Crystallography Open Database

Information card for entry 4075667

Preview

Coordinates	4075667.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C64.5 H59 Br Cl6 N2 P4 Pt
Calculated formula	C64 H58 Br Cl5 N2 P4 Pt
Title of publication	Synthesis of New Mixed Phosphineσim Iminophosphorane Bidentate Ligands and Their Coordination to Group 10 Metal Centers
Authors of publication	Boubekeur, Leïla; Ricard, Louis; Mézailles, Nicolas; Le Floch, Pascal
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	6
Pages of publication	1065
a	12.41 ± 0.001 Å
b	12.644 ± 0.001 Å
c	21.681 ± 0.001 Å
α	75.6 ± 0.001°
β	75.85 ± 0.001°
γ	81.04 ± 0.001°
Cell volume	3178.8 ± 0.4 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0486
Residual factor for significantly intense reflections	0.0379
Weighted residual factors for significantly intense reflections	0.0973
Weighted residual factors for all reflections included in the refinement	0.1012
Goodness-of-fit parameter for all reflections included in the refinement	1.058
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4075667.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4075667.cif
50609	2012-03-31	../uploads/cif-deposit/cod/cif Adding structures of 4075662, 4075663, 4075664, 4075665, 4075666, 4075667, 4075668 via cif-deposit CGI script.	4075667.cif