Crystallography Open Database

Information card for entry 4308155

Preview

Coordinates	4308155.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C41 H50 Cl2 N2 Pd S2
Calculated formula	C41 H50 Cl2 N2 Pd S2
Title of publication	Synthesis, Structure, and Luminescence of Di- and Trinuclear Palladium/Gold and Platinum/Gold Complexes with (2,7-Di-tert-butylfluoren-9-ylidene)methanedithiolate,1
Authors of publication	José Vicente; Pablo González-Herrero; María Pérez-Cadenas; Peter G. Jones; Delia Bautista
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	4718 - 4732
a	11.393 ± 0.0011 Å
b	17.702 ± 0.002 Å
c	19.709 ± 0.002 Å
α	90°
β	97.997 ± 0.005°
γ	90°
Cell volume	3936.2 ± 0.7 Å³
Cell temperature	133 ± 2 K
Ambient diffraction temperature	133 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0654
Residual factor for significantly intense reflections	0.0389
Weighted residual factors for significantly intense reflections	0.0981
Weighted residual factors for all reflections included in the refinement	0.1138
Goodness-of-fit parameter for all reflections included in the refinement	1.023
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179119 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/81.	4308155.cif
120081	2014-07-11	Adding DOIs to range 4/30 structures.	4308155.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4308155.cif
1194	2010-06-06	cif/4/ Adding data from Inorg-Chem-2007_01-13/ processing directory.	4308155.cif