data_4300789
_journal_name_full  'Inorganic Chemistry'
_journal_year      2005
_publ_section_title
;
Self-Assembly of Silver(I) Coordination Polymers and Macrocycle:
Influence of Stoichiometric Control and Noncovalent Interactions
on the Structure Formation
;
_chemical_formula_sum  'C26 H22 Ag F3 N2 O5 S'
_chemical_formula_weight  639.39
_symmetry_cell_setting  Triclinic
_symmetry_space_group_name_H-M  'P -1'
loop_
_symmetry_equiv_pos_as_xyz
 'x, y, z'
 '-x, -y, -z'
_cell_length_a  8.7805(6)
_cell_length_b  17.4841(12)
_cell_length_c  18.6170(12)
_cell_angle_alpha  113.7450(10)
_cell_angle_beta  102.7020(10)
_cell_angle_gamma  91.0730(10)
_cell_volume  2533.6(3)
_cell_formula_units_Z  4
_cell_measurement_temperature  153(2)
_exptl_crystal_density_diffrn  1.676
_diffrn_ambient_temperature  153(2)
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.50489(2) 0.362081(13) 0.073961(12) 0.03256(7) Uani 1 1 d . . .
Ag2 Ag 1.12949(2) 0.093449(13) 0.786639(12) 0.03313(7) Uani 1 1 d . . .
S1 S 0.35481(8) 0.14354(4) 0.00592(4) 0.03025(14) Uani 1 1 d . . .
S2 S 1.26598(7) 0.31523(4) 0.84108(4) 0.02867(14) Uani 1 1 d . . .
F1 F 0.0943(2) 0.09275(11) 0.02900(12) 0.0546(5) Uani 1 1 d . . .
F2 F 0.2987(2) 0.05343(13) 0.08286(12) 0.0633(5) Uani 1 1 d . . .
F3 F 0.2047(2) -0.00697(11) -0.04519(12) 0.0642(6) Uani 1 1 d . . .
F4 F 1.2705(3) 0.33703(17) 0.71026(14) 0.0881(8) Uani 1 1 d . . .
F5 F 1.4985(2) 0.35478(13) 0.78963(13) 0.0582(5) Uani 1 1 d . . .
F6 F 1.3428(3) 0.44774(13) 0.81868(19) 0.0930(9) Uani 1 1 d . . .
O1 O 0.4061(2) 0.40940(12) 0.32081(11) 0.0341(4) Uani 1 1 d . . .
O2 O 0.8335(2) 0.36487(11) 0.21102(11) 0.0375(4) Uani 1 1 d . . .
O3 O 0.7123(2) 0.18459(12) 0.64952(11) 0.0369(4) Uani 1 1 d . . .
O4 O 1.2908(2) 0.01554(12) 0.55296(11) 0.0370(4) Uani 1 1 d . . .
O5 O 0.4986(3) 0.10899(15) 0.00064(19) 0.0707(8) Uani 1 1 d . . .
O6 O 0.2637(3) 0.14609(16) -0.06632(13) 0.0651(7) Uani 1 1 d . . .
O7 O 0.3625(3) 0.21909(12) 0.07637(12) 0.0476(5) Uani 1 1 d . . .
O8 O 1.2683(2) 0.22794(11) 0.79119(13) 0.0460(5) Uani 1 1 d . . .
O9 O 1.3715(3) 0.34774(17) 0.91897(13) 0.0625(7) Uani 1 1 d . . .
O10 O 1.1119(2) 0.34150(12) 0.83885(13) 0.0410(5) Uani 1 1 d . . .
N1 N 0.8922(2) 0.11600(13) 0.80215(12) 0.0273(4) Uani 1 1 d . . .
N2 N 1.2934(2) 0.00269(13) 0.74059(12) 0.0278(4) Uani 1 1 d . . .
N3 N 0.3249(2) 0.42877(13) 0.12822(13) 0.0273(4) Uani 1 1 d . . .
N4 N 0.7183(2) 0.32607(13) 0.03636(12) 0.0277(4) Uani 1 1 d . . .
C1 C 0.3141(3) 0.34205(16) 0.31626(15) 0.0290(5) Uani 1 1 d . . .
C2 C 0.2492(3) 0.27055(17) 0.24646(15) 0.0322(6) Uani 1 1 d . . .
H2 H 0.2668 0.2643 0.1960 0.039 Uiso 1 1 calc R . .
C3 C 0.1572(3) 0.20775(17) 0.25149(16) 0.0327(6) Uani 1 1 d . . .
H3 H 0.1133 0.1586 0.2036 0.039 Uiso 1 1 calc R . .
C4 C 0.1278(3) 0.21441(16) 0.32338(15) 0.0295(5) Uani 1 1 d . . .
C5 C 0.1961(3) 0.28613(17) 0.39295(16) 0.0347(6) Uani 1 1 d . . .
H5 H 0.1796 0.2917 0.4435 0.042 Uiso 1 1 calc R . .
C6 C 0.2878(3) 0.34953(16) 0.38999(15) 0.0330(6) Uani 1 1 d . . .
H6 H 0.3330 0.3982 0.4382 0.040 Uiso 1 1 calc R . .
C7 C 0.4364(3) 0.40692(17) 0.24795(16) 0.0328(6) Uani 1 1 d . . .
H7A H 0.4482 0.3483 0.2131 0.039 Uiso 1 1 calc R . .
H7B H 0.5372 0.4420 0.2614 0.039 Uiso 1 1 calc R . .
C8 C 0.3090(3) 0.43770(15) 0.20125(15) 0.0279(5) Uani 1 1 d . . .
C9 C 0.1886(3) 0.47731(17) 0.23322(17) 0.0353(6) Uani 1 1 d . . .
H9 H 0.1787 0.4821 0.2846 0.042 Uiso 1 1 calc R . .
C10 C 0.0833(3) 0.50963(17) 0.18922(17) 0.0375(6) Uani 1 1 d . . .
H10 H 0.0001 0.5372 0.2099 0.045 Uiso 1 1 calc R . .
C11 C 0.1011(3) 0.50123(16) 0.11445(17) 0.0332(6) Uani 1 1 d . . .
H11 H 0.0304 0.5232 0.0832 0.040 Uiso 1 1 calc R . .
C12 C 0.2221(3) 0.46073(15) 0.08609(16) 0.0320(6) Uani 1 1 d . . .
H12 H 0.2335 0.4551 0.0347 0.038 Uiso 1 1 calc R . .
C13 C 0.7434(3) 0.33937(16) -0.02639(16) 0.0314(6) Uani 1 1 d . . .
H13 H 0.6654 0.3625 -0.0531 0.038 Uiso 1 1 calc R . .
C14 C 0.8778(3) 0.32098(16) -0.05385(16) 0.0342(6) Uani 1 1 d . . .
H14 H 0.8914 0.3312 -0.0986 0.041 Uiso 1 1 calc R . .
C15 C 0.9920(3) 0.28749(16) -0.01543(17) 0.0360(6) Uani 1 1 d . . .
H15 H 1.0853 0.2739 -0.0333 0.043 Uiso 1 1 calc R . .
C16 C 0.9674(3) 0.27429(16) 0.04961(17) 0.0339(6) Uani 1 1 d . . .
H16 H 1.0448 0.2519 0.0775 0.041 Uiso 1 1 calc R . .
C17 C 0.8299(3) 0.29374(15) 0.07428(15) 0.0283(5) Uani 1 1 d . . .
C18 C 0.8012(3) 0.28258(16) 0.14608(15) 0.0311(6) Uani 1 1 d . . .
H18A H 0.6908 0.2590 0.1350 0.037 Uiso 1 1 calc R . .
H18B H 0.8717 0.2442 0.1596 0.037 Uiso 1 1 calc R . .
C19 C 0.8163(3) 0.37251(16) 0.28527(15) 0.0301(5) Uani 1 1 d . . .
C20 C 0.7701(3) 0.30764(17) 0.30269(16) 0.0323(6) Uani 1 1 d . . .
H20 H 0.7514 0.2514 0.2623 0.039 Uiso 1 1 calc R . .
C21 C 0.7511(3) 0.32480(16) 0.37959(16) 0.0349(6) Uani 1 1 d . . .
H21 H 0.7199 0.2796 0.3912 0.042 Uiso 1 1 calc R . .
C22 C 0.7763(3) 0.40599(16) 0.43975(15) 0.0314(6) Uani 1 1 d . . .
C23 C 0.8274(3) 0.47062(17) 0.42107(16) 0.0358(6) Uani 1 1 d . . .
H23 H 0.8488 0.5268 0.4616 0.043 Uiso 1 1 calc R . .
C24 C 0.8472(3) 0.45423(17) 0.34515(16) 0.0351(6) Uani 1 1 d . . .
H24 H 0.8821 0.4989 0.3337 0.042 Uiso 1 1 calc R . .
C25 C 0.7430(4) 0.42822(17) 0.52213(16) 0.0375(6) Uani 1 1 d . . .
H25A H 0.8241 0.4742 0.5630 0.045 Uiso 1 1 calc R . .
H25B H 0.6404 0.4508 0.5213 0.045 Uiso 1 1 calc R . .
C26 C 0.7387(3) 0.35846(16) 0.55067(15) 0.0324(6) Uani 1 1 d . . .
C27 C 0.8753(3) 0.33497(16) 0.58505(16) 0.0339(6) Uani 1 1 d . . .
H27 H 0.9737 0.3594 0.5860 0.041 Uiso 1 1 calc R . .
C28 C 0.8729(3) 0.27663(16) 0.61828(15) 0.0312(6) Uani 1 1 d . . .
H28 H 0.9686 0.2619 0.6419 0.037 Uiso 1 1 calc R . .
C29 C 0.7310(3) 0.24045(16) 0.61662(15) 0.0313(6) Uani 1 1 d . . .
C30 C 0.5922(3) 0.26010(19) 0.57932(18) 0.0431(7) Uani 1 1 d . . .
H30 H 0.4938 0.2336 0.5759 0.052 Uiso 1 1 calc R . .
C31 C 0.5980(3) 0.3185(2) 0.54707(18) 0.0436(7) Uani 1 1 d . . .
H31 H 0.5023 0.3316 0.5216 0.052 Uiso 1 1 calc R . .
C32 C 0.8455(3) 0.17792(17) 0.70533(16) 0.0319(6) Uani 1 1 d . . .
H32A H 0.9116 0.2330 0.7359 0.038 Uiso 1 1 calc R . .
H32B H 0.9097 0.1362 0.6759 0.038 Uiso 1 1 calc R . .
C33 C 0.7875(3) 0.15053(15) 0.76267(15) 0.0276(5) Uani 1 1 d . . .
C34 C 0.6411(3) 0.16405(16) 0.77715(16) 0.0310(5) Uani 1 1 d . . .
H34 H 0.5695 0.1874 0.7477 0.037 Uiso 1 1 calc R . .
C35 C 0.5990(3) 0.14322(16) 0.83514(17) 0.0336(6) Uani 1 1 d . . .
H35 H 0.4996 0.1535 0.8471 0.040 Uiso 1 1 calc R . .
C36 C 0.7047(3) 0.10719(16) 0.87521(16) 0.0336(6) Uani 1 1 d . . .
H36 H 0.6784 0.0913 0.9145 0.040 Uiso 1 1 calc R . .
C37 C 0.8485(3) 0.09475(15) 0.85725(16) 0.0307(6) Uani 1 1 d . . .
H37 H 0.9205 0.0700 0.8851 0.037 Uiso 1 1 calc R . .
C38 C 1.3607(3) -0.04015(16) 0.78229(16) 0.0315(6) Uani 1 1 d . . .
H38 H 1.3474 -0.0253 0.8353 0.038 Uiso 1 1 calc R . .
C39 C 1.4486(3) -0.10480(17) 0.75171(18) 0.0364(6) Uani 1 1 d . . .
H39 H 1.4945 -0.1337 0.7831 0.044 Uiso 1 1 calc R . .
C40 C 1.4685(3) -0.12659(17) 0.67497(18) 0.0374(6) Uani 1 1 d . . .
H40 H 1.5278 -0.1711 0.6523 0.045 Uiso 1 1 calc R . .
C41 C 1.4006(3) -0.08260(16) 0.63120(17) 0.0349(6) Uani 1 1 d . . .
H41 H 1.4121 -0.0968 0.5779 0.042 Uiso 1 1 calc R . .
C42 C 1.3156(3) -0.01746(15) 0.66633(15) 0.0288(5) Uani 1 1 d . . .
C43 C 1.2398(3) 0.03537(16) 0.62515(15) 0.0311(6) Uani 1 1 d . . .
H43A H 1.1239 0.0235 0.6120 0.037 Uiso 1 1 calc R . .
H43B H 1.2702 0.0958 0.6614 0.037 Uiso 1 1 calc R . .
C44 C 1.2241(3) 0.05228(16) 0.50320(16) 0.0316(6) Uani 1 1 d . . .
C45 C 1.1141(3) 0.10930(17) 0.51897(17) 0.0367(6) Uani 1 1 d . . .
H45 H 1.0833 0.1275 0.5685 0.044 Uiso 1 1 calc R . .
C46 C 1.0499(3) 0.13930(17) 0.46165(17) 0.0361(6) Uani 1 1 d . . .
H46 H 0.9736 0.1775 0.4723 0.043 Uiso 1 1 calc R . .
C47 C 1.0942(3) 0.11500(16) 0.38920(16) 0.0310(6) Uani 1 1 d . . .
C48 C 1.2073(3) 0.05971(16) 0.37592(16) 0.0329(6) Uani 1 1 d . . .
H48 H 1.2410 0.0430 0.3272 0.039 Uiso 1 1 calc R . .
C49 C 1.2718(3) 0.02851(16) 0.43149(16) 0.0323(6) Uani 1 1 d . . .
H49 H 1.3488 -0.0092 0.4209 0.039 Uiso 1 1 calc R . .
C50 C 1.0225(3) 0.14677(17) 0.32634(17) 0.0340(6) Uani 1 1 d . . .
H50A H 0.9236 0.1693 0.3376 0.041 Uiso 1 1 calc R . .
H50B H 0.9953 0.0987 0.2724 0.041 Uiso 1 1 calc R . .
C51 C 0.2331(3) 0.06680(17) 0.01935(17) 0.0360(6) Uani 1 1 d . . .
C52 C 1.3484(3) 0.36650(19) 0.7875(2) 0.0430(7) Uani 1 1 d . . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
Ag1 0.03124(11) 0.03850(12) 0.03499(12) 0.01854(9) 0.01509(9) 0.01220(9)
Ag2 0.03275(12) 0.03896(12) 0.03375(12) 0.01820(9) 0.01339(9) 0.01386(9)
S1 0.0346(3) 0.0304(3) 0.0291(3) 0.0129(3) 0.0133(3) 0.0049(3)
S2 0.0268(3) 0.0306(3) 0.0316(3) 0.0146(3) 0.0096(3) 0.0074(3)
F1 0.0416(10) 0.0537(11) 0.0808(14) 0.0320(10) 0.0316(10) 0.0093(8)
F2 0.0769(14) 0.0683(13) 0.0644(13) 0.0530(11) 0.0066(10) 0.0061(11)
F3 0.0866(15) 0.0347(10) 0.0608(12) 0.0029(9) 0.0327(11) -0.0114(10)
F4 0.0759(15) 0.142(2) 0.0691(15) 0.0777(16) -0.0010(12) -0.0193(15)
F5 0.0405(10) 0.0702(13) 0.0831(14) 0.0433(11) 0.0302(10) 0.0089(9)
F6 0.0812(16) 0.0455(12) 0.178(3) 0.0602(16) 0.0551(17) 0.0131(11)
O1 0.0387(10) 0.0372(10) 0.0309(10) 0.0191(8) 0.0079(8) 0.0050(8)
O2 0.0522(12) 0.0342(10) 0.0262(9) 0.0133(8) 0.0094(8) -0.0020(9)
O3 0.0350(10) 0.0431(11) 0.0375(11) 0.0273(9) -0.0011(8) -0.0024(8)
O4 0.0454(11) 0.0436(11) 0.0344(10) 0.0230(9) 0.0202(9) 0.0188(9)
O5 0.0511(14) 0.0600(15) 0.123(2) 0.0430(16) 0.0528(15) 0.0230(12)
O6 0.0835(18) 0.0750(17) 0.0392(13) 0.0353(12) -0.0007(12) -0.0131(14)
O7 0.0660(14) 0.0327(11) 0.0428(12) 0.0064(9) 0.0302(11) -0.0041(10)
O8 0.0563(13) 0.0286(10) 0.0656(14) 0.0216(10) 0.0352(11) 0.0131(9)
O9 0.0412(12) 0.103(2) 0.0367(12) 0.0258(13) 0.0030(10) 0.0041(13)
O10 0.0316(10) 0.0392(11) 0.0581(13) 0.0220(10) 0.0187(9) 0.0132(8)
N1 0.0295(11) 0.0273(11) 0.0272(11) 0.0127(9) 0.0085(9) 0.0076(9)
N2 0.0260(11) 0.0272(11) 0.0296(11) 0.0115(9) 0.0059(9) 0.0049(8)
N3 0.0288(11) 0.0271(11) 0.0306(11) 0.0148(9) 0.0104(9) 0.0072(8)
N4 0.0269(11) 0.0302(11) 0.0275(11) 0.0125(9) 0.0087(9) 0.0062(9)
C1 0.0276(13) 0.0326(13) 0.0313(14) 0.0181(11) 0.0065(10) 0.0095(10)
C2 0.0353(14) 0.0405(15) 0.0262(13) 0.0179(12) 0.0101(11) 0.0100(12)
C3 0.0334(14) 0.0330(14) 0.0265(13) 0.0082(11) 0.0050(11) 0.0060(11)
C4 0.0297(13) 0.0308(13) 0.0305(14) 0.0151(11) 0.0081(10) 0.0069(10)
C5 0.0451(16) 0.0370(15) 0.0270(13) 0.0158(12) 0.0133(12) 0.0090(12)
C6 0.0440(16) 0.0293(13) 0.0247(13) 0.0111(11) 0.0069(11) 0.0060(11)
C7 0.0317(14) 0.0408(15) 0.0345(14) 0.0229(12) 0.0108(11) 0.0085(11)
C8 0.0287(13) 0.0257(12) 0.0323(13) 0.0146(11) 0.0085(10) 0.0048(10)
C9 0.0402(15) 0.0392(15) 0.0334(14) 0.0189(12) 0.0147(12) 0.0156(12)
C10 0.0371(15) 0.0400(15) 0.0418(16) 0.0191(13) 0.0167(12) 0.0198(12)
C11 0.0370(14) 0.0272(13) 0.0384(15) 0.0178(12) 0.0065(12) 0.0107(11)
C12 0.0394(15) 0.0292(13) 0.0295(14) 0.0136(11) 0.0098(11) 0.0053(11)
C13 0.0340(14) 0.0322(14) 0.0303(14) 0.0154(11) 0.0078(11) 0.0033(11)
C14 0.0408(15) 0.0319(14) 0.0306(14) 0.0107(11) 0.0149(12) -0.0008(11)
C15 0.0318(14) 0.0308(14) 0.0409(16) 0.0056(12) 0.0185(12) 0.0024(11)
C16 0.0298(13) 0.0294(13) 0.0387(15) 0.0110(12) 0.0066(11) 0.0078(11)
C17 0.0297(13) 0.0267(12) 0.0266(13) 0.0093(10) 0.0067(10) 0.0051(10)
C18 0.0345(14) 0.0290(13) 0.0288(13) 0.0119(11) 0.0057(11) 0.0073(11)
C19 0.0314(13) 0.0348(14) 0.0254(13) 0.0150(11) 0.0049(10) 0.0021(11)
C20 0.0385(15) 0.0298(13) 0.0296(14) 0.0150(11) 0.0055(11) 0.0039(11)
C21 0.0461(16) 0.0302(14) 0.0346(15) 0.0192(12) 0.0108(12) 0.0051(12)
C22 0.0337(14) 0.0346(14) 0.0297(14) 0.0188(12) 0.0047(11) 0.0058(11)
C23 0.0478(16) 0.0306(14) 0.0287(14) 0.0134(11) 0.0069(12) 0.0006(12)
C24 0.0431(16) 0.0317(14) 0.0321(14) 0.0170(12) 0.0058(12) -0.0009(12)
C25 0.0511(17) 0.0328(14) 0.0343(15) 0.0189(12) 0.0122(13) 0.0067(13)
C26 0.0434(15) 0.0318(14) 0.0270(13) 0.0157(11) 0.0116(11) 0.0076(12)
C27 0.0397(15) 0.0324(14) 0.0330(14) 0.0140(12) 0.0152(12) 0.0027(12)
C28 0.0345(14) 0.0295(13) 0.0315(14) 0.0137(11) 0.0098(11) 0.0071(11)
C29 0.0396(15) 0.0299(13) 0.0263(13) 0.0143(11) 0.0071(11) 0.0030(11)
C30 0.0351(15) 0.0570(19) 0.0462(18) 0.0350(15) 0.0016(13) -0.0003(13)
C31 0.0389(16) 0.0560(19) 0.0469(18) 0.0368(16) 0.0019(13) 0.0066(14)
C32 0.0328(14) 0.0352(14) 0.0317(14) 0.0193(12) 0.0049(11) 0.0058(11)
C33 0.0307(13) 0.0243(12) 0.0282(13) 0.0122(10) 0.0054(10) 0.0030(10)
C34 0.0289(13) 0.0288(13) 0.0357(14) 0.0153(11) 0.0054(11) 0.0048(10)
C35 0.0273(13) 0.0302(14) 0.0424(16) 0.0126(12) 0.0120(11) 0.0010(11)
C36 0.0394(15) 0.0300(14) 0.0361(15) 0.0158(12) 0.0147(12) 0.0022(11)
C37 0.0362(14) 0.0275(13) 0.0324(14) 0.0161(11) 0.0088(11) 0.0072(11)
C38 0.0302(13) 0.0331(14) 0.0297(13) 0.0129(11) 0.0052(11) 0.0022(11)
C39 0.0323(14) 0.0330(14) 0.0456(17) 0.0209(13) 0.0042(12) 0.0060(11)
C40 0.0322(14) 0.0313(14) 0.0485(17) 0.0148(13) 0.0126(12) 0.0105(11)
C41 0.0346(14) 0.0337(14) 0.0382(15) 0.0139(12) 0.0144(12) 0.0086(11)
C42 0.0267(13) 0.0274(13) 0.0311(13) 0.0112(11) 0.0069(10) 0.0025(10)
C43 0.0365(14) 0.0303(13) 0.0295(13) 0.0124(11) 0.0136(11) 0.0074(11)
C44 0.0369(14) 0.0289(13) 0.0331(14) 0.0147(11) 0.0131(11) 0.0057(11)
C45 0.0486(16) 0.0384(15) 0.0329(14) 0.0181(12) 0.0217(13) 0.0169(13)
C46 0.0424(15) 0.0339(14) 0.0380(15) 0.0170(12) 0.0168(12) 0.0149(12)
C47 0.0327(14) 0.0299(13) 0.0314(14) 0.0144(11) 0.0073(11) 0.0000(11)
C48 0.0388(15) 0.0327(14) 0.0306(14) 0.0132(11) 0.0154(11) 0.0052(11)
C49 0.0356(14) 0.0288(13) 0.0353(14) 0.0123(11) 0.0159(12) 0.0089(11)
C50 0.0330(14) 0.0377(15) 0.0347(15) 0.0190(12) 0.0072(11) 0.0025(11)
C51 0.0416(16) 0.0321(14) 0.0362(15) 0.0155(12) 0.0110(12) 0.0060(12)
C52 0.0351(15) 0.0400(16) 0.060(2) 0.0271(15) 0.0117(14) 0.0001(13)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 N4 2.159(2) . ?
Ag1 N3 2.168(2) . ?
Ag2 N1 2.188(2) . ?
Ag2 N2 2.204(2) . ?
Ag2 O6 2.498(2) 1_656 ?
Ag2 O8 2.5900(19) . ?
S1 O5 1.416(2) . ?
S1 O6 1.424(2) . ?
S1 O7 1.426(2) . ?
S1 C51 1.827(3) . ?
S2 O9 1.417(2) . ?
S2 O10 1.4340(19) . ?
S2 O8 1.4354(19) . ?
S2 C52 1.827(3) . ?
F1 C51 1.332(3) . ?
F2 C51 1.309(3) . ?
F3 C51 1.333(3) . ?
F4 C52 1.326(4) . ?
F5 C52 1.331(3) . ?
F6 C52 1.307(4) . ?
O1 C1 1.378(3) . ?
O1 C7 1.423(3) . ?
O2 C19 1.376(3) . ?
O2 C18 1.430(3) . ?
O3 C29 1.370(3) . ?
O3 C32 1.424(3) . ?
O4 C44 1.367(3) . ?
O4 C43 1.422(3) . ?
O6 Ag2 2.498(2) 1_454 ?
N1 C37 1.346(3) . ?
N1 C33 1.353(3) . ?
N2 C38 1.340(3) . ?
N2 C42 1.343(3) . ?
N3 C12 1.343(3) . ?
N3 C8 1.344(3) . ?
N4 C13 1.341(3) . ?
N4 C17 1.348(3) . ?
C1 C2 1.384(4) . ?
C1 C6 1.397(4) . ?
C2 C3 1.396(4) . ?
C2 H2 0.9500 . ?
C3 C4 1.378(4) . ?
C3 H3 0.9500 . ?
C4 C5 1.390(4) . ?
C4 C50 1.513(4) 1_455 ?
C5 C6 1.384(4) . ?
C5 H5 0.9500 . ?
C6 H6 0.9500 . ?
C7 C8 1.506(3) . ?
C7 H7A 0.9900 . ?
C7 H7B 0.9900 . ?
C8 C9 1.387(3) . ?
C9 C10 1.380(4) . ?
C9 H9 0.9500 . ?
C10 C11 1.384(4) . ?
C10 H10 0.9500 . ?
C11 C12 1.372(4) . ?
C11 H11 0.9500 . ?
C12 H12 0.9500 . ?
C13 C14 1.379(4) . ?
C13 H13 0.9500 . ?
C14 C15 1.380(4) . ?
C14 H14 0.9500 . ?
C15 C16 1.380(4) . ?
C15 H15 0.9500 . ?
C16 C17 1.385(3) . ?
C16 H16 0.9500 . ?
C17 C18 1.498(3) . ?
C18 H18A 0.9900 . ?
C18 H18B 0.9900 . ?
C19 C20 1.376(3) . ?
C19 C24 1.388(4) . ?
C20 C21 1.389(4) . ?
C20 H20 0.9500 . ?
C21 C22 1.385(4) . ?
C21 H21 0.9500 . ?
C22 C23 1.402(4) . ?
C22 C25 1.520(4) . ?
C23 C24 1.376(4) . ?
C23 H23 0.9500 . ?
C24 H24 0.9500 . ?
C25 C26 1.517(4) . ?
C25 H25A 0.9900 . ?
C25 H25B 0.9900 . ?
C26 C27 1.381(4) . ?
C26 C31 1.383(4) . ?
C27 C28 1.392(4) . ?
C27 H27 0.9500 . ?
C28 C29 1.376(4) . ?
C28 H28 0.9500 . ?
C29 C30 1.386(4) . ?
C30 C31 1.383(4) . ?
C30 H30 0.9500 . ?
C31 H31 0.9500 . ?
C32 C33 1.506(3) . ?
C32 H32A 0.9900 . ?
C32 H32B 0.9900 . ?
C33 C34 1.376(3) . ?
C34 C35 1.386(4) . ?
C34 H34 0.9500 . ?
C35 C36 1.382(4) . ?
C35 H35 0.9500 . ?
C36 C37 1.375(4) . ?
C36 H36 0.9500 . ?
C37 H37 0.9500 . ?
C38 C39 1.380(4) . ?
C38 H38 0.9500 . ?
C39 C40 1.375(4) . ?
C39 H39 0.9500 . ?
C40 C41 1.385(4) . ?
C40 H40 0.9500 . ?
C41 C42 1.389(3) . ?
C41 H41 0.9500 . ?
C42 C43 1.501(3) . ?
C43 H43A 0.9900 . ?
C43 H43B 0.9900 . ?
C44 C49 1.391(3) . ?
C44 C45 1.392(4) . ?
C45 C46 1.389(4) . ?
C45 H45 0.9500 . ?
C46 C47 1.388(4) . ?
C46 H46 0.9500 . ?
C47 C48 1.390(3) . ?
C47 C50 1.512(4) . ?
C48 C49 1.377(4) . ?
C48 H48 0.9500 . ?
C49 H49 0.9500 . ?
C50 C4 1.513(4) 1_655 ?
C50 H50A 0.9900 . ?
C50 H50B 0.9900 . ?