Information card for entry 4075778
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| Formula |
C71 H59 N4 O5 P4 Rh4 |
| Calculated formula |
C71 H59 N4 O5 P4 Rh4 |
| Title of publication |
Polynuclear Rhodium Complexes with Dinucleating PNNP Ligand: Dynamic and Diverse M···M Interactions in [(μ-X)Rh2(PNNP)(CO)2]n+and [(μ4-X)Rh4(PNNP)2(CO)4]n+[X = H, O, C⋮C−R, R−C⋮C−R, C⋮C, CHCH2, SMe2;n= 0, 1: PNNP = 3,5-bis(diphenylphosphinomethyl)pyrazolato] |
| Authors of publication |
Tanaka, Shukichi; Dubs, Christian; Inagaki, Akiko; Akita, Munetaka |
| Journal of publication |
Organometallics |
| Year of publication |
2005 |
| Journal volume |
24 |
| Journal issue |
1 |
| Pages of publication |
163 |
| a |
14.221 ± 0.002 Å |
| b |
21.678 ± 0.002 Å |
| c |
12.315 ± 0.002 Å |
| α |
105.141 ± 0.005° |
| β |
107.05 ± 0.01° |
| γ |
105.634 ± 0.008° |
| Cell volume |
3248 ± 0.8 Å3 |
| Cell temperature |
213.2 K |
| Number of distinct elements |
6 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for significantly intense reflections |
0.0785 |
| Weighted residual factors for all reflections included in the refinement |
0.2366 |
| Goodness-of-fit parameter for all reflections included in the refinement |
0.984 |
| Diffraction radiation wavelength |
0.7107 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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