Crystallography Open Database

Information card for entry 4075684

Preview

Coordinates	4075684.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C29 H25 N2 O8 Ru3
Calculated formula	C29 H25 N2 O8 Ru3
Title of publication	η2-Edge-Bridging and η3-Face-Capping Coordination of Conjugated Ynenyl Ligands in Triruthenium Carbonyl Cluster Complexes Derived from 1,1-Dimethylhydrazine
Authors of publication	Cabeza, Javier A.; del Río, Ignacio; García-Granda, Santiago; Martínez-Méndez, Lorena; Pérez-Carreño, Enrique
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	5
Pages of publication	831
a	9.5945 ± 0.0003 Å
b	12.305 ± 0.0003 Å
c	13.4399 ± 0.0004 Å
α	78.326 ± 0.002°
β	89.038 ± 0.002°
γ	78.554 ± 0.002°
Cell volume	1522.54 ± 0.08 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0542
Residual factor for significantly intense reflections	0.0513
Weighted residual factors for significantly intense reflections	0.1349
Weighted residual factors for all reflections included in the refinement	0.1378
Goodness-of-fit parameter for all reflections included in the refinement	1.021
Diffraction radiation wavelength	1.5418 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178645 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/56.	4075684.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4075684.cif
50620	2012-03-31	../uploads/cif-deposit/cod/cif Adding structures of 4075683, 4075684 via cif-deposit CGI script.	4075684.cif