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Information card for entry 4075695
Preview
| Coordinates | 4075695.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C32 H45 Cl2 Ni O0.5 P2 |
|---|---|
| Calculated formula | C32 H45 Cl2 Ni O0.5 P2 |
| Title of publication | Nine-Membered Trans Square-Planar Chelates Formed by a bisbi Analogue |
| Authors of publication | Eberhard, Michael R.; Heslop, Katie M.; Orpen, A. Guy; Pringle, Paul G. |
| Journal of publication | Organometallics |
| Year of publication | 2005 |
| Journal volume | 24 |
| Journal issue | 3 |
| Pages of publication | 335 |
| a | 10.999 ± 0.005 Å |
| b | 20.439 ± 0.006 Å |
| c | 27.982 ± 0.008 Å |
| α | 88.06 ± 0.03° |
| β | 80.25 ± 0.03° |
| γ | 74.94 ± 0.03° |
| Cell volume | 5986 ± 4 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1501 |
| Residual factor for significantly intense reflections | 0.0683 |
| Weighted residual factors for significantly intense reflections | 0.1264 |
| Weighted residual factors for all reflections included in the refinement | 0.1542 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.009 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
Version history
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Users of the data should acknowledge the original authors of the
structural data.