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Information card for entry 4308421
Preview
| Coordinates | 4308421.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C50 H44 Cl2 N6 Ni O10 |
|---|---|
| Calculated formula | C50 H44 Cl2 N6 Ni O10 |
| Title of publication | Novel Chiral "Calixsalen" Macrocycle and Chiral Robson-type Macrocyclic Complexes |
| Authors of publication | Gao, Jian; Reibenspies, Joseph H.; Zingaro, Ralph A.; Woolley, F. Ross; Martell, Arthur E.; Clearfield, Abraham |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2005 |
| Journal volume | 44 |
| Journal issue | 2 |
| Pages of publication | 232 - 241 |
| a | 9.522 ± 0.012 Å |
| b | 16.6 ± 0.02 Å |
| c | 14.844 ± 0.018 Å |
| α | 90° |
| β | 100.16 ± 0.02° |
| γ | 90° |
| Cell volume | 2310 ± 5 Å3 |
| Cell temperature | 110 ± 2 K |
| Ambient diffraction temperature | 110 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.0888 |
| Residual factor for significantly intense reflections | 0.0662 |
| Weighted residual factors for significantly intense reflections | 0.1482 |
| Weighted residual factors for all reflections included in the refinement | 0.1566 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.06 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
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