Crystallography Open Database

Information card for entry 4075781

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Original paper (by DOI)	HTML

Structure parameters

Formula	C31 H32 Ge Si
Calculated formula	C31 H32 Ge Si
SMILES	[Ge](C1c2ccccc2c2ccccc12)(C)(C)C1([Si](C)(C)C)c2ccccc2c2ccccc12
Title of publication	Difluorenylsilanes, -germanes, and -stannanes Exhibiting an Unprecedented Parallel Arrangement of the Fluorene Units
Authors of publication	Nemes, Gabriela Cretiu; Silaghi-Dumitrescu, Luminita; Silaghi-Dumitrescu, Ioan; Escudié, Jean; Ranaivonjatovo, Henri; Molloy, Kieran C.; Mahon, Mary F.; Zukerman-Schpector, Julio
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	6
Pages of publication	1134
a	8.5001 ± 0.0006 Å
b	10.0668 ± 0.0009 Å
c	15.399 ± 0.002 Å
α	85.918 ± 0.008°
β	87.093 ± 0.008°
γ	87.936 ± 0.009°
Cell volume	1311.9 ± 0.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0571
Residual factor for significantly intense reflections	0.0336
Weighted residual factors for significantly intense reflections	0.0883
Weighted residual factors for all reflections included in the refinement	0.0967
Goodness-of-fit parameter for all reflections included in the refinement	1.055
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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