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Information card for entry 4308508
Preview
| Coordinates | 4308508.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C37 H70 Cl N17 Ni4 O9 S4 |
|---|---|
| Calculated formula | C37 H70 Cl N17 Ni4 O9 S4 |
| Title of publication | Structural Variety and Magnetic Properties of Tetranuclear Nickel(II) Complexes with a Central μ4-Azide |
| Authors of publication | Serhiy Demeshko; Guido Leibeling; Walter Maringgele; Franc Meyer; Christopher Mennerich; Hans-Henning Klauss; Hans Pritzkow |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2005 |
| Journal volume | 44 |
| Pages of publication | 519 - 528 |
| a | 12.6894 ± 0.0009 Å |
| b | 19.3299 ± 0.0013 Å |
| c | 22.3243 ± 0.0015 Å |
| α | 90° |
| β | 91.48 ± 0.001° |
| γ | 90° |
| Cell volume | 5474 ± 0.6 Å3 |
| Cell temperature | 103 ± 2 K |
| Ambient diffraction temperature | 103 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.0714 |
| Residual factor for significantly intense reflections | 0.0658 |
| Weighted residual factors for significantly intense reflections | 0.1654 |
| Weighted residual factors for all reflections included in the refinement | 0.1686 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.107 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
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