#------------------------------------------------------------------------------ #$Date: 2015-01-23 12:30:19 +0000 (Fri, 23 Jan 2015) $ #$Revision: 130086 $ #$URL: svn://www.crystallography.net/cod/cif/4/30/83/4308369.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4308369 loop_ _publ_author_name 'Tatiana Y. Shvareva' 'Tyler A. Sullens' 'Thomas C. Shehee' 'Thomas E. Albrecht-Schmitt' _publ_section_title ; Syntheses, Structures, and Ion-Exchange Properties of the Three-Dimensional Framework Uranyl Gallium Phosphates, Cs4[(UO2)2(GaOH)2(PO4)4].H2O and Cs[UO2Ga(PO4)2] ; _journal_name_full 'Inorganic Chemistry' _journal_page_first 300 _journal_page_last 305 _journal_paper_doi 10.1021/ic048638p _journal_volume 44 _journal_year 2005 _chemical_formula_sum 'Cs Ga O10 P2 U' _chemical_formula_weight 662.60 _chemical_name_common 'Cesium Uranyl Gallium Phosphate' _chemical_name_systematic ; ? ; _space_group_IT_number 2 _symmetry_cell_setting triclinic _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-97 _cell_angle_alpha 66.6420(10) _cell_angle_beta 70.5630(10) _cell_angle_gamma 84.003(2) _cell_formula_units_Z 2 _cell_length_a 7.7765(6) _cell_length_b 8.5043(7) _cell_length_c 8.9115(7) _cell_measurement_reflns_used all _cell_measurement_temperature 193(2) _cell_measurement_theta_max 28.30 _cell_measurement_theta_min 2.61 _cell_volume 509.96(7) _computing_cell_refinement 'SMART, SAINT' _computing_data_collection SMART _computing_data_reduction SAINT _computing_molecular_graphics 'SHELXP-97 (Sheldrick, 1997)' _computing_publication_material 'SHELXCIF-97 (Sheldrick, 1997)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _diffrn_ambient_temperature 193(2) _diffrn_measured_fraction_theta_full 0.984 _diffrn_measured_fraction_theta_max 0.984 _diffrn_measurement_device_type 'Bruker APEX' _diffrn_measurement_method '0.3 wide w/ exposures' _diffrn_radiation_monochromator graphite _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0291 _diffrn_reflns_av_sigmaI/netI 0.0436 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 11 _diffrn_reflns_limit_l_min -11 _diffrn_reflns_number 5181 _diffrn_reflns_theta_full 28.30 _diffrn_reflns_theta_max 28.30 _diffrn_reflns_theta_min 2.61 _diffrn_standards_decay_% 0 _diffrn_standards_interval_count na _diffrn_standards_interval_time na _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 22.365 _exptl_absorpt_correction_T_max 0.61311 _exptl_absorpt_correction_T_min 0.27112 _exptl_absorpt_correction_type 'analytical, multiscan' _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 4.315 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_description 'rectangular plate' _exptl_crystal_F_000 576 _exptl_crystal_size_max 0.0420 _exptl_crystal_size_mid 0.0150 _exptl_crystal_size_min 0.0100 _refine_diff_density_max 2.346 _refine_diff_density_min -1.397 _refine_diff_density_rms 0.267 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.839 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 136 _refine_ls_number_reflns 2495 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.839 _refine_ls_R_factor_all 0.0326 _refine_ls_R_factor_gt 0.0283 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0274P)^2^+8.4775P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0613 _refine_ls_wR_factor_ref 0.0626 _reflns_number_gt 2250 _reflns_number_total 2495 _reflns_threshold_expression >2sigma(I) _[local]_cod_data_source_file ic048638psi20040929_015933_2.cif _[local]_cod_data_source_block UGaP-2 _cod_depositor_comments ; The following automatic conversions were performed: '_exptl_crystal_density_meas' value 'nm' was changed to '?' - the value is perceived as not measured. Automatic conversion script Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas ; _cod_database_code 4308369 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group U1 U 0.21442(3) 0.92139(3) 0.33450(3) 0.00955(7) Uani 1 1 d . . . Cs1 Cs 0.66307(6) 0.68745(6) 0.49084(6) 0.02003(11) Uani 1 1 d . . . Ga1 Ga 0.24602(10) 0.57980(9) 0.98833(9) 0.01023(14) Uani 1 1 d . . . P1 P -0.0413(2) 0.3270(2) 1.2841(2) 0.0103(3) Uani 1 1 d . . . P2 P 0.5302(2) 0.7365(2) 1.0581(2) 0.0099(3) Uani 1 1 d . . . O1 O 0.0560(6) 0.8460(6) 0.2720(6) 0.0159(10) Uani 1 1 d . . . O2 O 0.3671(7) 0.9913(6) 0.4080(6) 0.0145(9) Uani 1 1 d . . . O3 O -0.2013(6) 0.3571(6) 1.4219(6) 0.0150(10) Uani 1 1 d . . . O4 O 0.0248(7) 0.1492(6) 1.3771(6) 0.0140(9) Uani 1 1 d . . . O5 O -0.0888(6) 0.3241(6) 1.1313(6) 0.0137(9) Uani 1 1 d . . . O6 O 0.1153(7) 0.4610(6) 1.2133(6) 0.0158(10) Uani 1 1 d . . . O7 O 0.3828(7) 0.7476(6) 0.9725(6) 0.0153(10) Uani 1 1 d . . . O8 O 0.5978(6) 0.5503(6) 1.1144(6) 0.0131(9) Uani 1 1 d . . . O9 O 0.6848(7) 0.8614(6) 0.9304(6) 0.0156(10) Uani 1 1 d . . . O10 O 0.4475(6) 0.7700(6) 1.2225(6) 0.0141(9) Uani 1 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 U1 0.00882(12) 0.00943(11) 0.00863(11) -0.00326(8) -0.00089(8) 0.00043(8) Cs1 0.0176(2) 0.0199(2) 0.0252(2) -0.01054(18) -0.00810(18) 0.00157(17) Ga1 0.0092(3) 0.0101(3) 0.0100(3) -0.0032(3) -0.0020(3) 0.0005(2) P1 0.0097(7) 0.0091(7) 0.0082(7) -0.0009(6) -0.0013(6) 0.0017(6) P2 0.0092(7) 0.0086(7) 0.0104(7) -0.0039(6) -0.0011(6) -0.0001(6) O1 0.011(2) 0.021(2) 0.016(2) -0.007(2) -0.0049(19) -0.0030(19) O2 0.014(2) 0.019(2) 0.016(2) -0.010(2) -0.0095(19) 0.0047(19) O3 0.010(2) 0.013(2) 0.013(2) -0.0019(19) 0.0016(18) 0.0048(18) O4 0.016(2) 0.013(2) 0.006(2) -0.0004(17) -0.0001(18) 0.0028(18) O5 0.013(2) 0.016(2) 0.013(2) -0.0040(19) -0.0082(18) 0.0045(18) O6 0.015(2) 0.021(2) 0.012(2) -0.008(2) -0.0003(19) -0.0047(19) O7 0.016(2) 0.012(2) 0.019(2) -0.0042(19) -0.008(2) -0.0029(18) O8 0.015(2) 0.009(2) 0.012(2) -0.0037(18) -0.0012(18) 0.0010(17) O9 0.013(2) 0.019(2) 0.014(2) -0.005(2) -0.0037(19) -0.0001(19) O10 0.011(2) 0.019(2) 0.011(2) -0.0050(19) -0.0016(18) 0.0009(18) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ga Ga 0.2307 1.6083 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cs Cs -0.3680 2.1192 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' U U -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 U1 O2 177.2(2) . . ? O1 U1 O9 91.6(2) . 2_676 ? O2 U1 O9 91.1(2) . 2_676 ? O1 U1 O10 92.8(2) . 1_554 ? O2 U1 O10 88.3(2) . 1_554 ? O9 U1 O10 85.27(17) 2_676 1_554 ? O1 U1 O4 92.6(2) . 1_564 ? O2 U1 O4 87.04(19) . 1_564 ? O9 U1 O4 78.08(16) 2_676 1_564 ? O10 U1 O4 162.63(16) 1_554 1_564 ? O1 U1 O3 92.0(2) . 2_567 ? O2 U1 O3 85.8(2) . 2_567 ? O9 U1 O3 160.49(16) 2_676 2_567 ? O10 U1 O3 75.41(16) 1_554 2_567 ? O4 U1 O3 120.87(15) 1_564 2_567 ? O1 U1 O4 87.2(2) . 2_567 ? O2 U1 O4 90.2(2) . 2_567 ? O9 U1 O4 141.47(16) 2_676 2_567 ? O10 U1 O4 133.26(16) 1_554 2_567 ? O4 U1 O4 63.53(18) 1_564 2_567 ? O3 U1 O4 57.90(15) 2_567 2_567 ? O1 U1 P1 90.63(16) . 2_567 ? O2 U1 P1 86.59(16) . 2_567 ? O9 U1 P1 170.31(13) 2_676 2_567 ? O10 U1 P1 104.05(12) 1_554 2_567 ? O4 U1 P1 92.39(11) 1_564 2_567 ? O3 U1 P1 28.64(11) 2_567 2_567 ? O4 U1 P1 29.30(11) 2_567 2_567 ? O1 U1 Cs1 131.22(16) . . ? O2 U1 Cs1 48.38(15) . . ? O9 U1 Cs1 109.57(12) 2_676 . ? O10 U1 Cs1 48.36(12) 1_554 . ? O4 U1 Cs1 133.76(12) 1_564 . ? O3 U1 Cs1 54.93(11) 2_567 . ? O4 U1 Cs1 99.77(11) 2_567 . ? P1 U1 Cs1 75.72(3) 2_567 . ? O1 U1 Cs1 32.99(16) . 1_455 ? O2 U1 Cs1 144.32(16) . 1_455 ? O9 U1 Cs1 117.50(12) 2_676 1_455 ? O10 U1 Cs1 113.37(12) 1_554 1_455 ? O4 U1 Cs1 79.26(12) 1_564 1_455 ? O3 U1 Cs1 73.79(12) 2_567 1_455 ? O4 U1 Cs1 54.24(12) 2_567 1_455 ? P1 U1 Cs1 61.54(3) 2_567 1_455 ? Cs1 U1 Cs1 127.704(13) . 1_455 ? O1 U1 Cs1 146.14(16) . 2_676 ? O2 U1 Cs1 33.60(15) . 2_676 ? O9 U1 Cs1 82.37(13) 2_676 2_676 ? O10 U1 Cs1 119.65(12) 1_554 2_676 ? O4 U1 Cs1 53.52(12) 1_564 2_676 ? O3 U1 Cs1 104.71(12) 2_567 2_676 ? O4 U1 Cs1 77.68(12) 2_567 2_676 ? P1 U1 Cs1 90.56(3) 2_567 2_676 ? Cs1 U1 Cs1 81.625(11) . 2_676 ? Cs1 U1 Cs1 124.681(8) 1_455 2_676 ? O1 U1 Cs1 77.87(16) . 2_666 ? O2 U1 Cs1 101.08(15) . 2_666 ? O9 U1 Cs1 129.63(12) 2_676 2_666 ? O10 U1 Cs1 47.09(12) 1_554 2_666 ? O4 U1 Cs1 150.28(11) 1_564 2_666 ? O3 U1 Cs1 33.46(11) 2_567 2_666 ? O4 U1 Cs1 87.70(11) 2_567 2_666 ? P1 U1 Cs1 60.06(3) 2_567 2_666 ? Cs1 U1 Cs1 54.541(11) . 2_666 ? Cs1 U1 Cs1 77.664(10) 1_455 2_666 ? Cs1 U1 Cs1 130.636(12) 2_676 2_666 ? O3 Cs1 O1 87.53(13) 1_654 1_655 ? O3 Cs1 O2 162.78(13) 1_654 2_676 ? O1 Cs1 O2 81.36(13) 1_655 2_676 ? O3 Cs1 O10 88.29(13) 1_654 1_554 ? O1 Cs1 O10 105.69(12) 1_655 1_554 ? O2 Cs1 O10 107.32(12) 2_676 1_554 ? O3 Cs1 O2 139.94(13) 1_654 . ? O1 Cs1 O2 108.41(13) 1_655 . ? O2 Cs1 O2 56.88(15) 2_676 . ? O10 Cs1 O2 52.40(12) 1_554 . ? O3 Cs1 O8 90.13(12) 1_654 2_667 ? O1 Cs1 O8 143.79(12) 1_655 2_667 ? O2 Cs1 O8 91.11(12) 2_676 2_667 ? O10 Cs1 O8 110.36(12) 1_554 2_667 ? O2 Cs1 O8 96.35(12) . 2_667 ? O3 Cs1 O6 84.32(12) 1_654 2_667 ? O1 Cs1 O6 77.95(12) 1_655 2_667 ? O2 Cs1 O6 80.53(12) 2_676 2_667 ? O10 Cs1 O6 171.65(12) 1_554 2_667 ? O2 Cs1 O6 134.15(12) . 2_667 ? O8 Cs1 O6 65.87(12) 2_667 2_667 ? O3 Cs1 O3 100.52(10) 1_654 2_567 ? O1 Cs1 O3 155.66(12) 1_655 2_567 ? O2 Cs1 O3 94.94(12) 2_676 2_567 ? O10 Cs1 O3 52.26(12) 1_554 2_567 ? O2 Cs1 O3 51.76(12) . 2_567 ? O8 Cs1 O3 59.83(12) 2_667 2_567 ? O6 Cs1 O3 125.41(11) 2_667 2_567 ? O3 Cs1 O4 112.73(12) 1_654 2_667 ? O1 Cs1 O4 52.07(11) 1_655 2_667 ? O2 Cs1 O4 50.07(11) 2_676 2_667 ? O10 Cs1 O4 146.06(11) 1_554 2_667 ? O2 Cs1 O4 105.75(11) . 2_667 ? O8 Cs1 O4 96.49(11) 2_667 2_667 ? O6 Cs1 O4 41.80(11) 2_667 2_667 ? O3 Cs1 O4 139.49(11) 2_567 2_667 ? O3 Cs1 O10 49.83(11) 1_654 2_667 ? O1 Cs1 O10 125.25(12) 1_655 2_667 ? O2 Cs1 O10 128.82(12) 2_676 2_667 ? O10 Cs1 O10 105.34(10) 1_554 2_667 ? O2 Cs1 O10 126.28(12) . 2_667 ? O8 Cs1 O10 40.32(11) 2_667 2_667 ? O6 Cs1 O10 66.80(11) 2_667 2_667 ? O3 Cs1 O10 75.55(11) 2_567 2_667 ? O4 Cs1 O10 108.58(10) 2_667 2_667 ? O3 Cs1 P1 93.48(10) 1_654 2_667 ? O1 Cs1 P1 58.61(9) 1_655 2_667 ? O2 Cs1 P1 69.50(9) 2_676 2_667 ? O10 Cs1 P1 164.04(9) 1_554 2_667 ? O2 Cs1 P1 126.37(9) . 2_667 ? O8 Cs1 P1 85.51(9) 2_667 2_667 ? O6 Cs1 P1 21.78(8) 2_667 2_667 ? O3 Cs1 P1 142.27(9) 2_567 2_667 ? O4 Cs1 P1 22.28(8) 2_667 2_667 ? O10 Cs1 P1 87.72(8) 2_667 2_667 ? O3 Cs1 P2 70.75(9) 1_654 2_667 ? O1 Cs1 P2 132.16(10) 1_655 2_667 ? O2 Cs1 P2 107.45(9) 2_676 2_667 ? O10 Cs1 P2 115.31(9) 1_554 2_667 ? O2 Cs1 P2 115.66(9) . 2_667 ? O8 Cs1 P2 20.64(8) 2_667 2_667 ? O6 Cs1 P2 58.42(9) 2_667 2_667 ? O3 Cs1 P2 71.97(8) 2_567 2_667 ? O4 Cs1 P2 97.19(8) 2_667 2_667 ? O10 Cs1 P2 21.51(7) 2_667 2_667 ? P1 Cs1 P2 80.12(3) 2_667 2_667 ? O7 Ga1 O5 108.7(2) . 2_567 ? O7 Ga1 O8 106.6(2) . 2_667 ? O5 Ga1 O8 108.7(2) 2_567 2_667 ? O7 Ga1 O6 110.0(2) . . ? O5 Ga1 O6 108.7(2) 2_567 . ? O8 Ga1 O6 114.1(2) 2_667 . ? O7 Ga1 Cs1 77.55(16) . . ? O5 Ga1 Cs1 86.36(15) 2_567 . ? O8 Ga1 Cs1 45.34(14) 2_667 . ? O6 Ga1 Cs1 158.84(16) . . ? O3 P1 O5 114.5(3) . . ? O3 P1 O4 104.5(3) . . ? O5 P1 O4 108.6(3) . . ? O3 P1 O6 111.7(3) . . ? O5 P1 O6 108.4(3) . . ? O4 P1 O6 108.9(3) . . ? O3 P1 U1 51.86(18) . 2_567 ? O5 P1 U1 124.4(2) . 2_567 ? O4 P1 U1 52.74(18) . 2_567 ? O6 P1 U1 127.0(2) . 2_567 ? O3 P1 Cs1 95.8(2) . 2_667 ? O5 P1 Cs1 149.6(2) . 2_667 ? O4 P1 Cs1 63.2(2) . 2_667 ? O6 P1 Cs1 54.32(19) . 2_667 ? U1 P1 Cs1 75.88(4) 2_567 2_667 ? O9 P2 O10 112.0(3) . . ? O9 P2 O7 109.0(3) . . ? O10 P2 O7 110.4(3) . . ? O9 P2 O8 110.9(3) . . ? O10 P2 O8 105.9(3) . . ? O7 P2 O8 108.6(3) . . ? O9 P2 Cs1 149.2(2) . 2_667 ? O10 P2 Cs1 63.55(19) . 2_667 ? O7 P2 Cs1 100.59(19) . 2_667 ? O8 P2 Cs1 49.04(18) . 2_667 ? O9 P2 Cs1 95.2(2) . 1_556 ? O10 P2 Cs1 40.79(19) . 1_556 ? O7 P2 Cs1 149.4(2) . 1_556 ? O8 P2 Cs1 78.52(19) . 1_556 ? Cs1 P2 Cs1 60.78(3) 2_667 1_556 ? U1 O1 Cs1 129.0(2) . 1_455 ? U1 O2 Cs1 128.3(2) . 2_676 ? U1 O2 Cs1 107.8(2) . . ? Cs1 O2 Cs1 123.12(15) 2_676 . ? P1 O3 U1 99.5(2) . 2_567 ? P1 O3 Cs1 131.7(3) . 1_456 ? U1 O3 Cs1 120.49(17) 2_567 1_456 ? P1 O3 Cs1 130.6(3) . 2_567 ? U1 O3 Cs1 88.88(13) 2_567 2_567 ? Cs1 O3 Cs1 79.48(10) 1_456 2_567 ? P1 O4 U1 144.0(3) . 1_546 ? P1 O4 U1 98.0(2) . 2_567 ? U1 O4 U1 116.47(18) 1_546 2_567 ? P1 O4 Cs1 94.5(2) . 2_667 ? U1 O4 Cs1 94.50(15) 1_546 2_667 ? U1 O4 Cs1 91.67(14) 2_567 2_667 ? P1 O5 Ga1 139.5(3) . 2_567 ? P1 O6 Ga1 127.6(3) . . ? P1 O6 Cs1 103.9(2) . 2_667 ? Ga1 O6 Cs1 118.7(2) . 2_667 ? P2 O7 Ga1 129.8(3) . . ? P2 O8 Ga1 137.0(3) . 2_667 ? P2 O8 Cs1 110.3(2) . 2_667 ? Ga1 O8 Cs1 111.70(19) 2_667 2_667 ? P2 O9 U1 145.8(3) . 2_676 ? P2 O10 U1 138.7(3) . 1_556 ? P2 O10 Cs1 121.0(2) . 1_556 ? U1 O10 Cs1 99.00(16) 1_556 1_556 ? P2 O10 Cs1 94.9(2) . 2_667 ? U1 O10 Cs1 105.97(15) 1_556 2_667 ? Cs1 O10 Cs1 74.66(10) 1_556 2_667 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag U1 O1 1.774(5) . ? U1 O2 1.779(5) . ? U1 O9 2.283(5) 2_676 ? U1 O10 2.295(5) 1_554 ? U1 O4 2.385(5) 1_564 ? U1 O3 2.482(5) 2_567 ? U1 O4 2.501(5) 2_567 ? U1 P1 3.1119(16) 2_567 ? U1 Cs1 4.2022(6) . ? U1 Cs1 4.4600(6) 1_455 ? U1 Cs1 4.4889(6) 2_676 ? U1 Cs1 4.8688(6) 2_666 ? Cs1 O3 3.115(5) 1_654 ? Cs1 O1 3.125(5) 1_655 ? Cs1 O2 3.164(5) 2_676 ? Cs1 O10 3.180(5) 1_554 ? Cs1 O2 3.300(5) . ? Cs1 O8 3.323(5) 2_667 ? Cs1 O6 3.383(5) 2_667 ? Cs1 O3 3.440(5) 2_567 ? Cs1 O4 3.621(5) 2_667 ? Cs1 O10 3.709(5) 2_667 ? Cs1 P1 4.0431(18) 2_667 ? Cs1 P2 4.1272(17) 2_667 ? Ga1 O7 1.801(5) . ? Ga1 O5 1.807(5) 2_567 ? Ga1 O8 1.822(5) 2_667 ? Ga1 O6 1.824(5) . ? P1 O3 1.512(5) . ? P1 O5 1.534(5) . ? P1 O4 1.538(5) . ? P1 O6 1.546(5) . ? P1 U1 3.1119(16) 2_567 ? P1 Cs1 4.0431(18) 2_667 ? P2 O9 1.505(5) . ? P2 O10 1.519(5) . ? P2 O7 1.552(5) . ? P2 O8 1.552(5) . ? P2 Cs1 4.1272(17) 2_667 ? P2 Cs1 4.1708(18) 1_556 ? O1 Cs1 3.125(5) 1_455 ? O2 Cs1 3.164(5) 2_676 ? O3 U1 2.482(5) 2_567 ? O3 Cs1 3.115(5) 1_456 ? O3 Cs1 3.440(5) 2_567 ? O4 U1 2.385(5) 1_546 ? O4 U1 2.501(5) 2_567 ? O4 Cs1 3.621(5) 2_667 ? O5 Ga1 1.807(5) 2_567 ? O6 Cs1 3.383(5) 2_667 ? O8 Ga1 1.822(5) 2_667 ? O8 Cs1 3.323(5) 2_667 ? O9 U1 2.283(5) 2_676 ? O10 U1 2.295(5) 1_556 ? O10 Cs1 3.180(5) 1_556 ? O10 Cs1 3.709(5) 2_667 ?