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Information card for entry 4075762
Preview
| Coordinates | 4075762.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C64 H98 Al2 Cl2 N4 O2 |
|---|---|
| Calculated formula | C64 H98 Al2 Cl2 N4 O2 |
| Title of publication | Stepwise Hydrolysis of Aluminum Chloride Iodide LAlClI (L = HC[(CMe)(NAr)]2, Ar = 2,6-iPr2C6H3) in the Presence ofN-Heterocyclic Carbene as Hydrogen Halide Acceptor† |
| Authors of publication | Zhu, Hongping; Chai, Jianfang; He, Cheng; Bai, Guangcai; Roesky, Herbert W.; Jancik, Vojtech; Schmidt, Hans-Georg; Noltemeyer, Mathias |
| Journal of publication | Organometallics |
| Year of publication | 2005 |
| Journal volume | 24 |
| Journal issue | 3 |
| Pages of publication | 380 |
| a | 13.567 ± 0.002 Å |
| b | 13.263 ± 0.002 Å |
| c | 17.359 ± 0.005 Å |
| α | 90° |
| β | 103.76 ± 0.02° |
| γ | 90° |
| Cell volume | 3033.9 ± 1.1 Å3 |
| Cell temperature | 133 ± 2 K |
| Ambient diffraction temperature | 133 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0556 |
| Residual factor for significantly intense reflections | 0.0338 |
| Weighted residual factors for significantly intense reflections | 0.0729 |
| Weighted residual factors for all reflections included in the refinement | 0.0782 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.923 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
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