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Information card for entry 4116301
Preview
| Coordinates | 4116301.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Chemical name | {Cp*Ru}2{Fe(CO)3}(mu-CO)B4H4 |
|---|---|
| Formula | C24 H34 B4 Fe O4 Ru2 |
| Calculated formula | C24 H34 B4 Fe O4 Ru2 |
| Title of publication | Chemistry of Dimetallaboranes Derived from the Reaction of [Cp*MCl2]2 with Monoboranes (M = Ru, Rh; Cp* = η5-C5Me5) |
| Authors of publication | Xinjian Lei; Maoyu Shang; Thomas P. Fehlner |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 1999 |
| Journal volume | 121 |
| Pages of publication | 1275 - 1287 |
| a | 9.241 ± 0.003 Å |
| b | 15.112 ± 0.003 Å |
| c | 20.047 ± 0.003 Å |
| α | 90° |
| β | 99.944 ± 0.01° |
| γ | 90° |
| Cell volume | 2757.5 ± 1.1 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0363 |
| Residual factor for significantly intense reflections | 0.0323 |
| Weighted residual factors for all reflections | 0.0912 |
| Weighted residual factors for significantly intense reflections | 0.0866 |
| Goodness-of-fit parameter for all reflections | 1.108 |
| Goodness-of-fit parameter for significantly intense reflections | 1.11 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
Version history
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