#------------------------------------------------------------------------------ #$Date: 2022-04-03 19:55:15 +0100 (Sun, 03 Apr 2022) $ #$Revision: 274229 $ #$URL: svn://www.crystallography.net/cod/cif/4/51/93/4519373.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519373 loop_ _publ_author_name 'Xu, Tingting' 'Li, Yunyun' 'Nikl, Martin' 'Kucerkova, Romana' 'Zhou, Zhengyang' 'Chen, Jie' 'Sun, Yi-Yang' 'Niu, Guangda' 'Tang, Jiang' 'Wang, Qian' 'Ren, Guohao' 'Wu, Yuntao' _publ_section_title ; Lead-Free Zero-Dimensional Organic-Copper(I) Halides as Stable and Sensitive X-ray Scintillators. ; _journal_issue 12 _journal_name_full 'ACS applied materials & interfaces' _journal_page_first 14157 _journal_page_last 14164 _journal_paper_doi 10.1021/acsami.1c23839 _journal_volume 14 _journal_year 2022 _chemical_formula_moiety 'Br2 Cu, C10 H22 N' _chemical_formula_sum 'C10 H22 Br2 Cu N' _chemical_formula_weight 379.64 _space_group_crystal_system orthorhombic _space_group_IT_number 61 _space_group_name_Hall '-P 2ac 2ab' _space_group_name_H-M_alt 'P b c a' _atom_sites_solution_hydrogens geom _audit_creation_date 2021-01-19 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6226) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 13.832 _cell_length_b 12.061 _cell_length_c 17.097 _cell_measurement_reflns_used 1637 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 18.1800 _cell_measurement_theta_min 2.5210 _cell_volume 2852.254 _computing_cell_refinement 'CrysAlisPro 1.171.41.25a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.41.25a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.41.25a (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 293(2) _diffrn_detector 'CCD plate' _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -98.19 10.81 0.50 15.00 -- -11.75 -59.25 164.08 218 2 \w -98.19 10.81 0.50 15.00 -- -11.75 -59.25 20.08 218 3 \w -98.19 10.81 0.50 15.00 -- -11.75 -59.25-123.92 218 4 \w -98.19 10.81 0.50 15.00 -- -11.75 -59.25 92.08 218 5 \w -98.19 10.81 0.50 15.00 -- -11.75 -59.25 -51.92 218 ; _diffrn_measurement_device 'abstract diffractometer' _diffrn_measurement_device_type 'Saxi-CrysAlisPro-abstract goniometer imported SAXI images' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0406327000 _diffrn_orient_matrix_UB_12 0.0253261000 _diffrn_orient_matrix_UB_13 0.0218939000 _diffrn_orient_matrix_UB_21 0.0424076000 _diffrn_orient_matrix_UB_22 0.0268195000 _diffrn_orient_matrix_UB_23 0.0188276000 _diffrn_orient_matrix_UB_31 -0.0030536000 _diffrn_orient_matrix_UB_32 0.0356245000 _diffrn_orient_matrix_UB_33 -0.0297881000 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1134 _diffrn_reflns_av_unetI/netI 0.0501 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 45466 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.371 _diffrn_reflns_theta_min 2.382 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 7.105 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.47245 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.41.25a (Rigaku Oxford Diffraction, 2019) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_density_diffrn 1.768 _exptl_crystal_F_000 1504 _refine_diff_density_max 0.340 _refine_diff_density_min -0.611 _refine_diff_density_rms 0.078 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.025 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 129 _refine_ls_number_reflns 2909 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.025 _refine_ls_R_factor_all 0.0976 _refine_ls_R_factor_gt 0.0383 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0194P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0592 _refine_ls_wR_factor_ref 0.0708 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1658 _reflns_number_total 2909 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file am1c23839_si_002.cif _cod_data_source_block (Bmpip)2Cu2Br4 _cod_original_cell_volume 2852.1 _cod_database_code 4519373 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _reflns_odcompleteness_completeness 88.59 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 33.58 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Secondary CH2 refined with riding coordinates: C005(H00A,H00B), C006(H00C,H00D), C007(H00E,H00F), C008(H00G,H00H), C009(H00I, H00J), C00A(H00K,H00L), C00B(H00M,H00N), C00C(H00O,H00P) 2.b Idealised Me refined as rotating group: C00D(H00Q,H00R,H00S), C00E(H00T,H00U,H00V) ; _shelx_res_file ; TITL test_a.res in Pbca 0516-2.res created by SHELXL-2018/3 at 20:50:17 on 19-Jan-2021 REM Old TITL test REM SHELXT solution in Pbca: R1 0.151, Rweak 0.024, Alpha 0.040 REM 0.407 for 385 systematic absences, Orientation a'=b, b'=a, c'=-c REM Formula found by SHELXT: Cu Br2 C10 N CELL 0.71073 13.8315 12.0607 17.097 90 90 90 ZERR 8 0 0 0 0 0 0 LATT 1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H Br Cu N UNIT 80 176 16 8 8 L.S. 100 PLAN 8 CONF list 4 MORE -1 BOND $H fmap 2 53 acta SHEL 0.8 999 REM REM REM WGHT 0.019400 FVAR 0.19077 BR01 3 0.527679 0.484658 0.287965 11.00000 0.04626 0.06500 = 0.05705 0.00244 0.00369 0.00087 BR02 3 0.644966 0.484021 0.514093 11.00000 0.06091 0.07486 = 0.06548 0.00003 -0.00698 0.01195 CU03 4 0.512067 0.494797 0.422421 11.00000 0.09615 0.05544 = 0.05948 0.00212 -0.00446 0.00075 N004 5 0.267071 0.751718 0.295755 11.00000 0.04206 0.03955 = 0.05795 0.00593 -0.00214 -0.00313 C005 1 0.198245 0.668905 0.331874 11.00000 0.05361 0.04151 = 0.05653 0.01051 -0.00529 -0.00241 AFIX 23 H00A 2 0.163115 0.632307 0.290104 11.00000 -1.20000 H00B 2 0.235979 0.612769 0.358685 11.00000 -1.20000 AFIX 0 C006 1 0.332970 0.692121 0.239730 11.00000 0.04135 0.05589 = 0.09320 0.01016 0.00984 0.00735 AFIX 23 H00C 2 0.362580 0.629905 0.266540 11.00000 -1.20000 H00D 2 0.384251 0.742129 0.223816 11.00000 -1.20000 AFIX 0 C007 1 0.216078 0.843581 0.252502 11.00000 0.04983 0.03432 = 0.06249 0.00704 -0.00172 0.00396 AFIX 23 H00E 2 0.170865 0.879648 0.287625 11.00000 -1.20000 H00F 2 0.263253 0.898385 0.236141 11.00000 -1.20000 AFIX 0 C008 1 0.281365 0.649901 0.167412 11.00000 0.07441 0.05405 = 0.07625 -0.01039 0.03137 0.00192 AFIX 23 H00G 2 0.328057 0.616444 0.132270 11.00000 -1.20000 H00H 2 0.235181 0.593224 0.182392 11.00000 -1.20000 AFIX 0 C009 1 0.126072 0.716073 0.388747 11.00000 0.07203 0.05220 = 0.06257 0.00143 0.00639 -0.00816 AFIX 23 H00I 2 0.160055 0.758415 0.428382 11.00000 -1.20000 H00J 2 0.083094 0.766248 0.361230 11.00000 -1.20000 AFIX 0 C00A 1 0.162454 0.802203 0.182028 11.00000 0.07047 0.05396 = 0.06571 0.01734 -0.01422 0.00061 AFIX 23 H00K 2 0.132246 0.864357 0.155584 11.00000 -1.20000 H00L 2 0.111722 0.751925 0.198655 11.00000 -1.20000 AFIX 0 C00B 1 0.067385 0.627252 0.427611 11.00000 0.07509 0.06332 = 0.07608 0.00447 0.01626 -0.00945 AFIX 23 H00M 2 0.110845 0.576696 0.454272 11.00000 -1.20000 H00N 2 0.033455 0.585402 0.387688 11.00000 -1.20000 AFIX 0 C00C 1 0.229094 0.742605 0.125392 11.00000 0.09812 0.07303 = 0.05403 0.00626 0.01254 -0.00796 AFIX 23 H00O 2 0.191695 0.712425 0.082378 11.00000 -1.20000 H00P 2 0.275734 0.794532 0.104100 11.00000 -1.20000 AFIX 0 C00D 1 0.328071 0.802193 0.359096 11.00000 0.06529 0.07682 = 0.08060 0.01520 -0.02533 -0.02538 AFIX 137 H00Q 2 0.288416 0.848237 0.391786 11.00000 -1.50000 H00R 2 0.378284 0.846253 0.335930 11.00000 -1.50000 H00S 2 0.356507 0.744355 0.390063 11.00000 -1.50000 AFIX 0 C00E 1 -0.005532 0.670793 0.485913 11.00000 0.08353 0.08848 = 0.07932 -0.00170 0.02221 -0.01227 AFIX 137 H00T 2 -0.049436 0.720279 0.459977 11.00000 -1.50000 H00U 2 0.027550 0.709853 0.526869 11.00000 -1.50000 H00V 2 -0.041001 0.609891 0.507906 11.00000 -1.50000 AFIX 0 HKLF 4 REM test_a.res in Pbca REM wR2 = 0.0708, GooF = S = 1.025, Restrained GooF = 1.025 for all data REM R1 = 0.0383 for 1658 Fo > 4sig(Fo) and 0.0976 for all 2909 data REM 129 parameters refined using 0 restraints END WGHT 0.0193 0.0000 REM Highest difference peak 0.340, deepest hole -0.611, 1-sigma level 0.078 Q1 1 0.0249 0.4784 0.3488 11.00000 0.05 0.34 Q2 1 0.3560 0.5402 0.0821 11.00000 0.05 0.33 Q3 1 0.5768 0.4825 0.4000 11.00000 0.05 0.32 Q4 1 0.1741 0.5585 0.2429 11.00000 0.05 0.25 Q5 1 0.1427 0.4708 0.4428 11.00000 0.05 0.25 Q6 1 0.0928 0.6467 0.5549 11.00000 0.05 0.25 Q7 1 0.0986 0.6974 0.1234 11.00000 0.05 0.24 Q8 1 0.0779 0.5276 0.5588 11.00000 0.05 0.24 ; _shelx_res_checksum 2590 _shelx_hkl_file ; 0 0 -2 2.15 1.42 0 0 2 1.60 1.00 0 0 -2 2.57 1.31 0 0 -3 -1.21 1.23 0 0 3 -0.72 0.90 0 0 -3 2.07 1.98 0 0 3 2.51 2.12 0 0 -3 -0.85 1.11 0 0 4 2058.88 43.43 0 0 -4 2103.20 44.47 0 0 4 2042.02 45.50 0 0 -4 2089.94 46.53 0 0 -4 2122.58 51.01 0 0 5 0.79 1.10 0 0 5 -1.48 2.36 0 0 -5 4.54 2.55 0 0 -5 1.57 1.50 0 0 -5 0.92 1.19 0 0 6 0.93 1.42 0 0 6 1.26 2.57 0 0 -6 1.06 2.49 0 0 -6 2.07 2.28 0 0 -6 1.23 1.44 0 0 -7 -1.59 2.26 0 0 -7 -0.83 2.33 0 0 7 -0.70 1.69 0 0 7 -1.82 2.36 0 0 -7 1.08 2.95 0 0 -7 0.36 1.45 0 0 -8 -1.62 4.21 0 0 -8 4.06 4.67 0 0 8 4.82 2.55 0 0 8 5.43 4.83 0 0 -8 -0.38 2.70 0 0 -9 0.65 4.21 0 0 -9 3.10 5.78 0 0 -9 -4.57 3.52 0 0 9 1.94 2.14 0 0 -10 1290.57 65.96 0 0 10 1309.89 31.06 0 0 -10 1280.92 60.57 0 0 10 1367.41 60.54 0 0 -10 1357.62 58.25 0 0 -11 9.57 9.76 0 0 -11 1.80 6.20 0 0 11 6.42 2.53 0 0 11 12.28 6.64 0 0 -11 2.80 6.61 0 0 -12 52.66 15.68 0 0 -12 58.01 13.83 0 0 12 44.82 5.61 0 0 12 68.80 16.04 0 0 -12 53.27 13.93 0 0 -13 -7.50 8.26 0 0 13 5.11 7.45 0 0 -13 -1.56 8.39 0 0 -13 3.62 9.10 0 0 -14 743.12 51.64 0 0 -14 706.80 60.70 0 0 -14 682.14 54.27 0 0 14 715.09 54.41 0 0 -15 2.73 9.35 0 0 15 6.54 13.18 0 0 -15 4.98 7.22 0 0 -16 4.69 10.55 0 0 16 21.22 16.91 0 0 -16 21.51 11.26 0 0 -16 13.10 10.77 0 0 -17 -0.96 9.06 0 0 17 -5.86 11.18 0 0 -17 -23.66 15.45 0 0 -17 11.32 12.35 0 0 -18 5.79 13.50 0 0 -18 5.07 16.58 0 0 -19 26.61 17.05 0 0 -19 3.31 11.07 0 0 -19 -28.73 22.28 0 0 -20 29.44 20.93 0 0 -20 20.33 17.28 0 0 -21 21.08 20.11 0 0 -21 15.71 19.96 0 0 -22 5.58 19.34 0 0 -22 -9.25 17.94 0 0 -23 49.83 31.50 0 0 -23 -34.55 27.88 0 0 -24 26.83 21.39 0 0 -24 -41.92 30.40 0 0 -25 -50.01 32.11 0 0 -26 -70.24 46.10 -1 0 -26 -1.10 31.17 -1 0 -25 14.69 32.78 -1 0 -24 -12.48 25.17 -1 0 -24 10.34 25.52 -1 0 -23 39.03 29.96 -1 0 -23 -22.76 19.99 -1 0 -22 13.19 18.32 -1 0 -22 -43.61 27.20 -1 0 -21 30.70 18.01 -1 0 -21 -3.01 18.60 -1 0 -20 18.30 17.49 -1 0 -19 -8.34 11.76 -1 0 -19 12.37 16.00 -1 0 -19 -4.57 13.78 -1 0 -18 15.24 15.23 -1 0 -18 21.71 15.50 -1 0 -17 -2.67 9.22 1 0 17 -46.75 22.67 -1 0 -17 -8.77 9.58 -1 0 -17 -7.90 10.32 -1 0 -16 43.95 19.26 1 0 16 35.94 17.86 -1 0 -16 43.31 16.24 -1 0 -16 57.85 17.28 -1 0 -15 -8.75 11.12 1 0 15 6.50 7.44 -1 0 -15 -12.48 15.89 -1 0 -14 89.22 20.17 1 0 14 74.53 17.53 -1 0 -14 82.61 20.31 -1 0 -14 88.84 16.13 -1 0 -13 -0.10 6.35 1 0 13 3.78 9.87 -1 0 -13 -5.84 7.78 -1 0 -13 1.11 6.98 -1 0 -12 149.52 22.80 1 0 12 162.58 24.87 -1 0 -12 172.95 23.03 -1 0 -12 140.54 24.50 -1 0 -11 5.55 7.41 1 0 11 -3.85 6.96 -1 0 -11 4.73 6.93 -1 0 -11 -1.64 5.73 -1 0 -11 -0.45 2.06 -1 0 -10 192.38 12.38 1 0 10 199.21 23.20 -1 0 -10 180.90 22.39 -1 0 -10 193.02 21.61 -1 0 -10 185.03 24.76 -1 0 -9 -3.42 3.66 1 0 9 -2.73 4.43 -1 0 -9 2.12 4.19 -1 0 -9 2.89 4.94 -1 0 -9 -1.02 2.05 -1 0 -8 305.81 27.85 1 0 8 322.38 25.35 -1 0 -8 295.86 24.93 -1 0 -8 308.76 24.54 1 0 8 292.78 15.62 -1 0 -8 310.16 15.76 -1 0 -7 1.53 2.04 1 0 7 0.43 1.69 -1 0 -7 -5.06 3.80 -1 0 -7 -1.63 2.55 1 0 7 -3.88 5.01 -1 0 -7 0.34 3.93 -1 0 -6 95.96 8.04 1 0 6 90.21 8.13 -1 0 -6 94.35 14.02 -1 0 -6 93.89 11.73 1 0 6 100.76 12.32 -1 0 -5 0.30 1.31 1 0 5 2.08 1.64 1 0 5 0.34 1.73 -1 0 -5 0.60 2.07 1 0 4 308.74 13.95 -1 0 -4 313.83 13.44 -1 0 -4 318.35 19.67 -1 0 -4 305.37 17.46 1 0 4 316.54 17.45 -1 0 -3 -0.69 0.96 -1 0 -3 -0.04 1.37 -1 0 -3 0.35 1.02 1 0 3 -0.78 0.96 -1 0 -2 54.70 5.26 1 0 2 55.99 5.24 -1 0 -2 12.62 2.90 -1 0 1 0.97 1.17 1 0 -1 -0.26 0.73 -1 0 1 0.17 0.77 1 0 -1 -0.52 0.90 1 0 -1 0.66 0.67 -1 0 1 -0.28 0.77 1 0 -2 7.04 2.92 -1 0 2 53.08 6.44 1 0 -2 54.08 6.20 -1 0 2 56.63 6.27 1 0 -2 53.84 5.78 -1 0 3 -0.60 1.17 1 0 -3 0.05 1.61 1 0 -3 -0.32 1.63 1 0 -3 -1.19 1.81 -1 0 3 4.90 2.58 1 0 -4 312.75 19.37 -1 0 4 313.90 14.67 -1 0 4 308.24 19.21 1 0 -4 307.27 19.10 -1 0 4 302.50 18.79 1 0 -4 312.68 19.44 1 0 -5 1.09 3.34 -1 0 5 0.60 1.63 -1 0 5 -0.12 2.24 -1 0 5 0.03 1.40 -1 0 6 98.71 9.22 1 0 -6 87.38 12.49 1 0 -6 93.09 12.55 -1 0 6 99.14 13.10 -1 0 6 94.70 12.59 1 0 -6 88.49 13.47 -1 0 7 -1.05 2.62 1 0 -7 0.38 3.79 -1 0 7 2.77 4.26 -1 0 7 2.74 3.38 1 0 -7 0.15 3.54 1 0 -7 -0.70 3.45 1 0 -8 300.99 28.04 -1 0 8 309.51 17.32 1 0 -8 286.46 25.83 -1 0 8 303.21 26.60 -1 0 8 302.96 25.12 1 0 -8 288.95 25.34 -1 0 9 1.72 4.13 1 0 -9 0.78 3.38 1 0 -9 -8.46 5.37 -1 0 9 1.85 2.72 -1 0 9 -3.29 4.45 1 0 -9 -1.68 5.51 1 0 -10 188.79 25.28 1 0 -10 206.91 23.63 -1 0 10 176.39 13.06 -1 0 10 194.97 24.01 1 0 -10 187.36 23.61 1 0 -11 -10.19 8.14 1 0 -11 0.76 7.31 -1 0 11 3.29 3.55 -1 0 11 -1.99 4.63 1 0 -11 -3.41 4.03 1 0 -12 157.45 25.60 1 0 -12 140.84 20.31 -1 0 12 154.56 11.92 -1 0 12 160.34 24.44 1 0 -12 147.24 23.50 1 0 -13 -8.26 10.01 1 0 -13 7.76 9.58 -1 0 13 -0.77 8.65 1 0 -13 1.61 6.53 -1 0 13 0.06 2.68 1 0 -14 75.27 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2 13 45.16 14.12 0 -2 -12 32.14 10.12 0 -2 -12 58.28 16.07 0 -2 -12 17.24 10.22 0 2 12 39.77 10.18 0 -2 -11 -0.98 6.12 0 -2 -11 -5.14 8.20 0 -2 -11 -4.21 4.88 0 2 11 3.44 5.99 0 -2 -10 1046.23 61.04 0 2 10 1058.73 60.25 0 -2 -10 1067.34 53.02 0 -2 -9 23.93 7.21 0 -2 -9 22.20 9.83 0 2 9 24.29 9.35 0 -2 -9 22.49 8.66 0 2 9 34.25 8.62 0 -2 -8 121.58 15.88 0 -2 -8 129.40 20.01 0 -2 -8 143.08 19.91 0 2 8 144.83 20.21 0 2 8 131.33 16.35 0 -2 -7 87.19 12.51 0 -2 -7 94.26 15.95 0 -2 -7 96.77 15.56 0 2 7 87.64 14.52 0 2 7 86.30 12.06 0 -2 -6 90.50 14.99 0 2 6 82.79 13.43 0 -2 -6 83.33 13.64 0 2 6 93.49 11.74 0 -2 -6 80.92 11.07 0 -2 -5 0.98 0.94 0 -2 -5 0.64 1.91 0 2 5 1.54 2.85 0 -2 -5 3.05 3.63 0 -2 -5 14.03 4.98 0 2 5 1.96 2.41 0 2 5 1.67 1.37 0 2 4 3182.79 69.71 0 -2 -4 3013.06 54.56 0 2 4 3049.44 54.57 0 -2 -4 3035.26 77.96 0 2 4 3038.42 43.97 0 -2 -4 3036.38 43.47 0 -2 -3 368.00 22.36 0 2 3 393.85 22.63 0 -2 -3 367.52 17.20 0 2 3 374.08 16.94 0 -2 -3 385.13 25.38 0 -2 -3 370.46 16.44 0 2 3 379.41 16.82 0 2 2 1890.24 46.52 0 -2 -2 1948.37 46.87 0 2 2 1897.27 40.46 0 -2 -2 1917.29 39.71 0 2 2 1959.52 35.92 0 -2 -2 1959.49 52.85 0 2 1 0.87 1.29 0 -2 -1 0.20 1.77 0 2 1 -0.53 2.07 0 -2 -1 -0.39 1.12 0 -2 -1 1.96 2.47 0 -2 -1 2.23 1.48 0 2 1 3.92 2.62 0 -2 0 4691.76 69.73 0 2 0 4648.13 70.19 0 -2 0 4864.76 69.44 0 2 0 4504.48 67.29 0 -2 0 4714.11 67.19 0 2 0 4683.32 66.64 0 -2 1 -0.85 1.99 0 2 -1 1.56 1.85 0 2 -1 1.33 1.45 0 -2 1 0.32 1.23 0 2 -1 0.89 1.34 0 2 -1 1.51 1.42 0 -2 2 2002.23 49.82 0 2 -2 1900.54 49.75 0 2 -2 1952.45 46.00 0 -2 2 1855.44 44.91 0 2 -2 1977.21 44.60 0 -2 2 1932.11 43.98 0 -2 3 376.06 22.71 0 2 -3 377.72 23.15 0 2 -3 378.28 22.80 0 -2 3 379.81 22.75 0 2 -3 385.26 21.99 0 -2 3 376.49 21.42 0 2 -4 3023.94 68.15 0 -2 4 3066.83 66.89 0 2 -4 3060.05 71.74 0 -2 4 2957.16 69.32 0 -2 4 3156.88 67.32 0 -2 5 -0.08 2.92 0 2 -5 2.90 3.08 0 2 -5 3.61 3.04 0 -2 5 -1.78 3.94 0 2 -5 -1.07 3.85 0 -2 6 96.39 13.04 0 2 -6 78.72 14.40 0 -2 6 90.48 13.63 0 2 -6 89.08 13.80 0 2 -6 86.29 12.34 0 2 -7 91.58 7.63 0 -2 7 82.83 12.44 0 2 -7 94.75 16.54 0 2 -7 87.53 14.39 0 -2 7 87.33 14.15 0 2 -7 83.75 12.33 0 2 -8 136.67 10.92 0 -2 8 138.96 16.34 0 2 -8 144.90 22.27 0 2 -8 124.99 18.20 0 2 -9 29.71 6.13 0 2 -9 28.86 12.35 0 2 -9 27.25 8.64 0 -2 9 34.62 10.58 0 -2 9 30.16 8.74 0 2 -10 1103.34 68.53 0 2 -10 1034.55 48.22 0 -2 10 1040.07 46.62 0 -2 10 1003.31 55.55 0 2 -10 1025.48 57.82 0 2 -10 1104.68 37.93 0 2 -11 -3.38 4.06 0 -2 11 2.98 6.31 0 2 -11 -1.87 8.21 0 2 -11 2.11 6.47 0 -2 11 -6.25 5.76 0 2 -11 -2.45 4.73 0 2 -12 19.55 6.82 0 -2 12 40.46 10.98 0 2 -12 31.82 7.16 0 2 -12 30.19 14.87 0 2 -12 34.55 12.69 0 -2 12 35.68 11.73 0 2 -12 47.46 15.80 0 2 -13 48.26 11.11 0 2 -13 47.84 9.95 0 -2 13 50.30 16.65 0 2 -13 53.15 16.11 0 2 -13 57.57 18.51 0 2 -13 67.68 17.47 0 -2 13 59.99 12.44 0 2 -14 796.51 65.72 0 -2 14 820.28 43.15 0 2 -14 782.98 43.94 0 2 -14 886.48 79.63 0 -2 14 753.43 57.92 0 2 -14 797.95 62.47 0 2 -14 823.05 41.96 0 2 -15 6.30 8.72 0 2 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-21.10 24.87 1 2 -21 12.67 20.09 1 2 -22 6.16 19.77 1 2 -22 -2.62 18.23 1 2 -23 23.73 25.14 1 2 -23 -27.16 25.51 1 2 -24 51.35 39.69 1 2 -24 63.25 34.75 1 2 -25 -19.72 32.15 -2 -2 -25 -54.87 37.67 -2 -2 -24 -1.98 23.20 -2 -2 -24 66.58 37.44 -2 -2 -23 -7.64 19.38 -2 -2 -23 -12.59 30.10 -2 -2 -22 -1.74 17.76 -2 -2 -22 -0.13 19.93 -2 -2 -21 29.00 25.39 -2 -2 -20 4.50 16.27 -2 -2 -20 21.70 17.15 -2 -2 -19 39.62 21.48 -2 -2 -19 -22.63 13.96 -2 -2 -19 16.84 20.13 -2 -2 -18 -5.78 21.72 2 2 18 0.32 16.50 -2 -2 -18 24.72 17.77 -2 -2 -18 16.79 14.49 2 2 17 2.77 13.90 -2 -2 -17 6.86 11.26 -2 -2 -17 -7.22 17.88 -2 -2 -17 9.14 10.93 2 2 16 47.18 15.88 -2 -2 -16 44.31 19.44 -2 -2 -16 19.26 13.04 -2 -2 -16 34.36 13.90 2 2 15 13.08 8.88 -2 -2 -15 6.10 11.15 -2 -2 -15 -1.97 10.09 -2 -2 -15 2.03 6.72 2 2 14 396.81 36.88 -2 -2 -14 430.91 46.88 -2 -2 -14 419.92 46.49 -2 -2 -14 362.47 36.68 2 2 13 10.51 8.71 -2 -2 -13 -1.08 6.90 -2 -2 -13 -3.48 13.11 -2 -2 -13 -3.87 7.62 2 2 12 53.60 12.80 -2 -2 -12 48.36 14.42 -2 -2 -12 46.50 16.30 -2 -2 -12 55.42 12.85 -2 -2 -11 14.48 7.73 -2 -2 -11 0.57 6.29 -2 -2 -11 -2.63 6.53 2 2 10 242.99 22.78 2 2 10 262.74 31.26 -2 -2 -10 213.54 27.52 -2 -2 -10 215.24 22.03 2 2 9 21.28 7.46 -2 -2 -9 40.96 12.76 2 2 9 34.66 11.28 -2 -2 -9 20.67 7.76 -2 -2 -9 23.69 7.52 -2 -2 -8 984.30 23.97 -2 -2 -8 976.44 25.41 2 2 8 979.27 38.98 2 2 8 1005.14 51.04 -2 -2 -8 990.60 52.43 -2 -2 -7 41.80 7.72 2 2 7 48.02 7.95 -2 -2 -7 45.11 10.63 2 2 7 46.64 10.93 -2 -2 -7 44.79 5.78 -2 -2 -6 1592.67 37.51 2 2 6 1621.54 40.58 -2 -2 -6 1625.97 41.42 -2 -2 -6 1611.50 57.90 2 2 6 1600.00 55.76 -2 -2 -5 64.55 7.83 -2 -2 -5 69.73 7.39 2 2 5 66.38 7.04 -2 -2 -5 58.81 10.49 2 2 5 68.22 10.61 -2 -2 -4 68.53 8.77 -2 -2 -4 75.97 14.36 -2 -2 -4 63.61 5.70 -2 -2 -4 69.41 10.69 2 2 4 66.78 5.67 2 2 4 71.02 10.11 2 2 3 35.29 6.63 -2 -2 -3 35.67 9.53 -2 -2 -3 29.64 5.98 -2 -2 -3 33.19 6.89 2 2 2 2011.05 61.24 -2 -2 -2 2061.40 62.53 -2 -2 -2 2050.93 50.39 2 2 2 2062.45 45.97 -2 -2 -2 2076.38 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26.20 3 16 -6 -21.60 18.54 -3 -16 6 18.99 28.41 3 16 -6 -13.94 42.60 3 16 -7 43.35 27.56 -3 -16 7 20.33 30.45 3 16 -7 10.20 32.16 3 16 -8 11.89 27.94 -3 -16 8 30.56 33.06 3 16 -9 11.61 23.05 -3 -16 9 -11.15 30.10 -3 -16 10 10.74 31.79 3 16 -10 -40.80 27.28 -3 -16 11 18.79 32.74 3 16 -11 -27.85 29.27 -4 -16 -9 16.98 36.50 -4 -16 -9 -3.68 33.33 -4 -16 -8 3.18 34.64 -4 -16 -8 55.87 40.36 -4 -16 -7 -0.18 37.68 -4 -16 -7 39.53 32.72 -4 -16 -6 -24.82 34.27 4 16 6 -24.86 25.31 -4 -16 -6 -31.35 41.08 -4 -16 -5 -15.06 28.26 4 16 5 -0.15 30.15 -4 -16 -4 15.34 38.45 4 16 4 41.07 35.13 -4 -16 -3 0.33 37.10 4 16 3 -94.35 39.08 -4 -16 -2 -12.91 26.45 4 16 2 -22.77 41.94 -4 -16 -1 -3.45 31.40 4 16 1 42.05 38.36 -4 -16 0 -17.00 25.50 4 16 0 23.22 31.24 -4 -16 1 -0.92 34.53 4 16 -1 -9.25 30.89 4 16 -2 -9.18 18.00 -4 -16 2 -31.37 32.86 -4 -16 3 50.40 43.26 4 16 -3 -35.26 26.26 4 16 -4 12.20 16.68 -4 -16 4 -36.29 40.91 4 16 -4 47.37 38.39 4 16 -5 -2.35 18.07 -4 -16 5 -23.69 34.97 4 16 -5 14.80 39.17 4 16 -6 -16.02 25.09 4 16 -6 31.74 32.39 4 16 -7 -47.43 27.76 -4 -16 7 20.72 47.35 4 16 -7 41.02 47.07 -4 -16 8 -36.58 29.99 4 16 -8 -17.99 24.50 -4 -16 9 -70.61 47.42 4 16 -9 19.84 29.14 -4 -16 10 -34.34 37.41 4 16 -10 -37.70 25.38 -4 -16 11 62.99 48.32 4 16 -11 40.15 30.01 -4 -16 12 75.69 45.32 -5 -16 -9 21.08 34.54 -5 -16 -8 -41.40 40.26 -5 -16 -8 81.79 42.08 -5 -16 -7 51.55 48.65 -5 -16 -7 -8.75 24.70 -5 -16 -6 8.84 40.66 -5 -16 -6 -37.08 30.47 -5 -16 -5 -25.64 28.32 -5 -16 -4 -40.38 32.57 -5 -16 -3 36.25 37.69 5 16 3 41.82 42.02 -5 -16 -2 66.06 42.48 5 16 2 30.80 27.11 -5 -16 -1 15.35 31.46 5 16 1 76.77 41.99 -5 -16 0 -45.54 34.17 5 16 0 22.27 38.04 -5 -16 1 24.43 28.83 5 16 -1 60.21 32.11 -5 -16 2 -10.07 29.93 5 16 -2 14.74 28.73 -5 -16 3 28.09 32.29 5 16 -3 -34.81 43.42 5 16 -4 8.03 19.29 -5 -16 4 -5.96 35.58 5 16 -4 9.99 26.81 5 16 -5 28.66 18.57 5 16 -5 13.40 43.34 -5 -16 6 3.26 27.93 5 16 -6 -17.12 30.05 5 16 -6 16.39 18.81 -5 -16 6 30.09 42.06 5 16 -7 -30.67 27.00 -5 -16 7 83.63 46.69 5 16 -8 7.76 22.46 -5 -16 8 45.94 38.59 -5 -16 9 2.50 44.21 5 16 -9 -17.57 26.94 5 16 -10 13.31 28.20 -5 -16 10 61.47 37.61 5 16 -11 -18.69 26.84 -5 -16 11 -72.01 49.05 -6 -16 -8 11.50 33.98 -6 -16 -7 -24.67 34.42 -6 -16 -7 1.59 36.33 -6 -16 -6 -46.97 53.00 -6 -16 -5 14.45 33.60 -6 -16 -4 -33.50 43.21 -6 -16 -3 -93.07 53.28 -6 -16 -2 16.55 31.71 -6 -16 -1 44.64 33.97 -6 -16 0 -6.21 28.96 -6 -16 1 -29.03 34.71 -6 -16 2 50.10 39.34 -6 -16 3 25.97 46.49 6 16 -3 54.89 43.58 -6 -16 4 -11.28 34.53 6 16 -4 -11.39 37.51 -6 -16 5 52.37 40.67 6 16 -5 -21.46 33.20 -6 -16 5 85.37 56.91 -6 -16 6 8.16 36.43 6 16 -7 26.20 24.50 -6 -16 7 -140.26 52.32 6 16 -8 36.54 31.67 -6 -16 8 -37.30 50.87 6 16 -9 72.67 31.05 -6 -16 9 68.57 45.56 6 16 -10 6.37 24.76 -6 -16 10 56.10 49.97 6 16 -11 73.82 44.95 -7 -16 -8 98.97 43.99 -7 -16 -5 46.32 43.19 -7 -16 -4 82.26 44.30 -7 -16 -3 -5.63 34.00 -7 -16 -2 19.76 34.86 -7 -16 -1 65.10 44.89 -7 -16 0 64.67 47.11 -7 -16 1 -74.28 49.57 -7 -16 2 60.58 43.03 -7 -16 3 20.90 33.17 -7 -16 4 71.84 52.92 -7 -16 4 -79.72 50.64 -7 -16 5 -35.10 45.89 -7 -16 5 -12.57 31.81 -7 -16 6 -20.21 41.59 -7 -16 7 -59.21 51.88 -7 -16 8 -32.84 40.23 -8 -16 -3 0.20 34.94 -8 -16 -2 -19.74 47.88 -8 -16 -1 18.55 37.72 -8 -16 0 -4.39 40.38 -8 -16 1 34.05 44.11 -8 -16 2 66.29 35.38 -8 -16 3 57.34 49.49 -8 -16 3 88.68 51.20 -8 -16 4 17.25 36.74 -8 -16 4 -120.69 55.84 -8 -16 5 10.38 43.16 -8 -16 5 -64.23 58.79 -9 -16 1 -2.92 39.29 -9 -16 2 44.69 51.37 -9 -16 3 -104.42 61.22 -9 -16 4 -19.96 40.79 -9 -16 5 -94.84 54.16 -10 -16 2 68.42 64.79 -10 -16 3 -138.16 64.11 -10 -16 4 109.42 59.79 -10 -16 5 95.44 56.83 -7 17 1 -11.36 34.75 -7 17 0 84.63 39.74 -6 17 7 -54.44 42.53 -6 17 2 67.05 40.37 -6 17 1 -55.15 34.52 -6 17 0 -51.31 31.99 -6 17 -1 -6.54 28.24 -6 17 -2 -3.04 27.85 -6 17 -3 14.59 29.67 -5 17 8 -19.70 39.26 -5 17 7 -36.15 36.04 -5 17 6 114.69 62.56 -5 17 5 1.85 41.53 -5 17 4 -12.71 32.69 -5 17 3 28.35 31.45 -5 17 3 -62.46 47.65 -5 17 2 5.78 30.71 -5 17 2 -6.95 38.04 -5 17 1 -36.02 31.63 -5 17 1 -44.53 34.89 -5 17 0 -5.56 27.55 -5 17 0 10.00 37.02 -5 17 -1 -31.56 35.81 -5 17 -2 -83.05 44.77 -5 17 -3 3.86 24.37 -5 17 -4 -40.82 34.50 -5 17 -5 -20.26 32.43 -4 17 9 -15.80 39.72 -4 17 8 13.88 43.27 -4 17 7 13.31 34.78 -4 17 6 -17.28 33.77 -4 17 5 76.71 46.59 -4 17 5 46.69 45.04 -4 17 4 43.68 30.11 -4 17 4 -80.30 54.31 -4 17 3 -27.38 33.78 -4 17 3 -70.44 40.54 -4 17 2 0.11 25.05 -4 17 2 78.16 47.83 -4 17 1 -44.91 28.84 -4 17 1 8.71 34.85 -4 17 0 23.64 23.24 -4 17 0 84.54 43.95 -4 17 -1 -26.28 29.02 -4 17 -1 46.11 38.63 -4 17 -2 -28.97 29.17 -4 17 -2 11.46 42.50 -4 17 -3 -62.11 36.75 -4 17 -4 -25.77 33.90 -4 17 -5 9.10 23.59 -4 17 -6 35.83 31.17 -3 17 9 -36.53 38.82 -3 17 8 -99.18 47.01 -3 17 7 43.97 38.10 -3 17 6 -17.58 36.29 -3 17 5 -25.27 23.48 -3 17 5 24.73 39.41 -3 17 4 36.84 32.14 -3 17 4 98.12 48.03 -3 17 3 27.54 32.26 -3 17 3 9.63 37.47 -3 17 2 11.34 22.18 -3 17 2 27.49 51.00 -3 17 1 -18.74 26.25 -3 17 1 96.33 45.88 -3 17 0 20.84 24.99 -3 17 0 -19.04 36.94 -3 17 -1 -26.15 26.17 -3 17 -1 -56.71 39.39 -3 17 -2 -3.28 24.23 -3 17 -2 -37.83 34.65 -3 17 -3 -22.20 23.69 -3 17 -3 -39.10 36.74 -3 17 -4 17.04 23.04 -3 17 -5 55.47 36.33 -3 17 -6 46.35 41.76 -3 17 -7 0.69 28.51 2 -17 -10 -14.84 40.01 -2 17 9 12.23 37.59 2 -17 -9 41.75 40.60 -2 17 8 -113.73 48.60 2 -17 -8 2.41 32.02 -2 17 7 17.96 34.07 2 -17 -7 51.78 39.53 -2 17 6 42.76 32.29 2 -17 -6 68.23 36.63 -2 17 5 -32.06 41.70 -2 17 4 16.50 19.63 -2 17 4 -17.83 33.25 -2 17 3 -15.89 27.20 -2 17 3 -4.36 32.81 -2 17 2 28.00 29.81 -2 17 2 71.34 30.61 -2 17 1 -19.19 26.26 -2 17 1 12.46 33.84 -2 17 0 -23.64 23.17 -2 17 0 41.02 31.77 -2 17 -1 51.66 27.74 -2 17 -1 12.18 28.13 -2 17 -2 3.00 25.04 -2 17 -2 25.88 28.33 -2 17 -3 27.13 28.70 -2 17 -3 18.00 30.53 -2 17 -4 -36.92 25.46 -2 17 -4 -16.25 30.56 -2 17 -5 23.94 27.55 -2 17 -6 -9.72 27.08 -2 17 -7 -23.20 37.86 -2 17 -8 52.57 34.52 1 -17 -10 -9.98 50.01 -1 17 9 20.03 40.38 1 -17 -9 -101.36 51.94 -1 17 8 7.66 41.07 1 -17 -8 -101.43 42.88 -1 17 7 22.22 42.56 1 -17 -7 3.80 36.47 -1 17 6 -22.18 31.80 1 -17 -6 59.13 37.30 -1 17 5 43.16 42.12 1 -17 -5 -75.64 44.70 -1 17 4 54.14 39.67 1 -17 -4 -71.59 36.02 -1 17 3 23.23 34.93 1 -17 -3 -17.23 24.41 -1 17 2 -32.06 24.28 -1 17 2 5.60 36.91 1 -17 -2 -4.16 24.41 -1 17 1 9.46 25.49 -1 17 1 -65.75 40.94 1 -17 -1 -41.15 32.29 -1 17 0 -12.94 20.78 -1 17 0 -51.64 33.03 1 -17 0 27.01 29.77 -1 17 -1 -24.92 21.54 -1 17 -1 62.63 46.58 -1 17 -2 6.65 26.89 -1 17 -2 28.96 38.65 -1 17 -3 22.38 21.75 -1 17 -3 -11.23 29.37 -1 17 -4 1.37 27.08 -1 17 -4 0.19 32.96 -1 17 -5 -37.77 30.16 -1 17 -6 22.66 31.65 -1 17 -7 -34.08 24.16 -1 17 -8 30.82 29.82 0 -17 -10 -52.28 53.82 0 17 9 20.43 45.40 0 -17 -9 -18.62 46.74 0 17 8 50.52 41.85 0 -17 -8 -20.59 38.20 0 17 7 -39.03 41.79 0 -17 -7 -0.16 36.40 0 17 6 29.90 46.91 0 -17 -6 64.85 46.40 0 17 5 13.57 36.45 0 -17 -5 -20.28 32.64 0 17 4 26.47 30.52 0 -17 -4 11.25 28.88 0 17 3 -47.14 38.98 0 -17 -3 75.18 41.02 0 17 2 -17.46 36.44 0 -17 -2 -51.33 33.21 0 17 1 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38.33 38.83 -3 -17 -6 11.74 38.29 3 17 5 48.79 55.05 -3 -17 -5 68.35 43.89 3 17 4 12.02 39.06 -3 -17 -4 38.52 41.26 3 17 3 -0.17 30.06 -3 -17 -3 -3.94 41.24 3 17 2 90.27 53.07 -3 -17 -2 -54.16 37.07 3 17 1 -28.45 38.00 -3 -17 -1 40.54 37.01 3 17 0 6.63 30.45 -3 -17 0 8.98 40.45 3 17 -1 20.51 29.12 -3 -17 1 -4.30 30.22 3 17 -2 7.34 31.22 -3 -17 2 25.59 34.53 3 17 -3 46.71 36.49 -3 -17 3 32.31 36.42 3 17 -4 -9.48 21.96 -3 -17 4 26.13 26.91 3 17 -5 -27.69 22.45 -3 -17 5 58.40 37.00 3 17 -6 -6.89 26.43 -3 -17 6 -120.77 51.97 3 17 -7 77.10 38.01 -3 -17 7 -61.84 51.63 -3 -17 8 -39.48 41.11 3 17 -8 -17.93 32.68 3 17 -9 -66.95 41.21 -4 -17 -6 -2.98 44.59 4 17 5 17.71 32.78 -4 -17 -5 121.90 50.92 4 17 4 -16.92 41.51 -4 -17 -4 97.12 50.11 4 17 3 60.88 52.63 -4 -17 -3 79.92 49.86 4 17 2 -66.33 44.93 -4 -17 -2 -25.03 38.12 4 17 1 -63.97 47.84 -4 -17 -1 8.48 33.67 4 17 0 -60.87 52.05 -4 -17 0 36.17 28.28 4 17 -1 -119.51 58.04 -4 -17 1 2.45 33.47 4 17 -2 -35.27 42.36 -4 -17 2 27.97 39.19 -4 -17 3 -23.39 36.61 -4 -17 4 73.49 42.38 -4 -17 5 -58.63 37.03 -4 -17 6 -26.64 41.46 4 17 -7 -31.30 32.38 -4 -17 7 -62.13 56.02 -4 -17 8 1.13 36.38 4 17 -8 -56.57 29.90 -4 -17 9 16.28 37.27 4 17 -9 41.80 40.95 -5 -17 -5 -33.36 37.09 -5 -17 -4 25.00 45.82 -5 -17 -3 -31.72 40.48 5 17 2 -23.39 32.74 -5 -17 -2 -34.17 39.22 5 17 1 35.57 33.63 -5 -17 -1 -34.02 46.31 5 17 0 19.34 36.79 -5 -17 0 -16.21 31.22 -5 -17 1 49.02 45.94 -5 -17 2 19.92 41.45 -5 -17 3 -49.96 42.97 -5 -17 4 -52.31 46.42 -5 -17 5 34.37 47.87 -5 -17 6 64.00 43.81 -5 -17 7 9.13 38.65 -5 -17 8 106.08 53.73 -6 -17 -3 -10.07 37.16 -6 -17 -2 1.12 40.27 -6 -17 -1 -37.80 48.84 -6 -17 0 27.00 45.90 -6 -17 1 103.41 52.69 -6 -17 2 29.18 43.33 -6 -17 3 165.05 66.08 -6 -17 4 76.66 43.46 -6 -17 5 -4.91 38.12 -6 -17 6 -10.78 38.81 -7 -17 3 198.68 86.87 -8 -17 2 -28.87 55.99 -8 -17 3 -4.46 50.53 -5 18 3 43.96 33.82 -5 18 2 -35.99 37.28 -5 18 1 2.77 30.81 -4 18 2 -0.48 27.51 -4 18 1 -5.41 25.80 -4 18 0 103.09 41.13 -4 18 -1 -51.42 41.40 -4 18 -2 -73.38 41.61 -3 18 1 -44.26 35.33 -3 18 0 -12.54 32.00 -3 18 -1 38.77 29.92 -3 18 -2 55.64 36.48 -3 18 -3 6.44 30.87 -3 18 -4 -46.35 41.98 -2 18 0 -35.01 25.87 -2 18 -1 -23.18 34.99 -2 18 -2 -50.65 28.57 -2 18 -3 88.75 44.61 -2 18 -4 -1.14 29.24 -2 18 -5 76.19 39.76 -1 18 -2 4.95 27.37 -1 18 -3 -1.28 27.12 -1 18 -4 -1.33 34.40 -1 18 -5 -40.18 40.59 -1 18 -6 -0.13 29.77 0 18 -3 -80.99 38.51 0 18 -4 82.78 40.94 0 18 -5 12.45 27.62 0 18 -6 107.89 46.31 -1 -18 -6 75.57 63.37 -1 -18 -5 -17.04 45.19 -1 -18 -4 40.24 38.93 -1 -18 -3 -25.14 38.22 -1 -18 -2 43.45 37.66 1 18 -6 29.32 35.04 1 18 -7 -44.45 31.66 -2 -18 -5 -80.55 58.05 -2 -18 -4 -20.80 38.91 -2 -18 -3 -103.69 56.55 -2 -18 -2 -31.78 38.14 -2 -18 -1 -28.31 40.89 -2 -18 0 4.29 49.12 -2 -18 1 16.35 38.21 -3 -18 -4 49.17 44.63 -3 -18 -3 -19.15 36.28 -3 -18 -2 24.13 39.53 -3 -18 -1 -12.93 43.79 -3 -18 0 -23.58 40.09 -3 -18 1 62.41 49.59 -3 -18 2 6.02 46.80 -3 -18 3 -46.12 47.34 -4 -18 -2 42.79 42.71 -4 -18 -1 -4.04 37.09 -4 -18 0 -37.78 37.62 -4 -18 1 80.95 47.05 -4 -18 2 34.36 36.30 -4 -18 3 -28.74 38.03 -4 -18 4 10.23 39.38 -4 -18 5 8.70 42.35 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 39130 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.948 _oxdiff_exptl_absorpt_empirical_full_min 0.717 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Br01 Br 0.52768(3) 0.48466(3) 0.28797(2) 0.05610(15) Uani 1 1 d . . . . . Br02 Br 0.64497(3) 0.48402(4) 0.51409(3) 0.06708(17) Uani 1 1 d . . . . . Cu03 Cu 0.51207(4) 0.49480(4) 0.42242(3) 0.0704(2) Uani 1 1 d . . . . . N004 N 0.2671(2) 0.7517(2) 0.29576(19) 0.0465(9) Uani 1 1 d . . . . . C005 C 0.1982(3) 0.6689(3) 0.3319(2) 0.0505(11) Uani 1 1 d . . . . . H00A H 0.163115 0.632307 0.290104 0.061 Uiso 1 1 calc R U . . . H00B H 0.235979 0.612769 0.358685 0.061 Uiso 1 1 calc R U . . . C006 C 0.3330(3) 0.6921(3) 0.2397(3) 0.0635(13) Uani 1 1 d . . . . . H00C H 0.362580 0.629905 0.266540 0.076 Uiso 1 1 calc R U . . . H00D H 0.384251 0.742129 0.223816 0.076 Uiso 1 1 calc R U . . . C007 C 0.2161(3) 0.8436(3) 0.2525(2) 0.0489(11) Uani 1 1 d . . . . . H00E H 0.170865 0.879648 0.287625 0.059 Uiso 1 1 calc R U . . . H00F H 0.263253 0.898385 0.236141 0.059 Uiso 1 1 calc R U . . . C008 C 0.2814(3) 0.6499(3) 0.1674(3) 0.0682(14) Uani 1 1 d . . . . . H00G H 0.328057 0.616444 0.132270 0.082 Uiso 1 1 calc R U . . . H00H H 0.235181 0.593224 0.182392 0.082 Uiso 1 1 calc R U . . . C009 C 0.1261(3) 0.7161(3) 0.3887(2) 0.0623(12) Uani 1 1 d . . . . . H00I H 0.160055 0.758415 0.428382 0.075 Uiso 1 1 calc R U . . . H00J H 0.083094 0.766248 0.361230 0.075 Uiso 1 1 calc R U . . . C00A C 0.1625(3) 0.8022(3) 0.1820(3) 0.0634(13) Uani 1 1 d . . . . . H00K H 0.132246 0.864357 0.155584 0.076 Uiso 1 1 calc R U . . . H00L H 0.111722 0.751925 0.198655 0.076 Uiso 1 1 calc R U . . . C00B C 0.0674(3) 0.6273(3) 0.4276(3) 0.0715(14) Uani 1 1 d . . . . . H00M H 0.110845 0.576696 0.454272 0.086 Uiso 1 1 calc R U . . . H00N H 0.033455 0.585402 0.387688 0.086 Uiso 1 1 calc R U . . . C00C C 0.2291(3) 0.7426(4) 0.1254(3) 0.0751(15) Uani 1 1 d . . . . . H00O H 0.191695 0.712425 0.082378 0.090 Uiso 1 1 calc R U . . . H00P H 0.275734 0.794532 0.104100 0.090 Uiso 1 1 calc R U . . . C00D C 0.3281(3) 0.8022(4) 0.3591(3) 0.0742(15) Uani 1 1 d . . . . . H00Q H 0.288416 0.848237 0.391786 0.111 Uiso 1 1 calc R U . . . H00R H 0.378284 0.846253 0.335930 0.111 Uiso 1 1 calc R U . . . H00S H 0.356507 0.744355 0.390063 0.111 Uiso 1 1 calc R U . . . C00E C -0.0055(3) 0.6708(4) 0.4859(3) 0.0838(17) Uani 1 1 d . . . . . H00T H -0.049436 0.720279 0.459977 0.126 Uiso 1 1 calc R U . . . H00U H 0.027550 0.709853 0.526869 0.126 Uiso 1 1 calc R U . . . H00V H -0.041001 0.609891 0.507906 0.126 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br01 0.0463(3) 0.0650(3) 0.0570(3) 0.0024(2) 0.0037(2) 0.0009(2) Br02 0.0609(3) 0.0749(3) 0.0655(3) 0.0000(3) -0.0070(2) 0.0120(3) Cu03 0.0962(5) 0.0554(4) 0.0595(4) 0.0021(3) -0.0045(3) 0.0008(3) N004 0.042(2) 0.040(2) 0.058(2) 0.0059(17) -0.0021(17) -0.0031(17) C005 0.054(3) 0.042(2) 0.057(3) 0.011(2) -0.005(2) -0.002(2) C006 0.041(3) 0.056(3) 0.093(4) 0.010(3) 0.010(3) 0.007(2) C007 0.050(3) 0.034(2) 0.062(3) 0.007(2) -0.002(2) 0.004(2) C008 0.074(3) 0.054(3) 0.076(4) -0.010(3) 0.031(3) 0.002(3) C009 0.072(3) 0.052(3) 0.063(3) 0.001(2) 0.006(3) -0.008(2) C00A 0.070(3) 0.054(3) 0.066(3) 0.017(2) -0.014(3) 0.001(2) C00B 0.075(4) 0.063(3) 0.076(4) 0.004(3) 0.016(3) -0.009(3) C00C 0.098(4) 0.073(4) 0.054(3) 0.006(3) 0.013(3) -0.008(3) C00D 0.065(3) 0.077(3) 0.081(4) 0.015(3) -0.025(3) -0.025(3) C00E 0.084(4) 0.088(4) 0.079(4) -0.002(3) 0.022(3) -0.012(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cu03 Br02 Cu03 66.82(2) . 5_666 ? Br01 Cu03 Br02 124.77(3) . . ? Br01 Cu03 Br02 122.05(3) . 5_666 ? Br01 Cu03 Cu03 178.16(4) . 5_666 ? Br02 Cu03 Br02 113.18(2) . 5_666 ? Br02 Cu03 Cu03 56.19(2) 5_666 5_666 ? Br02 Cu03 Cu03 56.99(2) . 5_666 ? C006 N004 C005 109.0(3) . . ? C006 N004 C007 108.8(3) . . ? C007 N004 C005 113.0(3) . . ? C00D N004 C005 109.1(3) . . ? C00D N004 C006 108.2(3) . . ? C00D N004 C007 108.6(3) . . ? N004 C005 H00A 108.4 . . ? N004 C005 H00B 108.4 . . ? H00A C005 H00B 107.4 . . ? C009 C005 N004 115.6(3) . . ? C009 C005 H00A 108.4 . . ? C009 C005 H00B 108.4 . . ? N004 C006 H00C 108.9 . . ? N004 C006 H00D 108.9 . . ? N004 C006 C008 113.2(3) . . ? H00C C006 H00D 107.7 . . ? C008 C006 H00C 108.9 . . ? C008 C006 H00D 108.9 . . ? N004 C007 H00E 109.1 . . ? N004 C007 H00F 109.1 . . ? H00E C007 H00F 107.9 . . ? C00A C007 N004 112.4(3) . . ? C00A C007 H00E 109.1 . . ? C00A C007 H00F 109.1 . . ? C006 C008 H00G 109.4 . . ? C006 C008 H00H 109.4 . . ? H00G C008 H00H 108.0 . . ? C00C C008 C006 111.4(4) . . ? C00C C008 H00G 109.4 . . ? C00C C008 H00H 109.4 . . ? C005 C009 H00I 109.2 . . ? C005 C009 H00J 109.2 . . ? H00I C009 H00J 107.9 . . ? C00B C009 C005 112.0(3) . . ? C00B C009 H00I 109.2 . . ? C00B C009 H00J 109.2 . . ? C007 C00A H00K 109.3 . . ? C007 C00A H00L 109.3 . . ? C007 C00A C00C 111.7(4) . . ? H00K C00A H00L 107.9 . . ? C00C C00A H00K 109.3 . . ? C00C C00A H00L 109.3 . . ? C009 C00B H00M 108.8 . . ? C009 C00B H00N 108.8 . . ? C009 C00B C00E 113.9(4) . . ? H00M C00B H00N 107.7 . . ? C00E C00B H00M 108.8 . . ? C00E C00B H00N 108.8 . . ? C008 C00C C00A 109.7(4) . . ? C008 C00C H00O 109.7 . . ? C008 C00C H00P 109.7 . . ? C00A C00C H00O 109.7 . . ? C00A C00C H00P 109.7 . . ? H00O C00C H00P 108.2 . . ? N004 C00D H00Q 109.5 . . ? N004 C00D H00R 109.5 . . ? N004 C00D H00S 109.5 . . ? H00Q C00D H00R 109.5 . . ? H00Q C00D H00S 109.5 . . ? H00R C00D H00S 109.5 . . ? C00B C00E H00T 109.5 . . ? C00B C00E H00U 109.5 . . ? C00B C00E H00V 109.5 . . ? H00T C00E H00U 109.5 . . ? H00T C00E H00V 109.5 . . ? H00U C00E H00V 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Br01 Cu03 2.3121(7) . ? Br02 Cu03 2.4416(8) 5_666 ? Br02 Cu03 2.4191(7) . ? Cu03 Cu03 2.6767(11) 5_666 ? N004 C005 1.512(4) . ? N004 C006 1.505(5) . ? N004 C007 1.507(4) . ? N004 C00D 1.502(5) . ? C005 H00A 0.9700 . ? C005 H00B 0.9700 . ? C005 C009 1.505(5) . ? C006 H00C 0.9700 . ? C006 H00D 0.9700 . ? C006 C008 1.516(5) . ? C007 H00E 0.9700 . ? C007 H00F 0.9700 . ? C007 C00A 1.500(5) . ? C008 H00G 0.9700 . ? C008 H00H 0.9700 . ? C008 C00C 1.513(5) . ? C009 H00I 0.9700 . ? C009 H00J 0.9700 . ? C009 C00B 1.499(5) . ? C00A H00K 0.9700 . ? C00A H00L 0.9700 . ? C00A C00C 1.518(5) . ? C00B H00M 0.9700 . ? C00B H00N 0.9700 . ? C00B C00E 1.512(5) . ? C00C H00O 0.9700 . ? C00C H00P 0.9700 . ? C00D H00Q 0.9600 . ? C00D H00R 0.9600 . ? C00D H00S 0.9600 . ? C00E H00T 0.9600 . ? C00E H00U 0.9600 . ? C00E H00V 0.9600 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N004 C005 C009 C00B -174.4(3) . . . . ? N004 C006 C008 C00C 55.6(5) . . . . ? N004 C007 C00A C00C -57.6(4) . . . . ? C005 N004 C006 C008 68.8(4) . . . . ? C005 N004 C007 C00A -65.6(4) . . . . ? C005 C009 C00B C00E 179.4(4) . . . . ? C006 N004 C005 C009 -179.1(3) . . . . ? C006 N004 C007 C00A 55.7(4) . . . . ? C006 C008 C00C C00A -53.9(5) . . . . ? C007 N004 C005 C009 -58.0(4) . . . . ? C007 N004 C006 C008 -54.9(4) . . . . ? C007 C00A C00C C008 55.4(5) . . . . ? C00D N004 C005 C009 62.9(4) . . . . ? C00D N004 C006 C008 -172.7(3) . . . . ? C00D N004 C007 C00A 173.2(3) . . . . ?