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Information card for entry 4075628
Preview
| Coordinates | 4075628.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C53 H53 B9 Cl3 Ir Mn N O6 P2 |
|---|---|
| Calculated formula | C53 H47 B9 Cl3 Ir Mn N O6 P2 |
| Title of publication | Construction of Metal Butterflies on a Metallacarborane Scaffold. 1. Synthesis and Structures of Bimetallic Precursors§ |
| Authors of publication | McGrath, Thomas D.; Du, Shaowu; Hodson, Bruce E.; Lu, Xiu Lian; Stone, F. Gordon A. |
| Journal of publication | Organometallics |
| Year of publication | 2006 |
| Journal volume | 25 |
| Journal issue | 19 |
| Pages of publication | 4444 |
| a | 44.096 ± 0.01 Å |
| b | 9.566 ± 0.002 Å |
| c | 31.963 ± 0.007 Å |
| α | 90° |
| β | 120.92 ± 0.009° |
| γ | 90° |
| Cell volume | 11567 ± 5 Å3 |
| Cell temperature | 110 ± 2 K |
| Ambient diffraction temperature | 110 ± 2 K |
| Number of distinct elements | 9 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.2105 |
| Residual factor for significantly intense reflections | 0.0821 |
| Weighted residual factors for significantly intense reflections | 0.1548 |
| Weighted residual factors for all reflections included in the refinement | 0.1954 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.93 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
Version history
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