 H3 0.950 . ?
C3 C4 1.410(11) . ?
C4 H4 0.950 . ?
C4 C5 1.400(11) . ?
C5 C6 1.435(11) . ?
C5 C8 1.511(11) . ?
C6 H6 0.950 . ?
C6 C7 1.420(11) . ?
C7 H7 0.950 . ?
C8 H8 1.000 . ?
C8 C9 1.502(12) . ?
C8 C10 1.546(12) . ?
C9 H9A 0.980 . ?
C9 H9B 0.980 . ?
C9 H9C 0.980 . ?
C10 H10A 0.980 . ?
C10 H10B 0.980 . ?
C10 H10C 0.980 . ?
C11 C12 1.311(11) . ?
C11 C15 1.526(11) . ?
C12 C13 1.499(11) . ?
C12 C16 1.526(11) . ?
C13 C14 1.441(11) . ?
C13 C17 1.537(10) . ?
C14 C18 1.495(11) . ?
C15 H15A 0.980 . ?
C15 H15B 0.980 . ?
C15 H15C 0.980 . ?
C16 H16A 0.980 . ?
C16 H16B 0.980 . ?
C16 H16C 0.980 . ?
C17 H17A 0.980 . ?
C17 H17B 0.980 . ?
C17 H17C 0.980 . ?
C18 H18A 0.980 . ?
C18 H18B 0.980 . ?
C18 H18C 0.980 . ?
C19 C20 1.366(12) . ?
C19 C24 1.399(12) . ?
C20 H20 0.950 . ?
C20 C21 1.354(13) . ?
C21 H21 0.950 . ?
C21 C22 1.346(15) . ?
C22 H22 0.950 . ?
C22 C23 1.375(16) . ?
C23 H23 0.950 . ?
C23 C24 1.380(14) . ?
C24 H24 0.950 . ?
C25 C26 1.373(12) . ?
C25 C30 1.397(12) . ?
C26 H26 0.950 . ?
C26 C27 1.367(13) . ?
C27 H27 0.950 . ?
C27 C28 1.389(16) . ?
C28 H28 0.950 . ?
C28 C29 1.355(15) . ?
C29 H29 0.950 . ?
C29 C30 1.395(13) . ?
C30 H30 0.950 . ?
C31 C32 1.398(12) . ?
C31 C36 1.365(11) . ?
C32 H32 0.950 . ?
C32 C33 1.401(13) . ?
C33 H33 0.950 . ?
C33 C34 1.360(16) . ?
C34 H34 0.950 . ?
C34 C35 1.362(15) . ?
C35 H35 0.950 . ?
C35 C36 1.351(11) . ?
C36 H36 0.950 . ?
C37 C38 1.389(12) . ?
C37 C42 1.399(11) . ?
C38 H38 0.950 . ?
C38 C39 1.383(12) . ?
C39 H39 0.950 . ?
C39 C40 1.365(13) . ?
C40 H40 0.950 . ?
C40 C41 1.355(13) . ?
C41 H41 0.950 . ?
C41 C42 1.370(12) . ?
C42 H42 0.950 . ?
Sb1 F1 1.873(5) . ?
Sb1 F2 1.863(5) . ?
Sb1 F3 1.868(5) . ?
Sb1 F4 1.875(4) . ?
Sb1 F5 1.891(5) . ?
Sb1 F6 1.882(4) . ?
Sb2 F7 1.855(6) . ?
Sb2 F7 1.855(6) 2_656 ?
Sb2 F8 1.797(18) . ?
Sb2 F8 1.797(18) 2_656 ?
Sb2 F9 1.86(2) . ?
Sb2 F9 1.86(2) 2_656 ?
Sb2 F10 1.851(11) . ?
Sb2 F10 1.851(11) 2_656 ?
Sb2 F11 1.75(2) . ?
Sb2 F12 1.74(2) . ?
Sb3 F13 1.835(9) . ?
Sb3 F14 1.842(6) . ?
Sb3 F14 1.842(6) 2_655 ?
Sb3 F15 1.873(5) . ?
Sb3 F15 1.873(5) 2_655 ?
Sb3 F16 1.844(8) . ?