#------------------------------------------------------------------------------ #$Date: 2022-03-03 21:08:41 +0000 (Thu, 03 Mar 2022) $ #$Revision: 273252 $ #$URL: svn://www.crystallography.net/cod/cif/4/51/93/4519345.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519345 loop_ _publ_author_name 'Stepanova, Valeria A.' 'Guerrero, Andres' 'Schull, Cullen' 'Christensen, Joshua' 'Trudeau, Claire' 'Cook, Joshua' 'Wolmutt, Kyle' 'Blochwitz, Jordan' 'Ismail, Abdelrahman' 'West, Joseph K.' 'Wheaton, Amelia M.' 'Guzei, Ilia A.' 'Yao, Bin' 'Kubatova, Alena' _publ_section_title ; Hybrid Synthetic and Computational Study of an Optimized, Solvent-Free Approach to Curcuminoids ; _journal_issue 8 _journal_name_full 'ACS Omega' _journal_page_first 7257 _journal_page_last 7277 _journal_paper_doi 10.1021/acsomega.1c07006 _journal_volume 7 _journal_year 2022 _chemical_formula_moiety 'C24 H33 B3 N2 O8, C0.938 H1.877 Cl1.877' _chemical_formula_sum 'C24.94 H34.88 B3 Cl1.88 N2 O8' _chemical_formula_weight 589.66 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2020-08-25 _audit_creation_method ; Olex2 1.3-beta (compiled 2020.07.31 svn.rc2a77460 for OlexSys, GUI svn.r6145) ; _cell_angle_alpha 90 _cell_angle_beta 101.232(15) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 18.071(3) _cell_length_b 7.8493(16) _cell_length_c 21.159(3) _cell_measurement_reflns_used 8726 _cell_measurement_temperature 100.0 _cell_measurement_theta_max 70.088 _cell_measurement_theta_min 2.947 _cell_volume 2943.8(9) _computing_cell_refinement 'SAINT V8.40A (Bruker AXS Inc., 2018)' _computing_data_collection 'Bruker Instrument Service, BIS, v.6.2.12 (Bruker AXS Inc., 2019)' _computing_data_reduction 'SAINT V8.40A (Bruker AXS Inc., 2018)' _computing_molecular_graphics 'Olex2 1.3-beta (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3-beta (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2015b)' _computing_structure_solution 'XT (Sheldrick, 2015a)' _diffrn_ambient_temperature 100.0 _diffrn_detector '100 \\times 140 mm^2^ CMOS sensor' _diffrn_detector_area_resol_mean 7.41 _diffrn_detector_type 'Bruker PHOTON III' _diffrn_measured_fraction_theta_full 0.988 _diffrn_measured_fraction_theta_max 0.983 _diffrn_measurement_device '\k-geometry four-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 VENTURE' _diffrn_measurement_method '0.5\% \w and 0.5\% \f scans' _diffrn_radiation_collimation 'focusing mirror' _diffrn_radiation_detector 'Bruker PHOTON III' _diffrn_radiation_monochromator 'multilayer mirror' _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54178 _diffrn_radiation_xray_symbol K-L~3~ _diffrn_reflns_av_R_equivalents 0.0623 _diffrn_reflns_av_unetI/netI 0.0430 _diffrn_reflns_Laue_measured_fraction_full 0.988 _diffrn_reflns_Laue_measured_fraction_max 0.983 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_k_max 7 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 25 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 26354 _diffrn_reflns_point_group_measured_fraction_full 0.988 _diffrn_reflns_point_group_measured_fraction_max 0.983 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 70.139 _diffrn_reflns_theta_min 2.946 _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_current 1.1 _diffrn_source_power 0.055 _diffrn_source_type 'Incoatec I\mS 3.0' _diffrn_source_voltage 50.0 _exptl_absorpt_coefficient_mu 2.294 _exptl_absorpt_correction_T_max 0.7533 _exptl_absorpt_correction_T_min 0.6767 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Krause et al., 2015) was used for absorption correction.' _exptl_crystal_colour yellow _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.330 _exptl_crystal_description plate _exptl_crystal_F_000 1238 _exptl_crystal_size_max 0.03 _exptl_crystal_size_mid 0.02 _exptl_crystal_size_min 0.01 _refine_diff_density_max 0.345 _refine_diff_density_min -0.231 _refine_diff_density_rms 0.045 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.030 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 378 _refine_ls_number_reflns 5508 _refine_ls_number_restraints 5 _refine_ls_restrained_S_all 1.030 _refine_ls_R_factor_all 0.0534 _refine_ls_R_factor_gt 0.0360 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0411P)^2^+0.5803P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0831 _refine_ls_wR_factor_ref 0.0907 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4232 _reflns_number_total 5508 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ao1c07006_si_002.cif _cod_data_source_block stepanova09 _cod_database_code 4519345 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.977 _shelx_estimated_absorpt_t_min 0.934 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 2. Restrained distances O1-H1 0.87 with sigma of 0.01 Cl2A-C25A = Cl1-C25A 1.7602 with sigma of 0.01 Cl1-Cl2A 2.9338 with sigma of 0.01 3. Uiso/Uaniso restraints and constraints Uiso(C25A) = Uiso(Cl2A) Uiso(Cl2A) = Uiso(C25A) 4. Others -1*[Sof(Cl1)]+1*[Sof(Cl2)+Sof(C25)+Sof(H25A)+Sof(H25B)]+1*[Sof(C25A)+ Sof(H25C)+Sof(H25D)+Sof(Cl2A)]=0 with esd of 0 Sof(Cl2)=Sof(C25)=Sof(H25A)=Sof(H25B)=FVAR(2) Sof(C25A)=Sof(H25C)=Sof(H25D)=Sof(Cl2A)=FVAR(3) 5.a Secondary CH2 refined with riding coordinates: C9(H9A,H9B), C10(H10A,H10B), C11(H11A,H11B), C21(H21A,H21B), C22(H22A,H22B), C23(H23A,H23B), C25(H25A,H25B), C25A(H25C,H25D) 5.b Aromatic/amide H refined with riding coordinates: C3(H3), C4(H4), C5(H5), C7(H7), C15(H15), C16(H16), C17(H17), C19(H19) 5.c Idealised Me refined as rotating group: C8(H8A,H8B,H8C), C12(H12A,H12B,H12C), C20(H20A,H20B,H20C), C24(H24A,H24B,H24C) ; _shelx_res_file ; TITL Stepanova09_A_a.res in P2(1)/n stepanova09.res created by SHELXL-2018/3 at 10:53:20 on 25-Aug-2020 REM Old TITL Stepanova09_A in P2(1)/n REM SHELXT solution in P2(1)/n REM R1 0.209, Rweak 0.009, Alpha 0.019, Orientation as input REM Formula found by SHELXT: C25 O10 CELL 1.54178 18.071 7.8493 21.1593 90 101.232 90 ZERR 4 0.0029 0.0016 0.0032 0 0.015 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H B Cl N O UNIT 99.75 139.51 12 7.51 8 32 EQIV $1 1-X,1-Y,1-Z EADP C25A Cl2A EADP Cl2A C25A DFIX 0.87 0.01 O1 H1 DFIX 1.7602 0.01 Cl2A C25A Cl1 C25A DFIX 2.9338 0.01 Cl1 Cl2A SUMP 0 0 -1 2 1 3 1 4 L.S. 20 PLAN 5 SIZE 0.01 0.02 0.03 TEMP -173.15 CONF HTAB O1 O2_$1 BOND $H LIST 4 MORE -1 fmap 2 acta REM REM REM WGHT 0.041100 0.580300 FVAR 0.50359 0.93842 0.89278 0.04565 O1 6 0.474180 0.333747 0.437622 11.00000 0.02394 0.01833 = 0.02143 -0.00222 0.01036 -0.00375 H1 2 0.462786 0.372900 0.472789 11.00000 -1.50000 O2 6 0.555243 0.576165 0.444610 11.00000 0.02173 0.01516 = 0.02035 -0.00057 0.00954 -0.00282 O3 6 0.634811 0.605895 0.365206 11.00000 0.02089 0.01683 = 0.02223 -0.00046 0.00982 -0.00191 O4 6 0.553903 0.360689 0.364627 11.00000 0.01971 0.01742 = 0.02039 -0.00325 0.00683 -0.00230 O5 6 0.674871 0.720374 0.470081 11.00000 0.02022 0.01758 = 0.02365 -0.00162 0.00473 0.00001 O6 6 0.773015 0.711056 0.581018 11.00000 0.02986 0.03692 = 0.02941 -0.00062 -0.00193 0.00916 O7 6 0.579575 0.464206 0.266621 11.00000 0.02413 0.02699 = 0.01785 -0.00205 0.00888 0.00477 O8 6 0.513875 0.535540 0.147348 11.00000 0.04075 0.03653 = 0.01842 -0.00089 0.00435 0.00848 N1 5 0.566462 0.855781 0.397734 11.00000 0.01770 0.01693 = 0.02210 0.00097 0.00591 -0.00293 N2 5 0.683127 0.324814 0.345328 11.00000 0.01866 0.01786 = 0.02708 -0.00095 0.00607 -0.00186 C1 1 0.670413 0.842748 0.513108 11.00000 0.02055 0.01797 = 0.02156 -0.00151 0.00779 -0.00500 C2 1 0.722111 0.842316 0.572603 11.00000 0.02323 0.02273 = 0.02828 0.00091 0.00496 -0.00129 C3 1 0.717922 0.967949 0.617343 11.00000 0.03184 0.03616 = 0.02428 -0.00501 0.00042 -0.00209 AFIX 43 H3 2 0.751837 0.965756 0.657741 11.00000 -1.20000 AFIX 0 C4 1 0.664677 1.098056 0.604167 11.00000 0.03657 0.03145 = 0.02916 -0.01151 0.00622 -0.00141 AFIX 43 H4 2 0.662885 1.183879 0.635490 11.00000 -1.20000 AFIX 0 C5 1 0.614735 1.103176 0.546206 11.00000 0.02792 0.01994 = 0.03211 -0.00285 0.00915 -0.00050 AFIX 43 H5 2 0.578849 1.192667 0.537070 11.00000 -1.20000 AFIX 0 C6 1 0.617481 0.973930 0.500533 11.00000 0.02189 0.01677 = 0.02380 -0.00021 0.00869 -0.00461 C7 1 0.568103 0.978680 0.438349 11.00000 0.02032 0.01461 = 0.02573 0.00043 0.00796 -0.00132 AFIX 43 H7 2 0.536074 1.074365 0.427022 11.00000 -1.20000 AFIX 0 C8 1 0.815857 0.688645 0.644517 11.00000 0.03721 0.05239 = 0.03225 0.00780 -0.00021 0.00751 AFIX 137 H8A 2 0.848369 0.588354 0.645543 11.00000 -1.50000 H8B 2 0.781576 0.672406 0.674650 11.00000 -1.50000 H8C 2 0.847090 0.789761 0.657031 11.00000 -1.50000 AFIX 0 C9 1 0.517907 0.870151 0.333342 11.00000 0.01914 0.02015 = 0.02475 -0.00015 0.00159 -0.00010 AFIX 23 H9A 2 0.476191 0.950501 0.335317 11.00000 -1.20000 H9B 2 0.495515 0.757511 0.320064 11.00000 -1.20000 AFIX 0 C10 1 0.562041 0.932455 0.283492 11.00000 0.02402 0.02299 = 0.02417 0.00271 0.00201 -0.00422 AFIX 23 H10A 2 0.580202 1.049734 0.294569 11.00000 -1.20000 H10B 2 0.606701 0.858606 0.284674 11.00000 -1.20000 AFIX 0 C11 1 0.514498 0.931322 0.215856 11.00000 0.02785 0.02948 = 0.02471 -0.00267 0.00026 0.00491 AFIX 23 H11A 2 0.488576 0.820033 0.207907 11.00000 -1.20000 H11B 2 0.475348 1.020857 0.212571 11.00000 -1.20000 AFIX 0 C12 1 0.561180 0.961688 0.164500 11.00000 0.04049 0.03631 = 0.02504 0.00149 0.00252 -0.00413 AFIX 137 H12A 2 0.528048 0.961979 0.121910 11.00000 -1.50000 H12B 2 0.598732 0.870808 0.166388 11.00000 -1.50000 H12C 2 0.586883 1.071873 0.172063 11.00000 -1.50000 AFIX 0 C13 1 0.616756 0.423210 0.220432 11.00000 0.02517 0.01765 = 0.02402 -0.00566 0.01306 -0.00403 C14 1 0.583494 0.461598 0.155821 11.00000 0.03408 0.02044 = 0.02476 -0.00388 0.01184 -0.00337 C15 1 0.621901 0.419822 0.107078 11.00000 0.04677 0.03127 = 0.02324 -0.00568 0.01568 -0.00890 AFIX 43 H15 2 0.600358 0.448313 0.063765 11.00000 -1.20000 AFIX 0 C16 1 0.691670 0.336628 0.120562 11.00000 0.04202 0.03203 = 0.03585 -0.01366 0.02607 -0.01020 AFIX 43 H16 2 0.717189 0.310169 0.086564 11.00000 -1.20000 AFIX 0 C17 1 0.723229 0.293297 0.182558 11.00000 0.02751 0.02843 = 0.03945 -0.01201 0.01956 -0.00480 AFIX 43 H17 2 0.769899 0.233880 0.191579 11.00000 -1.20000 AFIX 0 C18 1 0.686018 0.337414 0.233130 11.00000 0.02433 0.01999 = 0.03016 -0.00765 0.01288 -0.00638 C19 1 0.715264 0.284657 0.298160 11.00000 0.01797 0.01825 = 0.03645 -0.00437 0.00862 -0.00154 AFIX 43 H19 2 0.759906 0.217749 0.306703 11.00000 -1.20000 AFIX 0 C20 1 0.477218 0.571297 0.082606 11.00000 0.05632 0.04533 = 0.02165 -0.00061 0.00184 0.00776 AFIX 137 H20A 2 0.470358 0.465111 0.057791 11.00000 -1.50000 H20B 2 0.508257 0.650138 0.062997 11.00000 -1.50000 H20C 2 0.427892 0.623171 0.082616 11.00000 -1.50000 AFIX 0 C21 1 0.715900 0.265387 0.411102 11.00000 0.02635 0.02491 = 0.03066 0.00556 0.00540 0.00280 AFIX 23 H21A 2 0.727005 0.142105 0.409616 11.00000 -1.20000 H21B 2 0.678224 0.280774 0.438899 11.00000 -1.20000 AFIX 0 C22 1 0.787579 0.359030 0.440851 11.00000 0.02499 0.03169 = 0.03431 0.00218 0.00560 0.00051 AFIX 23 H22A 2 0.777085 0.482788 0.441139 11.00000 -1.20000 H22B 2 0.826104 0.340115 0.414118 11.00000 -1.20000 AFIX 0 C23 1 0.818530 0.299927 0.509256 11.00000 0.03398 0.04693 = 0.03440 0.00137 0.00263 0.00485 AFIX 23 H23A 2 0.825754 0.174897 0.509344 11.00000 -1.20000 H23B 2 0.781333 0.325869 0.536618 11.00000 -1.20000 AFIX 0 C24 1 0.893191 0.385102 0.537764 11.00000 0.03432 0.05973 = 0.04448 -0.01149 -0.00274 0.00807 AFIX 137 H24A 2 0.930636 0.356944 0.511558 11.00000 -1.50000 H24B 2 0.910837 0.344357 0.581908 11.00000 -1.50000 H24C 2 0.886196 0.508877 0.538192 11.00000 -1.50000 AFIX 0 B1 3 0.527747 0.427101 0.415769 11.00000 0.01674 0.01767 = 0.01746 0.00257 0.00436 0.00143 B2 3 0.609805 0.679666 0.418160 11.00000 0.01909 0.01661 = 0.02201 0.00021 0.00695 -0.00211 B3 3 0.610444 0.447802 0.337163 11.00000 0.01880 0.01958 = 0.01859 0.00054 0.00722 0.00119 CL1 4 0.363956 0.525502 0.292589 21.00000 0.04036 0.02582 = 0.05664 -0.01204 -0.00348 0.00383 PART 1 CL2 4 0.328821 0.203702 0.226609 31.00000 0.03115 0.03630 = 0.04564 -0.01695 -0.00632 0.00020 C25 1 0.395674 0.317615 0.282088 31.00000 0.02476 0.02719 = 0.04934 -0.01348 -0.00785 0.00419 AFIX 23 H25A 2 0.443816 0.322889 0.266456 31.00000 -1.20000 H25B 2 0.405146 0.257507 0.324024 31.00000 -1.20000 AFIX 0 PART 2 C25A 1 0.408450 0.364776 0.255645 41.00000 0.03415 AFIX 23 H25C 2 0.444826 0.417703 0.232115 41.00000 -1.20000 H25D 2 0.437076 0.289524 0.289300 41.00000 -1.20000 AFIX 0 CL2A 4 0.343667 0.241915 0.201782 41.00000 0.03415 HKLF 4 REM Stepanova09_A_a.res in P2(1)/n REM wR2 = 0.090699, GooF = S = 1.03049, Restrained GooF = 1.03031 for all data REM R1 = 0.035968 for 4232 Fo > 4sig(Fo) and 0.053427 for all 5508 data REM 378 parameters refined using 5 restraints END WGHT 0.0411 0.5803 REM Highest difference peak 0.345, deepest hole -0.231, 1-sigma level 0.045 Q1 1 0.3716 0.2915 0.1799 11.00000 0.05 0.35 Q2 1 0.3156 0.4738 0.2864 11.00000 0.05 0.24 Q3 1 0.5870 0.9593 0.4776 11.00000 0.05 0.21 Q4 1 0.3609 0.4925 0.3342 11.00000 0.05 0.20 Q5 1 0.6636 0.4119 0.2357 11.00000 0.05 0.20 ; _shelx_res_checksum 44308 _shelx_hkl_file ; -1 0 0 -1.2170 1.00022 4 -2 0 0 0.80220 2.86859 4 3 0 0 1.69634 3.42175 5 -3 0 0 -1.2838 3.86682 4 4 0 0 958.054 28.1093 5 -4 0 0 928.459 28.6121 4 -5 0 0 -2.3264 5.99472 4 5 0 0 2.07259 4.99548 5 6 0 0 455.243 18.7333 5 -6 0 0 464.855 19.4142 4 -7 0 0 -1.4346 6.47546 4 7 0 0 3.41147 6.03587 5 -8 0 0 737.109 28.5607 4 8 0 0 719.343 28.0769 5 9 0 0 0.85015 6.87661 5 -9 0 0 -8.4588 6.96613 4 -10 0 0 144.261 15.7490 4 10 0 0 154.736 14.9476 5 11 0 0 5.68983 4.55745 3 -11 0 0 4.64547 3.82539 3 -11 0 0 -0.3741 8.23849 4 11 0 0 -0.0072 12.2632 5 12 0 0 116.682 11.8393 6 12 0 0 105.387 9.79029 3 -12 0 0 96.7402 15.2555 6 -12 0 0 86.1159 16.4696 4 12 0 0 112.464 16.2301 5 -12 0 0 99.1688 8.32715 3 -13 0 0 -14.998 8.84195 4 13 0 0 -0.6919 5.40411 6 -13 0 0 -8.2553 7.76804 6 13 0 0 1.57209 5.02885 3 -13 0 0 1.45465 4.13691 3 14 0 0 26.4337 7.10337 6 14 0 0 16.1240 9.20592 3 -14 0 0 8.18724 9.00097 6 -14 0 0 11.4829 11.8065 4 -14 0 0 9.42437 5.07228 2 -15 0 0 7.30424 9.56970 6 -15 0 0 -1.6738 17.2396 4 15 0 0 -0.5762 5.62865 3 15 0 0 0.07740 5.60724 6 -15 0 0 -0.8305 4.26450 3 16 0 0 94.0869 10.5798 3 -16 0 0 128.278 22.7702 4 -16 0 0 106.760 17.4115 6 -16 0 0 101.572 9.14628 3 -17 0 0 12.0716 13.4708 6 -17 0 0 -11.132 21.8860 4 -17 0 0 -1.5739 5.79198 3 -18 0 0 502.632 18.8963 3 -18 0 0 518.631 27.0467 6 18 0 0 535.069 20.1914 3 19 0 0 -2.8158 4.09816 3 -19 0 0 -6.1853 7.40230 6 -19 0 0 0.20325 3.59964 3 -20 0 0 774.409 29.8461 6 20 0 0 742.561 23.2835 3 -20 0 0 824.774 24.0986 3 -21 0 0 -0.4031 2.45959 3 -21 0 0 -1.2075 5.63785 6 0 -1 0 -0.0345 5.89507 5 -1 -1 0 2049.30 54.1704 4 -1 -1 0 2003.58 55.1587 5 1 -1 0 1974.77 56.2640 5 2 -1 0 966.673 31.0403 5 -2 -1 0 991.023 28.9653 4 -2 1 0 972.674 26.9997 4 3 -1 0 6.13497 7.80093 5 -3 -1 0 6.15905 5.85614 4 -3 -1 0 7.51678 1.85691 2 -3 1 0 8.41654 3.54579 4 -4 -1 0 627.951 22.7120 4 4 -1 0 645.522 25.7062 5 -4 1 0 657.360 20.6444 4 -5 -1 0 685.071 25.3415 4 5 -1 0 690.834 27.9170 5 -5 1 0 689.772 22.7396 4 -6 -1 0 177.541 14.1605 4 6 -1 0 163.884 16.6704 5 -6 1 0 187.139 11.5687 4 -7 -1 0 1186.04 40.0657 4 7 -1 0 1160.71 41.9431 5 7 1 0 1170.69 35.3902 5 -7 1 0 1211.28 37.8206 4 -8 -1 0 1385.43 46.5373 4 8 -1 0 1355.15 48.2438 5 -8 1 0 1426.43 44.4248 4 8 1 0 1334.51 40.8186 5 9 -1 0 53.6249 11.7750 5 -9 -1 0 66.0104 12.1522 4 9 1 0 52.0644 8.96241 5 -9 1 0 51.2723 9.38286 4 -10 -1 0 394.491 23.7146 4 10 -1 0 390.956 25.3366 5 -10 1 0 368.935 21.1814 4 10 1 0 344.306 17.2762 5 11 -1 0 114.910 19.2101 5 -11 -1 0 144.100 14.8024 6 -11 -1 0 125.728 9.69509 2 -11 -1 0 132.641 8.80372 3 -11 -1 0 162.021 18.5862 4 11 -1 0 94.0110 10.4766 6 -11 1 0 134.828 9.19778 3 11 1 0 114.934 9.62422 3 -11 1 0 149.523 16.1291 4 12 -1 0 193.534 22.8855 5 -12 -1 0 172.393 10.0651 3 12 -1 0 160.417 10.9202 3 12 -1 0 181.537 12.1898 6 -12 -1 0 143.399 19.4706 4 -12 -1 0 171.258 16.8118 6 12 1 0 168.710 12.7006 6 12 1 0 168.430 11.3926 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2 -5 0.93475 5.44377 3 -13 2 5 2.39539 8.93304 4 -12 -2 5 23.4822 8.78145 6 -12 -2 5 28.7848 4.78465 3 12 -2 -5 45.9954 7.54062 3 12 -2 -5 33.9170 13.4792 5 12 2 -5 29.2476 6.45546 3 -12 2 5 26.9375 4.93666 3 -12 2 5 33.7396 8.11414 2 -12 2 5 20.7621 9.65121 4 -11 -2 5 71.7489 12.8761 6 11 -2 -5 61.9564 14.3596 5 11 -2 -5 47.6012 8.08372 1 -11 -2 5 70.4022 6.66628 3 11 2 -5 56.5442 8.96857 3 -11 2 5 53.3730 11.9411 2 -11 2 5 54.5716 7.96890 3 -11 2 5 46.2852 9.66807 4 -10 -2 5 263.836 15.8314 6 10 -2 -5 243.272 24.0075 5 -10 2 5 248.105 15.2268 2 -10 2 5 278.916 17.0549 4 -9 -2 5 20.2512 3.38477 2 9 -2 -5 16.5749 11.7873 5 -9 2 5 26.4738 7.25570 4 -9 2 5 16.5019 5.78986 2 8 -2 -5 2246.08 71.6291 5 -8 -2 5 2071.08 56.4115 2 -8 2 5 2039.78 61.6523 2 -8 2 5 1986.31 60.3652 4 7 -2 -5 96.0101 18.2851 5 -7 -2 5 98.8336 5.84605 2 -7 2 5 85.7967 8.75963 4 -7 2 5 103.868 9.67523 2 -6 -2 5 829.972 23.7040 2 6 -2 -5 721.162 35.8237 5 -6 2 5 759.752 24.6104 4 -6 2 5 795.939 27.0149 2 5 -2 -5 2015.04 63.7131 5 -5 -2 5 1853.80 51.9486 2 -5 2 5 1861.78 54.8492 2 -4 -2 5 27.9955 4.36795 2 4 -2 -5 27.1228 11.0401 5 -4 -2 5 40.3734 6.33483 5 -4 2 5 24.9925 5.38296 2 3 -2 -5 312.399 22.5976 5 -3 -2 5 315.992 16.0701 5 -3 -2 5 349.501 13.0774 2 -3 2 5 332.882 13.7960 2 -2 -2 5 259.571 14.8421 5 2 -2 -5 236.298 19.2980 5 -2 -2 5 248.366 11.5297 2 -2 2 5 246.975 11.2900 2 -1 -2 5 72.7829 8.26249 2 -1 -2 5 76.8596 11.5764 5 -1 2 5 82.5812 6.93432 2 0 -2 -5 574.643 17.1547 4 0 -2 5 590.341 21.0866 2 0 -2 5 586.965 24.1115 5 0 2 5 573.410 18.9012 2 1 -2 5 1441.58 44.7069 5 -1 -2 -5 1326.17 38.6075 4 1 2 5 1342.98 38.5841 2 2 -2 5 7.56055 8.00443 5 -2 -2 -5 27.4460 5.79320 4 2 2 5 9.00706 3.43932 2 3 -2 5 763.323 40.9708 5 -3 -2 -5 746.304 26.2343 4 3 2 5 794.837 23.7966 2 -3 2 -5 750.544 31.4348 4 -4 -2 -5 81.8498 10.5326 4 4 -2 5 85.6200 15.4806 5 4 2 5 81.6657 6.69609 2 -4 2 -5 107.095 10.1832 4 -5 -2 -5 31.0169 9.64778 4 5 -2 5 37.1155 11.0374 5 -5 2 -5 40.4889 7.58902 4 -6 -2 -5 141.025 13.8874 4 6 -2 5 115.716 18.0867 5 -6 2 -5 153.544 12.1756 4 -7 -2 -5 740.460 30.9717 4 7 -2 5 753.832 36.0497 5 -7 2 -5 723.779 28.8284 4 8 -2 5 275.041 24.1738 5 -8 -2 -5 251.983 19.9514 4 -8 2 -5 286.812 17.9830 4 -9 -2 -5 141.353 17.5983 4 9 -2 5 163.228 22.2985 5 -9 -2 -5 137.792 8.37986 3 -9 2 -5 118.627 13.4427 4 9 2 5 149.362 10.4278 3 -9 2 -5 127.372 9.06797 3 -10 -2 -5 -5.5784 9.46970 4 10 -2 5 -4.8997 4.82535 6 -10 -2 -5 5.05141 8.30458 6 10 -2 5 1.72990 11.9318 5 -10 -2 -5 1.01366 3.73861 3 -10 2 -5 0.64967 7.79247 4 10 2 5 10.7427 5.24212 3 -10 2 -5 6.24703 4.43975 3 -11 -2 -5 343.644 27.4482 4 -11 -2 -5 318.872 13.6264 3 11 -2 5 288.580 13.6660 3 11 -2 5 318.288 30.5402 5 -11 -2 -5 322.489 21.0773 6 11 -2 5 327.278 16.3053 6 -11 2 -5 322.861 14.5409 3 11 2 5 316.936 15.4102 3 -11 2 -5 320.099 22.6039 4 11 2 5 349.839 21.7315 5 11 2 5 322.887 18.4901 6 12 -2 5 99.5480 11.4278 6 -12 -2 -5 99.2544 10.5194 3 12 -2 5 83.7454 19.7944 5 -12 -2 -5 118.812 15.5732 6 -12 -2 -5 111.884 20.4507 4 -12 2 -5 122.288 11.2071 3 -12 2 -5 123.540 17.3976 4 12 2 5 121.214 13.5687 6 12 2 5 108.534 10.2624 3 13 -2 5 10.6475 15.1626 5 13 -2 5 7.92863 6.24377 6 -13 -2 -5 13.1864 9.16612 6 -13 -2 -5 6.12147 4.27176 3 -13 -2 -5 5.36422 13.1750 4 13 2 5 -2.2616 5.30455 3 13 2 5 2.25389 6.97864 6 -13 2 -5 -1.7237 4.66635 3 -13 2 -5 9.92878 11.5256 4 14 -2 5 233.641 34.2280 5 14 -2 5 189.248 14.2161 6 -14 -2 -5 187.916 19.9002 6 -14 -2 -5 200.378 10.9134 3 -14 -2 -5 203.594 26.8128 4 -14 2 -5 203.565 22.9988 4 14 2 5 188.893 13.3516 3 14 2 5 202.611 15.6320 6 -14 2 -5 211.361 12.5862 3 -15 -2 -5 49.7593 22.9940 4 -15 -2 -5 77.8896 17.2126 6 15 -2 5 60.1139 10.5882 6 -15 -2 -5 62.0319 7.37158 3 15 2 5 75.3745 11.1116 6 -15 2 -5 67.5002 23.9301 4 15 2 5 42.2256 9.57123 3 16 -2 5 136.917 11.8468 6 -16 -2 -5 146.321 8.56355 3 -16 -2 -5 138.326 17.1337 6 -16 2 -5 142.587 10.2539 3 16 2 5 138.591 13.1301 6 16 2 5 112.708 10.9160 3 -17 -2 -5 -0.4279 3.27334 3 -17 -2 -5 5.50285 8.13020 6 -17 2 -5 1.67131 3.88675 3 17 2 5 1.97498 4.92219 3 -18 -2 -5 80.5858 13.9141 6 -18 2 -5 93.9307 8.23150 3 18 2 5 73.3094 12.1606 3 -19 -2 -5 -0.2940 5.80937 6 19 2 5 6.32852 3.65145 3 -19 2 -5 0.84014 3.01640 3 20 -3 -5 41.0837 7.86947 6 -20 -3 5 48.3914 8.53865 6 -20 3 5 35.0274 5.11890 3 20 3 -5 48.3487 6.92623 3 -19 -3 5 168.071 13.4529 6 19 3 -5 155.406 12.1601 3 -18 -3 5 -6.1289 5.79139 6 18 3 -5 3.52904 4.99064 3 -18 3 5 -0.5154 3.72783 3 -17 -3 5 -6.9953 6.45157 6 17 3 -5 11.1450 6.26148 3 -17 3 5 2.84181 3.78551 3 -16 -3 5 80.1388 15.3140 6 16 3 -5 85.2015 14.0293 3 -16 3 5 85.0254 12.4931 2 -16 3 5 62.3824 8.09043 3 15 -3 -5 5.93555 5.71623 1 -15 -3 5 0.61584 7.30510 6 15 3 -5 1.75529 5.56621 3 -15 3 5 7.34269 6.20405 2 -15 3 5 5.00453 4.27383 3 14 -3 -5 516.080 21.8227 1 14 -3 -5 494.366 40.7894 5 -14 -3 5 481.552 24.4168 6 -14 3 5 580.266 28.0624 2 14 3 -5 518.601 21.5183 3 -14 3 5 506.158 19.2706 3 -13 -3 5 39.0166 9.04180 6 13 -3 -5 48.0636 9.10944 1 13 -3 -5 43.2562 17.5357 5 13 3 -5 42.9718 7.05311 3 -13 3 5 43.3992 9.02911 2 -13 3 5 57.3152 7.65461 3 12 -3 -5 51.3952 10.5659 1 -12 -3 5 39.4121 8.95388 6 12 -3 -5 50.5075 15.5875 5 -12 3 5 56.4507 7.25152 3 12 3 -5 46.0392 7.42824 3 -12 3 5 57.6987 11.0098 2 11 -3 -5 83.8466 17.2175 5 -11 -3 5 61.7092 11.5621 6 11 -3 -5 69.9949 11.4900 1 -11 3 5 71.0786 10.9555 2 -11 3 5 53.0109 12.2978 4 -11 3 5 62.1187 7.38432 3 11 3 -5 50.9605 8.72810 3 10 -3 -5 54.3373 16.6212 5 10 -3 -5 69.4650 11.2602 1 -10 -3 5 81.9039 10.8972 6 -10 3 5 68.1810 9.85675 3 -10 3 5 76.8672 10.1245 4 10 3 -5 79.7450 13.1998 3 -10 3 5 99.2288 11.3292 2 9 -3 -5 240.596 26.8462 5 9 -3 -5 270.291 16.1856 1 -9 -3 5 244.772 14.9354 6 -9 3 5 270.846 14.3723 4 -9 3 5 259.612 16.1565 2 8 -3 -5 324.811 28.1451 5 -8 3 5 340.624 14.5049 4 -8 3 5 366.916 18.2831 2 7 -3 -5 1.66523 11.8712 5 -7 3 5 1.37215 4.72361 2 6 -3 -5 136.049 21.8429 5 -6 3 5 104.465 9.82896 2 5 -3 -5 31.3871 13.6372 5 -5 -3 5 27.8515 5.12045 5 -5 3 5 22.4504 5.92155 2 -4 -3 5 209.158 14.1380 5 4 -3 -5 208.197 22.0265 5 -4 3 5 196.633 11.6781 2 3 -3 -5 160.186 21.0812 5 -3 -3 5 167.775 15.9887 5 -3 3 5 166.260 10.3562 2 2 -3 -5 213.401 21.4200 5 -2 -3 5 215.515 18.3655 5 -2 3 5 225.776 11.4175 2 -1 -3 5 22.9926 10.0895 5 1 -3 -5 6.36418 9.55594 5 -1 3 5 17.8249 4.21204 2 0 -3 5 229.439 20.3730 5 0 3 5 219.790 10.3607 2 1 -3 5 29.0099 11.4312 5 1 3 5 36.9230 5.00778 2 2 -3 5 11.6133 11.7561 5 2 3 5 5.75307 2.93266 2 3 -3 5 154.763 20.6363 5 -3 -3 -5 125.445 11.5705 4 3 3 5 139.780 7.34656 2 -3 3 -5 130.162 10.8929 4 -4 -3 -5 204.308 14.9854 4 4 -3 5 244.760 23.2033 5 4 3 5 221.813 9.35554 2 -4 3 -5 231.448 14.0812 4 -5 -3 -5 0.82588 7.23922 4 5 -3 5 14.8442 12.1997 5 -5 3 -5 -2.8997 4.90766 4 -6 -3 -5 90.5956 13.9741 4 6 -3 5 59.1222 15.6676 5 -6 3 -5 80.5474 10.6960 4 -7 -3 -5 680.924 31.0114 4 7 -3 5 601.922 37.5944 5 -7 -3 -5 591.112 25.1503 6 -7 3 -5 626.524 26.2400 4 -8 -3 -5 368.246 24.7827 4 -8 -3 -5 358.968 19.2368 6 8 -3 5 332.552 22.1738 1 8 -3 5 356.106 31.6211 5 8 3 5 367.761 15.6493 3 -8 3 -5 370.615 20.6547 4 -9 -3 -5 17.6116 8.21549 6 9 -3 5 23.0897 9.93541 1 9 -3 5 28.5457 5.88534 6 9 -3 5 39.3716 17.2839 5 -9 -3 -5 6.18343 10.6439 4 -9 3 -5 18.5594 6.16903 3 -9 3 -5 23.2968 8.38136 4 9 3 5 29.4571 6.20251 3 10 -3 5 57.3018 19.2542 5 10 -3 5 64.8262 8.87825 6 -10 -3 -5 60.4153 11.1107 6 10 -3 5 64.5557 11.9831 1 -10 -3 -5 72.9737 7.04884 3 -10 -3 -5 53.3460 15.0627 4 -10 3 -5 91.5610 14.1963 4 -10 3 -5 67.7766 8.05493 3 10 3 5 54.0283 7.60265 3 11 -3 5 19.4397 8.95501 1 11 -3 5 7.06518 5.43354 6 -11 -3 -5 5.56137 12.3751 4 -11 -3 -5 21.1008 5.00553 3 -11 -3 -5 14.2230 8.85192 6 11 -3 5 -5.3817 15.3864 5 -11 3 -5 18.0809 10.4771 4 11 3 5 22.2745 6.30777 3 -11 3 -5 14.3959 5.07338 3 12 -3 5 143.956 15.3833 1 -12 -3 -5 150.728 17.1756 6 12 -3 5 169.809 12.3343 6 -12 3 -5 168.191 25.9450 4 -12 3 -5 174.665 11.1393 3 12 3 5 176.658 12.2297 3 13 -3 5 179.851 12.7558 6 -13 -3 -5 157.377 18.3892 6 13 -3 5 167.401 15.9232 1 -13 -3 -5 189.672 26.4360 4 13 -3 5 161.585 33.9805 5 -13 3 -5 155.082 20.7164 4 13 3 5 165.791 12.6700 3 -13 3 -5 174.427 11.1349 3 -14 -3 -5 6.55542 14.4807 4 14 -3 5 -29.492 22.5869 5 14 -3 5 -1.9402 4.70676 6 -14 -3 -5 5.27216 8.68345 6 -14 3 -5 -3.9829 9.93662 4 14 3 5 -4.6845 7.00334 6 14 3 5 -1.9654 5.36843 3 -14 3 -5 2.25612 4.52118 3 15 -3 5 38.8274 6.48622 6 -15 -3 -5 45.3096 10.2442 6 -15 3 -5 59.0411 8.12175 3 15 3 5 57.2132 9.61998 3 15 3 5 67.9480 12.5028 6 -16 -3 -5 17.6239 8.73514 6 16 3 5 20.3001 5.61087 3 -16 3 -5 14.6712 4.91697 3 -17 -3 -5 160.611 14.6393 6 17 3 5 161.887 11.0599 3 -17 3 -5 168.457 9.60163 3 -18 -3 -5 158.382 13.0822 6 18 3 5 176.242 9.97756 3 -18 3 -5 188.337 9.15769 3 -19 -3 -5 18.9502 5.48552 6 -19 3 -5 15.7880 3.44978 3 19 3 5 18.9566 3.88986 3 -20 -4 5 146.080 7.70336 6 -20 4 5 160.198 7.66126 3 20 4 -5 157.230 10.3353 3 -19 -4 5 37.6193 7.07835 6 19 -4 -5 30.5117 5.50798 6 19 4 -5 32.2511 5.24601 3 -19 4 5 36.1013 5.11083 3 -18 -4 5 122.079 18.6189 6 18 -4 -5 147.707 9.85971 6 -18 4 5 149.824 8.73440 3 17 -4 -5 -5.9060 4.44708 6 -17 -4 5 5.97941 5.73199 6 17 4 -5 5.80241 5.04110 3 -17 4 5 -0.0495 3.67920 3 16 -4 -5 -2.5987 5.12909 6 -16 -4 5 6.69136 6.46795 6 16 4 -5 0.14266 4.96414 3 -16 4 5 -3.2346 3.56305 3 -15 -4 5 99.8555 12.6601 6 15 -4 -5 97.3893 10.8337 1 15 4 -5 92.0457 10.7567 3 -15 4 5 91.4061 8.38034 3 14 -4 -5 46.3761 19.3867 5 14 -4 -5 51.6159 8.36812 1 -14 -4 5 65.3340 11.8772 6 -14 4 5 60.5762 7.70516 3 14 4 -5 60.0694 9.74367 3 -14 4 5 73.8859 12.4489 2 13 -4 -5 -4.3654 6.00644 1 -13 -4 5 0.45809 6.11682 6 13 -4 -5 -19.062 13.1886 5 -13 4 5 -4.0394 3.43220 3 13 4 -5 0.55561 5.40873 3 -13 4 5 -7.8073 5.37079 2 12 -4 -5 -3.9205 6.33603 1 -12 -4 5 -6.0326 5.61787 6 12 -4 -5 -9.5745 13.4909 5 -12 4 5 6.12934 8.96863 2 -12 4 5 -1.5025 3.93045 3 12 4 -5 -7.8689 4.70909 3 11 -4 -5 209.842 19.4300 1 11 -4 -5 202.990 27.9095 5 -11 -4 5 182.152 14.1966 6 -11 4 5 181.608 10.2605 3 -11 4 5 218.348 17.0298 2 11 4 -5 170.427 11.8124 3 10 -4 -5 0.26305 6.90597 1 -10 -4 5 8.54659 5.90077 6 10 -4 -5 0.45875 13.9132 5 -10 4 5 -2.4651 5.18195 2 -10 4 5 0.26672 4.04839 3 10 4 -5 11.3480 5.23190 3 9 -4 -5 18.2798 14.6941 5 9 -4 -5 11.8974 11.3851 7 9 -4 -5 -5.7486 6.66885 1 -9 -4 5 0.10577 5.23770 6 -9 4 5 3.15743 5.64864 3 -9 4 5 5.67933 6.26470 2 8 -4 -5 48.5399 13.5956 7 8 -4 -5 54.5136 10.3216 6 8 -4 -5 57.4190 9.89106 1 8 -4 -5 68.9192 19.1129 5 -8 -4 5 57.6459 8.74844 6 -8 4 5 55.3828 9.90935 2 7 -4 -5 48.6880 9.21835 1 -7 -4 5 48.2611 7.78183 6 7 -4 -5 68.5881 23.8526 7 7 -4 -5 57.8273 25.5946 5 -7 4 5 50.4607 8.92793 2 6 -4 -5 177.173 14.7158 1 6 -4 -5 216.146 25.3069 7 6 -4 -5 217.955 25.8385 5 -6 4 5 221.317 14.1706 2 5 -4 -5 380.559 30.2076 5 -5 4 5 330.404 17.0841 2 4 -4 -5 215.139 24.9138 5 -4 -4 5 211.564 16.0461 5 -4 4 5 228.735 13.3396 2 -3 -4 5 518.928 28.3770 5 3 -4 -5 583.414 34.3227 5 -3 4 5 625.269 22.6439 2 -2 -4 5 169.944 20.7126 5 2 -4 -5 188.827 21.7829 5 -2 4 5 203.214 11.4216 2 1 -4 -5 31.3834 13.3537 5 -1 -4 5 66.6897 14.9125 5 -1 4 5 50.8970 6.52519 2 0 -4 5 674.062 36.0122 5 0 4 5 652.079 22.8763 2 1 -4 5 997.587 46.3233 5 1 4 5 1015.55 30.6378 2 2 -4 5 2308.26 81.3036 5 2 4 5 2264.53 62.4382 2 3 -4 5 65.3076 16.7400 5 -3 4 -5 101.907 10.8802 4 3 4 5 67.1475 6.21829 2 4 -4 5 43.9679 16.2499 5 4 -4 5 18.4629 23.0295 7 4 -4 5 8.56050 9.68966 1 -4 4 -5 8.18450 6.43424 4 5 -4 5 187.206 37.5143 7 5 -4 5 145.343 20.6632 1 -5 -4 -5 172.373 12.0718 6 5 -4 5 203.798 27.8808 5 -5 4 -5 177.643 13.8928 4 6 -4 5 641.214 31.1774 1 -6 -4 -5 651.270 26.2037 6 6 -4 5 605.124 20.9602 6 6 -4 5 689.371 43.1479 5 -6 4 -5 663.663 27.7642 4 -7 -4 -5 60.0945 11.3180 6 7 -4 5 64.8476 6.74335 6 7 -4 5 76.3275 13.1617 1 7 -4 5 59.4299 19.1488 5 7 -4 5 73.3894 23.0622 7 7 4 5 68.0123 10.4340 3 -7 4 -5 43.4103 8.59190 4 8 -4 5 132.151 17.9483 1 8 -4 5 129.485 25.4818 5 8 -4 5 153.763 9.19620 6 8 -4 5 185.719 33.4565 7 -8 -4 -5 136.182 13.8740 6 -8 4 -5 157.446 14.8576 4 8 4 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41.0337 8.66246 2 15 2 -7 35.7809 7.92683 3 -15 2 7 44.9182 7.70108 3 -14 -2 7 18.8462 4.73235 3 -14 -2 7 4.47258 7.77007 6 -14 2 7 18.4714 5.34944 3 14 2 -7 16.0152 6.17091 3 -14 2 7 6.32922 5.90223 2 -13 -2 7 200.047 10.5771 3 13 -2 -7 179.188 11.0316 3 -13 2 7 195.085 11.0184 3 -13 2 7 197.456 15.5536 2 13 2 -7 221.611 18.5356 3 -12 -2 7 533.834 24.7694 6 12 -2 -7 543.443 21.9313 1 -12 -2 7 560.363 18.8291 3 12 -2 -7 504.743 19.2258 3 -12 2 7 575.856 25.7057 2 -12 2 7 554.979 19.6439 3 12 2 -7 533.978 21.3186 3 -11 -2 7 1.75514 7.03603 6 11 -2 -7 -5.2132 8.63850 5 -11 -2 7 2.18710 5.81189 3 11 2 -7 2.89491 5.09637 3 -11 2 7 2.10090 5.10387 2 -11 2 7 7.61869 4.16758 3 10 -2 -7 72.3654 9.45273 1 10 -2 -7 79.4299 15.6515 5 -10 -2 7 92.2722 18.1270 6 -10 2 7 75.8399 9.35460 2 10 2 -7 83.1039 8.97973 3 -10 2 7 60.1232 6.79768 3 9 -2 -7 1661.21 60.9784 5 -9 -2 7 2013.11 67.0156 6 -9 -2 7 1721.83 50.2441 2 -9 2 7 1713.74 54.6389 2 -8 -2 7 1524.32 45.2716 2 8 -2 -7 1651.19 56.7143 5 -8 2 7 1564.68 49.1652 2 -7 -2 7 3.50042 3.15150 2 7 -2 -7 -4.8754 8.55079 5 -7 2 7 -2.1234 4.24178 2 6 -2 -7 541.478 28.0458 5 -6 -2 7 523.030 18.9126 2 -6 2 7 545.700 21.2848 2 -5 -2 7 316.904 12.7798 5 -5 -2 7 325.501 13.4700 2 -5 2 7 292.905 14.5332 2 -4 -2 7 303.800 14.5844 5 -4 -2 7 328.736 14.0226 2 -4 2 7 331.518 14.8217 2 -3 -2 7 21.5404 6.48839 5 -3 -2 7 12.8079 4.89676 2 -3 2 7 11.7569 4.72252 2 -2 -2 7 572.525 21.1826 2 -2 -2 7 582.521 23.4030 5 -2 2 7 576.620 20.4963 2 -1 -2 7 274.520 16.3600 5 -1 -2 7 248.447 13.3254 2 -1 2 7 248.210 11.9751 2 0 -2 -7 223.840 8.81561 4 0 -2 7 190.724 12.8525 2 0 -2 7 243.359 16.3669 5 0 2 7 206.776 10.6452 2 1 -2 7 1663.56 49.6511 2 -1 -2 -7 1607.85 45.5761 4 1 -2 7 1509.72 55.5279 5 1 2 7 1665.11 46.7849 2 -2 -2 -7 603.204 22.1444 4 2 -2 7 644.677 28.3978 5 2 2 7 661.213 21.9907 2 -2 2 -7 648.646 24.4925 4 3 -2 7 183.112 17.3964 5 -3 -2 -7 207.257 12.5937 4 -3 2 -7 189.452 12.8999 4 3 2 7 194.792 10.6598 2 4 -2 7 94.5600 15.1957 5 -4 -2 -7 72.7473 10.3014 4 -4 2 -7 62.1791 9.90624 4 4 2 7 86.3006 7.89599 2 -5 -2 -7 388.989 19.8875 4 5 -2 7 396.042 25.1786 5 -5 2 -7 413.554 19.7499 4 5 2 7 400.105 16.8785 2 -6 -2 -7 102.760 13.3167 4 6 -2 7 134.346 18.8552 5 -6 2 -7 123.242 12.1345 4 7 -2 7 7.60071 4.58912 6 -7 -2 -7 7.17359 7.20114 6 7 -2 7 -3.2840 10.1306 5 -7 -2 -7 3.76321 8.07378 4 -7 2 -7 7.49397 6.78419 4 -8 -2 -7 14.9288 7.77598 6 8 -2 7 6.28107 4.69331 6 -8 -2 -7 4.04331 3.70236 3 -8 -2 -7 3.94875 8.14727 4 -8 2 -7 0.49368 6.76326 4 -8 2 -7 -1.6693 4.10063 3 9 -2 7 509.386 26.8905 1 9 -2 7 572.969 21.9338 6 -9 -2 -7 592.189 26.7402 6 9 -2 7 573.541 36.5003 5 -9 -2 -7 562.170 30.4429 4 -9 -2 -7 561.865 19.3114 3 9 2 7 536.248 20.8394 3 -9 2 -7 519.378 20.0376 3 -9 2 -7 555.205 27.7117 4 9 2 7 551.208 34.2094 6 10 -2 7 134.821 16.4639 1 10 -2 7 124.711 8.86479 3 10 -2 7 101.798 10.8524 6 -10 -2 -7 97.8082 8.55214 3 -10 -2 -7 106.530 18.5512 4 -10 -2 -7 97.3776 14.8571 6 10 -2 7 125.238 23.8435 5 -10 2 -7 89.8149 14.3407 4 10 2 7 115.262 10.1045 3 -10 2 -7 101.716 9.25796 3 10 2 7 94.9836 12.2560 6 -11 -2 -7 15.5053 9.60906 6 -11 -2 -7 12.9629 11.9318 4 -11 -2 -7 13.7727 7.71988 3 11 -2 7 8.47523 14.7410 5 11 -2 7 17.7741 6.35613 6 11 2 7 20.8010 9.87789 5 11 2 7 10.2442 6.51925 6 -11 2 -7 9.34563 8.92589 4 11 2 7 13.3600 5.84287 3 -11 2 -7 11.8870 6.63396 3 12 -2 7 902.117 31.8166 6 -12 -2 -7 873.931 27.9412 3 12 -2 7 827.126 68.8139 5 -12 -2 -7 887.230 37.3002 6 -12 2 -7 843.200 44.4410 4 12 2 7 884.863 33.5499 6 -12 2 -7 873.149 29.1902 3 12 2 7 900.216 30.3757 3 -13 -2 -7 518.840 35.2164 4 13 -2 7 463.538 41.3097 5 -13 -2 -7 546.037 19.1551 3 -13 -2 -7 527.188 27.5648 6 13 -2 7 565.047 23.1318 6 -13 2 -7 503.996 32.5130 4 13 2 7 527.362 23.8026 6 13 2 7 505.414 21.2236 3 -13 2 -7 514.070 20.2211 3 14 -2 7 1.21714 5.61380 6 -14 -2 -7 -2.7379 9.07798 6 14 -2 7 -0.8361 21.9730 5 -14 -2 -7 3.18870 14.1072 4 14 2 7 -0.0539 5.19281 3 -14 2 -7 -1.2642 4.70267 3 -14 2 -7 1.31838 11.3664 4 -15 -2 -7 32.2371 4.84784 3 15 -2 7 26.2686 7.00771 6 -15 -2 -7 36.7372 10.4529 6 15 2 7 23.7621 7.65337 6 -15 2 -7 19.0975 5.02131 3 15 2 7 30.8480 6.80994 3 -16 -2 -7 49.3813 11.0740 6 16 -2 7 27.3129 5.68917 6 -16 -2 -7 53.5084 6.91359 3 16 2 7 45.7106 7.03537 3 16 2 7 37.5638 7.56471 6 -16 2 -7 45.7642 6.39303 3 17 -2 7 11.8752 4.86926 6 -17 -2 -7 15.8136 7.91520 6 -17 2 -7 23.5980 4.72750 3 17 2 7 21.1745 5.02731 3 17 2 7 14.7153 5.38667 6 -18 -2 -7 5.86753 6.06505 6 18 2 7 2.25827 3.85923 3 -18 2 -7 9.33894 3.58250 3 -19 -2 -7 25.9110 6.89324 6 19 2 7 42.9399 5.06399 3 -19 2 -7 37.9674 4.79633 3 20 -3 -7 2.28969 4.39054 6 -20 -3 7 2.11947 4.63610 6 -20 3 7 3.32911 2.96385 3 20 3 -7 -1.7293 3.63355 3 19 -3 -7 80.9597 10.1650 6 -19 -3 7 69.6090 12.6337 6 19 3 -7 91.3682 13.7309 3 -19 3 7 92.3434 7.76966 3 18 -3 -7 158.579 13.6672 6 -18 -3 7 168.865 14.1071 6 18 3 -7 192.652 12.1544 3 -18 3 7 206.510 10.6369 3 -17 -3 7 99.8920 13.4602 6 -17 3 7 107.963 9.26735 3 17 3 -7 128.057 11.5571 3 -16 -3 7 174.496 15.9534 6 16 3 -7 172.043 13.5958 3 -16 3 7 184.304 11.0646 3 -15 -3 7 302.685 19.4505 6 -15 3 7 331.487 14.6935 3 -15 3 7 313.792 21.0192 2 15 3 -7 332.728 17.3521 3 14 -3 -7 157.377 12.8241 1 -14 -3 7 129.590 14.6280 6 -14 3 7 148.563 10.1049 3 -14 3 7 182.651 15.8173 2 14 3 -7 143.035 12.4951 3 -13 -3 7 4.01251 6.95313 6 13 -3 -7 0.59598 5.73567 1 -13 3 7 4.78596 5.81347 2 13 3 -7 -0.4043 5.57328 3 -13 3 7 8.88016 4.31694 3 12 -3 -7 61.0594 10.8464 1 12 -3 -7 72.7259 15.6903 5 -12 -3 7 62.6586 12.5260 6 -12 3 7 81.4853 8.05365 3 -12 3 7 79.4050 11.4818 2 12 3 -7 64.1041 10.1481 3 11 -3 -7 18.5368 6.71339 1 11 -3 -7 -2.3765 10.8130 5 -11 -3 7 15.0786 6.92075 6 11 3 -7 21.3000 6.11456 3 -11 3 7 13.5695 6.56074 2 -11 3 7 17.3505 4.66848 3 10 -3 -7 13.8412 6.60520 1 10 -3 -7 18.7543 14.2126 5 -10 -3 7 13.5696 6.65952 6 -10 3 7 4.49012 5.50245 2 -10 3 7 10.1140 4.13965 3 10 3 -7 11.2568 5.27040 3 9 -3 -7 623.958 24.7797 1 9 -3 -7 640.641 36.7028 5 -9 -3 7 623.593 24.1378 6 9 3 -7 628.323 22.2744 3 -9 3 7 600.965 21.9049 3 -9 3 7 649.339 26.7179 2 -8 -3 7 295.075 15.4521 6 8 -3 -7 313.602 26.4588 5 8 -3 -7 311.613 16.3935 1 -8 3 7 307.232 17.0447 2 7 -3 -7 1141.44 48.5305 5 -7 3 7 1120.41 38.3418 2 6 -3 -7 17.1166 11.1011 5 -6 3 7 22.4038 6.13689 2 -5 -3 7 407.935 19.8407 5 5 -3 -7 446.455 27.7831 5 -5 3 7 452.466 18.9956 2 4 -3 -7 380.506 25.3234 5 -4 -3 7 349.435 18.9727 5 -4 3 7 360.986 16.5407 2 -3 -3 7 90.8545 13.3898 5 -3 3 7 77.6641 8.35674 2 -2 -3 7 96.8447 15.2013 5 -2 3 7 118.616 8.98123 2 -1 -3 7 85.6214 13.4898 5 -1 3 7 90.3844 7.90107 2 0 -3 7 269.067 21.0405 5 0 3 7 251.320 12.0230 2 1 -3 7 13.1389 10.7892 5 1 3 7 33.7547 5.74239 2 -2 -3 -7 137.378 9.39207 4 2 -3 7 154.907 19.1507 5 -2 3 -7 132.189 11.9496 4 2 3 7 150.778 9.13805 2 3 -3 7 364.478 25.5391 5 -3 -3 -7 292.738 15.4694 4 3 3 7 291.583 13.1430 2 -3 3 -7 328.411 17.6033 4 4 -3 7 28.1859 12.8255 5 -4 3 -7 30.9236 8.04578 4 4 3 7 32.0212 5.65224 2 -5 -3 -7 76.7300 11.6488 4 5 -3 7 58.8454 15.0111 5 -5 3 -7 79.7307 11.1611 4 -6 -3 -7 -6.3654 6.61891 4 6 -3 7 4.90051 9.80505 1 6 -3 7 2.28599 3.87394 6 -6 -3 -7 8.83502 6.90365 6 6 -3 7 -2.4723 11.4847 5 -6 3 -7 3.29465 6.17312 4 7 -3 7 99.2041 8.75582 6 -7 -3 -7 109.811 13.1376 6 7 -3 7 110.606 18.2429 1 7 -3 7 79.7956 35.4020 7 -7 -3 -7 107.264 15.4404 4 7 -3 7 118.159 24.4867 5 -7 3 -7 95.4810 12.5207 4 -7 3 -7 114.159 9.59823 3 8 -3 7 23.6253 21.0709 7 8 -3 7 18.5237 9.97444 1 -8 -3 -7 31.8062 9.20245 6 8 -3 7 31.7601 15.8971 5 -8 -3 -7 25.9092 11.4271 4 8 -3 7 17.6151 5.09334 6 -8 3 -7 15.2092 4.98643 3 -8 3 -7 22.5783 8.15803 4 8 3 7 28.7460 5.96259 3 9 -3 7 2.84648 4.54104 6 9 -3 7 5.57469 13.9156 5 -9 -3 -7 1.90840 7.93313 6 -9 -3 -7 9.41693 3.95978 3 9 -3 7 6.16358 9.83322 1 -9 -3 -7 5.11651 9.32449 4 -9 3 -7 -5.3981 6.37985 4 -9 3 -7 -0.6643 4.08060 3 9 3 7 2.18262 5.06032 3 10 -3 7 104.565 10.2572 6 10 -3 7 85.9660 13.4305 1 -10 -3 -7 106.145 16.1995 6 10 -3 7 101.941 24.2042 5 -10 -3 -7 86.9272 15.8296 4 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15.4295 6 16 3 7 182.173 11.6082 3 -16 3 -7 176.315 9.96959 3 -17 -3 -7 86.4606 11.7982 6 17 3 7 92.5696 8.18146 3 -17 3 -7 97.2553 7.26742 3 -18 -3 -7 82.9068 10.0929 6 -18 3 -7 79.4196 6.18690 3 18 3 7 82.1736 6.88111 3 -19 -4 7 18.7134 4.54755 6 19 -4 -7 19.8298 4.25386 6 19 4 -7 17.9086 4.46246 3 -19 4 7 11.7880 3.27985 3 18 -4 -7 26.5107 5.25158 6 -18 -4 7 21.9485 5.59557 6 -18 4 7 24.3388 4.20150 3 18 4 -7 23.3229 5.42007 3 17 -4 -7 32.0756 6.30218 6 -17 -4 7 30.6156 7.04775 6 -17 4 7 37.2039 6.64157 3 17 4 -7 28.2295 6.01401 3 16 -4 -7 2.28762 5.67376 6 -16 -4 7 16.5445 6.78338 6 16 4 -7 9.66556 6.02947 3 -16 4 7 11.2402 4.18453 3 15 -4 -7 33.2007 7.54461 6 -15 -4 7 43.2706 8.12072 6 -15 4 7 62.9669 7.93078 3 15 4 -7 52.5272 9.78557 3 14 -4 -7 1.00371 5.39033 1 -14 -4 7 6.08745 6.60181 6 14 -4 -7 7.37817 6.02328 6 14 4 -7 6.02584 5.58328 3 -14 4 7 -0.6153 6.18027 2 -14 4 7 6.44355 4.33661 3 -13 -4 7 18.0112 7.20244 6 13 -4 -7 23.4508 7.08097 6 13 -4 -7 27.3813 7.68737 1 13 4 -7 18.6533 6.00798 3 -13 4 7 14.0561 7.23230 2 -13 4 7 15.9894 4.82849 3 12 -4 -7 3.44869 6.07657 1 -12 -4 7 2.51491 5.68806 6 12 -4 -7 2.48619 5.77809 6 12 4 -7 0.11468 5.44222 3 -12 4 7 -2.4331 5.80813 2 -12 4 7 1.90941 3.85711 3 11 -4 -7 40.0538 9.08159 1 11 -4 -7 27.4139 15.2538 5 -11 -4 7 37.9034 7.95913 6 11 -4 -7 23.1809 6.91276 6 11 4 -7 42.0151 7.69296 3 -11 4 7 42.0549 8.92878 2 -10 -4 7 703.546 26.4273 6 10 -4 -7 775.525 29.9018 1 10 -4 -7 722.740 26.5402 6 10 -4 -7 659.452 41.5744 5 -10 4 7 675.672 30.3902 2 10 4 -7 681.568 25.2052 3 -10 4 7 690.583 23.4590 3 9 -4 -7 84.3306 12.0440 1 -9 -4 7 66.3137 9.99060 6 9 -4 -7 67.1374 10.0210 6 9 -4 -7 87.8568 19.3605 5 -9 4 7 80.1009 10.8079 2 9 4 -7 75.8839 9.12065 3 -9 4 7 71.6385 7.75360 3 8 -4 -7 386.198 32.1773 5 8 -4 -7 374.343 19.5388 1 -8 -4 7 331.345 52.8970 7 -8 -4 7 395.061 17.2587 6 8 -4 -7 386.024 17.3771 6 8 4 -7 396.457 16.8828 3 -8 4 7 412.508 20.9390 2 7 -4 -7 34.0929 13.8222 5 7 -4 -7 30.9367 7.48206 1 -7 -4 7 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79.0107 13.9134 6 15 -3 -10 78.2570 14.9202 6 15 3 -10 99.1545 14.3949 3 -15 3 10 74.4367 12.6800 2 -15 3 10 87.1250 8.99294 3 14 -3 -10 24.3433 8.33589 6 -14 -3 10 18.2528 7.36059 6 14 3 -10 21.5169 6.27937 3 -14 3 10 22.8038 5.31054 3 -14 3 10 24.5898 8.67753 2 13 -3 -10 68.7359 10.8689 6 -13 -3 10 67.5117 10.6608 6 13 3 -10 47.8992 7.94964 3 -13 3 10 46.7048 7.63449 3 -13 3 10 37.5174 8.73381 2 12 -3 -10 518.449 23.9000 6 -12 -3 10 489.806 23.2229 6 -12 3 10 494.769 18.8291 3 -12 3 10 499.014 26.9512 2 12 3 -10 496.650 20.8640 3 -11 -3 10 52.8225 9.31193 6 11 -3 -10 31.1737 8.30656 6 -11 3 10 38.5790 8.63485 2 10 -3 -10 5.21981 6.11605 1 -10 -3 10 -8.6780 22.7497 7 -10 -3 10 9.51951 6.39547 6 10 -3 -10 10.6051 7.22895 6 -10 3 10 9.25035 4.53216 3 -10 3 10 6.83446 5.68330 2 10 3 -10 7.60411 5.55204 3 9 -3 -10 5.70522 6.03541 1 -9 -3 10 2.54624 22.8093 7 -9 -3 10 0.95786 6.02444 6 9 -3 -10 -3.4061 6.12549 6 9 3 -10 6.60674 4.98625 3 -9 3 10 -1.7209 5.21228 2 -9 3 10 3.41362 4.22292 3 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37.9084 6.77196 2 0 -3 10 9.98398 9.70661 5 0 -3 10 10.4048 24.8019 7 0 3 10 24.0278 5.90380 2 -1 -3 -10 355.102 18.7321 6 1 -3 10 359.141 26.6819 5 1 -3 10 410.314 50.1463 7 1 3 10 360.664 17.0631 2 -1 3 -10 348.806 20.1316 4 2 -3 10 464.654 47.4271 7 2 -3 10 398.168 16.2851 6 -2 -3 -10 387.381 20.2291 6 2 -3 10 370.237 28.4752 5 -2 3 -10 413.444 21.6753 4 2 3 10 431.935 18.7448 2 3 -3 10 137.510 22.7720 5 3 -3 10 139.776 28.0541 7 -3 -3 -10 154.096 15.6979 6 3 -3 10 166.602 21.0642 1 3 -3 10 145.647 10.5522 6 -3 3 -10 152.723 15.1682 4 3 3 10 149.185 11.0527 2 3 3 10 152.175 9.20023 3 4 -3 10 251.737 26.4280 5 4 -3 10 226.896 12.3740 6 -4 -3 -10 227.387 16.2087 6 4 -3 10 239.015 22.1090 1 4 -3 10 279.581 43.6354 7 4 3 10 238.927 14.2662 2 -4 3 -10 207.104 16.8032 4 -4 3 -10 215.491 12.0231 3 5 -3 10 82.1360 14.4647 1 5 -3 10 65.3289 24.0216 7 5 -3 10 78.6746 8.38714 6 5 -3 10 53.1607 16.0496 5 -5 -3 -10 62.0272 12.5986 6 5 3 10 78.7858 7.40341 3 -5 3 -10 89.0502 13.0283 4 -5 3 -10 66.7494 9.28125 3 5 3 10 87.9176 10.1138 2 6 -3 10 180.067 27.4978 5 6 -3 10 203.188 40.8297 7 6 -3 10 209.367 21.2661 1 -6 -3 -10 208.231 16.5093 4 -6 -3 -10 182.906 15.8975 6 6 -3 10 173.258 11.5771 6 -6 3 -10 198.533 11.7141 3 6 3 10 171.136 11.1078 3 -6 3 -10 199.525 17.0398 4 -7 -3 -10 42.1182 10.0922 6 -7 -3 -10 69.8459 7.03767 3 7 -3 10 80.5976 19.0867 5 7 -3 10 38.0020 22.6862 7 -7 -3 -10 51.8495 11.5833 4 7 -3 10 54.0158 8.53781 6 7 -3 10 51.2061 12.2968 1 7 3 10 58.6662 8.69484 3 -7 3 -10 51.9009 11.1499 4 -7 3 -10 62.8232 8.57800 3 -8 -3 -10 1365.56 47.6789 6 8 -3 10 1314.92 65.4859 7 -8 -3 -10 1332.01 53.0922 4 8 -3 10 1414.62 67.0957 5 8 -3 10 1345.56 51.8948 1 8 -3 10 1386.45 42.1896 6 8 3 10 1374.22 41.9599 3 -8 3 -10 1322.81 51.3193 4 -8 3 -10 1337.35 42.9933 3 9 -3 10 1957.67 85.5815 5 9 -3 10 1947.41 57.6628 6 -9 -3 -10 2013.66 63.9229 6 9 -3 10 1914.04 64.8295 1 -9 -3 -10 1881.65 70.8355 4 -9 3 -10 1938.56 56.7723 3 9 3 10 2040.16 57.7120 3 -10 -3 -10 1.85284 12.3552 4 10 -3 10 1.58897 5.02586 6 10 -3 10 5.09536 9.11168 1 -10 -3 -10 20.0671 9.07727 6 10 -3 10 -16.341 13.2289 5 -10 3 -10 0.86603 4.65017 3 10 3 10 -3.1715 5.06434 3 -10 3 -10 13.6141 10.2604 4 11 -3 10 81.4773 15.2508 1 11 -3 10 53.0358 20.1872 5 11 -3 10 72.9535 10.1016 6 -11 -3 -10 24.6937 15.1177 4 -11 -3 -10 96.7589 15.5920 6 -11 3 -10 81.4796 9.20889 3 11 3 10 91.6841 16.3694 6 -11 3 -10 61.4424 14.4225 4 11 3 10 93.6664 10.2447 3 -12 -3 -10 156.169 17.0494 6 12 -3 10 149.069 14.7428 1 12 -3 10 145.865 11.6910 6 12 -3 10 160.926 29.2558 5 12 3 10 161.567 11.9831 3 -12 3 -10 165.476 10.8048 3 -12 3 -10 231.481 21.1438 4 12 3 10 178.822 15.5482 6 -13 -3 -10 85.6308 14.0721 6 13 -3 10 71.2980 9.85934 6 13 3 10 69.6845 9.49405 3 13 3 10 82.7180 13.1250 6 -13 3 -10 74.6582 8.32148 3 -14 -3 -10 4.14107 7.67943 6 14 -3 10 5.64033 4.51573 6 -14 3 -10 -1.9722 3.99029 3 14 3 10 3.30923 4.98524 3 14 3 10 8.75118 6.47509 6 15 -3 10 12.5169 5.22956 6 -15 -3 -10 15.7005 6.93939 6 15 3 10 8.39279 5.10731 3 -15 3 -10 22.1467 7.99217 3 15 3 10 13.1231 8.14561 6 -16 -3 -10 15.3549 6.50617 6 -16 3 -10 29.5918 5.22297 3 16 3 10 15.1579 4.24240 3 -17 -3 -10 5.30304 5.08722 6 -17 3 -10 1.28088 4.97290 3 17 3 10 -3.5561 4.24377 3 -19 -4 10 6.24941 3.44516 6 19 4 -10 8.96191 3.76815 3 -19 4 10 3.86766 2.83719 3 -18 -4 10 21.5562 4.93323 6 18 -4 -10 16.6561 4.28215 6 18 4 -10 29.0892 5.35821 3 -18 4 10 29.2826 5.04843 3 17 -4 -10 3.56188 4.74448 6 -17 -4 10 3.43813 4.68640 6 17 4 -10 3.28110 4.61185 3 -17 4 10 -1.0205 4.54554 3 -16 -4 10 -2.3434 4.98139 6 16 -4 -10 6.46955 5.53592 6 16 4 -10 -0.0794 4.76525 3 -16 4 10 3.93774 3.84343 3 15 -4 -10 14.4341 6.46860 6 -15 -4 10 4.75468 5.53378 6 15 4 -10 5.57292 5.48874 3 -15 4 10 0.22613 3.92054 3 14 -4 -10 36.1908 7.86909 6 -14 -4 10 34.3537 7.18054 6 14 4 -10 38.6534 7.37883 3 -14 4 10 28.5558 8.82721 2 -14 4 10 29.3178 5.28355 3 -13 -4 10 48.5095 8.60990 6 13 -4 -10 49.1477 8.77627 6 -13 4 10 39.1852 8.90364 2 13 4 -10 66.7314 9.98568 3 -13 4 10 52.6908 7.68626 3 -12 -4 10 1592.82 48.5315 6 12 -4 -10 1493.22 48.7651 6 -12 4 10 1535.23 45.2690 3 12 4 -10 1510.08 47.0585 3 11 -4 -10 678.870 27.2848 6 11 -4 -10 668.605 27.2051 1 -11 -4 10 710.046 26.6321 6 11 4 -10 665.796 25.1392 3 -11 4 10 699.573 31.7480 2 -11 4 10 644.310 23.2156 3 -10 -4 10 341.087 17.5613 6 10 -4 -10 354.546 18.6651 1 10 -4 -10 326.123 18.5191 6 10 4 -10 337.654 16.4524 3 -10 4 10 330.111 14.5105 3 -10 4 10 350.391 21.3105 2 9 -4 -10 23.9883 7.19822 6 9 -4 -10 9.68825 6.40135 1 -9 -4 10 11.3975 23.2120 7 -9 -4 10 31.0520 6.90471 6 9 4 -10 26.9696 6.12536 3 -9 4 10 27.4265 5.25855 3 -9 4 10 27.5255 8.49757 2 8 -4 -10 30.6383 7.08846 6 8 -4 -10 35.3664 7.75014 1 -8 -4 10 47.6543 9.43632 6 -8 -4 10 14.6848 22.6472 7 8 4 -10 41.4295 6.87527 3 -8 4 10 48.3627 9.48147 2 -8 4 10 38.9823 6.33247 3 -7 -4 10 123.916 10.8251 6 -7 -4 10 141.374 29.5141 7 7 -4 -10 130.826 11.9797 6 7 -4 -10 128.623 12.8278 1 -7 -4 10 111.712 19.9790 1 -7 4 10 119.263 12.5598 2 -7 4 10 130.071 8.52960 3 7 4 -10 123.724 10.2187 3 -6 -4 10 8.28266 4.84870 6 6 -4 -10 8.77320 6.54590 1 -6 -4 10 8.91281 23.8443 7 6 -4 -10 12.3332 6.27476 6 6 4 -10 11.9189 7.24897 3 -6 4 10 4.60615 4.27707 3 -6 4 10 3.29468 5.26576 2 5 -4 -10 17.4119 6.63028 1 5 -4 -10 3.43406 6.05168 6 -5 -4 10 46.7174 26.2562 7 -5 -4 10 4.71978 4.22597 6 5 4 -10 13.8648 6.29823 3 -5 4 10 11.0997 5.65173 2 -5 4 10 9.76380 4.11846 3 4 -4 -10 12.3010 6.08951 6 4 -4 -10 4.62453 5.68231 1 -4 -4 10 3.78636 23.4246 7 -4 -4 10 10.0619 4.44147 6 -4 4 10 -1.6068 4.34402 2 -3 -4 10 508.531 18.7865 6 3 -4 -10 506.042 21.4677 6 -3 -4 10 581.205 52.5987 7 3 -4 -10 509.703 21.1114 1 -3 -4 10 539.104 30.2285 5 -2 -4 10 238.599 42.1816 7 2 -4 -10 247.107 15.2892 6 -2 -4 10 227.588 22.1382 1 -2 -4 10 238.984 24.5081 5 -2 4 10 256.562 14.7485 2 -1 -4 10 18.6785 13.2297 5 -1 -4 10 12.0517 11.1541 1 1 -4 -10 18.9081 6.85376 6 -1 -4 10 12.2633 24.3760 7 -1 4 10 11.0234 5.14882 2 0 -4 -10 355.475 17.9574 6 0 -4 10 354.846 25.4183 1 0 -4 10 359.957 30.9589 5 0 -4 10 314.018 46.0520 7 0 -4 10 318.716 16.9237 6 0 4 10 376.258 17.5944 2 1 -4 10 322.795 24.9633 1 1 -4 10 282.435 12.7171 6 -1 -4 -10 284.368 17.0099 6 1 -4 10 305.679 30.6992 5 1 -4 10 275.706 44.8628 7 1 4 10 303.151 15.7274 2 1 4 10 290.310 12.7913 3 -1 4 -10 282.161 19.3794 4 -2 -4 -10 108.435 12.6302 6 2 -4 10 15.4358 23.6042 7 2 -4 10 106.737 21.3931 5 2 -4 10 102.181 8.18289 6 2 -4 10 110.746 20.4046 1 -2 4 -10 118.306 14.1309 4 2 4 10 102.611 8.96234 3 2 4 10 126.565 10.3614 2 3 -4 10 18.8351 17.0747 5 3 -4 10 23.6432 11.6256 1 3 -4 10 26.7770 4.89001 6 3 -4 10 10.1444 22.9474 7 -3 -4 -10 33.6471 8.12273 6 -3 4 -10 33.3665 6.81850 3 3 4 10 48.9517 6.90189 3 -3 4 -10 43.1164 9.99094 4 3 4 10 38.8382 7.13040 2 4 -4 10 106.648 8.63932 6 4 -4 10 99.3094 20.8467 5 4 -4 10 92.7325 27.8265 7 -4 -4 -10 103.607 13.1174 6 4 -4 10 108.693 16.6617 1 -4 4 -10 110.327 13.9701 4 -4 4 -10 113.723 9.96341 3 4 4 10 123.486 8.58302 3 5 -4 10 23.4878 23.0842 7 5 -4 10 15.4591 4.71497 6 -5 -4 -10 19.6142 9.32808 6 5 -4 10 26.5606 17.9099 5 -5 4 -10 13.4828 5.42005 3 -5 4 -10 9.53781 8.30825 4 6 -4 10 -8.4117 15.4470 5 6 -4 10 18.3551 22.1906 7 6 -4 10 5.34534 4.14636 6 -6 -4 -10 4.66809 7.04588 6 6 -4 10 10.7955 11.7388 1 -6 4 -10 8.24393 4.99016 3 -6 4 -10 8.03601 8.13227 4 6 4 10 8.22377 4.89718 3 7 -4 10 22.0895 20.8429 7 7 -4 10 37.4641 12.9578 1 7 -4 10 55.8456 7.74871 6 -7 -4 -10 54.8776 9.70028 6 7 -4 10 20.7388 28.1590 5 -7 4 -10 50.8791 8.41717 3 7 4 10 63.3023 9.03331 3 -8 -4 -10 453.228 24.1997 6 8 -4 10 452.206 43.8801 7 8 -4 10 480.603 28.2061 1 8 -4 10 512.206 45.4134 5 8 -4 10 476.575 18.6390 6 -8 4 -10 477.202 28.1220 4 8 4 10 481.798 19.7087 3 -8 4 -10 469.603 18.7283 3 9 -4 10 993.419 32.1091 6 9 -4 10 956.239 53.1304 7 9 -4 10 993.180 61.7425 5 -9 -4 -10 1070.69 38.6896 6 9 -4 10 943.815 40.4309 1 -9 4 -10 1006.33 32.0730 3 9 4 10 1014.71 33.1569 3 -9 4 -10 1003.10 43.8726 4 -10 -4 -10 246.355 21.1381 6 10 -4 10 280.381 50.0341 5 10 -4 10 250.733 30.4221 1 -10 4 -10 285.309 18.7427 3 10 4 10 278.608 19.9851 3 -10 4 -10 237.931 28.5176 4 11 -4 10 1.51372 4.14170 6 -11 -4 -10 -0.5616 6.91369 6 11 -4 10 2.04873 8.26693 1 -11 4 -10 3.77263 4.06946 3 11 4 10 -1.8534 4.59115 3 12 -4 10 13.4023 4.40749 6 -12 -4 -10 16.8816 7.83138 6 12 -4 10 6.33286 7.42910 1 -12 4 -10 7.92559 4.26073 3 12 4 10 6.66321 5.03153 3 13 -4 10 23.4214 7.36293 1 13 -4 10 19.8398 4.09415 6 -13 -4 -10 23.5947 7.30870 6 13 4 10 21.1300 5.56220 3 -13 4 -10 23.3498 4.67899 3 -14 -4 -10 61.2468 15.6243 6 -14 4 -10 78.1158 6.75413 3 14 4 10 64.7538 10.2393 3 -15 -4 -10 168.608 11.5518 6 15 4 10 178.186 9.57136 3 -15 4 -10 170.960 8.41980 3 -16 -4 -10 49.3908 9.04548 6 -16 4 -10 58.3929 5.69715 3 16 4 10 44.6204 5.83980 3 -18 5 10 12.0525 2.97967 3 18 5 -10 15.0770 4.34830 3 -17 5 10 1.59072 2.65618 3 17 5 -10 4.25479 3.72400 3 -16 -5 10 14.2173 3.58654 6 -16 5 10 17.8892 3.64950 3 16 5 -10 26.6724 5.16853 3 -15 5 10 1.79944 3.16846 3 15 5 -10 1.96985 5.17722 3 -14 -5 10 1.04602 3.98500 6 14 5 -10 1.29848 4.51967 3 -14 5 10 1.99472 3.31909 3 13 -5 -10 148.253 10.0626 6 -13 -5 10 157.846 10.4766 6 -13 5 10 159.283 9.56263 3 13 5 -10 167.358 11.3522 3 -12 -5 10 27.0080 5.72654 6 12 -5 -10 32.5718 5.91800 6 -12 5 10 29.2771 8.17355 2 -12 5 10 24.2455 4.62296 3 12 5 -10 22.7312 5.83213 3 11 -5 -10 256.403 16.4175 1 -11 5 10 216.152 17.9955 2 -10 -5 10 26.6626 5.52447 6 10 -5 -10 35.3582 8.42787 1 10 -5 -10 31.2286 6.37522 6 10 5 -10 33.8234 6.49685 3 -10 5 10 26.6981 7.98574 2 -10 5 10 37.7285 6.48209 3 -9 -5 10 51.4302 22.9249 7 9 -5 -10 74.7266 9.74579 6 9 -5 -10 77.8067 11.6366 1 -9 -5 10 75.0743 8.52846 6 -9 5 10 71.8241 7.36030 3 -9 5 10 81.3562 12.4822 2 9 5 -10 67.6237 9.38233 3 -8 -5 10 -0.2734 3.80356 6 -8 -5 10 13.4634 22.4089 7 8 -5 -10 -0.0195 6.14430 1 8 -5 -10 8.66742 5.55105 6 8 5 -10 6.15457 5.14601 3 -8 5 10 1.55512 3.86727 3 -8 5 10 -2.7883 5.62100 2 -7 -5 10 -5.1689 21.6757 7 7 -5 -10 22.5899 6.91282 1 7 -5 -10 6.69798 5.34066 6 -7 -5 10 12.0124 4.33603 6 7 5 -10 16.7407 7.06367 3 -7 5 10 12.9549 7.30566 2 -7 5 10 21.1765 5.16242 3 -6 -5 10 6.17377 4.34371 6 6 -5 -10 3.22776 5.40135 6 6 -5 -10 0.62325 5.50322 1 -6 -5 10 15.7549 25.0973 7 -6 5 10 10.6368 4.70234 3 -6 5 10 5.50139 5.63590 2 -5 -5 10 517.956 36.3828 1 -5 -5 10 499.713 51.6272 7 5 -5 -10 487.656 19.4265 6 -5 -5 10 466.274 16.5623 6 5 -5 -10 485.967 21.7738 1 -5 5 10 491.391 23.3569 2 4 -5 -10 137.447 10.8670 6 4 -5 -10 124.004 13.2599 1 -4 -5 10 135.135 7.58251 6 -4 -5 10 114.143 20.7760 1 -4 -5 10 183.883 33.3549 7 -4 5 10 106.640 11.2608 2 -3 -5 10 11.6508 11.5743 1 -3 -5 10 19.3386 38.2945 7 -3 -5 10 31.0953 6.21082 6 3 -5 -10 18.9800 6.62918 1 3 -5 -10 17.7887 5.88049 6 -3 5 10 23.3288 6.65278 2 -2 -5 10 48.5163 14.2539 1 2 -5 -10 43.7724 6.92612 6 -2 -5 10 -0.8143 11.1504 5 -2 5 10 66.3786 9.68326 2 1 -5 -10 31.2156 6.41992 6 -1 -5 10 65.7566 21.1156 1 -1 -5 10 57.9724 33.2430 7 -1 -5 10 53.6654 17.0712 5 -1 5 10 57.7014 8.99766 2 0 -5 10 43.2294 13.4103 1 0 -5 10 60.9452 27.3739 7 0 -5 10 64.2430 18.7520 5 0 -5 -10 51.7753 8.99120 6 0 5 10 44.7219 7.55307 3 0 5 -10 52.7240 10.6440 4 0 5 10 38.3565 7.51661 2 -1 -5 -10 25.2210 6.50810 6 1 -5 10 3.48705 15.6137 5 1 -5 10 10.0266 11.1920 1 1 -5 10 55.0407 26.8138 7 -1 5 -10 5.40489 7.33319 4 1 5 10 6.27825 4.26119 3 -2 -5 -10 266.230 17.1350 6 2 -5 10 285.626 47.0433 7 2 -5 10 219.093 33.7964 5 2 -5 10 261.202 24.6591 1 2 5 10 233.856 11.7763 3 -2 5 -10 237.059 18.9716 4 3 -5 10 45.3932 25.0756 7 -3 -5 -10 64.6685 10.4191 6 3 -5 10 53.3585 13.3932 1 3 -5 10 103.976 23.6337 5 -3 5 -10 48.8468 10.7910 4 4 -5 10 122.376 28.6990 7 4 -5 10 98.4809 32.6139 5 4 -5 10 124.983 20.6237 1 -4 -5 -10 133.501 13.0131 6 -4 5 -10 137.864 18.8419 4 4 5 10 135.602 10.2755 3 5 -5 10 260.536 25.1511 1 -5 -5 -10 223.344 15.3823 6 5 -5 10 188.591 31.9670 7 5 -5 10 168.853 32.0989 5 -5 5 -10 226.016 19.6567 4 5 5 10 226.344 12.6832 3 -6 -5 -10 97.0984 12.5752 6 6 -5 10 43.7315 23.7010 5 6 -5 10 103.745 25.7753 7 6 -5 10 70.7231 15.0710 1 6 5 10 86.3958 9.13357 3 -6 5 -10 76.4254 9.28228 3 -6 5 -10 97.8604 14.5526 4 -7 -5 -10 98.0524 12.8092 6 7 -5 10 69.3055 13.8226 1 7 -5 10 54.9851 22.0829 7 7 -5 10 134.463 30.7404 5 7 5 10 92.3810 9.73731 3 -7 5 -10 90.6098 8.82611 3 -7 5 -10 91.7133 15.9120 4 8 -5 10 59.6749 34.5113 5 8 -5 10 94.0561 21.9319 7 -8 -5 -10 119.530 17.4355 6 -8 5 -10 108.990 18.3764 4 -8 5 -10 103.814 8.84702 3 8 5 10 104.505 10.9936 3 9 -5 10 60.1441 12.4689 1 -9 -5 -10 92.9724 12.5407 6 9 -5 10 83.5731 19.3204 7 -9 5 -10 80.5224 8.17959 3 9 5 10 77.8035 8.86584 3 10 -5 10 28.9313 16.1553 7 -10 -5 -10 67.9138 9.61813 6 10 -5 10 87.9636 16.5089 1 10 5 10 74.4455 9.11008 3 -10 5 -10 63.2255 7.78804 3 11 -5 10 80.4257 14.0433 1 -11 -5 -10 81.6456 11.1067 6 11 5 10 98.3337 8.98402 3 12 -5 10 123.751 12.4737 1 -12 -5 -10 84.9799 12.9076 6 12 5 10 91.6461 13.0087 3 -12 5 -10 95.6686 7.13113 3 13 -5 10 -4.2267 5.26446 1 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1 24 -1.1012 4.15574 6 -3 -1 24 144.062 25.5467 7 3 -1 -24 117.738 9.60730 3 3 -1 -24 96.7985 13.5708 6 -3 -1 24 98.6847 9.40120 6 3 1 -24 115.740 15.5779 6 -3 1 24 101.551 10.0915 6 3 1 -24 100.771 7.75394 3 -2 -1 24 28.6946 18.8482 7 -2 -1 24 16.9608 4.82783 6 2 -1 -24 25.1774 5.25022 3 2 -1 -24 29.8215 8.26827 6 -2 1 24 15.6113 3.89468 3 2 1 -24 13.5871 8.43096 6 -2 1 24 16.6293 5.35291 6 2 1 -24 18.3463 4.22782 3 -1 -1 24 4.26366 7.62844 1 -1 -1 24 10.1373 16.6132 7 1 -1 -24 4.87850 6.40703 6 1 -1 -24 6.59178 2.88661 3 -1 -1 24 10.7485 4.82465 6 1 1 -24 6.44051 3.50449 3 -1 1 24 0.78808 3.21357 3 -1 1 24 14.5271 16.4452 7 -1 1 24 6.16567 4.88841 6 1 1 -24 9.76595 8.49275 6 0 -1 24 -6.7551 15.1613 7 0 -1 -24 6.73411 6.29461 6 0 -1 -24 5.18058 2.62046 3 0 -1 24 5.25418 3.81831 6 0 -1 24 7.39147 8.16837 1 0 1 24 10.8947 25.2000 7 0 1 24 11.1863 3.39167 3 0 1 -24 8.67844 3.56331 3 0 1 -24 4.56532 7.73920 6 0 1 24 3.90607 3.81005 6 1 -1 24 12.1227 13.9367 7 1 -1 24 27.8604 7.94718 1 -1 -1 -24 8.73676 6.70973 6 1 -1 24 16.4045 4.44301 6 -1 1 -24 10.7136 7.48586 6 1 1 24 15.8340 4.44555 6 1 1 24 17.5284 3.72322 3 -1 1 -24 18.6656 3.72953 3 1 1 24 16.9233 7.90210 1 -2 -1 -24 -4.7215 5.94243 6 2 -1 24 -1.4668 3.79599 6 2 -1 24 -4.8359 6.65386 1 2 1 24 3.68542 5.20077 6 2 1 24 -0.1972 2.43394 3 -2 1 -24 -5.9511 7.71194 6 -2 1 -24 5.18899 2.99032 3 3 -1 24 6.02347 4.25100 6 -3 -1 -24 17.1674 10.9740 6 3 1 24 7.19896 4.27737 6 -3 1 -24 9.36415 3.57204 3 -10 -2 24 -8.6476 12.2662 7 10 -2 -24 1.56682 5.54796 6 -10 -2 24 8.98335 6.46534 1 -10 -2 24 0.74172 3.33541 6 10 2 -24 2.99600 3.35132 3 -10 2 24 -0.7741 2.48488 3 -9 -2 24 33.7976 6.45422 6 9 -2 -24 22.5292 6.41437 6 -9 -2 24 49.0291 15.6687 7 9 2 -24 40.3336 5.37231 3 -9 2 24 36.9183 4.30319 3 8 -2 -24 -1.0034 5.29473 6 -8 -2 24 -3.0024 3.43172 6 -8 -2 24 -6.7659 14.6102 7 -8 2 24 3.30189 5.98609 6 8 2 -24 2.01729 3.23704 3 -8 2 24 2.99542 2.50999 3 -7 -2 24 2.33130 3.78349 6 -7 -2 24 -17.750 15.1632 7 7 -2 -24 2.47942 5.66795 6 7 2 -24 -0.7539 3.17891 3 -7 2 24 2.80666 4.41277 6 -7 2 24 -1.0323 2.48554 3 -6 -2 24 -3.5101 15.7209 7 6 -2 -24 6.82008 6.41102 6 -6 -2 24 12.6687 4.50800 6 6 2 -24 12.1002 3.93900 3 -6 2 24 9.73294 4.78428 6 -6 2 24 15.5047 3.08311 3 5 -2 -24 35.5098 7.83023 6 -5 -2 24 8.65610 17.6907 7 -5 -2 24 19.0402 4.87867 6 -5 2 24 24.9432 5.51707 6 5 2 -24 24.6853 4.29279 3 -5 2 24 15.7942 3.19138 3 4 -2 -24 14.5201 6.56182 6 -4 -2 24 64.8314 19.9410 7 -4 -2 24 6.54985 4.13198 6 -4 -2 24 9.63371 7.73918 1 -4 2 24 2.70486 4.46596 6 -4 2 24 10.1127 3.06751 3 4 2 -24 9.13279 3.92547 3 -3 -2 24 16.1813 17.1900 7 3 -2 -24 12.2211 6.87545 6 -3 -2 24 11.2291 4.11470 6 -3 -2 24 11.9191 7.95823 1 -3 2 24 9.85062 4.80424 6 3 2 -24 10.9045 3.76068 3 -2 -2 24 12.1189 4.20738 6 2 -2 -24 5.83600 6.41548 6 -2 -2 24 23.8829 17.1862 7 -2 -2 24 12.2828 7.78318 1 2 2 -24 20.0806 4.20785 3 -2 2 24 3.89464 4.41029 6 -2 2 24 6.51556 3.33990 3 1 -2 -24 13.5713 6.02837 6 -1 -2 24 -0.4606 15.4399 7 -1 -2 24 5.69665 7.42205 1 -1 -2 24 2.90231 3.55586 6 -1 2 24 6.66579 4.66661 6 1 2 -24 4.41403 3.44738 3 -1 2 24 4.38335 3.13847 3 0 -2 24 4.35625 14.5724 7 0 -2 24 23.8011 4.32180 6 0 -2 24 55.5083 9.34353 1 0 -2 -24 23.3269 6.91180 6 0 2 -24 32.5238 5.42323 3 0 2 24 28.9676 5.21888 3 0 2 24 46.8411 7.81846 6 0 2 24 16.0682 17.2830 7 1 -2 24 -1.9479 7.32030 1 1 -2 24 -17.008 12.0319 7 -1 -2 -24 8.00346 6.16095 6 1 -2 24 3.84113 3.61648 6 -1 2 -24 3.06607 3.10091 3 1 2 24 3.44423 2.98003 3 1 2 24 1.62143 4.23077 6 2 -2 24 5.07790 3.39649 6 -2 -2 -24 -1.1955 6.01635 6 2 -2 24 -4.5773 7.30953 1 -2 2 -24 -0.5781 2.85831 3 2 2 24 -4.0142 4.14914 6 2 2 24 3.73207 2.86266 3 -8 -3 24 11.7593 6.61115 1 -8 -3 24 0.65265 13.9124 7 -8 -3 24 -0.6054 2.75371 6 8 -3 -24 4.16730 9.28430 6 8 3 -24 11.8247 4.30013 3 -8 3 24 3.64720 2.75829 3 -7 -3 24 33.2243 10.2291 1 7 -3 -24 46.6198 8.13191 6 -7 -3 24 33.5788 5.47258 6 -7 -3 24 48.7494 16.5485 7 7 3 -24 42.1033 5.92439 3 -7 3 24 47.3956 4.37246 3 -6 -3 24 16.7201 15.1313 7 6 -3 -24 22.3102 5.68056 6 -6 -3 24 15.4766 7.42352 1 -6 -3 24 25.7621 4.89889 6 6 3 -24 16.9258 3.83901 3 -6 3 24 30.6090 4.31871 3 -5 -3 24 -0.4145 15.5493 7 -5 -3 24 4.51686 3.10449 6 5 -3 -24 5.18919 5.08197 6 -5 -3 24 6.26167 7.08218 1 5 3 -24 0.25316 3.26733 3 -5 3 24 2.95146 2.57225 3 -4 -3 24 105.703 13.4505 1 -4 -3 24 119.646 7.08506 6 -4 -3 24 96.9324 19.3877 7 4 -3 -24 129.492 10.6563 6 4 3 -24 110.540 7.02125 3 -4 3 24 106.044 5.92004 3 -3 -3 24 15.4040 16.1162 7 -3 -3 24 26.1013 7.89459 1 3 -3 -24 44.8146 8.50080 6 -3 -3 24 34.2756 4.35766 6 3 3 -24 45.0954 5.60770 3 -2 -3 24 25.9662 8.30378 1 -2 -3 24 17.3081 3.55872 6 2 -3 -24 19.6989 5.63923 6 -2 -3 24 29.5288 17.7651 7 2 3 -24 11.4842 3.68246 3 -2 3 24 16.9081 3.64699 3 1 -3 -24 4.54125 5.16349 6 -1 -3 24 6.41548 3.93088 6 -1 -3 24 -26.320 18.0039 7 -1 -3 24 11.5667 7.97977 1 1 3 -24 5.13608 3.33731 3 -1 3 24 6.66941 3.00971 3 0 -3 -24 20.6659 6.57078 6 0 -3 24 19.1082 3.87534 6 0 -3 24 19.9006 15.8993 7 0 -3 24 27.6534 11.0043 1 0 3 24 22.8705 3.99315 3 0 3 -24 26.0380 5.82313 3 -9 0 25 234.637 11.7464 6 9 0 -25 233.489 14.9730 6 -9 0 25 229.708 26.6070 7 8 0 -25 3.83416 6.32560 6 -8 0 25 1.43069 14.8791 7 8 0 -25 -2.6553 2.78802 3 -8 0 25 -3.9365 4.34490 6 -7 0 25 7.68560 17.4004 7 -7 0 25 18.0583 4.84310 6 7 0 -25 11.7078 7.68209 6 7 0 -25 16.2145 2.94728 3 6 0 -25 -0.6698 6.66342 6 -6 0 25 -2.5544 16.2974 7 -6 0 25 0.83291 3.83151 6 6 0 -25 2.51380 2.83400 3 -5 0 25 50.2651 7.27173 6 5 0 -25 36.5112 5.76269 3 5 0 -25 20.0664 7.22746 6 -5 0 25 52.6827 18.9928 7 4 0 -25 2.43251 4.66619 3 -4 0 25 -22.182 15.9572 7 4 0 -25 -3.3577 6.03815 6 -4 0 25 2.65033 4.06135 6 -3 0 25 44.1026 7.32599 6 3 0 -25 37.3196 5.70705 3 3 0 -25 30.2396 8.74888 6 -3 0 25 45.4814 18.5538 7 -2 0 25 -1.0184 3.71319 6 -2 0 25 -20.799 14.0909 7 2 0 -25 1.63420 2.85984 3 2 0 -25 8.42251 7.52179 6 1 0 -25 0.48349 6.18628 6 -1 0 25 -2.1652 14.0677 7 -1 0 25 1.47189 3.73634 6 -1 0 25 -2.5776 10.8792 1 1 0 -25 0.03679 2.49760 3 0 0 25 -9.4091 6.70551 1 0 0 -25 -0.3968 2.26146 3 0 0 -25 -3.2977 6.15938 6 0 0 25 -0.7666 3.90544 6 -1 0 -25 23.4276 7.56815 6 1 0 25 11.8353 4.62500 6 -9 -1 25 11.4946 15.9919 7 -8 -1 25 8.61972 4.18678 6 8 -1 -25 8.04662 7.21709 6 -8 -1 25 8.46407 15.2053 7 8 1 -25 5.64516 3.19008 3 -8 1 25 1.07132 4.17362 6 8 1 -25 3.76033 10.2849 6 7 -1 -25 7.55689 6.22630 6 -7 -1 25 10.0869 16.4045 7 -7 -1 25 3.17172 3.72983 6 7 1 -25 1.98759 7.36339 6 7 1 -25 7.98520 3.19389 3 -7 1 25 7.62019 4.36632 6 -6 -1 25 12.5140 4.60377 6 -6 -1 25 29.3112 17.0436 7 6 -1 -25 6.43926 6.61978 6 -6 1 25 7.45187 4.29923 6 6 1 -25 14.3302 7.32643 6 6 1 -25 14.5294 3.51607 3 -5 -1 25 21.3152 17.3992 7 5 -1 -25 6.75255 6.40478 6 -5 -1 25 9.00016 4.28679 6 -5 1 25 4.65100 4.09951 6 5 1 -25 6.88628 6.69195 6 -5 1 25 5.65802 3.47519 3 5 1 -25 10.9447 3.42813 3 -4 -1 25 25.0401 17.7016 7 -4 -1 25 61.3386 7.32649 6 4 -1 -25 52.9940 8.35012 6 4 1 -25 42.0149 7.96514 6 4 1 -25 68.2144 5.73705 3 -4 1 25 54.9012 7.62959 6 -4 1 25 55.3052 6.44041 3 -3 -1 25 27.2616 8.48805 1 3 -1 -25 14.5611 6.63147 6 -3 -1 25 20.4054 4.62113 6 -3 -1 25 28.3329 16.7769 7 -3 1 25 24.4411 4.35080 3 3 1 -25 22.1897 7.30786 6 -3 1 25 14.5568 4.25508 6 3 1 -25 31.3896 5.11683 3 -3 1 25 8.68892 16.1175 7 -2 -1 25 36.7540 17.7067 7 -2 -1 25 45.4808 8.61679 1 -2 -1 25 45.1347 7.04941 6 2 -1 -25 67.0003 11.2303 6 2 1 -25 63.7534 5.46233 3 -2 1 25 52.7097 4.77574 3 2 1 -25 60.7947 9.70743 6 -2 1 25 43.9156 6.82882 6 -2 1 25 21.6422 16.6470 7 1 -1 -25 2.01009 6.09644 6 -1 -1 25 2.09337 3.36115 6 -1 -1 25 0.70122 7.91281 1 -1 -1 25 -1.9826 14.7649 7 -1 1 25 -23.412 12.6235 7 1 1 -25 15.0297 8.48318 6 -1 1 25 7.88909 4.29471 6 -1 1 25 8.53622 2.56665 3 1 1 -25 6.34248 2.92555 3 0 -1 25 -2.0244 3.49892 6 0 -1 25 7.69267 7.80556 1 0 -1 25 4.35468 13.8067 7 0 -1 -25 -9.5539 6.50163 6 0 1 -25 3.26902 3.01486 3 0 1 25 0.85295 4.11322 6 -7 -2 25 12.9355 10.8321 1 -7 -2 25 -15.595 19.4562 7 -6 -2 25 11.6627 6.89999 1 -6 -2 25 -9.7623 14.1220 7 -6 -2 25 3.34333 3.35961 6 6 -2 -25 4.60277 5.95478 6 6 2 -25 7.95722 3.23130 3 -5 -2 25 -11.833 15.3889 7 5 -2 -25 1.90329 5.69098 6 -5 -2 25 -9.0115 6.40933 1 -5 -2 25 -0.5138 3.22382 6 5 2 -25 5.56450 3.18002 3 -4 -2 25 4.75508 16.6280 7 4 -2 -25 10.6466 5.86526 6 -4 -2 25 24.2675 7.05004 1 -4 -2 25 9.95010 3.68981 6 4 2 -25 4.76601 3.21947 3 -3 -2 25 8.24876 3.42660 6 -3 -2 25 16.1598 20.6189 7 -3 -2 25 4.61566 7.43926 1 3 -2 -25 9.92450 6.27644 6 3 2 -25 6.60796 3.55234 3 -3 2 25 10.4615 3.92199 3 -2 -2 25 17.1942 10.0690 1 -2 -2 25 21.5472 18.0277 7 2 -2 -25 16.2319 7.10202 6 -2 -2 25 17.0370 3.62850 6 2 2 -25 11.3684 3.23659 3 -2 2 25 5.49367 14.7180 7 -2 2 25 22.3365 3.23874 3 0 0 0 0.00 0.00 0 _exptl_absorpt_process_details ) SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ) _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_max 0.7533 _exptl_absorpt_correction_T_min 0.6767 _exptl_special_details ) The following wavelength and cell were deduced by SADABS from the direction cosines etc. They are given here for emergency use only: CELL 1.54180 18.061 7.857 21.154 89.999 101.224 89.968 ) ; _shelx_hkl_checksum 74119 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.47418(6) 0.33375(16) 0.43762(5) 0.0204(3) Uani 1 1 d D . . . . H1 H 0.4628(11) 0.373(3) 0.4728(7) 0.031 Uiso 1 1 d D U . . . O2 O 0.55524(6) 0.57617(16) 0.44461(5) 0.0183(3) Uani 1 1 d . . . . . O3 O 0.63481(6) 0.60589(16) 0.36521(5) 0.0192(3) Uani 1 1 d . . . . . O4 O 0.55390(6) 0.36069(16) 0.36463(5) 0.0188(3) Uani 1 1 d . . . . . O5 O 0.67487(6) 0.72037(16) 0.47008(5) 0.0204(3) Uani 1 1 d . . . . . O6 O 0.77301(7) 0.7111(2) 0.58102(6) 0.0331(3) Uani 1 1 d . . . . . O7 O 0.57958(6) 0.46421(17) 0.26662(5) 0.0223(3) Uani 1 1 d . . . . . O8 O 0.51387(7) 0.53554(19) 0.14735(5) 0.0321(3) Uani 1 1 d . . . . . N1 N 0.56646(7) 0.8558(2) 0.39773(6) 0.0186(3) Uani 1 1 d . . . . . N2 N 0.68313(7) 0.3248(2) 0.34533(6) 0.0210(3) Uani 1 1 d . . . . . C1 C 0.67041(8) 0.8427(2) 0.51311(7) 0.0195(4) Uani 1 1 d . . . . . C2 C 0.72211(9) 0.8423(3) 0.57260(8) 0.0248(4) Uani 1 1 d . . . . . C3 C 0.71792(10) 0.9679(3) 0.61734(8) 0.0314(5) Uani 1 1 d . . . . . H3 H 0.751837 0.965756 0.657741 0.038 Uiso 1 1 calc R U . . . C4 C 0.66468(10) 1.0981(3) 0.60417(8) 0.0324(5) Uani 1 1 d . . . . . H4 H 0.662885 1.183879 0.635490 0.039 Uiso 1 1 calc R U . . . C5 C 0.61473(10) 1.1032(3) 0.54621(8) 0.0262(4) Uani 1 1 d . . . . . H5 H 0.578849 1.192667 0.537070 0.031 Uiso 1 1 calc R U . . . C6 C 0.61748(9) 0.9739(2) 0.50053(7) 0.0202(4) Uani 1 1 d . . . . . C7 C 0.56810(9) 0.9787(2) 0.43835(7) 0.0198(4) Uani 1 1 d . . . . . H7 H 0.536074 1.074365 0.427022 0.024 Uiso 1 1 calc R U . . . C8 C 0.81586(12) 0.6886(3) 0.64452(9) 0.0416(5) Uani 1 1 d . . . . . H8A H 0.848369 0.588354 0.645543 0.062 Uiso 1 1 calc R U . . . H8B H 0.781576 0.672406 0.674650 0.062 Uiso 1 1 calc R U . . . H8C H 0.847090 0.789761 0.657031 0.062 Uiso 1 1 calc R U . . . C9 C 0.51791(9) 0.8702(2) 0.33334(7) 0.0217(4) Uani 1 1 d . . . . . H9A H 0.476191 0.950501 0.335317 0.026 Uiso 1 1 calc R U . . . H9B H 0.495515 0.757511 0.320064 0.026 Uiso 1 1 calc R U . . . C10 C 0.56204(9) 0.9325(3) 0.28349(7) 0.0241(4) Uani 1 1 d . . . . . H10A H 0.580202 1.049734 0.294569 0.029 Uiso 1 1 calc R U . . . H10B H 0.606701 0.858606 0.284674 0.029 Uiso 1 1 calc R U . . . C11 C 0.51450(10) 0.9313(3) 0.21586(8) 0.0280(4) Uani 1 1 d . . . . . H11A H 0.488576 0.820033 0.207907 0.034 Uiso 1 1 calc R U . . . H11B H 0.475348 1.020857 0.212571 0.034 Uiso 1 1 calc R U . . . C12 C 0.56118(11) 0.9617(3) 0.16450(8) 0.0345(5) Uani 1 1 d . . . . . H12A H 0.528048 0.961979 0.121910 0.052 Uiso 1 1 calc R U . . . H12B H 0.598732 0.870808 0.166388 0.052 Uiso 1 1 calc R U . . . H12C H 0.586883 1.071873 0.172063 0.052 Uiso 1 1 calc R U . . . C13 C 0.61676(9) 0.4232(2) 0.22043(7) 0.0212(4) Uani 1 1 d . . . . . C14 C 0.58349(10) 0.4616(3) 0.15582(8) 0.0256(4) Uani 1 1 d . . . . . C15 C 0.62190(11) 0.4198(3) 0.10708(8) 0.0326(5) Uani 1 1 d . . . . . H15 H 0.600358 0.448313 0.063765 0.039 Uiso 1 1 calc R U . . . C16 C 0.69167(11) 0.3366(3) 0.12056(9) 0.0341(5) Uani 1 1 d . . . . . H16 H 0.717189 0.310169 0.086564 0.041 Uiso 1 1 calc R U . . . C17 C 0.72323(10) 0.2933(3) 0.18256(9) 0.0300(4) Uani 1 1 d . . . . . H17 H 0.769899 0.233880 0.191579 0.036 Uiso 1 1 calc R U . . . C18 C 0.68602(9) 0.3374(3) 0.23313(8) 0.0238(4) Uani 1 1 d . . . . . C19 C 0.71526(9) 0.2847(2) 0.29816(8) 0.0238(4) Uani 1 1 d . . . . . H19 H 0.759906 0.217749 0.306703 0.029 Uiso 1 1 calc R U . . . C20 C 0.47722(13) 0.5713(3) 0.08261(8) 0.0419(6) Uani 1 1 d . . . . . H20A H 0.470358 0.465111 0.057791 0.063 Uiso 1 1 calc R U . . . H20B H 0.508257 0.650138 0.062997 0.063 Uiso 1 1 calc R U . . . H20C H 0.427892 0.623171 0.082616 0.063 Uiso 1 1 calc R U . . . C21 C 0.71590(9) 0.2654(3) 0.41110(8) 0.0273(4) Uani 1 1 d . . . . . H21A H 0.727005 0.142105 0.409616 0.033 Uiso 1 1 calc R U . . . H21B H 0.678224 0.280774 0.438899 0.033 Uiso 1 1 calc R U . . . C22 C 0.78758(10) 0.3590(3) 0.44085(8) 0.0304(4) Uani 1 1 d . . . . . H22A H 0.777085 0.482788 0.441139 0.036 Uiso 1 1 calc R U . . . H22B H 0.826104 0.340115 0.414118 0.036 Uiso 1 1 calc R U . . . C23 C 0.81853(11) 0.2999(3) 0.50926(9) 0.0390(5) Uani 1 1 d . . . . . H23A H 0.825754 0.174897 0.509344 0.047 Uiso 1 1 calc R U . . . H23B H 0.781333 0.325869 0.536618 0.047 Uiso 1 1 calc R U . . . C24 C 0.89319(11) 0.3851(4) 0.53776(10) 0.0476(6) Uani 1 1 d . . . . . H24A H 0.930636 0.356944 0.511558 0.071 Uiso 1 1 calc R U . . . H24B H 0.910837 0.344357 0.581908 0.071 Uiso 1 1 calc R U . . . H24C H 0.886196 0.508877 0.538192 0.071 Uiso 1 1 calc R U . . . B1 B 0.52775(9) 0.4271(3) 0.41577(8) 0.0172(4) Uani 1 1 d . . . . . B2 B 0.60981(9) 0.6797(3) 0.41816(8) 0.0188(4) Uani 1 1 d . . . . . B3 B 0.61044(10) 0.4478(3) 0.33716(8) 0.0185(4) Uani 1 1 d . . . . . Cl1 Cl 0.36396(3) 0.52550(8) 0.29259(3) 0.04268(18) Uani 0.9384(17) 1 d D . P . . Cl2 Cl 0.32882(3) 0.20370(10) 0.22661(4) 0.0396(2) Uani 0.893(2) 1 d . . P A 1 C25 C 0.39567(12) 0.3176(3) 0.28209(12) 0.0358(6) Uani 0.893(2) 1 d . . P A 1 H25A H 0.443816 0.322889 0.266456 0.043 Uiso 0.893(2) 1 calc R U P A 1 H25B H 0.405146 0.257507 0.324024 0.043 Uiso 0.893(2) 1 calc R U P A 1 C25A C 0.4084(9) 0.365(4) 0.2556(19) 0.034(3) Uiso 0.046(2) 1 d D . P A 2 H25C H 0.444826 0.417703 0.232115 0.041 Uiso 0.046(2) 1 calc R U P A 2 H25D H 0.437076 0.289524 0.289300 0.041 Uiso 0.046(2) 1 calc R U P A 2 Cl2A Cl 0.3437(7) 0.2419(15) 0.2018(6) 0.034(3) Uiso 0.046(2) 1 d D . P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0239(5) 0.0183(7) 0.0214(5) -0.0022(5) 0.0104(4) -0.0038(5) O2 0.0217(5) 0.0152(7) 0.0204(5) -0.0006(5) 0.0095(4) -0.0028(5) O3 0.0209(5) 0.0168(7) 0.0222(5) -0.0005(5) 0.0098(4) -0.0019(5) O4 0.0197(5) 0.0174(7) 0.0204(5) -0.0032(5) 0.0068(4) -0.0023(5) O5 0.0202(5) 0.0176(7) 0.0236(5) -0.0016(5) 0.0047(4) 0.0000(5) O6 0.0299(6) 0.0369(10) 0.0294(6) -0.0006(6) -0.0019(5) 0.0092(6) O7 0.0241(5) 0.0270(8) 0.0178(5) -0.0021(5) 0.0089(4) 0.0048(5) O8 0.0408(7) 0.0365(9) 0.0184(5) -0.0009(5) 0.0043(5) 0.0085(6) N1 0.0177(6) 0.0169(9) 0.0221(6) 0.0010(6) 0.0059(5) -0.0029(6) N2 0.0187(6) 0.0179(9) 0.0271(7) -0.0009(6) 0.0061(5) -0.0019(6) C1 0.0206(7) 0.0180(10) 0.0216(7) -0.0015(7) 0.0078(6) -0.0050(7) C2 0.0232(8) 0.0227(11) 0.0283(8) 0.0009(8) 0.0050(6) -0.0013(7) C3 0.0318(9) 0.0362(14) 0.0243(8) -0.0050(8) 0.0004(7) -0.0021(9) C4 0.0366(10) 0.0314(13) 0.0292(9) -0.0115(8) 0.0062(7) -0.0014(9) C5 0.0279(8) 0.0199(11) 0.0321(8) -0.0029(8) 0.0091(7) -0.0005(8) C6 0.0219(7) 0.0168(10) 0.0238(7) -0.0002(7) 0.0087(6) -0.0046(7) C7 0.0203(7) 0.0146(10) 0.0257(8) 0.0004(7) 0.0080(6) -0.0013(7) C8 0.0372(10) 0.0524(17) 0.0322(9) 0.0078(10) -0.0002(8) 0.0075(10) C9 0.0191(7) 0.0202(11) 0.0248(8) -0.0001(7) 0.0016(6) -0.0001(7) C10 0.0240(8) 0.0230(12) 0.0242(8) 0.0027(7) 0.0020(6) -0.0042(7) C11 0.0278(8) 0.0295(13) 0.0247(8) -0.0027(8) 0.0003(6) 0.0049(8) C12 0.0405(10) 0.0363(14) 0.0250(8) 0.0015(8) 0.0025(7) -0.0041(9) C13 0.0252(8) 0.0176(11) 0.0240(7) -0.0057(7) 0.0131(6) -0.0040(7) C14 0.0341(9) 0.0204(11) 0.0248(8) -0.0039(7) 0.0118(7) -0.0034(8) C15 0.0468(11) 0.0313(13) 0.0232(8) -0.0057(8) 0.0157(7) -0.0089(9) C16 0.0420(10) 0.0320(13) 0.0358(10) -0.0137(9) 0.0261(8) -0.0102(9) C17 0.0275(8) 0.0284(13) 0.0394(9) -0.0120(9) 0.0196(7) -0.0048(8) C18 0.0243(8) 0.0200(11) 0.0302(8) -0.0077(8) 0.0129(6) -0.0064(7) C19 0.0180(7) 0.0182(11) 0.0365(9) -0.0044(8) 0.0086(6) -0.0015(7) C20 0.0563(12) 0.0453(16) 0.0216(8) -0.0006(9) 0.0018(8) 0.0078(11) C21 0.0263(8) 0.0249(12) 0.0307(8) 0.0056(8) 0.0054(6) 0.0028(8) C22 0.0250(8) 0.0317(13) 0.0343(9) 0.0022(8) 0.0056(7) 0.0005(8) C23 0.0340(10) 0.0469(16) 0.0344(9) 0.0014(10) 0.0026(7) 0.0048(10) C24 0.0343(10) 0.0597(19) 0.0445(11) -0.0115(11) -0.0027(8) 0.0081(11) B1 0.0167(8) 0.0177(12) 0.0175(7) 0.0026(7) 0.0044(6) 0.0014(7) B2 0.0191(8) 0.0166(12) 0.0220(8) 0.0002(8) 0.0070(6) -0.0021(8) B3 0.0188(8) 0.0196(12) 0.0186(8) 0.0005(8) 0.0072(6) 0.0012(8) Cl1 0.0404(3) 0.0258(3) 0.0566(3) -0.0120(3) -0.0035(2) 0.0038(2) Cl2 0.0312(3) 0.0363(4) 0.0456(4) -0.0169(3) -0.0063(3) 0.0002(3) C25 0.0248(10) 0.0272(15) 0.0493(12) -0.0135(11) -0.0079(9) 0.0042(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag B1 O1 H1 113.8(14) . . ? B1 O2 B2 121.02(12) . . ? B3 O3 B2 125.01(13) . . ? B1 O4 B3 121.33(14) . . ? C1 O5 B2 121.09(13) . . ? C2 O6 C8 116.31(15) . . ? C13 O7 B3 124.76(13) . . ? C14 O8 C20 116.92(14) . . ? C7 N1 C9 119.43(15) . . ? C7 N1 B2 121.22(13) . . ? C9 N1 B2 119.07(14) . . ? C19 N2 C21 119.61(14) . . ? C19 N2 B3 122.99(14) . . ? C21 N2 B3 117.30(12) . . ? O5 C1 C2 119.19(16) . . ? O5 C1 C6 122.04(14) . . ? C6 C1 C2 118.75(16) . . ? O6 C2 C1 115.35(16) . . ? O6 C2 C3 125.02(15) . . ? C3 C2 C1 119.62(17) . . ? C2 C3 H3 119.5 . . ? C2 C3 C4 120.98(16) . . ? C4 C3 H3 119.5 . . ? C3 C4 H4 119.7 . . ? C5 C4 C3 120.51(18) . . ? C5 C4 H4 119.7 . . ? C4 C5 H5 120.4 . . ? C4 C5 C6 119.10(18) . . ? C6 C5 H5 120.4 . . ? C1 C6 C5 121.00(15) . . ? C1 C6 C7 118.25(15) . . ? C5 C6 C7 120.67(17) . . ? N1 C7 C6 121.33(17) . . ? N1 C7 H7 119.3 . . ? C6 C7 H7 119.3 . . ? O6 C8 H8A 109.5 . . ? O6 C8 H8B 109.5 . . ? O6 C8 H8C 109.5 . . ? H8A C8 H8B 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? N1 C9 H9A 109.3 . . ? N1 C9 H9B 109.3 . . ? N1 C9 C10 111.55(12) . . ? H9A C9 H9B 108.0 . . ? C10 C9 H9A 109.3 . . ? C10 C9 H9B 109.3 . . ? C9 C10 H10A 109.2 . . ? C9 C10 H10B 109.2 . . ? H10A C10 H10B 107.9 . . ? C11 C10 C9 112.00(14) . . ? C11 C10 H10A 109.2 . . ? C11 C10 H10B 109.2 . . ? C10 C11 H11A 109.1 . . ? C10 C11 H11B 109.1 . . ? H11A C11 H11B 107.8 . . ? C12 C11 C10 112.47(14) . . ? C12 C11 H11A 109.1 . . ? C12 C11 H11B 109.1 . . ? C11 C12 H12A 109.5 . . ? C11 C12 H12B 109.5 . . ? C11 C12 H12C 109.5 . . ? H12A C12 H12B 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? O7 C13 C14 118.60(15) . . ? O7 C13 C18 122.44(15) . . ? C18 C13 C14 118.91(14) . . ? O8 C14 C13 115.13(14) . . ? O8 C14 C15 125.69(16) . . ? C15 C14 C13 119.16(17) . . ? C14 C15 H15 119.4 . . ? C14 C15 C16 121.28(17) . . ? C16 C15 H15 119.4 . . ? C15 C16 H16 119.9 . . ? C17 C16 C15 120.17(15) . . ? C17 C16 H16 119.9 . . ? C16 C17 H17 120.2 . . ? C16 C17 C18 119.62(17) . . ? C18 C17 H17 120.2 . . ? C13 C18 C17 120.78(16) . . ? C13 C18 C19 118.10(14) . . ? C17 C18 C19 120.96(17) . . ? N2 C19 C18 122.33(16) . . ? N2 C19 H19 118.8 . . ? C18 C19 H19 118.8 . . ? O8 C20 H20A 109.5 . . ? O8 C20 H20B 109.5 . . ? O8 C20 H20C 109.5 . . ? H20A C20 H20B 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? N2 C21 H21A 109.0 . . ? N2 C21 H21B 109.0 . . ? N2 C21 C22 113.04(15) . . ? H21A C21 H21B 107.8 . . ? C22 C21 H21A 109.0 . . ? C22 C21 H21B 109.0 . . ? C21 C22 H22A 109.2 . . ? C21 C22 H22B 109.2 . . ? C21 C22 C23 111.96(16) . . ? H22A C22 H22B 107.9 . . ? C23 C22 H22A 109.2 . . ? C23 C22 H22B 109.2 . . ? C22 C23 H23A 109.2 . . ? C22 C23 H23B 109.2 . . ? C22 C23 C24 112.16(19) . . ? H23A C23 H23B 107.9 . . ? C24 C23 H23A 109.2 . . ? C24 C23 H23B 109.2 . . ? C23 C24 H24A 109.5 . . ? C23 C24 H24B 109.5 . . ? C23 C24 H24C 109.5 . . ? H24A C24 H24B 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? O1 B1 O2 121.89(14) . . ? O1 B1 O4 116.19(16) . . ? O4 B1 O2 121.90(14) . . ? O2 B2 O5 109.37(12) . . ? O2 B2 N1 104.48(12) . . ? O3 B2 O2 114.69(15) . . ? O3 B2 O5 110.31(13) . . ? O3 B2 N1 110.75(13) . . ? O5 B2 N1 106.82(14) . . ? O3 B3 O4 115.83(13) . . ? O3 B3 O7 111.73(15) . . ? O3 B3 N2 107.52(13) . . ? O4 B3 O7 106.71(13) . . ? O4 B3 N2 107.41(14) . . ? O7 B3 N2 107.25(12) . . ? Cl1 C25 H25A 109.4 . . ? Cl1 C25 H25B 109.4 . . ? Cl2 C25 Cl1 111.00(11) . . ? Cl2 C25 H25A 109.4 . . ? Cl2 C25 H25B 109.4 . . ? H25A C25 H25B 108.0 . . ? Cl1 C25A H25C 109.2 . . ? Cl1 C25A H25D 109.2 . . ? H25C C25A H25D 107.9 . . ? Cl2A C25A Cl1 112.2(8) . . ? Cl2A C25A H25C 109.2 . . ? Cl2A C25A H25D 109.2 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 H1 0.866(9) . ? O1 B1 1.365(2) . ? O2 B1 1.368(2) . ? O2 B2 1.470(2) . ? O3 B2 1.411(2) . ? O3 B3 1.409(2) . ? O4 B1 1.366(2) . ? O4 B3 1.442(2) . ? O5 C1 1.337(2) . ? O5 B2 1.479(2) . ? O6 C2 1.370(2) . ? O6 C8 1.425(2) . ? O7 C13 1.3289(18) . ? O7 B3 1.494(2) . ? O8 C14 1.365(2) . ? O8 C20 1.429(2) . ? N1 C7 1.288(2) . ? N1 C9 1.4742(19) . ? N1 B2 1.606(3) . ? N2 C19 1.288(2) . ? N2 C21 1.478(2) . ? N2 B3 1.612(2) . ? C1 C2 1.414(2) . ? C1 C6 1.395(3) . ? C2 C3 1.379(3) . ? C3 H3 0.9500 . ? C3 C4 1.394(3) . ? C4 H4 0.9500 . ? C4 C5 1.374(3) . ? C5 H5 0.9500 . ? C5 C6 1.409(3) . ? C6 C7 1.439(2) . ? C7 H7 0.9500 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 H9A 0.9900 . ? C9 H9B 0.9900 . ? C9 C10 1.522(2) . ? C10 H10A 0.9900 . ? C10 H10B 0.9900 . ? C10 C11 1.519(2) . ? C11 H11A 0.9900 . ? C11 H11B 0.9900 . ? C11 C12 1.519(2) . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C13 C14 1.415(2) . ? C13 C18 1.400(3) . ? C14 C15 1.390(2) . ? C15 H15 0.9500 . ? C15 C16 1.399(3) . ? C16 H16 0.9500 . ? C16 C17 1.368(3) . ? C17 H17 0.9500 . ? C17 C18 1.413(2) . ? C18 C19 1.436(2) . ? C19 H19 0.9500 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C21 H21A 0.9900 . ? C21 H21B 0.9900 . ? C21 C22 1.515(3) . ? C22 H22A 0.9900 . ? C22 H22B 0.9900 . ? C22 C23 1.519(3) . ? C23 H23A 0.9900 . ? C23 H23B 0.9900 . ? C23 C24 1.521(3) . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? Cl1 C25 1.758(2) . ? Cl1 C25A 1.759(10) . ? Cl2 C25 1.756(2) . ? C25 H25A 0.9900 . ? C25 H25B 0.9900 . ? C25A H25C 0.9900 . ? C25A H25D 0.9900 . ? C25A Cl2A 1.755(10) . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag O1 H1 O2 0.866(9) 1.882(10) 2.7401(15) 170(2) 3_666 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O5 C1 C2 O6 -0.7(2) . . . . ? O5 C1 C2 C3 -179.94(16) . . . . ? O5 C1 C6 C5 -178.87(15) . . . . ? O5 C1 C6 C7 -1.9(2) . . . . ? O6 C2 C3 C4 179.18(17) . . . . ? O7 C13 C14 O8 -1.4(3) . . . . ? O7 C13 C14 C15 179.82(17) . . . . ? O7 C13 C18 C17 178.86(17) . . . . ? O7 C13 C18 C19 3.4(3) . . . . ? O8 C14 C15 C16 -176.87(19) . . . . ? N1 C9 C10 C11 174.44(16) . . . . ? N2 C21 C22 C23 177.97(16) . . . . ? C1 O5 B2 O2 -78.04(19) . . . . ? C1 O5 B2 O3 154.92(15) . . . . ? C1 O5 B2 N1 34.49(18) . . . . ? C1 C2 C3 C4 -1.7(3) . . . . ? C1 C6 C7 N1 7.7(2) . . . . ? C2 C1 C6 C5 -0.6(2) . . . . ? C2 C1 C6 C7 176.38(15) . . . . ? C2 C3 C4 C5 0.4(3) . . . . ? C3 C4 C5 C6 0.7(3) . . . . ? C4 C5 C6 C1 -0.7(3) . . . . ? C4 C5 C6 C7 -177.53(16) . . . . ? C5 C6 C7 N1 -175.33(15) . . . . ? C6 C1 C2 O6 -179.05(14) . . . . ? C6 C1 C2 C3 1.7(3) . . . . ? C7 N1 C9 C10 96.68(18) . . . . ? C7 N1 B2 O2 87.25(17) . . . . ? C7 N1 B2 O3 -148.75(14) . . . . ? C7 N1 B2 O5 -28.60(18) . . . . ? C8 O6 C2 C1 -168.36(16) . . . . ? C8 O6 C2 C3 10.8(3) . . . . ? C9 N1 C7 C6 -176.83(14) . . . . ? C9 N1 B2 O2 -86.62(15) . . . . ? C9 N1 B2 O3 37.38(18) . . . . ? C9 N1 B2 O5 157.53(12) . . . . ? C9 C10 C11 C12 -169.49(17) . . . . ? C13 O7 B3 O3 101.39(18) . . . . ? C13 O7 B3 O4 -131.06(16) . . . . ? C13 O7 B3 N2 -16.2(2) . . . . ? C13 C14 C15 C16 1.8(3) . . . . ? C13 C18 C19 N2 -5.4(3) . . . . ? C14 C13 C18 C17 1.5(3) . . . . ? C14 C13 C18 C19 -173.95(17) . . . . ? C14 C15 C16 C17 0.6(3) . . . . ? C15 C16 C17 C18 -1.8(3) . . . . ? C16 C17 C18 C13 0.8(3) . . . . ? C16 C17 C18 C19 176.12(18) . . . . ? C17 C18 C19 N2 179.08(18) . . . . ? C18 C13 C14 O8 176.01(16) . . . . ? C18 C13 C14 C15 -2.8(3) . . . . ? C19 N2 C21 C22 73.2(2) . . . . ? C19 N2 B3 O3 -106.49(17) . . . . ? C19 N2 B3 O4 128.21(16) . . . . ? C19 N2 B3 O7 13.8(2) . . . . ? C20 O8 C14 C13 -178.01(18) . . . . ? C20 O8 C14 C15 0.7(3) . . . . ? C21 N2 C19 C18 179.60(16) . . . . ? C21 N2 B3 O3 69.86(18) . . . . ? C21 N2 B3 O4 -55.45(19) . . . . ? C21 N2 B3 O7 -169.83(14) . . . . ? C21 C22 C23 C24 176.24(18) . . . . ? B1 O2 B2 O3 -4.8(2) . . . . ? B1 O2 B2 O5 -129.33(15) . . . . ? B1 O2 B2 N1 116.61(15) . . . . ? B1 O4 B3 O3 -1.7(2) . . . . ? B1 O4 B3 O7 -126.78(15) . . . . ? B1 O4 B3 N2 118.47(15) . . . . ? B2 O2 B1 O1 -176.55(14) . . . . ? B2 O2 B1 O4 5.4(2) . . . . ? B2 O3 B3 O4 2.0(2) . . . . ? B2 O3 B3 O7 124.46(15) . . . . ? B2 O3 B3 N2 -118.11(15) . . . . ? B2 O5 C1 C2 159.57(15) . . . . ? B2 O5 C1 C6 -22.1(2) . . . . ? B2 N1 C7 C6 9.3(2) . . . . ? B2 N1 C9 C10 -89.35(18) . . . . ? B3 O3 B2 O2 1.1(2) . . . . ? B3 O3 B2 O5 125.13(16) . . . . ? B3 O3 B2 N1 -116.82(16) . . . . ? B3 O4 B1 O1 179.87(13) . . . . ? B3 O4 B1 O2 -2.0(2) . . . . ? B3 O7 C13 C14 -173.63(17) . . . . ? B3 O7 C13 C18 9.0(3) . . . . ? B3 N2 C19 C18 -4.1(3) . . . . ? B3 N2 C21 C22 -103.23(17) . . . . ?