Crystallography Open Database

Information card for entry 4075632

Preview

Coordinates	4075632.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H44 N2 O Pd
Calculated formula	C74 H88 N4 O2 Pd2
Title of publication	Neutral N‒O Chelated Palladium(II) Complexes: Syntheses, Characterization, and Reactivity
Authors of publication	Kang, Myeongsoon; Sen, Ayusman
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	14
Pages of publication	3508 - 3515
a	11.9939 ± 0.0016 Å
b	12.1298 ± 0.0016 Å
c	13.9255 ± 0.0018 Å
α	82.955 ± 0.002°
β	69.19 ± 0.002°
γ	60.381 ± 0.002°
Cell volume	1642.8 ± 0.4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0577
Residual factor for significantly intense reflections	0.0492
Weighted residual factors for significantly intense reflections	0.1041
Weighted residual factors for all reflections included in the refinement	0.1073
Goodness-of-fit parameter for all reflections included in the refinement	1.145
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
210320 (current)	2018-09-01	cif/4/ Updating bibliography in entries 4075631-4075633, 4075820-4075822, 4082243. Marking entry 4082243 as a duplicate of entry 4075820.	4075632.cif
176467	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4075632.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4075632.cif
49992	2012-03-30	../uploads/cif-deposit/cod/cif Adding structures of 4075632 via cif-deposit CGI script.	4075632.cif