Crystallography Open Database

Information card for entry 4075789

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Coordinates	Coordinates are not available: file is not found.
Original paper (by DOI)	HTML

Structure parameters

Formula	C49 H40 Cl4 I N2 O3 P2 Rh
Calculated formula	C49 H40 Cl4 I N2 O3 P2 Rh
Title of publication	Rhodium-Catalyzed Dimerization of Terminal Alkynes Assisted by MeI
Authors of publication	Lee, Chrong-Ching; Lin, Ying-Chih; Liu, Yi-Hung; Wang, Yu
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	1
Pages of publication	136
a	12.915 ± 0.002 Å
b	13.21 ± 0.003 Å
c	15.975 ± 0.003 Å
α	77.06 ± 0.02°
β	71.678 ± 0.013°
γ	66.884 ± 0.015°
Cell volume	2363.7 ± 0.8 Å³
Cell temperature	295 ± 2 K
Ambient diffraction temperature	295 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0738
Residual factor for significantly intense reflections	0.0454
Weighted residual factors for all reflections	0.1475
Weighted residual factors for significantly intense reflections	0.1301
Goodness-of-fit parameter for all reflections	0.943
Goodness-of-fit parameter for significantly intense reflections	1.007
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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