Crystallography Open Database

Information card for entry 4308832

Preview

Coordinates	4308832.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C51 H62 Ag2 F12 N8 O P2 Si4
Calculated formula	C51 H62 Ag2 F12 N8 O P2 Si4
Title of publication	Relationship between the Ratio of Ligand to Metal and the Coordinating Ability of Anions. Synthesis and Structural Properties of AgX-Bearing Bis(4-pyridyl)dimethylsilane (X-= NO2-, NO3-, CF3SO3-, and PF6-)
Authors of publication	Jung Woon Lee; Eun Ae Kim; Yun Ju Kim; Young-A Lee; Youngshang Pak; Ok-Sang Jung
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	3151 - 3155
a	11.1074 ± 0.0008 Å
b	16.54 ± 0.0011 Å
c	18.6656 ± 0.0013 Å
α	77.082 ± 0.001°
β	80.911 ± 0.001°
γ	76.968 ± 0.001°
Cell volume	3235.3 ± 0.4 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1727
Residual factor for significantly intense reflections	0.0537
Weighted residual factors for significantly intense reflections	0.126
Weighted residual factors for all reflections included in the refinement	0.1834
Goodness-of-fit parameter for all reflections included in the refinement	0.925
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179126 (current)	2016-03-22	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/88.	4308832.cif
120081	2014-07-11	Adding DOIs to range 4/30 structures.	4308832.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4308832.cif
5312	2011-01-03	cif/ Adding files, updated with the 'cif_fix_enum' program and the cif_core.dic dictionary. The enumerator values were fixed, mostly incorrect case, but also some values that had extra underscores, dashes or spaces. Unfortunately, 22 had non-ASCII characters with the 8-th bit set, and these got incorrectly interpreted as latin1 characters and converted to their UTF8 equivalents by Perl. To fix the structures, however, they need to be redeposited from the original files with the new CIFParser/cif_filter version.	4308832.cif
1526	2010-09-26	cif/4/ Adding new CIFs from Inorg. Chem. 2005 deposited via Web deposition site to the COD test database (and transferede to the main COD database after renaming).	4308832.cif