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Information card for entry 4308454
Preview
| Coordinates | 4308454.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C22 H36 N5 Yb |
|---|---|
| Calculated formula | C22 H36 N5 Yb |
| SMILES | [Yb]123456789([N](=C(N1C(C)C)N=C(N(C)C)N(C)C)C(C)C)([cH]1[cH]2[cH]3[cH]4[cH]51)[cH]1[cH]9[cH]8[cH]7[cH]61 |
| Title of publication | Reactivity of Organolanthanide and Organolithium Complexes Containing the Guanidinate Ligands toward Isocyanate or Carbodiimide: Synthesis and Crystal Structures |
| Authors of publication | Jie Zhang; Xigeng Zhou; Ruifang Cai; Linhong Weng |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2005 |
| Journal volume | 44 |
| Pages of publication | 716 - 722 |
| a | 9.686 ± 0.004 Å |
| b | 10.351 ± 0.004 Å |
| c | 13.23 ± 0.005 Å |
| α | 72.912 ± 0.005° |
| β | 70.051 ± 0.004° |
| γ | 83.91 ± 0.005° |
| Cell volume | 1191.8 ± 0.8 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0388 |
| Residual factor for significantly intense reflections | 0.034 |
| Weighted residual factors for significantly intense reflections | 0.0894 |
| Weighted residual factors for all reflections included in the refinement | 0.0911 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.143 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 179122 (current) | 2016-03-22 | cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/84. |
4308454.cif |
| 120081 | 2014-07-11 | Adding DOIs to range 4/30 structures. | 4308454.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4308454.cif |
| 1526 | 2010-09-26 | cif/4/ Adding new CIFs from Inorg. Chem. 2005 deposited via Web deposition site to the COD test database (and transferede to the main COD database after renaming). |
4308454.cif |
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Users of the data should acknowledge the original authors of the
structural data.