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Information card for entry 4116304
Preview
| Coordinates | 4116304.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C31 H55 O Si2 Y |
|---|---|
| Calculated formula | C31 H55 O Si2 Y |
| Title of publication | C-H Bonds Are Not Elongated by Coordination to Lanthanide Metals: Single-Crystal Neutron Diffraction Structures of (C5Me5)Y(OC6H3tBu2)CH(SiMe3)2 at 20 K and (C5Me5)La{CH(SiMe3)2}2 at 15 K |
| Authors of publication | Wim T. Klooster; Lee Brammer; Colin J. Schaverien; Peter H. M. Budzelaar |
| Journal of publication | Journal of the American Chemical Society |
| Year of publication | 1999 |
| Journal volume | 121 |
| Pages of publication | 1381 - 1382 |
| a | 9.393 ± 0.001 Å |
| b | 22.099 ± 0.004 Å |
| c | 15.768 ± 0.003 Å |
| α | 90° |
| β | 92.52 ± 0.01° |
| γ | 90° |
| Cell volume | 3269.9 ± 0.9 Å3 |
| Cell temperature | 20 ± 0.5 K |
| Ambient diffraction temperature | 20 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.164 |
| Residual factor for significantly intense reflections | 0.164 |
| Weighted residual factors for all reflections | 0.112 |
| Weighted residual factors for significantly intense reflections | 0.112 |
| Goodness-of-fit parameter for all reflections | 1.064 |
| Goodness-of-fit parameter for significantly intense reflections | 1.064 |
| Diffraction radiation probe | neutron |
| Diffraction radiation wavelength | 1.15863 Å |
| Diffraction radiation type | neutron |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
Version history
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