Crystallography Open Database

Information card for entry 4075851

Preview

Coordinates	4075851.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C65 H32 Cl6 N2 O28 P2 Rh12
Calculated formula	C65 H26 Cl6 N2 O28 P2 Rh12
Title of publication	Supermolecular Assembly of Tetra- and Hexanuclear Carbonyl Clusters Using a Novel Polydentate Pyridylphosphine Ligand
Authors of publication	Koshevoy, Igor O.; Haukka, Matti; Pakkanen, Tapani A.; Tunik, Sergey P.; Vainiotalo, Pirjo
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	14
Pages of publication	3516
a	16.7 ± 0.003 Å
b	23.066 ± 0.005 Å
c	21.127 ± 0.004 Å
α	90°
β	90°
γ	90°
Cell volume	8138 ± 3 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	7
Space group number	20
Hermann-Mauguin space group symbol	C 2 2 21
Hall space group symbol	C 2c 2
Residual factor for all reflections	0.0387
Residual factor for significantly intense reflections	0.0311
Weighted residual factors for significantly intense reflections	0.0643
Weighted residual factors for all reflections included in the refinement	0.0674
Goodness-of-fit parameter for all reflections included in the refinement	1.045
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178647 (current)	2016-03-21	cif/4/07/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/07/58.	4075851.cif
120075	2014-07-11	Adding DOIs to range 4/07 structures.	4075851.cif
50702	2012-03-31	../uploads/cif-deposit/cod/cif Adding structures of 4075851, 4075852, 4075853 via cif-deposit CGI script.	4075851.cif