Crystallography Open Database

Information card for entry 4075536

Preview

Coordinates	4075536.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H24 F3 O3 P Pd S
Calculated formula	C23 H24 F3 O3 P Pd S
Title of publication	Syntheses and Structures of Bulky Monophosphine-Ligated Methylpalladium Complexes: Application to Homo- and Copolymerization of Norbornene and/or Methoxycarbonylnorbornene
Authors of publication	Yamashita, Makoto; Takamiya, Ikuko; Jin, Koichiro; Nozaki, Kyoko
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	19
Pages of publication	4588
a	9.727 ± 0.002 Å
b	10.568 ± 0.002 Å
c	13.079 ± 0.003 Å
α	67.835 ± 0.011°
β	74.702 ± 0.012°
γ	72.953 ± 0.011°
Cell volume	1172.4 ± 0.4 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0211
Residual factor for significantly intense reflections	0.0202
Weighted residual factors for significantly intense reflections	0.0519
Weighted residual factors for all reflections included in the refinement	0.0524
Goodness-of-fit parameter for all reflections included in the refinement	1.055
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178644 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/55.	4075536.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4075536.cif
49299	2012-03-27	../uploads/cif-deposit/cod/cif Adding structures of 4075533, 4075534, 4075535, 4075536 via cif-deposit CGI script.	4075536.cif