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Information card for entry 4075687
Preview
| Coordinates | 4075687.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C53 H48 Cl2 O2 P2 Pd2 |
|---|---|
| Calculated formula | C53 H48 Cl2 O2 P2 Pd2 |
| Title of publication | Investigations of Benzyl and Aryl Palladium Complexes with Pendant Hydroxy Substituents and Their Transformation into Benzolactones on Carbonylation |
| Authors of publication | Lindsell, W. Edward; Palmer, Daniel D.; Preston, Peter N.; Rosair, Georgina M.; Jones, Ray V. H.; Whitton, Alan J. |
| Journal of publication | Organometallics |
| Year of publication | 2005 |
| Journal volume | 24 |
| Journal issue | 6 |
| Pages of publication | 1119 |
| a | 12.047 ± 0.001 Å |
| b | 15.569 ± 0.002 Å |
| c | 13.581 ± 0.002 Å |
| α | 90° |
| β | 112.96 ± 0.01° |
| γ | 90° |
| Cell volume | 2345.4 ± 0.5 Å3 |
| Cell temperature | 160 ± 2 K |
| Ambient diffraction temperature | 160 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0801 |
| Residual factor for significantly intense reflections | 0.051 |
| Weighted residual factors for significantly intense reflections | 0.1213 |
| Weighted residual factors for all reflections included in the refinement | 0.1396 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.98 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
Version history
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