Crystallography Open Database

Information card for entry 4075614

Preview

Coordinates	4075614.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H60 P4 Pt2 Si4
Calculated formula	C34 H60 P4 Pt2 Si4
SMILES	[Pt]12([P](CC[P]1(C)C)(C)C)([SiH]1c3ccccc3[Si]([Pt]134[P](CC[P]3(C)C)(C)C)(C)C)[SiH]4c1ccccc1[Si]2(C)C.c1ccccc1
Title of publication	A PtIII2Si2Four-Membered Cycle and a Dinuclear Platinum Complex Bridged by a Cyclodisiloxane Ring
Authors of publication	Shimada, Shigeru; Li, Yong-Hua; Rao, Maddali L. N.; Tanaka, Masato
Journal of publication	Organometallics
Year of publication	2006
Journal volume	25
Journal issue	16
Pages of publication	3796
a	14.957 ± 0.0009 Å
b	15.2972 ± 0.001 Å
c	18.6367 ± 0.0012 Å
α	90°
β	96.821 ± 0.001°
γ	90°
Cell volume	4233.9 ± 0.5 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for significantly intense reflections	0.0208
Weighted residual factors for all reflections included in the refinement	0.0507
Goodness-of-fit parameter for all reflections included in the refinement	1.027
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
211332 (current)	2018-10-05	cif/ Fixing enumeration values for CIF data items _atom_sites_solution_* using cif_fix_values. Data item relocations and exclusion of CIF comment lines might have occurred due to the usage of cif_filter.	4075614.cif
176467	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4075614.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4075614.cif
49353	2012-03-27	../uploads/cif-deposit/cod/cif Adding structures of 4075614, 4075615 via cif-deposit CGI script.	4075614.cif