#------------------------------------------------------------------------------ #$Date: 2022-04-03 20:21:38 +0100 (Sun, 03 Apr 2022) $ #$Revision: 274239 $ #$URL: svn://www.crystallography.net/cod/cif/4/51/93/4519383.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519383 loop_ _publ_author_name 'Takahashi, Kohei' 'Sakurazawa, Yuji' 'Iwai, Asaki' 'Iwasawa, Nobuharu' _publ_section_title ; Catalytic Synthesis of a Methylmalonate Salt from Ethylene and Carbon Dioxide through Photoinduced Activation and Photoredox-Catalyzed Reduction of Nickelalactones ; _journal_issue 7 _journal_name_full 'ACS Catalysis' _journal_page_first 3776 _journal_page_last 3781 _journal_paper_doi 10.1021/acscatal.2c01053 _journal_volume 12 _journal_year 2022 _chemical_formula_moiety 'C29 H41 N2 Ni O4 P, C4 H9 N O' _chemical_formula_sum 'C33 H50 N3 Ni O5 P' _chemical_formula_weight 658.44 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2020-01-08 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 90 _cell_angle_beta 97.271(5) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 16.5365(9) _cell_length_b 15.9821(6) _cell_length_c 12.9995(6) _cell_measurement_reflns_used 7103 _cell_measurement_temperature 123 _cell_measurement_theta_max 74.1380 _cell_measurement_theta_min 3.8560 _cell_volume 3408.0(3) _computing_cell_refinement 'CrysAlisPro 1.171.40.37a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.37a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.37a (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 123 _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -18.00 23.00 0.50 18.39 -- 46.86 -40.00 21.00 82 2 \w 35.00 69.00 0.50 73.57 -- 104.75 -61.00 -30.00 68 3 \w 75.00 102.00 0.50 73.57 -- 104.75 -94.00-120.00 54 4 \w 34.00 68.00 0.50 73.57 -- 104.75 -94.00-120.00 68 5 \w 146.00 174.00 0.50 73.57 -- 104.75 30.00 -90.00 56 6 \w 92.00 133.00 0.50 73.57 -- 104.75 30.00 -90.00 82 7 \w 76.00 114.00 0.50 18.39 -- 46.86 40.00 175.00 76 8 \w 108.00 134.00 0.50 73.57 -- 104.75 40.00 175.00 52 9 \w -24.00 23.00 0.50 18.39 -- -46.86 19.00 -30.00 94 10 \w -57.00 -31.00 0.50 73.57 -- -102.00 61.00 90.00 52 11 \w -61.00 -34.00 0.50 73.57 -- -102.00 61.00 120.00 54 12 \w -63.00 -38.00 0.50 73.57 -- -102.00 61.00 150.00 50 13 \w -29.00 26.00 0.50 18.39 -- -46.86 40.00 175.00 110 14 \w -115.00 -46.00 0.50 18.39 -- -46.86 -40.00 21.00 138 15 \w -112.00 -84.00 0.50 18.39 -- -46.86-125.00 90.00 56 16 \w -159.00-101.00 0.50 73.57 -- -102.00 -94.00 120.00 116 17 \w -166.00 -86.00 0.50 73.57 -- -102.00 -40.00 21.00 160 18 \w -69.00 -29.00 0.50 73.57 -- -102.00 61.00 0.00 80 19 \w -64.00 -37.00 0.50 73.57 -- -102.00 61.00 30.00 54 20 \w -69.00 -41.00 0.50 73.57 -- -102.00 61.00 -30.00 56 21 \w -67.00 -42.00 0.50 73.57 -- -102.00 61.00 -90.00 50 22 \w -69.00 -30.00 0.50 73.57 -- -102.00 61.00 -60.00 78 23 \w -69.00 -30.00 0.50 73.57 -- -102.00 61.00-180.00 78 24 \w -113.00 -81.00 0.50 18.39 -- -46.86-125.00-180.00 64 25 \w -167.00 -93.00 0.50 73.57 -- -102.00 -30.00 -60.00 148 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy R, DW system, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0868416000 _diffrn_orient_matrix_UB_12 -0.0065985000 _diffrn_orient_matrix_UB_13 -0.0584694000 _diffrn_orient_matrix_UB_21 0.0277751000 _diffrn_orient_matrix_UB_22 0.0476577000 _diffrn_orient_matrix_UB_23 -0.0924348000 _diffrn_orient_matrix_UB_31 0.0226269000 _diffrn_orient_matrix_UB_32 -0.0834962000 _diffrn_orient_matrix_UB_33 -0.0480380000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0754 _diffrn_reflns_av_unetI/netI 0.0614 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_h_min -19 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_number 21916 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 68.246 _diffrn_reflns_theta_min 3.862 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'Rigaku (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 1.605 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.68685 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.37a (Rigaku Oxford Diffraction, 2019) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour yellow _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.283 _exptl_crystal_description needle _exptl_crystal_F_000 1408 _exptl_crystal_size_max 0.263 _exptl_crystal_size_mid 0.041 _exptl_crystal_size_min 0.023 _refine_diff_density_max 0.653 _refine_diff_density_min -0.446 _refine_diff_density_rms 0.072 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.075 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 395 _refine_ls_number_reflns 6223 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.075 _refine_ls_R_factor_all 0.0849 _refine_ls_R_factor_gt 0.0608 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0913P)^2^+1.3346P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1585 _refine_ls_wR_factor_ref 0.1731 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4467 _reflns_number_total 6223 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cs2c01053_si_002.cif _cod_data_source_block 191128ai-706 _cod_database_code 4519383 _shelx_shelxl_version_number 2016/6 _chemical_oxdiff_formula NiO4PN2C31H43 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _reflns_odcompleteness_completeness 99.66 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 68.13 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C15(H15), C21(H21), C32(H32) 2.b Secondary CH2 refined with riding coordinates: C16(H16A,H16B), C13(H13A,H13B), C20(H20A,H20B), C26(H26A,H26B), C19(H19A, H19B), C18(H18A,H18B), C22(H22A,H22B), C17(H17A,H17B), C24(H24A,H24B), C25(H25A,H25B), C23(H23A,H23B) 2.c Aromatic/amide H refined with riding coordinates: C6(H6), C4(H4), C12(H12), C11(H11) 2.d Idealised Me refined as rotating group: C28(H28A,H28B,H28C), C29(H29A,H29B,H29C), C27(H27A,H27B,H27C), C36(H36A,H36B, H36C), C42(H42A,H42B,H42C), C41(H41A,H41B,H41C), C43(H43A,H43B,H43C) ; _shelx_res_file ; TITL 191128ai-706_a.res in P2(1)/c 191128ai-706.res created by SHELXL-2016/6 at 09:37:42 on 08-Jan-2020 REM Old TITL 191128AI-706 in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.163, Rweak 0.007, Alpha 0.040, Orientation as input REM Formula found by SHELXT: C34 N2 O5 P Ni CELL 1.54184 16.5365 15.9821 12.9995 90 97.271 90 ZERR 4 0.0009 0.0006 0.0006 0 0.005 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N Ni O P UNIT 132 200 12 4 20 4 L.S. 4 PLAN 13 BOND $H LIST 6 fmap 2 acta REM REM REM WGHT 0.091300 1.334600 FVAR 0.79983 NI1 4 0.694052 0.726206 0.833510 11.00000 0.04848 0.02693 = 0.03611 -0.00320 -0.00518 0.00319 P14 6 0.628157 0.830275 0.885508 11.00000 0.04709 0.02620 = 0.03594 -0.00185 -0.00509 0.00324 O35 5 0.598842 0.686389 0.751640 11.00000 0.05633 0.03134 = 0.04300 -0.00426 -0.00495 -0.00007 O30 5 0.756493 0.643592 0.776693 11.00000 0.05909 0.03660 = 0.04463 -0.00224 0.00181 0.00346 N8 3 0.767597 0.822833 1.004129 11.00000 0.04396 0.03702 = 0.03604 -0.00518 -0.00464 0.00297 N10 3 0.860609 0.748394 0.948117 11.00000 0.04723 0.03484 = 0.03832 -0.00388 -0.00386 0.00630 O37 5 0.760668 0.514993 0.715679 11.00000 0.08398 0.03751 = 0.06598 -0.01000 0.01315 0.00385 O34 5 0.518410 0.576414 0.716200 11.00000 0.06723 0.04622 = 0.05572 -0.00050 -0.01039 -0.01313 C9 1 0.779744 0.765950 0.929145 11.00000 0.04856 0.03436 = 0.03532 -0.00293 0.00062 0.00136 C6 1 0.999822 0.673512 0.767279 11.00000 0.04749 0.03224 = 0.03872 -0.00022 -0.00583 -0.00138 AFIX 43 H6 2 1.030206 0.695451 0.718128 11.00000 -1.20000 AFIX 0 C15 1 0.523036 0.814788 0.909064 11.00000 0.05374 0.02992 = 0.03688 0.00063 -0.00671 0.00116 AFIX 13 H15 2 0.490298 0.806855 0.841491 11.00000 -1.20000 AFIX 0 C3 1 0.911456 0.607968 0.917795 11.00000 0.04711 0.03386 = 0.04845 0.00565 -0.00290 0.00128 C5 1 1.003771 0.588473 0.788418 11.00000 0.04445 0.03343 = 0.04712 -0.00357 -0.00131 0.00225 C2 1 0.907849 0.692916 0.892128 11.00000 0.04136 0.03203 = 0.04014 -0.00238 -0.00281 0.00329 C21 1 0.629899 0.922438 0.802025 11.00000 0.04578 0.03247 = 0.04218 -0.00053 0.00269 0.00378 AFIX 13 H21 2 0.590428 0.962776 0.822931 11.00000 -1.20000 AFIX 0 C7 1 0.951622 0.726384 0.817795 11.00000 0.04514 0.02860 = 0.04015 0.00159 -0.00430 0.00076 O38 5 0.894561 0.293985 0.426538 11.00000 0.08860 0.09439 = 0.06971 0.01590 0.02745 -0.00049 C4 1 0.959190 0.557362 0.863665 11.00000 0.05232 0.02625 = 0.06065 0.00412 0.00049 0.00062 AFIX 43 H4 2 0.961530 0.500370 0.878183 11.00000 -1.20000 AFIX 0 C16 1 0.514395 0.735139 0.972802 11.00000 0.06591 0.03130 = 0.05251 0.00623 0.00048 0.00124 AFIX 23 H16A 2 0.533660 0.687407 0.936747 11.00000 -1.20000 H16B 2 0.547903 0.740063 1.039381 11.00000 -1.20000 AFIX 0 C13 1 0.686485 0.856656 1.011847 11.00000 0.04643 0.03647 = 0.04311 -0.00660 -0.00128 0.00563 AFIX 23 H13A 2 0.688612 0.916724 1.022529 11.00000 -1.20000 H13B 2 0.662598 0.830691 1.068335 11.00000 -1.20000 AFIX 0 C20 1 0.487707 0.890496 0.960961 11.00000 0.05001 0.03325 = 0.04729 -0.00018 0.00173 0.00495 AFIX 23 H20A 2 0.521449 0.902448 1.025884 11.00000 -1.20000 H20B 2 0.489139 0.939030 0.916424 11.00000 -1.20000 AFIX 0 C12 1 0.838153 0.840696 1.068097 11.00000 0.05270 0.04707 = 0.04050 -0.01062 -0.00594 0.00045 AFIX 43 H12 2 0.844063 0.877055 1.124405 11.00000 -1.20000 AFIX 0 C31 1 0.728112 0.569610 0.763819 11.00000 0.06253 0.03182 = 0.04473 0.00335 -0.00121 0.00161 C11 1 0.896996 0.794730 1.032497 11.00000 0.04692 0.04853 = 0.04157 -0.00513 -0.00705 0.00158 AFIX 43 H11 2 0.951873 0.794013 1.059283 11.00000 -1.20000 AFIX 0 C33 1 0.583039 0.607422 0.754823 11.00000 0.06377 0.03357 = 0.04083 0.00091 0.00257 -0.00009 C26 1 0.601345 0.896922 0.689689 11.00000 0.07567 0.03831 = 0.04324 -0.00029 -0.00244 -0.00172 AFIX 23 H26A 2 0.547279 0.872595 0.685351 11.00000 -1.20000 H26B 2 0.637943 0.854840 0.668044 11.00000 -1.20000 AFIX 0 C32 1 0.650152 0.552299 0.812692 11.00000 0.06279 0.03617 = 0.05338 0.00254 0.00255 0.00253 AFIX 13 H32 2 0.659485 0.572224 0.884512 11.00000 -1.20000 AFIX 0 C28 1 0.863276 0.573017 0.998150 11.00000 0.06419 0.04760 = 0.05675 0.01898 0.00816 0.00319 AFIX 137 H28A 2 0.874517 0.604775 1.061016 11.00000 -1.50000 H28B 2 0.878311 0.515649 1.011492 11.00000 -1.50000 H28C 2 0.806154 0.576250 0.973384 11.00000 -1.50000 AFIX 0 C29 1 0.945407 0.817857 0.790105 11.00000 0.06951 0.03078 = 0.05941 0.00491 0.00756 0.00172 AFIX 137 H29A 2 0.982505 0.830531 0.741128 11.00000 -1.50000 H29B 2 0.959023 0.850891 0.851534 11.00000 -1.50000 H29C 2 0.890732 0.830458 0.760003 11.00000 -1.50000 AFIX 0 C27 1 1.054386 0.532865 0.729231 11.00000 0.06913 0.04028 = 0.06426 -0.00521 0.00720 0.01112 AFIX 137 H27A 2 1.019262 0.498569 0.682207 11.00000 -1.50000 H27B 2 1.088227 0.497817 0.776791 11.00000 -1.50000 H27C 2 1.088095 0.566584 0.690774 11.00000 -1.50000 AFIX 0 C19 1 0.401153 0.875691 0.981884 11.00000 0.05387 0.04931 = 0.05983 0.00023 0.00710 0.00101 AFIX 23 H19A 2 0.365915 0.872238 0.916438 11.00000 -1.20000 H19B 2 0.383274 0.922787 1.020314 11.00000 -1.20000 AFIX 0 C18 1 0.393050 0.795716 1.043247 11.00000 0.05476 0.05995 = 0.05330 0.00110 0.00790 -0.01103 AFIX 23 H18A 2 0.422581 0.801831 1.112210 11.00000 -1.20000 H18B 2 0.336086 0.786201 1.050328 11.00000 -1.20000 AFIX 0 C22 1 0.712542 0.965690 0.810740 11.00000 0.05296 0.05094 = 0.06737 0.01223 -0.00204 -0.00606 AFIX 23 H22A 2 0.753314 0.926939 0.791784 11.00000 -1.20000 H22B 2 0.728582 0.983322 0.881794 11.00000 -1.20000 AFIX 0 C17 1 0.426358 0.720933 0.989794 11.00000 0.06560 0.04934 = 0.05182 0.00829 -0.00018 -0.01222 AFIX 23 H17A 2 0.422797 0.671328 1.031979 11.00000 -1.20000 H17B 2 0.393556 0.711605 0.923496 11.00000 -1.20000 AFIX 0 N11 3 0.841118 0.315637 0.569723 11.00000 0.06343 0.12957 = 0.07551 -0.01805 -0.00741 0.03089 C24 1 0.680813 1.016526 0.626701 11.00000 0.07443 0.05322 = 0.07594 0.02290 0.02829 0.01358 AFIX 23 H24A 2 0.677023 1.065687 0.582594 11.00000 -1.20000 H24B 2 0.721251 0.979328 0.603669 11.00000 -1.20000 AFIX 0 C25 1 0.599368 0.972899 0.616514 11.00000 0.08652 0.04706 = 0.04392 0.00856 0.00291 0.00444 AFIX 23 H25A 2 0.585038 0.954455 0.545456 11.00000 -1.20000 H25B 2 0.557892 1.011911 0.632823 11.00000 -1.20000 AFIX 0 C23 1 0.707612 1.042451 0.738279 11.00000 0.05562 0.05040 = 0.09106 0.02214 0.00409 -0.00655 AFIX 23 H23A 2 0.669092 1.082544 0.759925 11.00000 -1.20000 H23B 2 0.760588 1.069251 0.743112 11.00000 -1.20000 AFIX 0 C36 1 0.629079 0.460481 0.816097 11.00000 0.08083 0.04484 = 0.06872 0.00582 0.00329 -0.00443 AFIX 137 H36A 2 0.617628 0.439333 0.746660 11.00000 -1.50000 H36B 2 0.581987 0.453365 0.851479 11.00000 -1.50000 H36C 2 0.674228 0.430378 0.852317 11.00000 -1.50000 AFIX 0 C39 1 0.859497 0.265667 0.499072 11.00000 0.06621 0.08383 = 0.09459 -0.00422 -0.01113 0.01065 C42 1 0.837883 0.175887 0.512811 11.00000 0.09222 0.05327 = 0.12785 0.01636 -0.02722 -0.01363 AFIX 137 H42A 2 0.779898 0.170713 0.511197 11.00000 -1.50000 H42B 2 0.864368 0.156074 0.578257 11.00000 -1.50000 H42C 2 0.855501 0.143220 0.457800 11.00000 -1.50000 AFIX 0 C41 1 0.859262 0.409982 0.556727 11.00000 0.11401 0.05667 = 0.08958 -0.00778 0.00451 0.01922 AFIX 137 H41A 2 0.914901 0.416932 0.544438 11.00000 -1.50000 H41B 2 0.850454 0.439435 0.618704 11.00000 -1.50000 H41C 2 0.823662 0.431983 0.498995 11.00000 -1.50000 AFIX 0 C43 1 0.803599 0.293856 0.664295 11.00000 0.07732 0.13655 = 0.06031 0.01696 0.00598 0.02463 AFIX 137 H43A 2 0.771905 0.243705 0.651946 11.00000 -1.50000 H43B 2 0.768944 0.338795 0.680826 11.00000 -1.50000 H43C 2 0.845722 0.285005 0.721176 11.00000 -1.50000 AFIX 0 HKLF 4 REM 191128ai-706_a.res in P2(1)/c REM R1 = 0.0608 for 4467 Fo > 4sig(Fo) and 0.0849 for all 6223 data REM 395 parameters refined using 0 restraints END WGHT 0.0913 1.3346 REM Highest difference peak 0.653, deepest hole -0.446, 1-sigma level 0.072 Q1 1 0.8679 0.3329 0.5060 11.00000 0.05 0.65 Q2 1 0.8346 0.2602 0.5765 11.00000 0.05 0.52 Q3 1 0.6070 0.7277 0.8227 11.00000 0.05 0.52 Q4 1 0.7761 0.7308 0.8438 11.00000 0.05 0.49 Q5 1 0.7413 0.7393 0.8758 11.00000 0.05 0.39 Q6 1 0.6665 0.6203 0.7701 11.00000 0.05 0.39 Q7 1 0.6612 0.8282 0.9226 11.00000 0.05 0.35 Q8 1 0.7152 0.8274 0.8970 11.00000 0.05 0.34 Q9 1 0.5938 0.8274 0.8989 11.00000 0.05 0.32 Q10 1 0.5363 0.8274 0.8802 11.00000 0.05 0.32 Q11 1 0.6392 0.5423 0.7345 11.00000 0.05 0.31 Q12 1 0.5837 0.5378 0.7002 11.00000 0.05 0.29 Q13 1 0.6952 0.7708 0.9343 11.00000 0.05 0.29 ; _shelx_res_checksum 7667 _shelx_hkl_file ; 2 0 0 734.294 39.7097 14 3 0 0 2980.91 157.402 14 4 0 0 6219.06 326.693 15 5 0 0 635.458 36.0694 15 6 0 0 137.452 14.6141 15 7 0 0 355.264 23.9331 15 8 0 0 1822.52 97.7478 15 9 0 0 2084.09 114.176 13 10 0 0 2178.03 117.110 17 10 0 0 2252.77 120.848 13 11 0 0 2397.47 133.548 17 -11 0 0 2832.46 137.362 7 11 0 0 2485.23 137.710 13 12 0 0 164.356 30.2269 13 12 0 0 154.358 21.0013 17 -12 0 0 93.2014 22.9597 7 13 0 0 2509.75 136.950 17 13 0 0 2398.71 142.313 13 -13 0 0 2786.27 141.102 7 14 0 0 7.39111 21.1611 17 -14 0 0 24.0176 24.9895 7 14 0 0 21.1859 32.0385 13 15 0 0 729.196 48.6287 17 15 0 0 690.452 56.8546 13 16 0 0 42.8107 25.2802 25 16 0 0 99.4932 23.0778 17 17 0 0 56.3040 22.6265 17 18 0 0 104.249 20.6151 17 19 0 0 48.8614 28.0375 23 -19 0 0 298.131 17.8579 8 1 -1 0 24291.1 1277.54 15 1 1 0 24424.7 1277.38 14 2 -1 0 6607.27 352.061 15 2 1 0 6797.36 352.002 14 3 1 0 17.7406 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103.152 18.5886 19 5 -9 0 79.0077 16.4980 16 5 -9 0 86.9582 22.1719 22 -5 -9 0 100.999 22.7279 9 5 -9 0 74.5585 10.4538 4 -5 -9 0 116.241 19.7580 18 6 -9 0 256.298 17.9184 4 -6 -9 0 298.577 25.2522 18 6 -9 0 306.408 31.4505 21 -6 -9 0 254.032 18.2583 3 -6 -9 0 326.263 23.3860 19 -6 -9 0 251.453 29.1074 9 6 -9 0 275.320 29.2329 22 -7 -9 0 65.3179 26.2393 9 7 -9 0 124.409 29.2670 21 -7 -9 0 106.751 20.8263 18 -7 -9 0 111.801 19.9814 19 -7 -9 0 33.0352 59.8879 24 -7 -9 0 103.292 12.7509 3 7 -9 0 91.6306 11.7415 4 -8 -9 0 119.268 27.3980 9 8 -9 0 58.5483 31.3062 21 8 -9 0 88.5672 11.6633 4 -8 -9 0 61.8334 63.0486 24 -8 -9 0 95.2379 20.2541 19 -8 -9 0 92.2181 21.8900 18 -9 -9 0 6.06630 19.1438 19 -9 -9 0-5.83167 21.5066 18 -9 -9 0 21.0215 25.9566 9 -9 -9 0-60.0532 68.0112 24 9 -9 0-1.63394 10.4167 4 10 -9 0 379.971 23.3659 4 -10 -9 0 415.409 28.9722 19 -10 -9 0 368.554 31.7493 18 -10 -9 0 363.070 72.2418 24 -11 -9 0 108.675 68.9948 24 11 -9 0 75.0288 10.9471 4 -11 -9 0 71.4052 23.6294 18 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53.9851 18 10 -10 0 956.552 48.9434 4 -10 -10 0 776.366 60.1848 9 -11 -10 0 3.11339 27.5355 9 -11 -10 0 26.9760 22.1424 18 11 -10 0 29.8916 10.4556 4 -11 -10 0-24.7856 64.9161 24 -12 -10 0 376.497 32.1831 18 12 -10 0 425.404 24.4228 4 13 -10 0 7.32178 7.50141 4 -13 -10 0 18.4819 20.7096 18 -14 -10 0 89.8638 18.7460 18 14 -10 0 71.5886 35.0189 23 14 10 0 107.499 38.1900 25 -15 -10 0-4.35080 14.7865 18 15 -10 0 20.9684 30.7388 23 15 10 0 7.12008 33.9222 25 16 -10 0-36.3419 26.4706 23 16 10 0 0.57714 29.5720 25 0 -11 0 6.18147 14.0558 16 0 -11 0-2.38034 10.6255 4 0 -11 0 2.63190 20.0727 20 0 -11 0 5.28914 17.2135 18 0 -11 0-0.79897 19.6213 22 -1 -11 0 809.253 46.6906 18 -1 -11 0 814.620 43.7682 4 1 -11 0 755.119 47.2360 20 1 -11 0 798.948 45.5387 16 1 -11 0 788.610 43.8340 4 -1 -11 0 823.021 44.7926 16 1 -11 0 738.804 47.5241 22 1 -11 0 773.804 46.2985 18 2 -11 0 237.592 21.2715 16 -2 -11 0 220.527 23.0080 9 2 -11 0 261.292 17.6448 4 2 -11 0 214.609 22.5509 20 -2 -11 0 279.237 18.9420 16 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730.212 39.8890 3 4 -13 0 851.085 55.2897 21 4 -13 0 871.617 53.8543 22 -4 -13 0 817.757 46.9850 3 -5 -13 0-13.8569 23.0519 18 -5 -13 0 3.27337 14.4928 3 5 -13 0-6.55498 13.1387 4 5 -13 0 6.49957 29.9949 22 5 -13 0-3.20844 32.7533 21 -6 -13 0 723.758 46.4461 18 6 -13 0 701.236 52.6793 21 6 -13 0 680.423 51.4656 22 6 -13 0 720.355 41.3307 4 -6 -13 0 770.391 42.2815 3 7 -13 0 1227.35 89.1367 21 7 -13 0 1502.51 81.9093 4 -7 -13 0 1410.29 85.5428 18 8 -13 0 49.8815 37.1362 21 -8 -13 0 28.0010 23.3777 18 8 -13 0 14.7125 11.6373 4 8 13 0-16.1362 34.1512 25 9 -13 0 41.3070 11.7833 4 -9 -13 0 17.8303 22.7645 18 10 13 0 163.166 37.1193 25 10 -13 0 189.863 15.0393 4 -10 -13 0 181.288 25.0163 18 -11 -13 0 77.6757 20.0294 18 11 13 0 42.8284 35.1151 25 11 -13 0 57.9642 10.3622 4 12 13 0 9.19400 32.9143 25 12 -13 0 7.07856 8.29498 4 -12 -13 0-15.4810 18.4425 18 13 13 0-25.2213 30.8066 25 -13 -13 0 29.8582 15.5427 18 -14 -13 0 21.2031 11.9575 18 14 13 0 28.4102 27.2027 25 0 -14 0 345.043 30.1385 20 0 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39.9491 17.4440 18 1 -12 -2 19.2111 18.9390 22 -1 -12 2 45.9790 11.1617 4 0 -12 -2 48.0931 19.1100 18 0 -12 2 61.8998 16.5866 16 0 -12 2 66.5326 24.3999 22 0 -12 -2 25.8797 18.6774 20 0 -12 2 45.4548 11.1563 4 0 -12 -2 58.2070 18.6243 22 -1 -12 -2 43.0773 19.6893 18 -1 -12 -2 30.1370 18.3593 22 1 -12 2 31.4045 23.1507 22 -1 -12 -2 41.2978 20.1002 20 1 -12 2 19.5341 17.0485 16 -1 -12 -2 22.0054 12.8943 3 1 -12 2 39.2722 11.5750 4 -2 -12 -2 108.282 21.8886 18 -2 -12 -2 79.9862 13.7461 3 2 -12 2 100.689 18.0719 16 -2 -12 -2 96.4690 19.5344 22 2 -12 2 78.0551 13.1843 4 2 -12 2 117.092 25.0202 22 2 -12 2 104.246 22.7720 20 3 -12 2 423.475 29.3699 16 -3 -12 -2 427.603 32.0826 19 3 -12 2 406.987 25.6006 4 -3 -12 -2 382.427 26.3815 3 3 -12 2 400.198 34.2064 22 3 -12 2 398.033 32.2041 20 -3 -12 -2 388.640 31.7949 18 -4 -12 -2-0.31594 14.8930 3 -4 -12 -2-6.83717 21.7018 19 -4 -12 -2 11.1469 23.6369 18 4 -12 2-19.4093 27.5251 22 4 -12 2 3.76008 12.2224 4 -5 -12 -2 4.54851 14.8553 3 -5 -12 -2 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247.918 32.8179 22 -5 -13 -2 39.9299 17.6331 3 5 -13 2 56.7112 22.2617 16 5 -13 2 84.8878 32.1788 22 -5 -13 -2 103.838 25.3192 18 5 -13 2 103.527 35.9372 21 -6 -13 -2 97.4426 20.5361 3 6 -13 2 23.8983 33.1112 22 6 -13 2 10.8425 35.7708 21 7 -13 2 95.1129 14.0125 4 7 -13 2 79.3242 37.7402 21 -8 -13 -2 254.401 28.4731 18 8 -13 2 192.064 17.1871 4 8 -13 2 209.101 39.5206 21 9 -13 2 28.5863 12.2748 4 -9 -13 -2-8.16839 24.1716 18 10 -13 2 6.17634 11.0470 4 -10 -13 -2-10.1804 22.9273 18 11 -13 2 195.712 14.9978 4 -11 -13 -2 196.480 24.8592 18 11 13 2 160.742 35.7434 25 12 13 2 27.4149 31.7295 25 -12 -13 -2 28.4384 19.2715 18 12 -13 2 26.3242 9.24003 4 13 13 2 10.1996 28.5198 25 -13 -13 -2 3.56545 16.0350 18 13 -13 2 20.5384 7.20811 4 -14 -13 -2 38.7822 12.9347 18 14 13 2 7.56907 24.2777 25 13 14 -2 13.5471 26.3042 25 -12 -14 2 58.4135 14.1683 18 12 14 -2 0.26785 29.2209 25 -11 -14 2 14.0664 16.1724 18 11 14 -2 18.6951 30.9042 25 10 14 -2 340.865 40.4931 25 -10 -14 2 444.316 29.2848 18 9 14 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282.887 15 4 -8 3 5514.38 279.417 22 5 -8 3 0.98771 13.2226 16 5 -8 3 18.6837 21.7809 22 -5 -8 -3-0.97132 12.8238 3 6 -8 3 223.892 18.6299 16 6 -8 3 222.342 31.5313 15 6 -8 3 152.598 28.5637 22 -7 -8 -3 956.551 54.7041 19 7 -8 3 866.214 51.6386 16 7 -8 3 992.373 60.4175 15 7 -8 3 942.945 53.4665 13 7 -8 3 792.517 58.0703 22 7 -8 3 983.323 57.9538 21 8 -8 3 35.1098 16.7185 16 8 -8 3 63.2632 32.1145 21 8 -8 3 37.1997 19.7754 13 -8 -8 -3 15.2934 22.5196 19 -9 -8 -3 1182.03 68.8903 19 9 -8 3 1217.39 72.9080 21 10 -8 3 14.1632 36.7884 21 -10 -8 -3 4.22500 22.4925 19 -11 -8 -3 75.2221 23.0097 19 12 -8 3-10.4085 16.8708 17 -12 -8 -3 36.7718 21.2821 19 13 -8 3 308.308 22.8903 17 -13 -8 -3 294.723 26.0263 19 -14 -8 -3 274.564 22.5840 19 -15 -8 -3-12.7856 20.0796 18 -16 -8 -3 101.273 17.2854 18 -17 -8 -3 9.70658 10.6630 18 17 -9 -3-9.36173 26.2873 23 16 -9 -3 55.2830 32.4985 23 15 9 -3 37.4305 35.3858 25 15 -9 -3 42.2459 35.9909 23 14 9 -3 79.9180 19.2498 5 14 -9 -3 3.45054 37.9578 23 14 9 -3 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30.8819 25 -6 -9 3 93.3330 26.1983 9 -6 -9 3 82.0857 17.1433 18 6 -9 -3 63.3271 27.2934 21 -6 -9 3 35.3871 61.3391 24 6 -9 -3 68.2647 28.8637 23 6 9 -3 62.1491 10.9907 6 5 -9 -3 337.951 29.7784 21 -5 -9 3 362.615 23.6093 16 -5 -9 3 325.210 32.3124 9 -5 -9 3 420.683 25.4892 18 5 -9 -3 294.656 20.1255 4 -5 -9 3 433.814 64.8343 24 5 9 -3 383.222 34.4332 25 -4 -9 3 417.216 28.0327 18 -4 -9 3 387.659 34.6122 9 -4 -9 3 428.333 26.8976 16 -4 -9 3 395.142 61.4681 24 4 9 -3 366.848 35.2865 25 -3 -9 3 304.924 22.1656 18 -3 -9 3 257.300 52.2084 24 -3 -9 3 271.537 28.8486 9 -3 -9 3 271.427 21.3954 16 -2 -9 3 308.051 29.4229 9 -2 -9 3 292.877 21.2153 16 -2 -9 3 246.946 21.2290 18 -1 -9 3 369.358 24.5791 18 -1 -9 3 333.103 23.8432 16 -1 -9 3 406.756 27.3555 20 0 -9 3 3803.63 207.564 16 0 -9 3 4134.47 208.486 20 -1 -9 -3 362.775 27.2014 19 1 -9 3 374.747 28.3509 22 1 -9 3 393.570 27.0695 20 -2 -9 -3 1701.24 88.8685 18 2 -9 3 1818.43 88.8990 20 2 -9 3 1667.58 87.4619 16 2 -9 3 1840.45 89.2657 22 -2 -9 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107.502 1 1 -3 -4 2557.20 145.865 1 -1 -3 4 3066.71 147.669 9 1 3 -4 2781.43 146.060 1 0 3 -4 4008.31 198.983 1 0 -3 -4 3764.71 198.885 1 0 -3 4 3765.14 199.805 9 0 -3 4 3341.68 200.230 24 1 3 4 870.279 53.7323 14 -1 3 -4 992.313 53.1783 1 -1 -3 -4 943.533 53.1471 1 1 -3 4 958.669 53.7265 14 2 3 4 332.826 25.1333 14 2 -3 4 372.202 25.9172 14 3 3 4 46.9067 15.5487 14 3 -3 4 26.0118 16.1251 14 4 -3 4 14.0030 15.8048 14 4 3 4 3.64142 15.9340 14 5 -3 4 3961.02 202.056 14 5 3 4 3646.48 201.931 14 6 -3 4 2203.08 107.249 14 6 3 4 2078.05 107.261 14 -6 3 -4 1957.61 106.588 7 -6 -3 -4 1992.91 106.755 7 7 -3 4 47.3052 19.9701 14 -7 -3 -4 38.9577 18.8856 7 -7 -3 -4 33.3921 27.7928 24 7 3 4 20.5809 18.9648 14 -7 3 -4 42.6975 18.5629 7 8 3 4 799.045 51.4288 14 8 -3 4 864.592 46.4680 17 -8 3 -4 846.299 50.6901 7 -8 -3 -4 875.317 50.9403 7 8 -3 4 825.461 52.1286 15 8 -3 4 839.340 51.3579 14 8 3 4 853.230 46.4496 17 -9 3 -4 288.210 27.6610 7 9 -3 4 275.908 29.3417 15 -9 -3 -4 258.354 19.3349 8 -9 3 -4 281.558 19.2857 8 9 -3 4 292.280 28.5860 14 -9 -3 -4 289.896 27.8929 7 9 3 4 316.952 22.2128 17 9 3 4 295.396 28.3376 14 9 -3 4 365.949 33.8213 21 9 -3 4 328.124 22.2661 17 10 3 4 1616.08 84.4580 17 10 -3 4 1449.02 89.1448 15 10 -3 4 1571.52 84.5247 17 -10 -3 -4 1539.06 83.5748 8 -10 3 -4 1520.85 83.4268 8 -10 -3 -4 1688.79 89.1598 7 -10 3 -4 1588.19 88.5831 7 11 -3 4 356.410 27.4814 17 -11 3 -4 355.032 32.5757 7 11 -3 4 298.377 33.2670 15 -11 -3 -4 415.044 24.3014 8 -11 3 -4 371.688 23.8763 8 11 3 4 340.595 27.2671 17 -11 -3 -4 388.605 33.8578 7 -12 -3 -4 269.751 30.1195 7 12 3 4 256.837 25.4734 17 12 -3 4 295.859 24.7496 17 -12 3 -4 266.893 29.7332 7 -12 -3 -4 278.628 20.3944 8 -12 3 -4 265.406 20.1557 8 12 -3 4 182.812 29.7606 15 -13 3 -4 24.4440 14.0197 8 13 -3 4 6.70694 21.2151 17 13 3 4 28.2393 21.6216 17 13 3 4 42.1134 29.2024 13 -13 -3 -4 4.49651 14.5247 8 13 -3 4-21.0215 28.5744 13 -14 3 -4 89.9243 15.0307 8 -14 -3 -4 95.8633 15.6432 8 14 -3 4 53.8316 22.1029 17 14 3 4 42.7580 22.4421 17 -15 3 -4 100.048 15.4773 8 15 -3 4 76.1739 22.2870 17 15 3 4 83.9256 22.3170 17 -15 -3 -4 108.623 15.6596 8 16 -3 4 41.5359 19.9537 17 16 3 4 17.0272 19.9636 17 -16 -3 -4 59.6315 14.0513 8 -16 3 -4 52.3597 13.4609 8 17 -3 4 110.041 19.3437 17 17 3 4 117.889 19.8360 17 -17 -3 -4 162.163 14.3976 8 -17 3 -4 145.135 14.1910 8 18 -3 4 82.5322 15.4755 17 18 3 4 79.6966 15.4541 17 -18 -3 -4 93.6128 10.6478 8 -18 3 -4 91.9086 10.5471 8 19 -4 -4 22.6281 24.8613 23 18 4 -4-18.4248 26.2041 25 18 -4 -4 59.8180 30.8884 23 17 4 -4 32.8823 30.4801 25 17 -4 -4-7.68451 34.8843 23 16 -4 -4-56.7278 38.2088 23 16 4 -4 16.0349 33.3271 25 15 -4 -4 39.8617 38.5463 23 15 4 -4 67.1654 35.9134 25 15 4 -4 51.4975 22.5711 5 14 4 -4 19.8621 35.7093 25 14 4 -4 11.4521 20.8638 5 14 4 -4-4.72323 34.5899 13 -14 -4 4 18.2815 27.3304 9 14 -4 -4-37.1678 38.7788 23 14 -4 -4-25.7902 36.8704 13 13 4 -4 5.15622 20.0771 5 13 4 -4-25.6961 35.9477 25 13 -4 -4 91.5750 38.4029 23 13 -4 -4 15.6103 35.2444 13 13 4 -4 18.5702 35.1699 13 12 4 -4 151.816 19.6990 5 12 4 -4 160.625 35.2880 25 12 -4 -4 189.272 37.2456 23 12 -4 -4 113.246 35.1669 13 12 4 -4 98.5378 34.6066 13 11 4 -4 27.0270 16.2643 5 11 4 -4-28.1157 32.2776 25 11 -4 -4 60.7761 32.6493 13 11 4 -4 24.0595 30.6134 13 10 -4 -4 414.576 29.4485 5 10 -4 -4 384.003 40.5828 13 10 4 -4 401.503 38.5679 25 10 4 -4 461.187 40.2321 13 9 -4 -4 912.865 63.1606 13 9 4 -4 956.891 60.6491 25 9 4 -4 1069.50 62.7989 13 8 -4 -4 34.1940 29.0361 13 8 4 -4 7.96949 26.2885 13 7 -4 -4 2698.84 161.944 13 7 4 -4 3043.76 161.840 13 -7 -4 4 3187.71 161.677 9 -6 -4 4 6.19275 21.8217 9 6 -4 -4-8.32440 29.1629 13 6 4 -4-2.02053 27.5657 13 -5 -4 4-4.17549 21.2764 9 5 -4 -4-13.0980 29.2821 13 5 4 -4-23.5701 26.3811 13 -4 -4 4 9639.80 480.987 9 -4 -4 4 8971.99 478.505 15 -3 -4 4 3487.65 186.407 9 -2 -4 4 7197.09 379.977 9 -1 -4 4 1119.81 60.6754 9 1 -4 -4 943.219 57.5894 1 1 4 -4 1122.81 57.8071 1 -1 -4 4 1057.64 65.7944 24 0 -4 4 3399.13 172.345 24 0 -4 4 3379.53 170.898 9 0 4 -4 3236.67 169.257 1 0 -4 -4 2988.21 169.059 1 1 4 4 491.387 33.0819 14 -1 4 -4 521.739 32.1298 1 -1 -4 -4 514.275 32.4279 1 1 -4 4 524.549 32.9182 14 2 -4 4 816.090 45.7254 14 2 4 4 774.072 45.2981 14 3 -4 4 331.249 24.2096 14 3 4 4 341.011 24.6351 14 4 4 4 1534.05 85.6487 14 4 -4 4 1613.97 85.7963 14 5 -4 4 114.986 17.7771 14 5 4 4 105.518 18.5206 14 6 4 4 292.534 25.4203 14 6 -4 4 320.442 25.9864 14 7 -4 4 72.8529 24.4270 15 7 4 4 84.6032 20.3438 14 7 -4 4 70.2992 21.1263 14 -7 -4 -4 27.2155 33.4034 24 -7 4 -4 80.2445 18.3915 7 8 -4 4 1081.28 58.8908 17 8 4 4 1061.61 63.2971 14 -8 4 -4 1052.71 62.2844 7 8 -4 4 1115.41 64.6522 15 -8 -4 -4 1111.08 58.0722 8 -8 4 -4 1054.27 57.8853 8 8 4 4 1064.82 58.7581 17 -8 -4 -4 1174.54 63.2518 7 8 -4 4 1203.06 63.4225 21 8 -4 4 1059.92 63.2518 14 9 4 4 2011.95 108.253 17 9 -4 4 1936.20 112.108 14 -9 -4 -4 2047.15 107.708 8 -9 4 -4 1997.00 107.681 8 9 4 4 1855.19 111.854 14 -9 4 -4 2024.35 111.980 7 9 -4 4 2081.04 111.827 21 9 -4 4 2050.07 108.305 17 9 -4 4 2183.47 113.604 15 -9 -4 -4 2130.17 112.023 7 10 -4 4 883.434 50.4966 17 10 4 4 900.971 50.4070 17 -10 -4 -4 941.823 55.6486 7 -10 -4 -4 907.018 49.0567 8 10 -4 4 698.640 56.3912 15 -10 4 -4 873.882 48.8399 8 -10 4 -4 939.038 55.3715 7 -11 4 -4 1398.49 80.9330 7 11 -4 4 1430.12 76.8367 17 -11 -4 -4 1467.02 75.6418 8 -11 4 -4 1374.37 75.4202 8 11 -4 4 1160.84 82.2394 15 11 4 4 1392.97 76.8762 17 12 4 4 65.2106 20.7821 17 12 -4 4 79.8385 20.4934 17 12 -4 4 26.6626 26.0503 15 -12 -4 -4 84.0720 14.4116 8 -12 4 -4 68.7075 13.8817 8 -13 4 -4 166.792 17.0404 8 13 4 4 183.154 23.7851 17 13 -4 4 175.801 23.4190 17 -13 -4 -4 190.802 17.4976 8 13 4 4 157.487 30.8952 13 13 -4 4 156.788 30.7248 13 -13 -4 -4 124.828 22.0149 19 14 4 4 374.662 31.8238 17 -14 4 -4 413.097 26.9797 8 14 -4 4 347.674 31.8124 17 15 -4 4 106.539 22.2947 17 15 4 4 106.106 22.1615 17 -15 -4 -4 146.727 16.2683 8 -15 4 -4 125.609 15.7338 8 16 -4 4 78.6067 20.3212 17 16 4 4 98.0128 20.5131 17 -16 4 -4 102.225 13.8424 8 -16 -4 -4 109.519 14.3641 8 17 -4 4 1.67268 16.7716 17 -17 -4 -4 17.6723 11.0273 8 -17 4 -4-5.77804 10.6772 8 18 4 4-3.51897 13.2771 17 18 -4 4 11.6659 13.1619 17 19 -5 -4 58.4832 23.5644 23 18 5 -4 81.1937 26.8250 25 18 -5 -4 87.4809 30.6492 23 17 5 -4 19.9119 31.0964 25 17 -5 -4 51.0744 34.7609 23 16 5 -4 85.1000 22.0795 5 16 5 -4 39.7852 34.4972 25 16 -5 -4 26.5412 37.1632 23 15 5 -4-25.1193 36.3074 25 15 -5 -4 15.1396 39.3566 23 15 5 -4 17.3953 21.5797 5 14 -5 -4 25.6328 37.0339 13 14 5 -4 22.5365 20.8888 5 14 5 -4-9.27698 35.4616 13 14 5 -4-10.1190 37.9745 25 14 -5 -4-2.04611 40.4005 23 -14 -5 4 47.1591 27.0747 9 -14 -5 4 30.0710 23.7554 7 13 5 -4-22.9592 36.4783 25 13 5 -4-1.30584 18.9885 5 -13 -5 4 0.50483 27.2177 9 13 -5 -4 3.21100 35.6054 13 13 5 -4-13.1086 34.5489 13 -12 -5 4 13.4928 26.4008 9 12 5 -4-3.54355 18.0198 5 12 5 -4 18.7034 35.7078 25 12 -5 -4-11.5033 34.6213 13 12 5 -4 15.4989 33.7820 13 11 -5 -4 193.270 37.1615 13 11 5 -4 187.141 34.6133 13 11 5 -4 227.351 36.7917 25 -10 -5 4 54.8912 24.3794 9 10 -5 -4 34.2600 31.7033 23 10 -5 -4 52.3160 33.0763 13 10 5 -4 65.8858 30.5459 13 -9 -5 4 612.003 41.6732 9 9 -5 -4 504.545 44.0933 23 9 -5 -4 482.203 45.0352 13 9 5 -4 558.863 43.7318 13 -8 -5 4 2613.38 133.045 9 8 -5 -4 2409.93 131.785 23 8 -5 -4 2117.58 133.514 13 8 5 -4 2460.03 133.109 13 -7 -5 4-3.77528 22.6184 9 7 -5 -4 30.9571 28.5880 13 7 5 -4 4.89644 27.5557 25 7 5 -4-10.3360 26.9524 13 -6 -5 4 119.891 24.1033 9 6 5 -4 167.058 27.7274 13 6 -5 -4 108.195 30.2819 13 -5 -5 4 4976.30 265.000 9 -4 -5 4 2494.16 120.496 9 -4 -5 4 2115.83 116.465 15 -3 -5 4 10790.8 582.159 9 -3 -5 4 11163.8 580.388 15 -2 -5 4 100.065 23.1828 9 -2 -5 4 99.4650 17.7753 15 -1 -5 4 2519.33 133.091 9 1 5 -4 2601.43 130.721 1 1 -5 -4 2281.60 130.535 1 -1 -5 4 2539.03 137.945 24 0 5 4 665.465 36.8454 14 0 -5 4 677.238 36.9912 14 0 -5 4 623.826 46.7948 24 0 5 -4 612.344 35.4795 1 0 -5 -4 518.274 35.0532 1 1 -5 4 71.0195 15.6835 14 1 5 4 72.3680 16.0968 14 -1 5 -4 75.6743 13.3359 1 -1 -5 -4 64.1882 13.8835 1 -2 5 -4 275.326 21.1917 1 -2 -5 -4 301.727 21.1259 1 2 5 4 227.741 19.7304 14 2 -5 4 241.203 20.4314 14 3 -5 4 1983.16 101.699 14 3 5 4 1805.04 101.465 14 4 5 4 367.848 27.0828 14 4 -5 4 429.720 27.2970 14 5 -5 4 44.5115 23.7400 15 5 -5 4 19.6280 16.6691 14 5 5 4 29.8563 16.0998 14 6 -5 4 16.6141 22.1570 15 6 5 4 11.6556 17.5999 14 6 -5 4 24.2700 17.8170 14 7 -5 4 807.786 44.8490 17 7 5 4 763.538 44.7682 17 7 -5 4 876.668 51.0518 21 7 5 4 759.860 49.1575 14 7 -5 4 818.216 49.2359 14 8 -5 4 28.3915 25.8405 15 8 -5 4 17.3118 13.9698 17 8 5 4 18.6546 13.8896 17 -8 -5 -4 43.0648 10.4128 8 -8 5 -4 41.3287 9.93844 8 8 -5 4 48.4012 28.7676 21 8 -5 4 39.7867 19.9339 14 8 5 4 30.2034 19.6465 14 9 5 4 1410.48 78.2725 17 -9 -5 -4 1477.03 77.5089 8 -9 5 -4 1393.47 77.3847 8 9 -5 4 1431.17 84.6699 15 9 -5 4 1636.09 83.3094 21 9 -5 4 1453.12 78.2821 17 10 -5 4 3402.58 180.364 17 10 5 4 3425.04 180.333 17 -10 -5 -4 3472.23 179.869 8 -10 5 -4 3315.57 179.744 8 10 -5 4 3310.27 185.652 15 10 -5 4 3503.21 183.607 21 11 5 4-5.95736 18.3447 17 11 -5 4-8.60105 26.9623 15 -11 -5 -4-3.73935 13.0300 8 -11 5 -4 1.00621 12.6291 8 11 -5 4 4.72011 18.6816 17 12 5 4 895.093 62.2274 13 12 5 4 944.801 56.5169 17 12 -5 4 864.274 62.1240 13 -12 5 -4 962.744 54.2575 8 -12 -5 -4 1098.23 54.6115 8 12 -5 4 961.237 56.5144 17 13 -5 4 56.5657 20.5844 17 -13 -5 -4 60.8220 14.3724 8 -13 5 -4 32.8606 13.5476 8 13 -5 4 18.5358 28.1034 13 13 5 4 17.6370 20.8390 17 -13 -5 -4 38.5717 20.4679 19 13 5 4 47.4886 28.4957 13 14 -5 4-13.8440 20.6222 17 14 5 4-1.41401 20.6997 17 -14 -5 -4-8.69298 13.7331 8 -14 5 -4 3.52952 13.2351 8 15 -5 4 187.127 23.5295 17 15 5 4 204.862 24.3365 17 -15 -5 -4 272.654 18.8112 8 -15 5 -4 243.647 18.6540 8 16 -5 4 9.21830 17.7994 17 16 5 4 17.5704 18.1638 17 -16 -5 -4 7.44143 11.4574 8 -16 5 -4 7.33323 11.1259 8 17 -5 4 13.3437 15.1803 17 17 5 4-21.8820 15.2380 17 -17 5 -4-3.65337 9.45581 8 18 -6 -4 6.65810 28.2069 23 18 6 -4 9.16576 25.6510 25 17 6 -4 199.724 32.8176 25 16 6 -4 112.778 35.6065 25 15 6 -4 190.255 23.4353 5 15 6 -4 93.6523 37.8983 25 14 6 -4 11.0962 20.4193 5 -14 -6 4 22.0140 27.5148 9 -14 -6 4 46.2686 22.4127 7 14 6 -4 19.5192 36.1929 25 -14 -6 4 29.1124 69.6646 24 -14 6 4 18.3747 21.5746 7 13 6 -4 1.18850 19.5662 5 -13 -6 4 3.09561 28.4307 9 13 6 -4-16.1772 37.0513 25 13 -6 -4 3.81527 39.4829 23 13 -6 -4-27.2157 35.2937 13 13 6 -4-47.7865 34.6629 13 12 6 -4 205.225 20.9759 5 -12 -6 4 198.420 32.3434 9 12 6 -4 121.558 35.6167 13 12 -6 -4 238.031 41.2450 23 12 -6 -4 92.0206 36.9775 13 -11 -6 4 60.3862 29.3534 9 11 6 -4 63.1145 32.8600 13 11 -6 -4 31.7374 36.2088 23 11 -6 -4 41.9981 34.7909 13 -10 -6 4-3.57095 26.6294 9 10 6 -4 20.8167 30.7967 13 10 -6 -4-47.5250 34.9319 23 10 -6 -4 11.2828 32.2229 13 9 6 -4 128.878 32.5600 25 9 6 -4 107.349 30.0423 13 9 -6 -4 121.667 33.2201 23 -9 -6 4 120.375 27.4120 9 9 -6 -4 110.209 31.8897 13 -8 -6 4 1344.48 73.5950 9 8 6 -4 1346.23 72.7746 25 8 -6 -4 1112.91 74.3837 13 8 -6 -4 1244.75 73.8338 23 8 6 -4 1268.92 73.4027 13 8 6 -4 1171.53 65.8185 6 -7 -6 4 166.068 27.1165 9 7 6 -4 164.998 30.1956 25 7 -6 -4 188.193 30.9635 23 7 -6 -4 121.353 30.7480 13 7 6 -4 171.981 28.5814 13 6 6 -4 918.381 55.5971 25 -6 -6 4 856.590 55.7837 9 -5 -6 4 12.0536 23.8638 9 -4 -6 4 7039.53 377.557 24 -3 -6 4 100.066 16.3008 15 -3 -6 4 37.2363 46.2532 24 -2 -6 4 8799.08 456.856 15 -2 -6 4 8320.57 461.090 24 -1 -6 4 5103.01 289.509 24 -1 -6 4 5548.68 286.211 15 0 -6 4 585.983 32.4623 14 0 6 4 488.119 32.4030 14 0 6 -4 568.169 31.3666 1 0 -6 -4 462.994 31.0461 1 0 -6 4 588.447 36.2662 15 1 -6 4 1316.58 57.6428 14 1 6 4 1176.76 57.3674 14 -1 6 -4 1333.00 57.3212 1 -1 -6 -4 1261.14 57.2641 1 2 -6 4 233.245 24.9129 15 -2 6 -4 180.271 17.3731 1 -2 -6 -4 175.584 17.8131 1 2 -6 4 218.398 17.5129 14 2 6 4 173.660 17.1185 14 -3 6 -4 768.578 42.6552 1 3 -6 4 715.342 42.2586 14 3 -6 4 788.538 47.4706 15 -3 -6 -4 786.242 42.7393 1 3 6 4 646.801 41.9158 14 4 6 4 3.11615 13.6503 14 4 -6 4 7.34265 14.5114 14 5 -6 4 19.8534 15.6367 14 5 -6 4-12.9006 25.8687 15 5 6 4 8.79471 16.0122 14 6 -6 4 136.978 20.3233 14 6 -6 4 135.147 14.2538 16 6 -6 4 118.565 25.8672 22 6 -6 4 198.080 28.9556 15 6 6 4 141.210 20.1510 14 7 -6 4 10.1244 12.6311 17 7 6 4 17.1399 12.2716 17 7 -6 4 4.25518 12.5116 16 7 -6 4 24.7767 27.5513 15 7 -6 4 3.53587 17.8297 14 7 6 4 0.99292 17.9307 14 7 -6 4 6.58771 27.6354 21 8 6 4 773.852 44.3010 17 8 -6 4 801.671 44.6703 16 -8 -6 -4 803.997 43.3849 8 -8 6 -4 758.348 43.1900 8 8 -6 4 759.504 52.8583 15 8 -6 4 890.663 51.4342 21 8 -6 4 779.996 44.3303 17 9 6 4 929.144 51.6357 17 -9 -6 -4 936.711 50.5341 8 -9 6 -4 923.900 50.3549 8 9 -6 4 831.133 60.5263 15 9 -6 4 892.141 51.6805 17 9 -6 4 957.610 59.5143 21 -10 -6 -4 72.7966 12.9831 8 -10 6 -4 51.9840 12.1713 8 10 -6 4 80.9886 17.9347 17 10 6 4 107.309 18.0486 17 10 -6 4 16.1886 29.5816 15 10 -6 4 122.867 35.8277 21 11 -6 4 1243.50 68.5140 17 11 6 4 1258.79 68.5694 17 11 -6 4 1124.35 73.3746 13 -11 -6 -4 1329.29 67.1038 8 -11 6 -4 1205.08 66.8823 8 11 -6 4 984.770 74.5071 15 11 6 4 1228.45 73.2626 13 12 -6 4 79.7131 27.4748 13 -12 -6 -4 62.2015 23.0611 19 12 6 4 78.2244 20.1483 17 -12 6 -4 65.4644 13.6209 8 -12 -6 -4 67.6122 14.2208 8 12 -6 4 61.3438 20.1286 17 12 6 4 52.1424 26.9182 13 13 -6 4 270.384 26.1579 17 13 6 4 272.437 26.3175 17 -13 6 -4 289.895 20.7130 8 -13 -6 -4 323.739 21.1371 8 -13 -6 -4 224.442 26.2141 19 14 -6 4 352.482 29.1846 17 14 6 4 357.845 29.1953 17 -14 6 -4 412.784 24.4955 8 15 -6 4 57.5483 19.3775 17 15 6 4 79.0158 19.2488 17 -15 6 -4 112.420 13.0840 8 -15 -6 -4 93.6285 13.3734 8 16 -6 4 7.71994 16.3067 17 16 6 4 7.60712 16.3501 17 -16 -6 -4 7.00986 10.3495 8 -16 6 -4 12.5067 10.0868 8 -17 -6 -4 2.58185 13.4803 18 -17 -6 -4-1.97920 5.96323 2 17 6 4-14.5191 12.7919 17 18 7 -4 79.7958 25.5385 25 17 -7 -4 25.1117 31.8768 23 17 7 -4 60.8205 29.7768 25 16 7 -4-3.18469 33.1201 25 16 -7 -4 17.9322 34.5520 23 15 7 -4 94.3163 20.7348 5 15 -7 -4 47.4494 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34.1147 25 15 6 -5 227.541 23.3749 5 15 6 -5 111.618 38.1852 25 14 6 -5 16.2613 19.9793 5 14 6 -5-33.0140 37.7473 25 13 6 -5 7.63420 18.9557 5 -13 -6 5 6.55625 26.3206 9 13 6 -5 6.56440 38.1401 25 -13 -6 5-5.06689 73.2097 24 -12 -6 5 67.8146 28.9139 9 12 6 -5 89.2000 18.9054 5 12 6 -5 120.758 38.4656 25 12 -6 -5 93.0381 40.1532 23 -11 -6 5 53.8568 26.7158 9 11 -6 -5 1.69273 38.9440 23 -10 -6 5 20.4106 25.5844 9 10 -6 -5 28.2243 35.2817 23 -9 -6 5 116.010 27.5320 9 9 6 -5 44.8438 34.3756 25 9 -6 -5 34.5161 33.6672 23 9 6 -5 88.3371 13.3018 6 -8 -6 5 1851.23 93.9635 9 8 6 -5 1699.51 92.7462 25 8 -6 -5 1540.82 93.2205 23 8 6 -5 1564.52 86.3134 6 7 6 -5 2802.57 139.499 25 -7 -6 5 2900.70 141.446 9 7 -6 -5 2604.72 140.288 23 7 6 -5 2430.28 135.061 6 -6 -6 5 76.3286 24.3462 9 6 6 -5 103.907 30.5995 25 6 -6 -5 82.8834 30.2565 23 -5 -6 5 1973.24 112.606 9 5 6 -5 2107.97 111.864 25 -5 -6 5 1897.98 124.513 24 -4 -6 5 2520.81 139.013 24 -4 -6 5 2610.98 130.873 9 -4 -6 5 2284.97 126.767 15 -3 -6 5 297.625 30.2761 9 -3 -6 5 292.635 23.5580 15 -3 -6 5 303.045 45.9979 24 -2 -6 5 918.384 58.1644 9 -2 -6 5 972.258 55.1597 15 -2 -6 5 994.947 70.3055 24 -1 -6 5-6.19911 15.4970 14 -1 -6 5-9.97542 22.2198 9 -1 -6 5 9.84618 19.6191 15 -1 6 5 9.91216 15.9701 14 -1 -6 5-9.48799 36.1243 24 1 -6 -5 0.14862 12.2629 1 0 -6 -5 70.1837 13.4905 1 0 6 -5 83.3067 13.8825 1 0 -6 5 38.6360 21.0403 15 0 -6 5 12.6614 15.7180 14 0 6 5 27.1673 16.2270 14 1 -6 5 423.559 32.2419 15 1 -6 5 423.378 26.8816 14 1 6 5 339.038 26.7128 14 -1 6 -5 420.313 26.0647 1 -1 -6 -5 391.388 25.8617 1 -2 6 -5 796.140 42.6459 1 -2 -6 -5 784.642 42.7708 1 2 -6 5 735.196 47.6955 15 2 -6 5 695.614 42.5850 14 2 6 5 637.219 42.2240 14 3 6 5 1829.63 113.090 14 3 -6 5 1951.62 113.326 14 -3 6 -5 2313.01 114.614 1 -3 -6 -5 2399.13 114.630 1 3 -6 5 2378.86 117.223 15 4 6 5 216.708 20.8473 14 4 -6 5 190.977 18.2210 16 -4 6 -5 254.252 21.3039 1 4 -6 5 218.918 20.6561 14 5 6 5 8.59646 17.4429 14 5 -6 5 19.1572 12.2166 16 5 -6 5-1.63981 17.3347 14 5 -6 5 1.47045 22.9662 22 6 6 5 674.706 39.5951 17 6 -6 5 767.588 44.2236 14 6 -6 5 725.159 39.6778 16 6 -6 5 805.921 49.8115 15 6 6 5 724.286 43.9703 14 6 -6 5 677.979 39.6256 17 6 -6 5 625.074 46.4737 22 7 -6 5 610.866 38.2241 17 7 6 5 633.605 38.3752 17 7 -6 5 660.642 38.2814 16 7 6 5 687.446 43.2697 14 7 -6 5 704.164 43.7088 14 -7 -6 -5 712.150 37.3288 8 -7 6 -5 682.621 37.1654 8 7 -6 5 658.459 48.4254 15 7 -6 5 614.031 45.6146 21 8 -6 5 863.625 47.1683 17 8 6 5 879.668 46.9571 17 -8 -6 -5 824.377 45.9293 8 -8 6 -5 786.526 45.7954 8 8 -6 5 814.442 56.5104 15 8 6 5 764.443 51.3053 14 8 -6 5 797.938 51.5462 14 8 -6 5 997.864 54.4655 21 9 6 5 268.669 21.9590 17 -9 -6 -5 277.315 19.0528 8 -9 6 -5 253.321 18.6208 8 9 -6 5 261.880 36.3078 15 9 -6 5 240.624 36.0844 21 9 -6 5 254.516 22.1721 17 10 -6 5 49.9985 18.2285 17 10 6 5 45.4174 18.2533 17 -10 -6 -5 77.5057 13.3936 8 -10 6 -5 76.0666 12.9007 8 10 -6 5 63.8700 31.8599 15 10 -6 5 17.9930 34.6764 21 11 6 5 385.022 28.5618 17 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40.2094 23 -13 -7 5-31.2077 67.7509 24 12 7 -5 393.219 27.2771 5 -12 -7 5 388.034 39.1237 9 11 7 -5 978.235 62.6782 25 -11 -7 5 937.318 61.2170 9 -11 -7 5 673.651 89.9011 24 11 -7 -5 783.864 64.3812 23 -10 -7 5 3.58116 28.0470 9 10 7 -5 13.2273 36.3016 25 -10 -7 5 18.2930 69.9744 24 10 -7 -5 26.1293 38.4087 23 -9 -7 5 1003.31 57.1707 9 9 7 -5 935.934 58.6242 25 -9 -7 5 724.597 87.0436 24 9 -7 -5 806.135 59.4566 23 9 7 -5 800.693 47.1651 6 -8 -7 5 977.490 55.1669 9 8 7 -5 945.745 55.9369 25 -8 -7 5 905.341 83.0524 24 8 -7 -5 795.202 57.1051 23 8 7 -5 753.910 45.4477 6 7 7 -5 139.725 33.0620 25 -7 -7 5 139.925 26.9224 9 -7 -7 5 101.293 59.7216 24 7 -7 -5 129.865 34.5282 23 7 7 -5 137.524 13.9377 6 6 7 -5 28.1584 10.6672 6 -6 -7 5 58.4507 13.0782 18 -6 -7 5 49.5218 25.0985 9 -6 -7 5 82.9792 55.6173 24 6 7 -5 96.7472 31.4372 25 6 -7 -5 57.4558 30.4428 23 6 -7 -5 47.3033 17.2317 12 6 -7 -5 45.1504 21.1012 11 5 7 -5 219.498 32.2473 25 -5 -7 5 168.251 50.8837 24 -5 -7 5 191.587 27.2803 9 5 -7 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32.7520 19.5159 22 -3 7 -5 40.5705 13.9927 1 -3 -7 -5 40.4993 13.7718 1 4 -7 5 1711.70 98.5408 14 4 7 5 1684.18 98.4934 14 4 -7 5 1740.18 96.9691 16 -4 7 -5 1943.05 99.2009 1 -4 -7 -5 2050.23 99.6389 1 4 -7 5 1979.96 103.558 15 4 -7 5 1804.41 99.1104 22 -5 -7 -5 286.915 22.3645 1 -5 7 -5 261.257 22.0351 1 5 -7 5 216.405 22.2120 14 5 7 5 187.218 22.0162 14 5 -7 5 215.147 27.6162 22 5 -7 5 224.821 18.6519 16 6 -7 5 60.5135 13.3276 16 6 -7 5 44.9388 18.7634 14 6 7 5 82.3966 19.3221 14 6 -7 5 61.7108 27.4403 22 7 -7 5 1862.53 98.8009 17 7 -7 5 1776.64 102.283 14 7 -7 5 1838.96 99.3104 16 7 7 5 1739.95 102.066 14 7 -7 5 1967.76 106.974 15 7 -7 5 1991.86 103.511 21 8 -7 5 302.933 23.5334 17 8 -7 5 339.096 24.2590 16 -8 -7 -5 336.747 21.2782 8 8 -7 5 318.754 38.3009 15 8 -7 5 332.167 36.9256 21 9 -7 5 90.8555 17.2739 17 9 7 5 91.2062 17.0941 17 -9 -7 -5 100.648 12.8345 8 -9 7 -5 65.8348 12.2826 8 9 -7 5 46.5540 31.2885 15 9 -7 5 115.840 34.2513 21 10 -7 5 667.934 42.4358 17 10 7 5 679.186 42.6038 17 -10 -7 -5 800.667 40.5736 8 -10 7 -5 712.595 40.3518 8 10 -7 5 618.129 52.6051 15 10 -7 5 623.738 53.6909 21 11 -7 5 102.130 19.9871 17 11 7 5 117.893 19.9691 17 -11 -7 -5 149.259 15.0258 8 -11 7 -5 132.566 14.3705 8 -11 -7 -5 122.595 26.6193 19 12 -7 5 200.351 22.6626 17 12 7 5 200.799 22.6473 17 -12 -7 -5 238.828 17.4211 8 -12 7 -5 207.570 16.8823 8 -12 -7 -5 161.513 26.2260 19 13 -7 5 18.7136 18.3861 17 13 7 5-4.23128 18.7331 17 -13 -7 -5-18.3673 20.3711 19 14 -7 5 203.544 18.9710 17 14 7 5 224.316 20.7993 17 -14 -7 -5 160.339 20.4697 19 -15 -7 -5 56.4676 9.38485 2 -16 -7 -5-1.47898 15.5830 18 -16 -7 -5 10.1693 7.22967 2 17 -8 -5-6.30586 28.7030 23 17 8 -5-0.25803 27.3497 25 16 8 -5 73.5572 32.4126 25 16 -8 -5 0.86328 33.5376 23 15 -8 -5 147.498 37.8721 23 15 8 -5 234.292 21.8078 5 15 -8 -5 147.889 20.4547 12 14 8 -5-10.5325 18.6517 5 14 -8 -5 10.5394 38.6980 23 13 8 -5 273.105 45.3360 25 13 -8 -5 246.778 46.6390 23 12 8 -5 1098.58 79.1021 25 12 8 -5 1376.13 69.2546 5 -12 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59.7505 58.9811 24 5 -8 -5 42.3852 31.4376 23 5 -8 -5 39.5482 16.7445 12 -4 -8 5 540.528 61.8894 24 4 8 -5 495.656 40.0789 25 4 8 -5 463.465 26.9779 6 4 -8 -5 366.106 39.5997 23 4 -8 -5 409.176 29.7785 12 4 -8 -5 580.336 34.6435 11 3 8 -5 10.1514 30.0493 25 -3 -8 5-4.86091 17.8900 16 3 8 -5 7.29886 10.3945 6 -3 -8 5 1.26753 12.9635 14 -3 -8 5-18.9299 17.2682 20 -3 -8 5-18.8175 48.0354 24 -2 -8 5 2449.90 131.021 20 2 8 -5 2363.66 133.248 25 -2 -8 5 2592.67 131.235 16 -2 -8 5 2404.19 132.538 15 -2 -8 5 2049.03 139.432 24 -2 -8 5 2428.54 134.812 9 -2 -8 5 2498.57 131.071 14 1 -8 -5 299.194 29.6998 10 -1 -8 5 311.013 30.7370 9 -1 -8 5 330.768 28.9021 15 -1 -8 5 320.727 21.5448 14 -1 -8 5 331.689 24.4334 20 0 -8 -5 2246.91 119.308 10 0 -8 5 2189.20 117.488 16 0 -8 5 2218.82 120.822 15 0 -8 5 2347.30 117.662 20 0 -8 5 2052.64 117.037 14 1 -8 5 709.482 36.7083 16 -1 -8 -5 560.866 34.8232 1 1 -8 5 675.559 42.9258 15 1 -8 5 690.330 37.4822 20 1 -8 5 719.442 38.6652 22 -1 -8 -5 488.666 34.3925 3 1 -8 5 618.334 35.0436 14 2 -8 5 1107.52 64.4973 14 2 -8 5 1221.91 64.8734 16 2 -8 5 1260.84 71.0911 15 -2 -8 -5 1296.06 64.6495 1 2 -8 5 1097.56 66.0597 22 -2 -8 -5 1135.23 63.9716 3 3 -8 5 3961.40 215.982 14 3 -8 5 4177.46 215.289 16 3 -8 5 4415.46 220.071 15 3 -8 5 4116.15 216.215 22 -3 -8 -5 3901.63 215.720 1 4 -8 5 8.28893 22.9676 22 4 -8 5 2.05482 14.3248 16 4 -8 5-18.5763 28.0656 15 -4 -8 -5-6.56424 13.1721 1 4 -8 5-11.3528 14.5487 14 5 -8 5 643.783 40.4440 16 5 -8 5 747.327 51.5136 15 5 -8 5 635.419 42.0502 14 5 -8 5 671.661 46.2512 22 6 -8 5 1216.30 69.0488 16 6 -8 5 1270.50 74.5644 22 6 -8 5 1131.68 70.9066 14 7 -8 5 70.5704 16.3296 16 7 -8 5 34.3458 31.3290 15 7 -8 5 53.7646 33.0234 21 8 -8 5 1156.67 64.8022 16 8 -8 5 1110.56 74.8162 15 8 -8 5 1215.36 71.4733 21 9 -8 5 120.795 32.7383 15 9 -8 5 160.311 35.8545 21 10 -8 5 150.266 18.0017 17 10 -8 5 123.273 37.6196 21 -10 -8 -5 139.378 29.0620 19 11 -8 5 319.938 24.0847 17 -11 -8 -5 333.467 31.9297 19 12 -8 5 50.7815 14.7440 17 -12 -8 -5 69.3587 23.0770 19 -13 -8 -5 420.245 31.5543 19 -14 -8 -5 13.1684 16.5542 19 -15 -8 -5 33.7380 19.5766 18 15 -8 5 89.8064 9.75550 4 -16 -8 -5 53.4798 15.6637 18 -16 -8 -5 129.523 9.27210 2 17 9 -5 9.62955 24.5125 25 17 -9 -5-19.7720 23.9670 23 16 -9 -5 1.70416 29.4799 23 15 9 -5 61.4787 17.6602 5 15 -9 -5-1.13427 34.2688 23 14 9 -5 249.076 41.3808 25 14 -9 -5 224.137 42.6302 23 14 -9 -5 317.004 23.7590 12 13 9 -5 68.4274 38.6700 25 13 9 -5 43.6691 18.2195 5 13 -9 -5 1.95129 38.5848 23 13 -9 -5 43.4413 17.6009 12 12 9 -5 80.2026 18.2349 5 12 9 -5 42.6410 38.8581 25 12 -9 -5 24.3969 39.9647 23 12 -9 -5 84.6792 19.7488 12 11 9 -5 1131.54 72.4833 25 -11 -9 5 850.665 103.363 24 11 -9 -5 1163.80 62.4221 12 11 -9 -5 909.041 72.8897 23 10 9 -5 119.838 40.5721 25 10 -9 -5 77.4287 39.0297 23 10 -9 -5 87.9958 20.4116 12 -10 -9 5 11.4701 75.0219 24 -9 -9 5 333.565 25.8659 16 9 9 -5 322.258 42.7499 25 9 -9 -5 322.682 43.5573 23 9 -9 -5 382.453 27.5986 12 -8 -9 5 1917.39 98.1539 18 8 9 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4 -9 -5 146.037 18.4430 12 -3 -9 5 704.273 38.5781 16 -3 -9 5 661.996 45.2580 9 3 9 -5 683.532 46.8799 25 -3 -9 5 570.341 60.2181 24 -3 -9 5 680.744 39.1279 20 3 9 -5 652.025 34.9765 6 3 -9 -5 537.194 34.5764 3 2 9 -5 387.124 37.5089 25 -2 -9 5 434.909 29.0111 16 -2 -9 5 452.370 35.8710 9 -2 -9 5 405.812 29.3457 20 2 -9 -5 395.742 24.2202 3 1 -9 -5 814.529 45.0060 19 1 -9 -5 754.407 41.9712 2 -1 -9 5 764.159 41.9565 4 1 -9 -5 708.037 42.4551 3 0 -9 -5-0.21779 15.5829 18 0 -9 -5 16.9630 9.23061 2 0 -9 -5 10.9996 11.0674 3 0 -9 5 3.20797 24.3309 15 0 -9 -5-12.0382 18.6618 19 0 -9 5 8.71479 20.4195 22 0 -9 5-13.2072 17.9284 20 -1 -9 -5 1676.00 94.7009 2 1 -9 5 2110.68 96.5876 16 1 -9 5 2015.25 101.658 15 1 -9 5 1902.85 97.6197 22 1 -9 5 1978.01 97.1687 20 -1 -9 -5 1633.19 95.3905 3 -1 -9 -5 1751.14 97.8451 19 -1 -9 -5 1713.88 96.8219 18 2 -9 5 637.064 28.8605 16 2 -9 5 603.495 39.2072 15 2 -9 5 725.991 32.4069 22 -2 -9 -5 347.186 26.4985 3 3 -9 5 223.622 20.1750 16 3 -9 5 214.371 32.7500 15 3 -9 5 218.140 26.2953 22 4 -9 5 2319.17 128.826 16 4 -9 5 2597.92 135.675 15 4 -9 5 2508.44 130.989 22 5 -9 5 1104.67 62.4542 16 5 -9 5 1293.45 73.2989 15 5 -9 5 1102.57 67.8660 22 6 -9 5 308.512 24.4758 16 6 -9 5 324.083 39.2151 15 6 -9 5 311.410 36.0324 22 7 -9 5 534.820 34.9900 16 7 -9 5 572.964 46.0414 21 -7 -9 -5 561.446 42.0170 19 8 -9 5 633.695 39.3086 16 8 -9 5 633.766 49.5573 21 -8 -9 -5 607.782 45.1028 19 9 -9 5 68.9832 36.0244 21 -9 -9 -5 43.4118 26.5659 19 10 -9 5 137.346 38.1226 21 -10 -9 -5 133.399 27.1855 19 -11 -9 -5 138.551 25.6147 19 -12 -9 -5 158.819 23.8670 19 -13 -9 -5 91.1934 19.6958 19 14 -9 5 87.3033 10.5737 4 -14 -9 -5 71.6287 16.3505 19 -15 -9 -5 43.2288 17.5177 18 15 -9 5 47.6619 7.37603 4 16 -10 -5 10.8768 25.8381 23 16 10 -5-7.50789 27.3315 25 15 10 -5 20.4547 32.3788 25 15 10 -5 60.4616 16.0690 5 15 -10 -5 20.6746 30.9774 23 14 10 -5 27.6981 16.7153 5 14 10 -5-18.1927 34.9021 25 14 -10 -5-35.0681 34.6881 23 13 -10 -5 320.553 45.0484 23 13 10 -5 334.405 46.2761 25 12 10 -5 523.643 51.5694 25 12 -10 -5 432.666 51.4535 23 11 10 -5 6.93768 40.1282 25 11 10 -5 24.6013 16.9441 5 11 -10 -5 45.9444 39.1987 23 11 -10 -5 41.2003 15.8516 12 10 10 -5 983.022 65.6775 25 -10 -10 5 980.165 62.8367 9 -10 -10 5 819.874 93.9005 24 10 -10 -5 971.605 53.2993 12 9 10 -5 220.463 40.1935 25 -9 -10 5 119.413 16.8630 18 -9 -10 5 156.206 31.4681 9 -9 -10 5 104.194 17.1340 16 9 -10 -5 171.276 38.8945 23 -9 -10 5 162.205 75.2356 24 9 -10 -5 137.408 18.8736 12 -8 -10 5 86.3787 17.1067 18 -8 -10 5 75.6987 18.1287 16 -8 -10 5 79.4817 29.5973 9 8 10 -5 416.586 40.2977 25 -8 -10 5 336.713 72.3465 24 8 -10 -5 74.3565 37.2185 23 8 10 -5 80.5132 15.0633 6 -7 -10 5 1319.73 70.3182 18 7 -10 -5 1324.53 68.3519 3 -7 -10 5 1278.19 78.6737 9 -7 -10 5 1193.46 70.9096 16 7 10 -5 1352.79 78.4473 25 -7 -10 5 1156.27 101.123 24 7 10 -5 1270.25 69.3490 6 6 -10 -5 308.999 18.8427 3 -6 -10 5 298.450 34.9166 9 -6 -10 5 307.814 25.0691 16 -6 -10 5 226.386 68.3575 24 6 10 -5 282.420 39.9988 25 6 -10 -5 251.606 39.2577 23 6 10 -5 292.917 20.6671 6 5 10 -5 41.5680 11.8152 6 5 -10 -5 38.2458 9.42358 3 -5 -10 5 55.4374 18.6327 16 -5 -10 5 20.2919 27.8313 9 5 10 -5 22.8111 34.4234 25 -5 -10 5 32.6836 55.3773 24 4 -10 -5 371.352 24.7046 3 4 10 -5 506.462 41.2727 25 -4 -10 5 455.124 29.7664 16 -4 -10 5 443.740 38.2584 9 -4 -10 5 435.289 61.8952 24 -4 -10 5 455.459 31.6137 20 4 10 -5 427.591 25.3368 6 3 10 -5 492.707 39.8325 25 -3 -10 5 500.710 30.2754 16 -3 -10 5 411.891 36.5120 9 -3 -10 5 467.086 30.9967 20 3 10 -5 413.090 25.5914 6 3 -10 -5 374.550 25.1411 3 2 10 -5 32.4196 11.6784 6 2 -10 -5 38.8521 11.4026 3 -2 -10 5 42.3127 17.7385 16 -2 -10 5 41.8234 25.7133 9 -2 -10 5 50.4219 9.52802 4 2 -10 -5 43.0788 9.34137 2 -2 -10 5 32.7257 19.7623 20 -1 -10 5 201.734 21.2766 16 1 -10 -5 215.684 14.6018 2 -1 -10 5 186.585 14.7546 4 -1 -10 5 171.952 21.7385 20 1 -10 -5 201.966 16.1340 3 1 -10 -5 165.656 20.6516 19 0 -10 -5 1273.18 70.2476 2 0 -10 5 1344.29 70.4360 4 0 -10 5 1552.55 73.6497 20 0 -10 5 1485.48 74.4467 22 0 -10 -5 1171.44 70.8981 3 0 -10 -5 1368.61 73.2899 19 0 -10 -5 1261.04 72.0623 18 1 -10 5 780.171 40.3429 16 -1 -10 -5 650.082 36.8279 2 1 -10 5 691.179 43.1284 22 1 -10 5 704.790 41.8374 20 -1 -10 -5 598.413 38.1957 3 -1 -10 -5 674.145 42.0233 19 -1 -10 -5 644.743 40.5870 18 -2 -10 -5 1304.59 72.7575 2 2 -10 5 1528.96 74.9895 16 2 -10 5 1445.84 76.8225 22 -2 -10 -5 1323.90 76.8938 19 -2 -10 -5 1302.52 75.5496 18 3 -10 5 2132.96 112.349 16 3 -10 5 2221.33 114.509 22 -3 -10 -5 2031.10 114.274 19 -3 -10 -5 1974.89 113.461 18 4 -10 5 77.6371 17.6669 16 4 -10 5 66.3848 28.0762 22 -4 -10 -5 81.2890 26.3813 19 5 -10 5 746.875 43.5973 16 5 -10 5 730.165 50.6730 22 -5 -10 -5 722.242 49.0929 19 6 -10 5 802.414 46.1692 16 6 -10 5 726.533 54.2374 22 7 -10 5 200.036 21.9979 16 7 -10 5 187.800 38.0649 21 -7 -10 -5 178.282 29.3672 19 8 -10 5 59.4129 20.1506 16 8 -10 5 56.8993 37.1075 21 -8 -10 -5 68.5338 27.7425 19 9 -10 5 36.5750 37.2835 21 -9 -10 -5 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49.6723 23 7 11 -5 587.036 52.3731 25 -7 -11 5 487.812 74.6520 24 7 11 -5 623.795 37.6804 6 7 -11 -5 736.117 36.3924 3 6 -11 -5 20.7796 10.3833 3 -6 -11 5 45.3182 18.1294 16 -6 -11 5 25.0864 28.0865 9 -6 -11 5 19.4868 60.8073 24 6 11 -5 36.6876 36.9960 25 6 11 -5 22.8804 12.8008 6 -5 -11 5 338.444 26.1070 16 5 11 -5 368.905 40.3945 25 5 11 -5 321.914 21.8688 6 -5 -11 5 284.739 28.7992 20 5 -11 -5 317.946 20.9483 3 4 -11 -5 0.48945 10.9319 3 4 11 -5 5.11211 11.7064 6 -4 -11 5-8.56019 18.8410 16 -4 -11 5-19.9215 27.2155 9 4 11 -5-14.9384 34.4700 25 -4 -11 5-2.12834 21.7257 20 3 11 -5 1.25119 11.5478 6 3 -11 -5 2.48804 11.1228 3 -3 -11 5 12.0334 19.1529 16 -3 -11 5 46.1813 27.7080 9 -3 -11 5 0.17197 21.2732 20 2 11 -5 65.8616 12.6657 6 2 -11 -5 43.5391 13.0949 3 -2 -11 5 91.8342 19.2795 16 -2 -11 5 72.9272 10.4106 4 -2 -11 5 101.952 21.3549 20 -1 -11 5 1717.41 91.4943 16 1 -11 -5 1804.31 89.4235 2 -1 -11 5 1737.78 89.4201 4 -1 -11 5 1352.29 92.9686 22 -1 -11 5 1496.21 92.1415 20 1 11 -5 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33.2143 25 15 8 -7-9.96612 16.8649 5 15 -8 -7 10.1150 34.0173 23 15 -8 -7-6.59798 15.9618 12 14 8 -7 168.782 19.5292 5 14 -8 -7 140.476 20.2960 12 13 8 -7 198.308 20.5217 5 13 -8 -7 137.272 41.8816 23 13 -8 -7 205.402 22.8269 12 -12 -8 7 50.1367 14.4435 16 12 8 -7 22.9485 40.4468 25 12 -8 -7-26.9603 40.8605 23 12 -8 -7 59.0553 21.4861 12 -11 -8 7 432.214 31.2691 16 11 8 -7 389.567 48.9756 25 11 -8 -7 353.667 48.9077 23 11 -8 -7 481.724 32.9540 12 11 -8 -7 449.072 33.2569 11 10 -8 -7 42.3941 24.6940 11 -10 -8 7 167.619 66.0592 24 -10 -8 7 67.5111 28.0278 9 10 8 -7 72.7086 42.0100 25 10 -8 -7 48.1320 42.9353 23 10 -8 -7 58.6848 22.2763 12 9 -8 -7 19.5144 26.2107 11 -9 -8 7 7.63203 28.8352 9 9 8 -7-37.0217 41.1756 25 -9 -8 7-62.2205 66.6644 24 9 -8 -7-26.1980 41.4175 23 9 -8 -7-2.52919 21.6351 12 9 8 -7 20.4452 14.5416 6 -8 -8 7 441.775 39.0407 9 8 8 -7 431.555 47.0992 25 -8 -8 7 264.598 67.4438 24 8 -8 -7 261.736 46.3217 23 8 8 -7 367.637 25.7432 6 8 -8 -7 362.016 30.4888 12 8 -8 -7 523.606 35.8492 11 7 -8 -7 60.3355 28.0294 11 -7 -8 7 39.3861 29.8160 9 7 8 -7 90.0225 40.4059 25 -7 -8 7-19.8001 62.5919 24 7 -8 -7 27.6835 39.8105 23 7 -8 -7 38.0553 20.8207 12 7 8 -7 46.3126 13.6482 6 6 8 -7 50.7229 12.7470 6 6 -8 -7 94.1278 28.7588 11 -6 -8 7 61.8509 27.5127 9 6 8 -7 114.346 39.4344 25 -6 -8 7 59.7095 58.0057 24 6 -8 -7 51.3363 21.3248 12 6 -8 -7 31.9833 39.5390 23 5 -8 -7 937.317 53.4679 10 -5 -8 7 1019.20 57.8414 9 5 8 -7 845.680 60.6389 25 -5 -8 7 602.169 73.1565 24 5 8 -7 842.035 47.3939 6 5 -8 -7 720.627 50.4446 12 5 -8 -7 1042.65 55.4623 11 4 -8 -7 207.149 31.0910 11 4 -8 -7 175.172 27.7860 10 -4 -8 7 161.947 28.6513 9 4 8 -7 152.374 37.7606 25 -4 -8 7 100.645 48.0787 24 4 -8 -7 170.446 14.5925 3 4 8 -7 155.000 15.2149 6 -4 -8 7 161.735 18.2680 20 3 -8 -7 1652.16 92.2828 10 3 -8 -7 1562.40 87.4626 2 -3 -8 7 1804.43 95.6486 9 -3 -8 7 1768.56 90.8947 14 3 8 -7 1545.56 95.3119 25 3 -8 -7 1663.58 87.8469 3 -3 -8 7 1639.57 88.8169 20 3 8 -7 1595.95 87.6949 6 3 -8 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22 -3 -8 -7-6.31061 10.4836 2 3 -8 7 8.32618 17.2908 16 3 -8 7 24.0205 29.7932 15 3 -8 7 16.2656 23.4485 22 4 -8 7 1665.12 93.9918 16 4 -8 7 1804.61 102.019 15 4 -8 7 1857.91 97.1354 22 5 -8 7 1284.33 70.8556 16 5 -8 7 1321.71 80.7144 15 5 -8 7 1286.15 76.0195 22 6 -8 7 84.8123 16.7822 16 6 -8 7 67.5999 33.6684 15 -6 -8 -7 102.661 12.8311 2 7 -8 7 1165.04 65.3216 16 -7 -8 -7 1211.72 64.1247 2 7 -8 7 1093.29 71.5539 21 8 -8 7 1098.79 65.4519 17 8 -8 7 1129.62 77.6601 15 -8 -8 -7 1320.73 65.1460 2 8 -8 7 1109.56 72.7714 21 9 -8 7 41.0135 14.8838 17 -9 -8 -7 44.6240 11.8742 2 9 -8 7 25.3154 33.5452 21 10 -8 7 261.898 21.1298 17 -10 -8 -7 331.194 20.0325 2 -10 -8 -7 255.227 32.1261 19 -11 -8 -7 27.8545 11.1388 2 -11 -8 -7 24.4864 25.7605 19 -12 -8 -7 391.098 22.1299 2 -12 -8 -7 214.544 29.1032 19 -13 -8 -7 16.2063 9.85684 2 -13 -8 -7 31.6155 18.1104 19 -14 -8 -7 22.4764 8.34907 2 -14 -8 -7-2.07907 13.1984 19 16 9 -7 46.2292 13.8417 5 15 9 -7 235.495 19.4768 5 15 -9 -7 95.9941 32.3064 23 14 9 -7 1.92838 16.5130 5 14 -9 -7-22.1610 35.2421 23 14 -9 -7 29.9833 15.4268 12 14 9 -7-12.7891 34.2120 25 13 9 -7 177.510 39.3951 25 13 -9 -7 241.355 23.2167 12 12 9 -7 350.525 24.3083 5 12 9 -7 266.278 43.5454 25 12 -9 -7 217.318 43.8110 23 12 -9 -7 287.407 26.1338 12 -11 -9 7 20.9710 15.6394 16 11 9 -7 73.5865 41.2141 25 11 -9 -7-23.5385 41.5294 23 11 -9 -7 40.6579 20.0105 12 -10 -9 7 497.704 40.0426 9 -10 -9 7 403.017 30.0691 16 10 9 -7 384.104 48.0782 25 10 -9 -7 429.733 31.1639 12 -9 -9 7 31.4765 20.9568 16 -9 -9 7-14.8875 28.6137 9 9 9 -7 13.7737 39.9753 25 -9 -9 7 77.2800 66.9989 24 9 -9 -7 13.9611 41.0820 23 9 9 -7 16.5252 14.7118 6 9 -9 -7 26.8179 21.2335 12 8 -9 -7 88.8948 27.5390 11 -8 -9 7 57.1430 22.5938 16 -8 -9 7 123.716 31.2199 9 8 9 -7 87.1991 41.6785 25 -8 -9 7 63.2183 65.3435 24 8 -9 -7 133.872 42.7588 23 8 -9 -7 77.3933 21.6092 12 8 9 -7 56.4795 15.1697 6 -7 -9 7 589.426 42.1834 16 -7 -9 7 740.215 50.0770 9 7 9 -7 660.480 54.5445 25 -7 -9 7 439.861 73.8821 24 7 -9 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9 -7 267.432 19.2767 6 1 -9 -7 123.865 17.7290 3 1 -9 -7 121.889 30.4309 10 -1 -9 7 81.9337 20.8991 16 1 -9 -7 115.096 12.0672 2 -1 -9 7 82.1776 24.3517 15 1 9 -7 50.4686 37.7014 25 -1 -9 7 74.0499 22.8280 22 -1 -9 7 74.4731 18.9002 20 1 -9 -7 55.0560 20.2051 19 0 -9 7 318.211 25.9708 16 0 -9 -7 281.562 19.7623 2 0 -9 7 302.332 32.8343 15 0 9 -7 288.423 41.8129 25 0 -9 7 347.207 28.3638 22 1 -9 7 888.862 47.7024 16 1 -9 7 820.571 54.8224 15 -1 -9 -7 732.743 44.3228 2 1 -9 7 883.385 49.3524 22 2 -9 7 1689.03 91.9508 16 2 -9 7 1684.66 98.4202 15 -2 -9 -7 1752.40 90.4385 2 2 -9 7 1528.51 93.4163 22 3 -9 7 2212.70 113.362 16 3 -9 7 2232.79 120.464 15 -3 -9 -7 2014.10 111.888 2 3 -9 7 2144.74 115.394 22 -4 -9 -7 191.637 17.1080 2 4 -9 7 241.081 21.1334 16 4 -9 7 191.240 34.9777 15 4 -9 7 258.400 31.5192 22 5 -9 7 359.757 26.2761 16 5 -9 7 347.655 39.7450 15 -5 -9 -7 366.554 23.2046 2 5 -9 7 329.448 36.0550 22 6 -9 7 845.381 48.6369 16 6 -9 7 821.339 60.7041 15 7 -9 7 731.056 41.9262 16 7 -9 7 639.409 54.6535 15 7 -9 7 651.101 51.5611 21 -8 -9 -7 34.5642 12.1928 2 8 -9 7 32.3944 16.9856 16 8 -9 7 24.2539 33.8665 21 -8 -9 -7 32.0411 28.8485 19 9 -9 7 1020.90 75.6791 21 -9 -9 -7 986.526 73.9283 19 -10 -9 -7-3.66311 11.3945 2 -10 -9 -7 13.5716 25.9934 19 -11 -9 -7 166.483 14.0995 2 -11 -9 -7 90.8779 25.4444 19 -12 -9 -7 146.043 12.6807 2 -12 -9 -7 54.3055 21.2780 19 -13 -9 -7 2.67597 9.56969 2 -13 -9 -7-7.88896 16.3747 19 15 10 -7 12.2853 13.8649 5 15 10 -7 4.95089 27.1399 25 14 10 -7 161.672 35.7023 25 14 10 -7 291.464 21.1771 5 13 10 -7 48.3657 35.1209 25 13 10 -7 37.1807 15.8931 5 13 -10 -7 47.8894 34.9095 23 12 10 -7 129.598 17.0381 5 12 10 -7 51.8861 37.6442 25 12 -10 -7 71.6960 37.5949 23 12 -10 -7 72.7533 14.6683 12 11 10 -7 408.718 43.1712 25 11 -10 -7 312.615 43.6653 23 11 -10 -7 415.760 24.4948 12 -10 -10 7 79.1288 17.7123 16 10 10 -7 113.598 41.6362 25 10 -10 -7 91.5698 41.3078 23 10 -10 -7 100.799 19.9129 12 -9 -10 7 85.9891 19.6978 16 9 10 -7 115.010 41.7282 25 9 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23.5291 22 -2 -10 7 14.5370 18.3991 20 1 -10 -7 143.738 13.4378 2 -1 -10 7 121.726 22.2548 16 1 10 -7 113.229 38.7144 25 -1 -10 7 88.9145 25.0433 22 1 -10 -7 183.445 19.8702 3 -1 -10 7 113.458 21.5781 20 1 -10 -7 90.3934 20.0248 19 0 -10 7 262.943 24.5442 16 0 -10 -7 212.073 17.2042 2 0 -10 7 222.101 16.4927 4 0 -10 7 276.787 27.4420 22 0 -10 -7 237.788 25.2025 19 1 -10 7 872.054 48.0642 16 -1 -10 -7 794.044 44.6016 2 1 -10 7 721.919 54.1363 15 1 -10 7 841.981 50.0866 22 -1 -10 -7 736.515 50.0201 19 2 -10 7 507.716 30.6569 16 2 -10 7 430.209 39.8355 15 -2 -10 -7 381.752 26.1102 2 2 -10 7 511.991 35.7009 22 -2 -10 -7 398.740 35.3869 19 -2 -10 -7 381.339 30.4134 18 -3 -10 -7 108.152 22.5805 18 3 -10 7 122.142 20.2369 16 3 -10 7 158.251 33.5951 15 -3 -10 -7 159.197 14.5769 2 3 -10 7 122.394 27.6601 22 -3 -10 -7 92.4177 28.0730 19 -4 -10 -7 253.828 19.3589 2 4 -10 7 264.259 23.0818 16 4 -10 7 255.574 36.5516 15 4 -10 7 301.476 33.6172 22 -4 -10 -7 248.357 31.6747 19 5 -10 7 757.696 45.1508 16 -5 -10 -7 804.296 43.0738 2 5 -10 7 741.307 56.5639 15 5 -10 7 641.598 53.3345 22 -5 -10 -7 730.977 52.0426 19 -6 -10 -7 19.3855 12.2916 2 6 -10 7 12.3637 17.8896 16 6 -10 7-12.5451 33.2465 15 6 -10 7 80.5117 35.3767 21 -6 -10 -7 20.0949 28.7182 19 7 -10 7 231.654 22.3107 16 7 -10 7 220.912 37.7900 21 8 -10 7 369.864 27.1677 16 8 -10 7 385.903 39.9432 21 -8 -10 -7 347.463 35.8023 19 -9 -10 -7 20.6263 12.1034 2 9 -10 7 16.6766 34.0324 21 -9 -10 -7 30.5525 26.2013 19 -10 -10 -7 469.385 26.6942 2 -10 -10 -7 340.033 34.1764 19 -11 -10 -7 39.8874 23.6536 18 -11 -10 -7 79.3850 23.0311 19 -12 -10 -7 17.0238 10.2012 2 -12 -10 -7 0.22463 18.0355 19 -13 -10 -7 12.3169 8.38755 2 13 -10 7 11.2805 7.54105 4 -13 -10 -7-12.4399 13.5954 19 14 11 -7 48.0740 13.4088 5 14 11 -7 38.3914 28.7438 25 13 11 -7 57.6773 14.4543 5 13 11 -7 28.7719 32.5368 25 12 11 -7 251.506 20.2533 5 12 11 -7 175.800 37.7199 25 11 11 -7 57.1820 36.8638 25 -10 -11 7 355.698 23.8232 16 10 11 -7 467.318 44.7853 25 -9 -11 7 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37.7172 25 13 -3 -8 45.1905 39.9109 23 12 -3 -8 271.828 24.2291 5 12 3 -8 333.656 24.0873 5 12 -3 -8 169.503 43.1635 23 12 3 -8 167.133 42.2108 25 11 -3 -8-1.95759 17.6878 5 -11 -3 8 5.89814 22.3793 9 11 3 -8-3.37995 39.2942 25 11 -3 -8-35.8973 39.3813 23 10 -3 -8 1147.71 62.0996 5 -10 -3 8 1258.10 67.8373 9 10 3 -8 965.283 72.8060 25 10 -3 -8 922.531 74.0485 23 9 3 -8 78.8787 39.7691 25 -9 -3 8 117.392 23.8542 9 9 -3 -8 49.5065 39.5068 23 -8 -3 8 18.9975 21.6877 9 8 3 -8-28.5777 38.3115 25 8 -3 -8-53.7951 38.9849 23 8 3 -8 8.38845 12.8229 6 7 -3 -8 1998.62 111.999 25 7 3 -8 1868.24 112.772 25 7 -3 -8 1749.39 112.968 23 7 3 -8 1950.08 104.873 6 7 3 -8 1918.96 105.692 12 7 -3 -8 2009.92 106.668 12 -6 -3 8 67.2852 22.3979 9 6 3 -8 36.0938 37.4938 25 6 -3 -8 44.3185 37.7277 25 6 -3 -8 20.9948 37.6397 23 6 3 -8 51.5364 15.7853 12 6 -3 -8 44.0037 19.4492 12 6 3 -8 48.5219 10.7285 6 5 -3 -8 309.294 40.8424 25 -5 -3 8 295.312 27.3615 9 5 3 -8 244.255 17.5036 6 5 -3 -8 255.993 24.0246 12 5 3 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4 -8 317.714 42.9080 25 4 4 -8 354.339 22.3883 6 4 -4 -8 363.524 34.1280 11 3 4 -8 1012.09 64.2545 25 3 4 -8 922.453 50.6568 6 2 4 -8-4.11779 37.7084 25 2 -4 -8 39.0183 17.3452 1 1 4 -8 2018.16 147.230 25 1 4 -8 3082.80 144.473 1 1 -4 -8 2880.71 144.269 1 -1 -4 8 2770.73 145.464 14 -1 4 8 2668.19 145.750 14 1 -4 -8 2377.82 144.092 11 0 -4 8 1157.68 55.7552 14 0 4 -8 1021.96 63.6837 25 0 -4 -8 779.426 47.8225 2 0 4 8 1089.89 56.2679 14 0 4 -8 884.452 52.1119 1 0 -4 -8 877.417 52.0941 1 0 -4 -8 852.480 55.4134 11 -1 -4 -8 1814.11 108.671 10 -1 -4 -8 1894.30 103.764 2 -1 4 -8 1926.43 112.836 25 1 -4 8 2104.68 108.488 14 1 4 8 2007.81 108.384 14 -1 4 -8 2096.63 107.487 1 -1 -4 -8 2113.76 107.440 1 -1 -4 -8 1792.77 108.379 11 -2 -4 -8 2470.32 134.458 10 2 -4 8 2340.25 131.003 16 -2 -4 -8 2375.64 129.995 2 2 -4 8 2650.44 134.312 14 2 4 8 2455.73 134.074 14 -2 4 -8 2713.69 133.779 1 -2 -4 -8 2607.38 133.637 1 -3 -4 -8 53.8645 11.3714 2 -3 -4 -8 70.5847 28.0560 10 3 -4 8 63.8843 14.4781 16 3 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168.244 43.0471 25 11 -3 -9 150.892 44.7875 23 11 3 -9 224.471 22.5217 12 11 -3 -9 208.323 25.5883 12 10 3 -9 54.3150 42.1726 25 10 -3 -9 20.4873 43.1169 23 10 3 -9 14.7172 18.2658 12 10 -3 -9 25.6890 23.1933 12 -9 -3 9-3.04953 22.1570 9 9 3 -9 36.6129 41.8334 25 9 -3 -9 53.9730 42.7593 23 9 3 -9 35.8016 18.0458 12 9 -3 -9 20.7495 22.5201 12 -8 -3 9 32.5180 22.1940 9 8 3 -9-2.14700 41.9208 25 8 -3 -9 12.1336 39.1539 25 8 -3 -9-4.66527 41.4464 23 8 3 -9 11.6716 18.0056 12 8 -3 -9-2.41869 22.2518 12 8 3 -9 0.56929 13.3364 6 -7 -3 9 41.9751 22.4028 9 7 3 -9 12.9873 41.8919 25 7 -3 -9 75.5999 40.6941 25 7 -3 -9 17.3242 20.1736 12 7 3 -9 28.7675 17.3139 12 7 3 -9 23.0198 12.1745 6 -6 -3 9 181.257 24.9744 9 6 3 -9 204.352 42.8527 25 6 -3 -9 240.758 42.8463 25 6 3 -9 152.116 14.6143 6 6 -3 -9 143.478 22.5031 12 6 3 -9 133.215 19.2173 12 5 3 -9 366.217 21.6162 6 5 -3 -9 317.225 28.0093 12 5 3 -9 319.576 25.0330 12 4 3 -9 239.519 16.0614 6 4 -3 -9 195.839 24.2067 12 4 3 -9 211.873 20.4012 12 4 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138.725 28.0419 14 8 3 9 156.541 28.3501 14 9 3 9 187.654 22.5368 17 9 -3 9 164.859 22.6194 17 -9 -3 -9 214.628 15.8704 2 10 -3 9 148.939 21.3983 17 10 3 9 157.057 21.8933 17 -10 -3 -9 186.227 14.3535 2 11 -3 9 1.14156 18.2411 17 11 3 9 23.9721 19.3928 17 -11 -3 -9 7.11428 9.32796 2 12 -3 9 863.185 50.2194 17 12 3 9 881.514 50.5392 17 13 -3 9 259.053 22.4588 17 13 3 9 265.138 22.5055 17 14 -3 9 66.7148 14.9653 17 14 3 9 68.9924 15.3876 17 -14 -3 -9 37.1477 13.1086 19 16 4 -9 63.8144 16.5208 5 16 4 -9 34.5785 26.3122 25 16 4 -9 33.4410 11.6891 12 16 -4 -9 47.7618 18.0870 11 15 4 -9 29.6055 17.0289 5 15 4 -9 25.3814 31.4125 25 15 -4 -9 0.22992 33.9703 23 15 4 -9 26.8207 14.0408 12 14 4 -9 59.6993 17.4413 5 14 4 -9 33.0130 35.0594 25 14 -4 -9 44.5744 38.0309 23 14 4 -9 14.6827 15.6116 12 13 4 -9 74.1133 17.5012 5 13 4 -9 20.3358 37.9611 25 13 -4 -9 26.6010 40.5700 23 13 4 -9 47.7708 16.7503 12 12 4 -9 51.4505 17.6682 5 12 4 -9-1.34796 39.7876 25 12 -4 -9 62.2522 41.9162 23 12 4 -9 25.5565 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14 -1 4 9 1152.44 60.8698 14 1 -4 -9 856.950 59.7375 11 0 -4 -9 48.5873 31.8442 11 0 -4 -9 35.3982 29.3006 10 0 -4 9 33.5792 23.7118 14 0 4 -9 65.5443 45.2273 25 0 4 9 45.5124 24.6848 14 0 -4 -9 35.0663 10.6934 2 0 4 -9 48.9778 19.0098 1 0 -4 -9 59.6620 20.6255 1 -1 -4 -9 1713.73 104.281 10 -1 4 -9 1640.97 109.893 25 -1 -4 -9 1800.03 98.3836 2 1 -4 9 1924.20 103.596 14 1 4 9 1815.58 103.598 14 -1 4 -9 1986.31 102.626 1 -1 -4 -9 2013.69 102.750 1 -2 -4 -9 1586.15 91.6804 10 2 -4 9 1500.52 87.0800 16 -2 -4 -9 1564.43 85.9381 2 2 -4 9 1721.04 91.3471 14 2 4 9 1592.12 91.1791 14 -2 4 -9 1819.23 90.9805 1 -2 -4 -9 1736.39 90.6102 1 -3 -4 -9 349.618 36.1336 10 3 -4 9 295.756 24.3446 16 -3 -4 -9 357.391 22.2163 2 3 -4 9 371.136 31.6443 14 3 4 9 358.027 31.8114 14 -3 4 -9 385.124 29.0551 1 -3 -4 -9 383.094 29.1211 1 -4 -4 -9 31.4293 31.2119 10 -4 4 -9 65.2149 19.9499 1 -4 -4 -9 78.7793 20.1630 1 4 -4 9 54.0614 22.4566 14 4 4 9 24.3002 22.7614 14 -4 -4 -9 56.6956 12.0573 2 -5 -4 -9 205.291 24.4735 1 -5 -4 -9 149.375 33.1895 10 -5 -4 -9 190.203 15.1798 2 5 -4 9 128.658 25.8738 14 5 4 9 136.463 26.6437 14 -5 4 -9 142.508 23.8890 1 6 -4 9 29.1814 18.0157 17 6 4 9 33.4589 18.5352 17 6 -4 9 53.3223 24.4357 14 6 4 9 34.1162 24.5705 14 -6 4 -9 34.0466 21.4756 1 -6 -4 -9 49.5648 22.6811 1 -6 -4 -9 59.5476 11.8250 2 -7 4 -9 69.0567 22.5810 1 -7 -4 -9 44.2313 22.5417 1 7 -4 9 5.49119 18.8201 17 7 4 9 2.95737 18.5602 17 7 -4 9-2.92328 31.1131 15 7 -4 9 32.9337 24.8149 14 7 4 9 31.7725 24.7846 14 -7 -4 -9 52.5009 12.2918 2 -8 4 -9 85.1473 23.1529 1 8 -4 9 54.9602 19.5261 17 8 4 9 67.5971 19.8943 17 -8 -4 -9 86.1473 23.5581 1 8 -4 9 59.0840 31.9728 15 8 -4 9 107.537 27.0978 14 8 4 9 77.1099 26.7266 14 -8 -4 -9 72.6048 12.4721 2 9 -4 9 134.259 20.9496 17 9 4 9 141.351 21.4358 17 -9 -4 -9 179.701 14.7941 2 10 -4 9 169.219 21.8252 17 10 4 9 205.076 22.9074 17 -10 -4 -9 231.318 16.4158 2 11 -4 9 169.702 21.6574 17 11 4 9 198.889 22.4255 17 -11 -4 -9 232.029 15.4789 2 12 -4 9 422.770 33.2948 17 12 4 9 461.222 33.5337 17 13 -4 9 263.830 21.7843 17 13 4 9 279.714 22.1605 17 14 -4 9 128.833 14.5286 17 14 4 9 129.759 14.7857 17 16 -5 -9 152.212 16.5365 12 16 5 -9 22.6776 27.1266 25 15 -5 -9 91.2408 20.5172 11 15 5 -9 80.4855 31.4637 25 15 -5 -9 87.1176 17.9510 12 14 5 -9 36.8814 34.2361 25 14 -5 -9-14.4468 37.5614 23 14 -5 -9 22.8794 19.3758 12 14 -5 -9 25.3358 23.3537 11 13 5 -9 31.2200 37.4733 25 13 -5 -9 27.0387 41.4971 23 13 -5 -9 87.2287 22.1666 12 12 5 -9 201.341 43.1925 25 12 -5 -9 184.248 44.5926 23 12 -5 -9 257.608 26.1978 12 11 5 -9 233.579 44.7016 25 11 -5 -9 261.244 27.0637 12 -10 -5 9 120.078 26.5861 9 10 5 -9 52.6704 43.5344 25 10 -5 -9 122.249 24.0178 12 -9 -5 9 36.4728 24.8478 9 9 -5 -9-2.42159 24.0398 12 9 5 -9 17.1579 14.3933 6 -8 -5 9 467.017 35.6718 9 8 5 -9 390.235 26.4531 6 8 -5 -9 390.035 32.4630 12 -7 -5 9 66.4676 24.5975 9 7 -5 -9 23.5836 22.8640 12 7 5 -9 24.4781 12.9305 6 7 -5 -9 53.0145 30.5304 11 6 5 -9 385.306 46.8915 25 6 5 -9 317.411 22.0696 6 6 -5 -9 307.617 29.6603 12 6 -5 -9 343.435 36.4501 11 5 5 -9 326.939 46.2117 25 5 5 -9 275.482 19.9395 6 5 -5 -9 336.273 34.5489 11 4 -5 -9-3.00652 30.2307 11 4 5 -9 33.4119 12.0717 6 4 5 -9-43.8384 43.2301 25 -3 5 9 636.740 44.4740 14 -3 -5 9 704.474 43.5794 14 3 5 -9 628.057 56.4337 25 3 5 -9 593.418 35.1143 6 2 -5 -9 1534.01 83.9704 10 -2 5 9 1524.88 83.2170 14 -2 -5 9 1613.48 82.7808 14 2 5 -9 1355.54 75.8285 6 1 5 -9 6.72596 44.3886 25 -1 -5 9 24.5898 23.8972 14 -1 5 9 8.48560 25.1055 14 1 -5 -9-0.31237 17.6891 1 0 -5 -9 433.452 28.6786 2 0 5 -9 485.358 33.8741 1 0 -5 -9 481.515 34.0307 1 0 5 -9 599.936 55.0477 25 0 -5 9 635.989 37.9574 14 0 5 9 543.459 37.5359 14 0 -5 -9 475.835 42.8084 11 -1 -5 -9 97.7336 20.2770 1 -1 -5 -9 148.109 33.0676 10 1 -5 9 92.1233 19.8250 16 -1 5 -9 147.918 46.7814 25 1 -5 9 144.916 24.0050 14 1 5 9 124.077 23.8742 14 -1 -5 -9 92.6825 13.3449 2 -1 5 -9 118.980 20.5761 1 -2 5 -9-19.0000 18.6811 1 -2 -5 -9-12.0767 32.9693 10 -2 -5 -9 27.4314 19.6901 1 2 -5 9-13.4791 16.8220 16 2 -5 9 10.8135 21.9508 14 2 5 9-16.8340 22.8818 14 -2 -5 -9-1.44840 11.6303 2 -3 -5 -9 405.841 39.0113 10 3 -5 9 343.628 27.1300 16 -3 -5 -9 402.196 25.1845 2 3 -5 9 429.699 33.6482 14 3 5 9 413.639 33.4030 14 -3 5 -9 417.276 31.1008 1 -3 -5 -9 449.533 31.8785 1 -4 -5 -9 350.514 38.2231 10 4 -5 9 262.212 23.3568 16 -4 -5 -9 386.241 22.5452 2 4 -5 9 309.327 30.6653 14 4 5 9 316.362 30.7494 14 -4 5 -9 354.941 28.4449 1 -4 -5 -9 384.749 29.3223 1 5 -5 9 37.4644 17.5850 17 5 5 9 25.6621 18.0653 17 -5 5 -9 22.7816 19.5815 1 -5 -5 -9 16.9601 20.0179 1 5 -5 9 34.0564 23.3090 14 5 5 9 39.7521 23.2390 14 -5 -5 -9 25.9734 12.4787 2 -6 -5 -9 8.58385 12.2952 2 6 -5 9 18.8493 17.9469 17 6 5 9 24.5785 18.1807 17 -6 5 -9 8.52090 19.6305 1 6 -5 9 12.1281 23.7788 14 6 5 9-3.78037 25.1223 14 -6 -5 -9-1.58179 20.8393 1 -7 -5 -9-8.99800 12.2544 2 7 -5 9-16.8563 18.0314 17 7 5 9 17.4106 18.3383 17 7 -5 9 38.8268 29.9011 15 7 -5 9-7.07801 24.4426 14 7 5 9-14.8596 25.0021 14 -7 5 -9 1.53916 19.9164 1 -7 -5 -9 12.9930 21.1396 1 8 -5 9 182.097 21.7760 17 8 5 9 205.357 21.8988 17 -8 -5 -9 226.413 16.9953 2 9 -5 9 42.6419 18.4012 17 9 5 9 53.8398 18.5195 17 -9 -5 -9 46.4232 11.9202 2 10 -5 9 28.7715 18.1284 17 10 5 9 10.9428 17.9659 17 -10 -5 -9 59.0523 11.2923 2 11 -5 9 10.9353 17.2149 17 11 5 9-1.78125 17.6037 17 -11 -5 -9 23.5799 9.99130 2 12 -5 9 147.269 18.9001 17 12 5 9 139.914 19.3159 17 -12 -5 -9 188.565 12.9465 2 13 -5 9 159.077 16.8516 17 13 5 9 185.578 17.4197 17 16 6 -9 58.9512 25.6560 25 16 -6 -9 67.0400 14.5550 12 15 6 -9 27.6432 30.7478 25 15 -6 -9 46.1918 16.4636 12 14 -6 -9 10.4044 19.3138 11 14 6 -9 59.9765 33.9535 25 14 -6 -9 91.3521 18.9906 12 13 -6 -9 32.1576 24.3318 11 13 6 -9 15.8356 37.5299 25 13 -6 -9 52.3202 20.0691 12 12 6 -9 57.6878 39.4143 25 12 -6 -9 115.126 22.2694 12 12 -6 -9 123.940 27.1862 11 11 -6 -9 21.6922 22.7530 12 11 -6 -9-11.7081 27.7861 11 -10 -6 9 205.181 28.6419 9 10 -6 -9 145.036 45.9626 23 10 -6 -9 206.004 26.0343 12 10 -6 -9 187.637 31.8938 11 9 -6 -9 459.486 37.5291 10 -9 -6 9 499.555 39.1781 9 9 -6 -9 425.601 34.1952 12 9 -6 -9 537.299 40.8240 11 8 -6 -9 34.4376 31.0498 11 -8 -6 9 39.2486 26.0686 9 8 6 -9 24.2219 43.9917 25 8 -6 -9 34.6131 23.4183 12 7 -6 -9 121.463 32.0762 11 -7 -6 9 131.863 27.1574 9 7 6 -9 52.5146 42.4107 25 7 -6 -9 104.526 23.4742 12 6 6 -9 71.3840 13.2973 6 6 -6 -9 63.0892 30.7909 11 -6 -6 9 105.405 26.7794 9 6 6 -9 54.5738 41.6816 25 6 -6 -9 39.9630 23.1828 12 5 -6 -9 22.4166 31.7962 11 5 6 -9 3.82435 12.0851 6 5 -6 -9-4.48460 31.5289 10 5 6 -9-3.48806 43.6021 25 5 -6 -9 6.27117 22.4138 12 4 -6 -9 188.419 34.0512 11 4 -6 -9 218.022 35.5607 10 4 6 -9 197.792 44.8889 25 4 6 -9 173.558 15.8163 6 3 -6 -9 352.114 37.6090 10 -3 6 9 332.192 32.9428 14 -3 -6 9 407.907 32.1155 14 3 6 -9 394.308 48.6420 25 3 6 -9 303.715 21.8464 6 3 -6 -9 347.250 39.0259 11 2 -6 -9 153.457 35.2498 11 2 -6 -9 210.727 34.9082 10 -2 6 9 203.117 28.8237 14 -2 -6 9 124.814 24.5097 15 -2 -6 9 227.344 27.3580 14 2 6 -9 164.140 46.2481 25 2 6 -9 175.279 15.8365 6 1 -6 -9 656.763 46.4661 10 1 -6 -9 537.818 33.6413 2 1 6 -9 511.895 56.9248 25 -1 -6 9 723.231 41.7626 14 -1 6 9 635.322 42.5206 14 0 -6 9 633.868 46.7581 16 0 6 -9 947.425 48.5763 1 0 -6 -9 892.366 48.4900 1 0 6 -9 507.040 63.5697 25 0 -6 9 780.472 49.3841 14 0 6 9 736.830 49.7286 14 1 -6 9 865.723 55.5108 16 -1 6 -9 1093.17 57.6415 1 -1 -6 -9 1036.53 57.4178 1 -1 6 -9 897.888 70.9852 25 1 -6 9 1006.90 58.2341 14 1 6 9 886.276 58.5167 14 -2 -6 -9 463.399 44.3671 10 2 -6 9 460.868 32.6842 16 -2 -6 -9 497.113 29.8646 2 -2 6 -9 549.422 35.5753 1 -2 -6 -9 572.768 35.9752 1 2 -6 9 519.880 36.8388 14 2 6 9 465.147 36.9560 14 -3 -6 -9 199.297 34.6951 10 3 -6 9 162.593 20.3624 16 -3 -6 -9 244.272 17.8688 2 3 -6 9 175.586 32.5010 15 -3 6 -9 255.533 24.1625 1 -3 -6 -9 314.319 24.7687 1 3 -6 9 184.139 25.2083 14 3 6 9 154.979 25.2931 14 4 -6 9 30.5338 16.7409 17 4 6 9 60.8013 17.4398 17 -4 6 -9 6.47475 19.0294 1 -4 -6 -9 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79.9480 15.1611 17 12 6 9 76.0850 15.6780 17 -12 -6 -9 75.9710 9.63070 2 13 6 9 18.4953 12.7609 17 -13 -6 -9 12.0733 6.25786 2 -13 -6 -9 10.3564 15.9138 19 15 7 -9 27.4284 15.0166 5 15 7 -9 1.51632 28.2932 25 15 -7 -9 0.40169 14.9856 12 14 7 -9 52.9967 15.7968 5 14 7 -9 34.0544 32.7146 25 14 -7 -9 29.7786 17.7004 12 13 7 -9 63.5939 16.2869 5 -13 -7 9 27.3859 14.2988 16 13 -7 -9 68.5295 19.6836 12 12 -7 -9 8.57319 25.0188 11 12 -7 -9 16.0099 20.2605 12 11 -7 -9 316.627 28.8269 12 11 -7 -9 341.752 32.9966 11 10 -7 -9 28.4287 28.4059 11 10 7 -9 6.24692 42.2324 25 10 -7 -9 59.7323 22.8637 12 9 -7 -9 105.142 29.8882 11 -9 -7 9 51.5443 25.7477 9 9 7 -9 76.5433 43.7852 25 9 7 -9 70.2168 15.5168 6 9 -7 -9 110.303 23.7993 12 8 -7 -9 209.109 32.9600 11 8 -7 -9 161.639 27.6756 10 -8 -7 9 207.685 29.9729 9 8 7 -9 169.143 45.7157 25 8 7 -9 167.826 18.0219 6 8 -7 -9 150.280 25.2153 12 7 -7 -9 267.994 35.0459 11 7 -7 -9 221.099 32.0779 10 -7 -7 9 221.323 31.4505 9 7 7 -9 210.651 46.3291 25 7 -7 -9 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12.3792 19.2889 1 -5 -4 -10 23.5605 20.0575 1 5 -4 10 20.5780 23.6818 14 5 4 10 31.0387 24.2622 14 -5 -4 -10 7.93969 12.2560 2 6 -4 10 105.539 19.8884 17 6 4 10 107.209 20.0592 17 -6 4 -10 115.615 21.2571 1 -6 -4 -10 92.0944 21.5305 1 6 -4 10 105.466 25.7350 14 6 4 10 78.4000 26.7094 14 -6 -4 -10 85.1881 13.2226 2 7 -4 10-6.21419 18.8940 17 7 4 10 39.0719 19.3041 17 -7 -4 -10 0.08823 11.4816 2 8 -4 10 51.0110 18.8570 17 8 4 10 60.6465 19.3399 17 -8 -4 -10 78.3912 11.7963 2 9 -4 10 67.0207 18.3151 17 9 4 10 58.2594 18.9067 17 -9 -4 -10 63.3807 11.1650 2 10 -4 10 7.36259 17.0022 17 10 4 10 1.87921 17.1218 17 -10 -4 -10-1.56625 9.25992 2 11 -4 10 22.9978 16.3576 17 11 4 10 57.9718 16.6758 17 -11 -4 -10 31.7824 8.00484 2 12 -4 10-5.58504 14.7983 17 12 4 10 11.6915 15.1591 17 13 -4 10 299.569 18.1730 17 13 4 10 296.615 18.5133 17 15 5 -10 5.27762 14.5164 5 15 5 -10 24.3747 28.0121 25 15 -5 -10 9.66166 15.1846 12 14 -5 -10 48.8482 21.8529 11 14 5 -10 57.8649 15.7151 5 14 5 -10 7.22888 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435.973 27.8903 6 5 -6 -10 534.458 44.6280 11 4 -6 -10 176.251 38.4650 11 4 -6 -10 255.381 36.0089 10 -4 6 10 226.310 29.6551 14 -4 -6 10 232.729 28.7800 14 4 6 -10 148.326 48.2787 25 4 6 -10 179.561 16.6736 6 3 6 -10 76.1007 13.1923 6 3 -6 -10 64.1236 35.5940 11 3 -6 -10 108.641 34.4183 10 3 6 -10 138.769 50.4515 25 -3 6 10 95.5400 27.4541 14 -3 -6 10 59.8839 25.2364 14 2 -6 -10 696.475 52.4564 10 2 6 -10 563.801 62.9306 25 -2 -6 10 742.823 46.4922 14 -2 6 10 702.151 47.3721 14 2 6 -10 656.699 38.2801 6 1 -6 -10 220.762 37.8815 10 -1 -6 10 191.878 25.0423 16 -1 -6 10 121.220 27.8648 15 -1 -6 10 271.298 27.4918 14 -1 6 10 240.162 28.2177 14 1 6 -10 297.180 51.8355 25 1 6 -10 204.527 17.0822 6 0 -6 10 313.088 27.6855 16 0 -6 10 234.094 33.3153 15 0 -6 10 408.035 30.8325 14 0 6 10 402.871 31.7948 14 0 6 -10 273.258 53.8495 25 -1 -6 -10 726.591 53.5428 10 1 -6 10 630.012 43.7445 16 -1 6 -10 818.369 46.1035 1 -1 -6 -10 801.178 46.6922 1 -1 -6 -10 700.714 41.0977 2 1 -6 10 569.799 50.1786 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11 9 4 -11 85.0452 45.0518 25 9 -4 -11 98.4445 23.4279 12 8 4 -11 171.154 48.5241 25 8 4 -11 185.109 17.3282 6 8 -4 -11 214.936 25.7084 12 7 4 -11 15.1736 12.9244 6 6 4 -11 173.527 16.1569 6 5 -4 -11 10.0606 34.0942 11 -5 4 11 18.4046 26.4054 14 -5 -4 11 29.6817 25.6377 14 5 4 -11 6.82425 24.2632 11 5 4 -11-10.7886 12.0041 6 4 4 -11 81.3959 24.4675 11 4 4 -11 82.0265 12.6410 6 4 -4 -11 89.1099 34.7857 11 4 4 -11 29.3863 53.2676 25 -4 4 11 83.8755 28.2649 14 -4 -4 11 71.4537 27.2020 14 -3 4 11 649.577 45.9651 14 -3 -4 11 652.879 44.8988 14 3 4 -11 415.611 62.3136 25 3 4 -11 549.842 31.8033 6 3 4 -11 433.748 38.8659 11 3 -4 -11 589.331 47.6549 11 2 4 -11 65.9109 12.0319 6 2 -4 -11 68.7126 35.2096 11 2 4 -11-28.0034 52.0427 25 -2 4 11 53.0066 27.8152 14 -2 -4 11 37.0830 26.2108 14 1 4 -11 58.3751 12.0732 6 1 -4 -11 89.5022 36.9725 11 1 -4 -11 86.2626 36.3737 10 -1 -4 11 85.3085 25.4753 14 -1 4 11 47.1430 26.2570 14 0 -4 -11 326.564 39.7516 10 0 -4 11 222.499 24.4635 16 0 -4 11 306.195 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7.68517 9.80517 2 9 -4 11-7.64115 15.8578 17 9 4 11-15.4406 16.4877 17 10 -4 11 1.93797 14.9016 17 10 4 11 7.02524 15.3612 17 11 -4 11 13.4875 13.6453 17 11 4 11 2.73501 14.0296 17 14 -5 -11 13.1594 19.1334 11 14 5 -11 53.5666 13.2292 5 -14 -5 11 26.2494 12.4394 16 14 5 -11 25.6465 29.0844 25 13 -5 -11-2.93497 22.4829 11 13 5 -11 11.3141 14.1258 5 13 5 -11-25.3362 33.4174 25 12 -5 -11 83.4267 26.1764 11 12 5 -11 133.170 16.1572 5 12 5 -11 39.6611 37.5312 25 11 -5 -11 24.7639 26.7643 11 11 5 -11 53.0081 40.7659 25 10 -5 -11-22.9002 29.5336 11 10 -5 -11 20.9774 25.4683 10 10 5 -11-0.47169 42.2688 25 9 -5 -11 26.1532 31.2447 11 9 -5 -11-12.8200 28.2823 10 9 5 -11-50.0352 44.8409 25 8 5 -11 485.069 30.4956 6 8 -5 -11 561.759 42.7910 11 7 -5 -11 196.963 36.4681 11 7 5 -11 203.709 17.6548 6 6 -5 -11 159.186 36.0976 11 6 -5 -11 151.013 34.5636 10 -6 5 11 98.7527 27.3911 14 -6 -5 11 128.566 26.5063 14 6 5 -11 144.641 14.9151 6 5 5 -11 98.4326 24.6971 11 5 -5 -11 191.928 35.8880 10 5 5 -11 136.801 53.2200 25 -5 5 11 190.811 29.9033 14 -5 -5 11 195.624 28.5705 14 5 5 -11 178.051 15.8600 6 4 5 -11 46.8842 12.3833 6 4 -5 -11 79.5133 36.8077 10 4 5 -11 90.5309 52.5417 25 -4 5 11 16.2370 28.4358 14 -4 -5 11 58.4969 27.2221 14 3 -5 -11 469.534 44.5636 10 -3 5 11 535.624 40.5982 14 -3 -5 11 542.539 39.4957 14 3 5 -11 407.642 59.7809 25 3 5 -11 439.335 27.5985 6 3 -5 -11 420.716 45.7544 11 2 -5 -11 299.902 42.1566 11 -2 -5 11 364.742 32.7440 14 -2 5 11 329.073 33.5809 14 2 5 -11 220.606 54.5654 25 2 5 -11 320.735 21.2381 6 -1 -5 11 120.045 21.9344 16 1 5 -11 88.1023 53.3495 25 -1 -5 11 159.893 26.1707 14 -1 5 11 137.321 26.9491 14 1 5 -11 141.127 14.0557 6 0 5 -11-0.17253 11.7720 6 0 -5 -11-22.8293 36.1264 10 0 -5 11-13.4896 18.7120 16 0 -5 11 23.1172 22.6487 14 0 5 11-23.5969 23.7714 14 -1 -5 -11 456.256 41.8854 10 1 -5 11 287.499 27.4034 16 -1 5 -11 461.032 30.6806 1 -1 -5 -11 421.806 30.9753 1 1 -5 11 426.099 33.0435 14 1 5 11 367.814 33.5240 14 -1 5 -11 343.672 23.6895 6 -2 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116.051 26.1214 11 12 6 -11 192.737 17.1239 5 12 6 -11 128.069 37.5800 25 11 -6 -11 10.9269 26.1668 11 11 6 -11-86.8987 39.0136 25 10 -6 -11 219.926 31.9913 11 9 -6 -11 41.3726 30.3525 11 9 -6 -11 89.7613 26.6031 10 8 -6 -11 181.274 34.9177 11 8 -6 -11 171.659 30.8186 10 8 6 -11 194.756 17.3098 6 7 -6 -11 312.736 39.1288 11 7 -6 -11 346.951 36.5065 10 7 6 -11 268.193 49.7153 25 7 6 -11 328.515 22.5558 6 6 -6 -11 55.2049 35.5829 11 6 -6 -11 63.1186 32.7349 10 6 6 -11 42.8438 13.1386 6 5 -6 -11 334.987 41.3564 11 5 -6 -11 353.836 39.4330 10 5 6 -11 232.292 54.7374 25 5 6 -11 360.703 23.1700 6 4 -6 -11 191.390 39.1137 11 4 -6 -11 163.093 36.0576 10 4 6 -11 166.445 52.4120 25 -4 6 11 174.598 28.6424 14 -4 -6 11 203.547 27.9647 14 4 6 -11 174.031 16.0555 6 3 -6 -11 285.930 38.5695 10 -3 6 11 211.661 28.5130 14 -3 -6 11 234.239 27.7029 14 3 6 -11 212.094 17.2567 6 2 6 -11 56.7500 12.7516 6 2 -6 -11 37.1910 36.1825 10 -2 -6 11 67.0127 22.2080 16 2 6 -11 43.6445 52.2401 25 -2 -6 11 80.4037 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11.5740 6 -4 -11 11 59.5677 17.5891 16 4 11 -11 98.8732 12.8014 6 -3 -11 11 375.027 35.2452 16 3 11 -11 682.522 33.0325 6 2 11 -11 7.43445 11.3663 6 -2 -11 11-0.92707 16.9415 16 1 11 -11-8.81843 11.3877 6 -1 -11 11-10.7488 16.5922 16 0 11 -11 55.0804 11.7384 6 0 -11 11 43.9168 16.0183 16 -1 11 -11 42.6911 11.3571 6 1 -11 11 23.8468 15.2113 16 -2 11 -11 25.0555 10.8205 6 2 -11 11 17.2284 13.8840 16 -3 11 -11 11.7851 10.4074 6 3 -11 11-2.76031 13.1701 16 3 -11 11 20.5559 23.2566 21 -3 -11 -11 34.6183 14.8138 19 4 -11 11 169.797 14.4948 16 -4 11 -11 163.761 12.1812 6 -4 -11 -11 135.950 18.5213 19 -5 11 -11 12.4058 9.37001 6 5 -11 11 27.9561 6.68215 4 -5 -11 -11 28.8466 15.9887 19 6 -11 11 70.8183 7.41337 4 -6 -11 -11 105.508 16.3263 19 -8 -12 11 26.5033 10.9727 16 8 12 -11 23.4232 27.1072 25 -7 -12 11 133.609 15.1020 16 7 12 -11 173.663 30.3703 25 -6 -12 11 9.52641 13.9290 16 6 12 -11 10.7666 10.0826 6 -5 -12 11 248.202 24.3645 16 5 12 -11 411.897 22.0255 6 4 12 -11 50.3139 10.8389 6 -3 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32.8937 11 4 3 -13-9.98890 10.4059 6 3 -3 -13 404.753 41.4895 10 3 3 -13 420.940 24.2774 6 3 3 -13 332.328 33.2330 11 2 -3 -13 7.01722 33.6232 10 -2 -3 13 8.97470 17.5927 16 2 3 -13 0.56826 9.59701 6 1 -3 -13 23.9109 32.6747 10 -1 -3 13 8.79167 16.1655 16 1 3 -13-0.48267 9.15844 6 0 -3 -13 231.010 33.8026 10 0 3 -13 189.294 13.6635 6 -1 -3 -13 388.299 38.3661 10 -1 3 -13 395.502 21.8684 6 -2 3 -13 37.7070 7.34814 6 -2 -3 -13 72.7228 29.3607 10 3 -3 13 222.996 21.7678 17 3 3 13 247.860 22.1644 17 4 -3 13 350.681 25.9243 17 4 3 13 367.100 26.1609 17 5 -3 13 9.72793 15.6384 17 5 3 13 14.6212 16.0340 17 6 -3 13-2.79199 14.7848 17 6 3 13 1.77845 15.4104 17 7 -3 13 25.4682 13.8148 17 7 3 13 20.1346 14.2602 17 8 -3 13 55.0935 12.6156 17 8 3 13 60.6261 13.0935 17 12 4 -13 7.84437 15.2630 11 12 -4 -13 36.8924 19.4309 11 11 4 -13 118.950 20.1286 11 11 -4 -13 150.740 24.8509 11 11 4 -13 209.476 14.5690 5 11 4 -13 137.073 32.9859 25 10 4 -13 70.0882 19.5184 11 10 -4 -13 48.4257 21.4729 10 10 4 -13 83.4331 12.1571 5 10 4 -13 17.1550 35.4020 25 9 4 -13 1.57982 20.2873 11 9 -4 -13 1.01281 24.2908 10 9 4 -13 57.7196 38.5150 25 8 4 -13 27.3892 21.0776 11 8 -4 -13 39.0319 27.1597 10 8 4 -13-31.6279 42.3000 25 7 4 -13 17.1943 22.1028 11 7 -4 -13 41.2063 29.9346 11 7 -4 -13 1.09924 28.7740 10 7 4 -13 36.8455 44.6576 25 6 4 -13 4.32225 22.6263 11 6 -4 -13 36.0091 30.9707 11 6 -4 -13-5.11168 31.0181 10 6 4 -13 2.13844 10.9078 6 5 -4 -13 90.6058 33.3667 11 5 -4 -13 46.1597 31.8863 10 5 4 -13 65.0030 11.5103 6 4 -4 -13-9.89052 33.1777 11 4 4 -13 0.06960 10.5971 6 -3 -4 13 30.0677 18.4810 16 3 4 -13 44.8094 10.5562 6 2 -4 -13 175.663 34.2535 10 -2 -4 13 142.008 20.6557 16 2 4 -13 190.342 14.1597 6 1 4 -13 12.6462 9.79729 6 1 -4 -13-19.9413 31.5527 10 -1 -4 13 9.14903 15.8804 16 0 4 -13 113.997 26.5162 10 0 -4 -13 222.079 33.5927 10 0 -4 13 120.112 17.0303 16 0 4 -13 193.894 13.4707 6 -1 4 -13 49.7571 9.79809 6 -1 -4 -13 100.406 31.5546 10 -2 -4 -13 122.366 30.8884 10 -2 4 -13 101.146 10.7118 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30.9971 10.8807 6 -3 -5 13 197.858 22.4332 16 3 5 -13 233.612 16.4704 6 -2 -5 13 15.8937 17.3025 16 2 5 -13-0.40056 10.0210 6 1 5 -13 13.1674 9.97034 6 1 5 -13 16.9879 24.3139 10 -1 -5 13-3.97913 15.6471 16 0 5 -13 2.08082 9.69813 6 0 -5 -13 11.3129 30.3645 10 0 -5 13 20.6754 14.2590 16 -1 -5 -13 376.234 36.3722 10 -1 5 -13 319.697 20.0353 6 -2 5 -13-5.65622 8.99515 6 2 5 13 19.5237 15.8628 17 2 -5 13 4.58232 15.0140 17 3 -5 13 241.506 20.9476 17 3 5 13 271.806 21.4587 17 -3 5 -13 274.652 17.0790 6 4 -5 13 247.291 19.5399 17 4 5 13 270.833 20.1966 17 -4 5 -13 225.014 15.4989 6 5 -5 13 17.1460 13.5042 17 5 5 13 20.5720 14.1072 17 6 -5 13 25.5394 12.6040 17 6 5 13 32.2545 13.0190 17 7 -5 13 13.3091 11.0418 17 7 5 13 11.5849 11.4658 17 11 6 -13 111.264 10.8427 5 -11 -6 13 50.0296 12.9737 16 11 6 -13 61.6872 28.5417 25 10 -6 -13 26.5479 22.3677 11 -10 -6 13 34.7757 14.3644 16 10 6 -13 32.3013 11.0456 5 10 6 -13 39.2381 32.5507 25 9 -6 -13-11.7490 24.9318 11 8 -6 -13 45.1379 27.7518 11 8 -6 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14.2492 16 3 9 -13 48.8030 9.95756 6 -2 -9 13 38.0204 13.4562 16 2 9 -13 29.1521 9.60213 6 -1 -9 13 43.9829 13.0570 16 1 9 -13 87.5847 9.92021 6 0 9 -13 33.9496 8.80298 6 0 -9 13-1.79368 11.4746 16 1 -9 13 39.8498 11.0044 16 -1 9 -13 85.1783 9.31278 6 -2 9 -13 0.93700 7.98399 6 -3 9 -13 17.8998 7.61011 6 -6 -10 13 163.503 14.8906 16 -5 -10 13 84.7772 15.2318 16 5 10 -13 225.949 13.0873 6 -4 -10 13 3.45768 12.1495 16 4 10 -13 5.96504 8.62232 6 -3 -10 13 69.7628 14.3859 16 3 10 -13 189.396 12.0622 6 -2 -10 13 45.3663 12.0951 16 2 10 -13 88.8131 9.51224 6 -1 -10 13-7.31247 10.9194 16 1 10 -13 9.77149 8.29239 6 0 -10 13 18.2055 10.4204 16 0 10 -13 66.8905 8.53680 6 -1 10 -13 28.6939 8.02028 6 1 -10 13 15.9080 9.26326 16 11 0 -14 14.7652 18.1475 11 11 0 -14-1.02291 17.9525 10 10 0 -14 85.2131 21.4740 11 9 0 -14-22.6457 22.4106 11 8 0 -14-13.5397 23.5260 11 7 0 -14 151.923 26.8451 11 6 0 -14 278.258 30.4769 11 5 0 -14 137.403 27.8549 11 4 0 -14 552.925 42.2316 10 3 0 -14 756.361 50.9866 10 2 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105.533 26.8123 10 -1 1 -14 200.851 26.7152 10 -1 -1 -14 219.761 28.6328 10 2 1 14 25.4804 16.3256 17 -2 1 -14 23.1517 20.8302 10 -2 -1 -14 42.9283 23.0265 10 3 1 14 125.774 17.2831 17 4 1 14 10.1496 14.6443 17 5 1 14 1.35830 13.8198 17 6 1 14 16.4300 12.8233 17 10 2 -14 29.2758 18.5121 11 10 -2 -14 32.2566 21.0591 11 10 -2 -14 25.4324 19.6522 10 9 2 -14-10.3593 20.1290 11 9 -2 -14 4.00743 22.7034 11 9 -2 -14 12.9478 22.6193 10 8 2 -14-15.1984 21.4312 11 8 -2 -14 25.4441 24.8973 11 8 -2 -14 22.1291 24.5385 10 7 2 -14 90.4735 23.2578 11 7 -2 -14 121.834 27.7280 11 7 -2 -14 89.0139 27.0321 10 6 2 -14 114.873 24.1376 11 6 -2 -14 163.471 28.6541 11 5 2 -14 21.2439 22.7764 11 4 -2 -14 90.6127 29.7896 10 3 2 -14 255.886 29.9890 10 3 -2 -14 277.736 31.4887 10 -3 -2 14 178.338 19.4039 16 2 2 -14 133.818 27.2547 10 2 -2 -14 162.080 29.4717 10 -2 -2 14 87.8119 14.8537 16 1 2 -14 15.3511 24.8712 10 1 -2 -14-5.43177 27.8007 10 0 2 -14 59.9500 23.4107 10 0 -2 -14 60.2740 27.0210 10 -1 2 -14-1.44682 21.3101 10 -1 -2 -14 17.0877 25.7875 10 2 2 14 10.7018 15.4998 17 2 -2 14-9.93963 15.5087 17 3 -2 14-4.79668 14.7267 17 3 2 14 20.4781 15.0210 17 4 -2 14 68.9743 14.7276 17 4 2 14 74.5655 14.9790 17 5 -2 14 31.2368 13.3074 17 5 2 14 42.2288 13.6301 17 6 -2 14 53.9923 12.6214 17 6 2 14 71.3256 12.9239 17 10 3 -14 21.7307 16.3349 11 10 -3 -14 24.6054 20.6096 11 10 -3 -14 2.53230 17.1230 10 9 3 -14-1.55731 18.1617 11 9 -3 -14-8.52053 23.0660 11 9 -3 -14-3.43088 20.0722 10 8 3 -14 55.2737 19.8160 11 8 -3 -14 89.5051 25.4457 11 8 -3 -14 92.3443 23.8977 10 7 3 -14 12.0875 20.4908 11 7 -3 -14 11.1815 25.7726 11 7 -3 -14 23.4114 25.3315 10 6 3 -14-35.2667 21.1249 11 6 -3 -14 36.3943 28.1431 11 6 -3 -14-38.1903 26.4382 10 -5 -3 14 64.9352 16.8708 16 -4 -3 14 99.6525 17.0761 16 3 3 -14 140.057 26.6059 10 3 -3 -14 180.126 28.8956 10 -3 -3 14 109.492 16.6623 16 2 3 -14-3.84735 24.4596 10 2 -3 -14-5.68426 27.7317 10 -2 -3 14 12.3351 13.4342 16 1 3 -14 3.67424 22.8072 10 1 -3 -14-0.69511 26.6859 10 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14 49.1025 11.7269 17 8 -6 -14 163.087 16.6717 10 -8 -6 14 46.9511 13.4608 16 7 -6 -14 4.15304 18.7741 10 -7 -6 14 11.2572 13.1469 16 6 -6 -14 2.04709 21.2311 10 -6 -6 14 5.38521 13.6297 16 5 -6 -14 10.7927 22.9597 10 -5 -6 14 23.9828 13.8810 16 4 -6 -14 16.1156 24.4411 10 -4 -6 14 2.89054 13.3562 16 4 6 -14 2.98385 8.67210 6 3 6 -14-11.5588 18.4843 10 3 -6 -14 33.8251 24.6248 10 -3 -6 14-11.5217 13.1761 16 3 6 -14 11.7706 8.58804 6 -2 -6 14 4.71153 12.2859 16 2 6 -14-7.66284 8.42914 6 -1 6 14 20.7308 12.5907 17 -1 -6 14 13.2987 11.1251 16 1 6 -14 33.4215 8.51959 6 0 6 14-1.75494 11.9245 17 0 6 -14 7.18973 7.77422 6 1 6 14 99.7633 13.5787 17 -1 6 -14 130.599 9.88416 6 2 6 14 207.064 15.8965 17 3 6 14 26.8107 10.1998 17 -7 -7 14-11.1504 11.4165 16 -6 -7 14 33.5218 12.6044 16 -5 -7 14 4.00268 12.5713 16 -4 -7 14 23.3490 12.5762 16 4 7 -14 14.3280 8.33582 6 -3 -7 14 12.3109 11.9570 16 3 7 -14 12.5755 8.39156 6 -2 -7 14 9.37933 11.4644 16 2 7 -14-1.52663 8.12002 6 -1 -7 14 20.5616 10.4742 16 1 7 -14 50.7874 8.30301 6 0 7 -14 49.7987 8.05393 6 -1 7 -14 14.2007 6.98141 6 -2 7 -14 56.6103 7.02694 6 -5 -8 14 7.14857 10.9776 16 -4 -8 14 7.55680 11.0523 16 4 8 -14 14.8176 7.92709 6 -3 -8 14 30.5771 10.9182 16 3 8 -14 38.1229 8.14534 6 -2 -8 14 52.6010 11.2705 16 2 8 -14 112.711 9.38060 6 -1 -8 14 0.79944 9.08374 16 1 8 -14 9.88395 7.35165 6 0 8 -14 5.17930 6.93545 6 -1 8 -14 64.3956 7.48459 6 7 0 -15-24.9981 20.6389 10 6 0 -15 16.0205 21.3147 10 5 0 -15-8.67736 22.6783 10 -5 0 15 14.1457 10.7472 16 4 0 -15 4.52653 22.5557 10 3 0 -15 0.25705 22.9344 10 2 0 -15-11.4262 22.1945 10 1 0 -15 19.8311 20.3673 10 0 0 -15-0.95438 19.5744 10 1 0 15 10.3365 12.9690 17 2 0 15-4.01344 12.3656 17 3 0 15 9.48112 11.6726 17 8 1 -15 1.20319 19.0172 10 8 -1 -15-11.4368 17.3257 10 7 1 -15 35.1969 20.2603 10 -7 -1 15 23.7484 11.7357 16 6 1 -15 53.6570 21.5482 10 6 -1 -15 1.21427 22.0140 10 -6 -1 15 16.0377 11.6398 16 5 1 -15 5.08370 21.5729 10 5 -1 -15-4.47053 22.2013 10 -5 -1 15 14.9763 10.7449 16 4 1 -15 35.6612 22.3977 10 4 -1 -15 28.9588 22.6853 10 3 1 -15 8.82100 21.7331 10 3 -1 -15-6.94969 22.7984 10 2 1 -15 21.5723 20.7418 10 2 -1 -15 32.9837 22.8527 10 1 1 -15 34.1267 20.6575 10 1 -1 -15 63.8369 22.1389 10 0 1 -15-8.34673 18.3181 10 0 -1 -15 11.8241 20.6160 10 1 1 15 20.2677 13.0626 17 2 1 15 94.1277 13.5995 17 3 1 15-6.26894 11.5522 17 7 2 -15-13.8840 19.0455 10 7 -2 -15 30.9020 19.6072 10 -7 -2 15 6.09046 11.4698 16 6 2 -15 8.37411 20.3610 10 -6 -2 15 2.74244 11.4971 16 5 2 -15 31.1432 20.8956 10 5 -2 -15-8.65011 21.8209 10 -5 -2 15 6.58784 11.1663 16 4 2 -15 3.39184 21.2137 10 4 -2 -15-21.7303 22.4590 10 -4 -2 15-10.8402 10.4048 16 3 2 -15 8.84549 20.8334 10 3 -2 -15 0.78238 22.4779 10 2 2 -15 9.07039 19.1818 10 2 -2 -15 18.4961 22.1843 10 1 2 -15 3.75182 18.4578 10 1 -2 -15 61.8185 21.6758 10 0 2 -15 68.4956 16.3964 10 0 -2 -15 58.9181 21.2153 10 1 2 15 96.9700 13.8556 17 1 -2 15 85.5669 13.6394 17 2 2 15 8.79155 11.7914 17 2 -2 15-6.07876 11.6642 17 7 3 -15 52.0794 18.6492 10 7 -3 -15 19.3795 17.8061 10 -7 -3 15 12.6021 10.9773 16 6 3 -15 10.2633 19.7581 10 6 -3 -15 15.7211 19.6741 10 -6 -3 15 14.0044 11.0084 16 5 3 -15 50.4832 19.5554 10 -5 -3 15 19.5742 10.8723 16 4 3 -15 17.3581 19.9493 10 4 -3 -15-2.86782 21.6389 10 -4 -3 15-4.37522 10.1697 16 3 3 -15 22.3433 18.9405 10 3 -3 -15-23.2205 22.5841 10 2 3 -15-13.6586 17.6749 10 2 -3 -15 47.3452 22.1048 10 1 3 -15 25.2512 16.0753 10 1 -3 -15-4.89260 21.6597 10 0 3 15 80.2729 13.0446 17 0 -3 15 66.8914 12.7475 17 1 3 15 121.800 13.6819 17 1 -3 15 111.134 13.3033 17 2 3 15 146.479 13.8299 17 2 -3 15 140.873 13.4475 17 6 4 -15-4.27587 17.5224 10 6 -4 -15 17.9423 18.2391 10 -6 -4 15 0.59363 10.2654 16 5 4 -15-25.0606 18.3650 10 5 -4 -15 11.0495 19.7573 10 -5 -4 15-10.6476 10.1525 16 4 4 -15 8.84296 18.1339 10 -4 -4 15 3.14092 9.94654 16 3 4 -15-2.67653 16.3569 10 3 -4 -15-12.8692 21.2066 10 -3 -4 15 2.53917 8.81512 16 2 4 -15 43.1067 15.0885 10 2 -4 -15 32.0127 21.3936 10 -1 4 15 9.37941 11.5382 17 -1 -4 15 0.80586 10.9560 17 0 4 15-4.46515 11.3152 17 0 -4 15 2.53789 10.7252 17 1 4 15 98.4329 12.1888 17 1 -4 15 101.144 11.7901 17 4 5 -15 17.3758 14.0781 10 4 -5 -15 39.9186 18.8033 10 -4 -5 15 6.14098 9.05874 16 -3 -5 15 9.05237 8.07814 16 -2 5 15-7.90796 10.0946 17 -2 -5 15 0.40695 9.37303 17 -1 5 15 0.46244 9.85590 17 -1 -5 15-0.16035 9.32467 17 0 -5 15 86.2382 9.56185 17 0 5 15 43.5307 10.0743 17 0 0 0 0.00 0.00 0 TITL 191128AI-706 in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 1.54184 16.536479 15.982069 12.999478 90.0000 97.2709 90.0000 ZERR 5.00 0.000877 0.000574 0.000608 0.0000 0.0046 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O P Ni UNIT 155.00 215.00 10.00 20.00 5.00 5.00 TREF HKLF 4 END ; _shelx_hkl_checksum 44317 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.308 _oxdiff_exptl_absorpt_empirical_full_min 0.490 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ni1 Ni 0.69405(3) 0.72621(3) 0.83351(4) 0.0381(2) Uani 1 1 d . . . . . P14 P 0.62816(5) 0.83028(5) 0.88551(6) 0.0373(2) Uani 1 1 d . . . . . O35 O 0.59884(15) 0.68639(13) 0.75164(18) 0.0445(6) Uani 1 1 d . . . . . O30 O 0.75649(16) 0.64359(14) 0.77669(18) 0.0472(6) Uani 1 1 d . . . . . N8 N 0.76760(17) 0.82283(17) 1.0041(2) 0.0398(6) Uani 1 1 d . . . . . N10 N 0.86061(18) 0.74839(17) 0.9481(2) 0.0409(7) Uani 1 1 d . . . . . O37 O 0.76067(19) 0.51499(16) 0.7157(2) 0.0622(8) Uani 1 1 d . . . . . O34 O 0.51841(17) 0.57641(16) 0.7162(2) 0.0579(7) Uani 1 1 d . . . . . C9 C 0.7797(2) 0.7659(2) 0.9291(3) 0.0398(8) Uani 1 1 d . . . . . C6 C 0.9998(2) 0.6735(2) 0.7673(3) 0.0404(8) Uani 1 1 d . . . . . H6 H 1.030206 0.695451 0.718128 0.049 Uiso 1 1 calc R . . . . C15 C 0.5230(2) 0.81479(19) 0.9091(3) 0.0412(8) Uani 1 1 d . . . . . H15 H 0.490298 0.806855 0.841491 0.049 Uiso 1 1 calc R . . . . C3 C 0.9115(2) 0.6080(2) 0.9178(3) 0.0439(8) Uani 1 1 d . . . . . C5 C 1.0038(2) 0.5885(2) 0.7884(3) 0.0423(8) Uani 1 1 d . . . . . C2 C 0.9078(2) 0.6929(2) 0.8921(3) 0.0385(8) Uani 1 1 d . . . . . C21 C 0.6299(2) 0.9224(2) 0.8020(3) 0.0404(8) Uani 1 1 d . . . . . H21 H 0.590428 0.962776 0.822931 0.048 Uiso 1 1 calc R . . . . C7 C 0.9516(2) 0.72638(19) 0.8178(3) 0.0388(8) Uani 1 1 d . . . . . O38 O 0.8946(2) 0.2940(2) 0.4265(3) 0.0827(10) Uani 1 1 d . . . . . C4 C 0.9592(2) 0.5574(2) 0.8637(3) 0.0470(9) Uani 1 1 d . . . . . H4 H 0.961530 0.500370 0.878183 0.056 Uiso 1 1 calc R . . . . C16 C 0.5144(3) 0.7351(2) 0.9728(3) 0.0505(9) Uani 1 1 d . . . . . H16A H 0.533660 0.687407 0.936747 0.061 Uiso 1 1 calc R . . . . H16B H 0.547903 0.740063 1.039381 0.061 Uiso 1 1 calc R . . . . C13 C 0.6865(2) 0.8567(2) 1.0118(3) 0.0426(8) Uani 1 1 d . . . . . H13A H 0.688612 0.916724 1.022529 0.051 Uiso 1 1 calc R . . . . H13B H 0.662598 0.830691 1.068335 0.051 Uiso 1 1 calc R . . . . C20 C 0.4877(2) 0.8905(2) 0.9610(3) 0.0439(8) Uani 1 1 d . . . . . H20A H 0.521449 0.902448 1.025884 0.053 Uiso 1 1 calc R . . . . H20B H 0.489139 0.939030 0.916424 0.053 Uiso 1 1 calc R . . . . C12 C 0.8382(2) 0.8407(2) 1.0681(3) 0.0478(9) Uani 1 1 d . . . . . H12 H 0.844063 0.877055 1.124405 0.057 Uiso 1 1 calc R . . . . C31 C 0.7281(2) 0.5696(2) 0.7638(3) 0.0470(9) Uani 1 1 d . . . . . C11 C 0.8970(2) 0.7947(2) 1.0325(3) 0.0468(9) Uani 1 1 d . . . . . H11 H 0.951873 0.794013 1.059283 0.056 Uiso 1 1 calc R . . . . C33 C 0.5830(2) 0.6074(2) 0.7548(3) 0.0464(9) Uani 1 1 d . . . . . C26 C 0.6013(3) 0.8969(2) 0.6897(3) 0.0533(10) Uani 1 1 d . . . . . H26A H 0.547279 0.872595 0.685351 0.064 Uiso 1 1 calc R . . . . H26B H 0.637943 0.854840 0.668044 0.064 Uiso 1 1 calc R . . . . C32 C 0.6502(2) 0.5523(2) 0.8127(3) 0.0512(9) Uani 1 1 d . . . . . H32 H 0.659485 0.572224 0.884512 0.061 Uiso 1 1 calc R . . . . C28 C 0.8633(3) 0.5730(2) 0.9981(3) 0.0561(10) Uani 1 1 d . . . . . H28A H 0.874517 0.604775 1.061016 0.084 Uiso 1 1 calc GR . . . . H28B H 0.878311 0.515649 1.011492 0.084 Uiso 1 1 calc GR . . . . H28C H 0.806154 0.576250 0.973384 0.084 Uiso 1 1 calc GR . . . . C29 C 0.9454(3) 0.8179(2) 0.7901(3) 0.0533(10) Uani 1 1 d . . . . . H29A H 0.982505 0.830531 0.741128 0.080 Uiso 1 1 calc GR . . . . H29B H 0.959023 0.850891 0.851534 0.080 Uiso 1 1 calc GR . . . . H29C H 0.890732 0.830458 0.760003 0.080 Uiso 1 1 calc GR . . . . C27 C 1.0544(3) 0.5329(2) 0.7292(3) 0.0580(10) Uani 1 1 d . . . . . H27A H 1.019262 0.498569 0.682207 0.087 Uiso 1 1 calc GR . . . . H27B H 1.088227 0.497817 0.776791 0.087 Uiso 1 1 calc GR . . . . H27C H 1.088095 0.566584 0.690774 0.087 Uiso 1 1 calc GR . . . . C19 C 0.4012(2) 0.8757(2) 0.9819(3) 0.0543(10) Uani 1 1 d . . . . . H19A H 0.365915 0.872238 0.916438 0.065 Uiso 1 1 calc R . . . . H19B H 0.383274 0.922787 1.020314 0.065 Uiso 1 1 calc R . . . . C18 C 0.3931(3) 0.7957(2) 1.0432(3) 0.0559(10) Uani 1 1 d . . . . . H18A H 0.422581 0.801831 1.112210 0.067 Uiso 1 1 calc R . . . . H18B H 0.336086 0.786201 1.050328 0.067 Uiso 1 1 calc R . . . . C22 C 0.7125(2) 0.9657(3) 0.8107(3) 0.0579(10) Uani 1 1 d . . . . . H22A H 0.753314 0.926939 0.791784 0.070 Uiso 1 1 calc R . . . . H22B H 0.728582 0.983322 0.881794 0.070 Uiso 1 1 calc R . . . . C17 C 0.4264(3) 0.7209(2) 0.9898(3) 0.0562(10) Uani 1 1 d . . . . . H17A H 0.422797 0.671328 1.031979 0.067 Uiso 1 1 calc R . . . . H17B H 0.393556 0.711605 0.923496 0.067 Uiso 1 1 calc R . . . . N11 N 0.8411(3) 0.3156(3) 0.5697(4) 0.0909(14) Uani 1 1 d . . . . . C24 C 0.6808(3) 1.0165(3) 0.6267(4) 0.0663(12) Uani 1 1 d . . . . . H24A H 0.677023 1.065687 0.582594 0.080 Uiso 1 1 calc R . . . . H24B H 0.721251 0.979328 0.603669 0.080 Uiso 1 1 calc R . . . . C25 C 0.5994(3) 0.9729(2) 0.6165(3) 0.0596(11) Uani 1 1 d . . . . . H25A H 0.585038 0.954455 0.545456 0.072 Uiso 1 1 calc R . . . . H25B H 0.557892 1.011911 0.632823 0.072 Uiso 1 1 calc R . . . . C23 C 0.7076(3) 1.0425(3) 0.7383(4) 0.0661(12) Uani 1 1 d . . . . . H23A H 0.669092 1.082544 0.759925 0.079 Uiso 1 1 calc R . . . . H23B H 0.760588 1.069251 0.743112 0.079 Uiso 1 1 calc R . . . . C36 C 0.6291(3) 0.4605(2) 0.8161(4) 0.0653(12) Uani 1 1 d . . . . . H36A H 0.617628 0.439333 0.746660 0.098 Uiso 1 1 calc GR . . . . H36B H 0.581987 0.453365 0.851479 0.098 Uiso 1 1 calc GR . . . . H36C H 0.674228 0.430378 0.852317 0.098 Uiso 1 1 calc GR . . . . C39 C 0.8595(3) 0.2657(4) 0.4991(5) 0.0834(16) Uani 1 1 d . . . . . C42 C 0.8379(4) 0.1759(3) 0.5128(5) 0.0946(19) Uani 1 1 d . . . . . H42A H 0.779898 0.170713 0.511197 0.142 Uiso 1 1 calc GR . . . . H42B H 0.864368 0.156074 0.578257 0.142 Uiso 1 1 calc GR . . . . H42C H 0.855501 0.143220 0.457800 0.142 Uiso 1 1 calc GR . . . . C41 C 0.8593(4) 0.4100(3) 0.5567(4) 0.0875(16) Uani 1 1 d . . . . . H41A H 0.914901 0.416932 0.544438 0.131 Uiso 1 1 calc GR . . . . H41B H 0.850454 0.439435 0.618704 0.131 Uiso 1 1 calc GR . . . . H41C H 0.823662 0.431983 0.498995 0.131 Uiso 1 1 calc GR . . . . C43 C 0.8036(3) 0.2939(4) 0.6643(4) 0.0916(18) Uani 1 1 d . . . . . H43A H 0.771905 0.243705 0.651946 0.137 Uiso 1 1 calc GR . . . . H43B H 0.768944 0.338795 0.680826 0.137 Uiso 1 1 calc GR . . . . H43C H 0.845722 0.285005 0.721176 0.137 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ni1 0.0485(4) 0.0269(3) 0.0361(3) -0.0032(2) -0.0052(2) 0.0032(2) P14 0.0471(5) 0.0262(4) 0.0359(4) -0.0019(3) -0.0051(4) 0.0032(3) O35 0.0563(15) 0.0313(12) 0.0430(13) -0.0043(9) -0.0049(11) -0.0001(10) O30 0.0591(16) 0.0366(13) 0.0446(13) -0.0022(10) 0.0018(11) 0.0035(11) N8 0.0440(16) 0.0370(14) 0.0360(14) -0.0052(11) -0.0046(12) 0.0030(12) N10 0.0472(17) 0.0348(14) 0.0383(15) -0.0039(11) -0.0039(13) 0.0063(12) O37 0.084(2) 0.0375(14) 0.0660(17) -0.0100(12) 0.0132(15) 0.0039(14) O34 0.0672(18) 0.0462(14) 0.0557(16) -0.0005(12) -0.0104(14) -0.0131(13) C9 0.049(2) 0.0344(17) 0.0353(17) -0.0029(13) 0.0006(14) 0.0014(15) C6 0.0475(19) 0.0322(16) 0.0387(17) -0.0002(13) -0.0058(15) -0.0014(14) C15 0.054(2) 0.0299(16) 0.0369(17) 0.0006(13) -0.0067(15) 0.0012(15) C3 0.047(2) 0.0339(17) 0.0484(19) 0.0057(14) -0.0029(16) 0.0013(15) C5 0.0445(19) 0.0334(17) 0.0471(19) -0.0036(14) -0.0013(15) 0.0023(15) C2 0.0414(19) 0.0320(16) 0.0401(17) -0.0024(13) -0.0028(15) 0.0033(14) C21 0.0458(19) 0.0325(16) 0.0422(18) -0.0005(13) 0.0027(15) 0.0038(14) C7 0.0451(19) 0.0286(16) 0.0402(17) 0.0016(13) -0.0043(15) 0.0008(14) O38 0.089(2) 0.094(2) 0.070(2) 0.0159(18) 0.0275(19) 0.000(2) C4 0.052(2) 0.0262(16) 0.061(2) 0.0041(15) 0.0005(18) 0.0006(15) C16 0.066(3) 0.0313(18) 0.053(2) 0.0062(15) 0.0005(19) 0.0012(16) C13 0.046(2) 0.0365(17) 0.0431(19) -0.0066(14) -0.0013(15) 0.0056(15) C20 0.050(2) 0.0332(17) 0.0473(19) -0.0002(14) 0.0017(16) 0.0050(15) C12 0.053(2) 0.047(2) 0.0405(19) -0.0106(15) -0.0059(16) 0.0005(17) C31 0.063(2) 0.0318(18) 0.0447(19) 0.0034(15) -0.0012(17) 0.0016(17) C11 0.047(2) 0.049(2) 0.0416(19) -0.0051(15) -0.0071(16) 0.0016(17) C33 0.064(2) 0.0336(18) 0.0408(18) 0.0009(14) 0.0026(17) -0.0001(17) C26 0.076(3) 0.0383(19) 0.043(2) -0.0003(15) -0.0024(18) -0.0017(18) C32 0.063(2) 0.0362(18) 0.053(2) 0.0025(15) 0.0025(19) 0.0025(17) C28 0.064(3) 0.048(2) 0.057(2) 0.0190(18) 0.0082(19) 0.0032(19) C29 0.070(3) 0.0308(18) 0.059(2) 0.0049(16) 0.008(2) 0.0017(17) C27 0.069(3) 0.040(2) 0.064(2) -0.0052(17) 0.007(2) 0.0111(19) C19 0.054(2) 0.049(2) 0.060(2) 0.0002(18) 0.0071(18) 0.0010(18) C18 0.055(2) 0.060(2) 0.053(2) 0.0011(18) 0.0079(18) -0.0110(19) C22 0.053(2) 0.051(2) 0.067(3) 0.0122(19) -0.002(2) -0.0061(18) C17 0.066(3) 0.049(2) 0.052(2) 0.0083(17) -0.0002(19) -0.0122(19) N11 0.063(3) 0.130(4) 0.076(3) -0.018(3) -0.007(2) 0.031(3) C24 0.074(3) 0.053(2) 0.076(3) 0.023(2) 0.028(2) 0.014(2) C25 0.087(3) 0.047(2) 0.044(2) 0.0086(16) 0.003(2) 0.004(2) C23 0.056(3) 0.050(2) 0.091(3) 0.022(2) 0.004(2) -0.0066(19) C36 0.081(3) 0.045(2) 0.069(3) 0.0058(19) 0.003(2) -0.004(2) C39 0.066(3) 0.084(4) 0.095(4) -0.004(3) -0.011(3) 0.011(3) C42 0.092(4) 0.053(3) 0.128(5) 0.016(3) -0.027(4) -0.014(3) C41 0.114(4) 0.057(3) 0.090(4) -0.008(2) 0.005(3) 0.019(3) C43 0.077(4) 0.137(5) 0.060(3) 0.017(3) 0.006(3) 0.025(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ni Ni -3.0029 0.5091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist -2 10 0 0.0230 4 -9 -4 0.0420 -10 -2 -1 0.0076 10 2 1 0.0152 2 -10 -1 0.0060 -2 10 0 0.0170 -2 10 0 0.0247 -3 0 8 0.1480 3 1 -8 0.1105 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O35 Ni1 P14 91.05(8) . . ? O30 Ni1 P14 173.25(9) . . ? O30 Ni1 O35 90.12(11) . . ? C9 Ni1 P14 84.24(11) . . ? C9 Ni1 O35 172.34(14) . . ? C9 Ni1 O30 95.26(13) . . ? C15 P14 Ni1 118.81(11) . . ? C15 P14 C21 107.22(16) . . ? C15 P14 C13 106.51(16) . . ? C21 P14 Ni1 112.97(12) . . ? C21 P14 C13 107.33(16) . . ? C13 P14 Ni1 103.21(11) . . ? C33 O35 Ni1 117.9(2) . . ? C31 O30 Ni1 119.4(3) . . ? C9 N8 C13 120.9(3) . . ? C9 N8 C12 112.3(3) . . ? C12 N8 C13 126.7(3) . . ? C9 N10 C2 128.4(3) . . ? C9 N10 C11 110.5(3) . . ? C11 N10 C2 121.1(3) . . ? N8 C9 Ni1 122.1(3) . . ? N10 C9 Ni1 134.0(3) . . ? N10 C9 N8 103.8(3) . . ? C5 C6 H6 119.3 . . ? C7 C6 H6 119.3 . . ? C7 C6 C5 121.4(4) . . ? P14 C15 H15 107.3 . . ? C16 C15 P14 111.1(2) . . ? C16 C15 H15 107.3 . . ? C16 C15 C20 110.5(3) . . ? C20 C15 P14 113.0(2) . . ? C20 C15 H15 107.3 . . ? C2 C3 C28 121.2(3) . . ? C4 C3 C2 117.2(3) . . ? C4 C3 C28 121.6(3) . . ? C6 C5 C4 118.3(3) . . ? C6 C5 C27 119.7(4) . . ? C4 C5 C27 122.0(3) . . ? C3 C2 N10 119.2(3) . . ? C7 C2 N10 118.7(3) . . ? C7 C2 C3 122.1(3) . . ? P14 C21 H21 107.7 . . ? C26 C21 P14 108.9(2) . . ? C26 C21 H21 107.7 . . ? C22 C21 P14 113.7(2) . . ? C22 C21 H21 107.7 . . ? C22 C21 C26 110.9(3) . . ? C6 C7 C2 118.6(3) . . ? C6 C7 C29 120.4(3) . . ? C2 C7 C29 121.0(3) . . ? C3 C4 C5 122.5(3) . . ? C3 C4 H4 118.8 . . ? C5 C4 H4 118.8 . . ? C15 C16 H16A 109.4 . . ? C15 C16 H16B 109.4 . . ? H16A C16 H16B 108.0 . . ? C17 C16 C15 111.1(3) . . ? C17 C16 H16A 109.4 . . ? C17 C16 H16B 109.4 . . ? P14 C13 H13A 111.0 . . ? P14 C13 H13B 111.0 . . ? N8 C13 P14 103.6(2) . . ? N8 C13 H13A 111.0 . . ? N8 C13 H13B 111.0 . . ? H13A C13 H13B 109.0 . . ? C15 C20 H20A 109.2 . . ? C15 C20 H20B 109.2 . . ? H20A C20 H20B 107.9 . . ? C19 C20 C15 112.2(3) . . ? C19 C20 H20A 109.2 . . ? C19 C20 H20B 109.2 . . ? N8 C12 H12 127.1 . . ? C11 C12 N8 105.9(3) . . ? C11 C12 H12 127.1 . . ? O30 C31 C32 115.3(3) . . ? O37 C31 O30 123.0(4) . . ? O37 C31 C32 121.7(3) . . ? N10 C11 H11 126.2 . . ? C12 C11 N10 107.5(3) . . ? C12 C11 H11 126.2 . . ? O35 C33 C32 116.1(3) . . ? O34 C33 O35 123.5(3) . . ? O34 C33 C32 120.4(3) . . ? C21 C26 H26A 109.4 . . ? C21 C26 H26B 109.4 . . ? C21 C26 C25 111.0(3) . . ? H26A C26 H26B 108.0 . . ? C25 C26 H26A 109.4 . . ? C25 C26 H26B 109.4 . . ? C31 C32 C33 106.7(3) . . ? C31 C32 H32 107.3 . . ? C33 C32 H32 107.3 . . ? C36 C32 C31 113.4(3) . . ? C36 C32 C33 114.6(3) . . ? C36 C32 H32 107.3 . . ? C3 C28 H28A 109.5 . . ? C3 C28 H28B 109.5 . . ? C3 C28 H28C 109.5 . . ? H28A C28 H28B 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C7 C29 H29A 109.5 . . ? C7 C29 H29B 109.5 . . ? C7 C29 H29C 109.5 . . ? H29A C29 H29B 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C5 C27 H27A 109.5 . . ? C5 C27 H27B 109.5 . . ? C5 C27 H27C 109.5 . . ? H27A C27 H27B 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? C20 C19 H19A 109.2 . . ? C20 C19 H19B 109.2 . . ? C20 C19 C18 112.0(3) . . ? H19A C19 H19B 107.9 . . ? C18 C19 H19A 109.2 . . ? C18 C19 H19B 109.2 . . ? C19 C18 H18A 109.4 . . ? C19 C18 H18B 109.4 . . ? H18A C18 H18B 108.0 . . ? C17 C18 C19 111.1(3) . . ? C17 C18 H18A 109.4 . . ? C17 C18 H18B 109.4 . . ? C21 C22 H22A 109.7 . . ? C21 C22 H22B 109.7 . . ? C21 C22 C23 109.8(3) . . ? H22A C22 H22B 108.2 . . ? C23 C22 H22A 109.7 . . ? C23 C22 H22B 109.7 . . ? C16 C17 C18 111.0(3) . . ? C16 C17 H17A 109.4 . . ? C16 C17 H17B 109.4 . . ? C18 C17 H17A 109.4 . . ? C18 C17 H17B 109.4 . . ? H17A C17 H17B 108.0 . . ? C39 N11 C41 117.4(5) . . ? C39 N11 C43 127.4(6) . . ? C43 N11 C41 115.1(5) . . ? H24A C24 H24B 108.0 . . ? C25 C24 H24A 109.4 . . ? C25 C24 H24B 109.4 . . ? C25 C24 C23 111.1(4) . . ? C23 C24 H24A 109.4 . . ? C23 C24 H24B 109.4 . . ? C26 C25 H25A 109.4 . . ? C26 C25 H25B 109.4 . . ? C24 C25 C26 111.2(3) . . ? C24 C25 H25A 109.4 . . ? C24 C25 H25B 109.4 . . ? H25A C25 H25B 108.0 . . ? C22 C23 H23A 109.5 . . ? C22 C23 H23B 109.5 . . ? C24 C23 C22 110.6(4) . . ? C24 C23 H23A 109.5 . . ? C24 C23 H23B 109.5 . . ? H23A C23 H23B 108.1 . . ? C32 C36 H36A 109.5 . . ? C32 C36 H36B 109.5 . . ? C32 C36 H36C 109.5 . . ? H36A C36 H36B 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? O38 C39 N11 119.2(6) . . ? O38 C39 C42 125.3(6) . . ? N11 C39 C42 115.5(6) . . ? C39 C42 H42A 109.5 . . ? C39 C42 H42B 109.5 . . ? C39 C42 H42C 109.5 . . ? H42A C42 H42B 109.5 . . ? H42A C42 H42C 109.5 . . ? H42B C42 H42C 109.5 . . ? N11 C41 H41A 109.5 . . ? N11 C41 H41B 109.5 . . ? N11 C41 H41C 109.5 . . ? H41A C41 H41B 109.5 . . ? H41A C41 H41C 109.5 . . ? H41B C41 H41C 109.5 . . ? N11 C43 H43A 109.5 . . ? N11 C43 H43B 109.5 . . ? N11 C43 H43C 109.5 . . ? H43A C43 H43B 109.5 . . ? H43A C43 H43C 109.5 . . ? H43B C43 H43C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ni1 P14 2.1441(10) . ? Ni1 O35 1.895(2) . ? Ni1 O30 1.884(2) . ? Ni1 C9 1.874(3) . ? P14 C15 1.820(4) . ? P14 C21 1.832(3) . ? P14 C13 1.845(3) . ? O35 C33 1.291(4) . ? O30 C31 1.275(4) . ? N8 C9 1.366(4) . ? N8 C13 1.461(4) . ? N8 C12 1.374(4) . ? N10 C9 1.358(5) . ? N10 C2 1.439(5) . ? N10 C11 1.395(4) . ? O37 C31 1.236(5) . ? O34 C33 1.226(4) . ? C6 H6 0.9300 . ? C6 C5 1.386(5) . ? C6 C7 1.383(5) . ? C15 H15 0.9800 . ? C15 C16 1.535(5) . ? C15 C20 1.536(5) . ? C3 C2 1.398(5) . ? C3 C4 1.383(5) . ? C3 C28 1.500(5) . ? C5 C4 1.389(5) . ? C5 C27 1.498(5) . ? C2 C7 1.386(5) . ? C21 H21 0.9800 . ? C21 C26 1.532(5) . ? C21 C22 1.523(5) . ? C7 C29 1.506(4) . ? O38 C39 1.252(7) . ? C4 H4 0.9300 . ? C16 H16A 0.9700 . ? C16 H16B 0.9700 . ? C16 C17 1.517(6) . ? C13 H13A 0.9700 . ? C13 H13B 0.9700 . ? C20 H20A 0.9700 . ? C20 H20B 0.9700 . ? C20 C19 1.509(6) . ? C12 H12 0.9300 . ? C12 C11 1.347(5) . ? C31 C32 1.533(6) . ? C11 H11 0.9300 . ? C33 C32 1.537(5) . ? C26 H26A 0.9700 . ? C26 H26B 0.9700 . ? C26 C25 1.540(5) . ? C32 H32 0.9800 . ? C32 C36 1.510(5) . ? C28 H28A 0.9600 . ? C28 H28B 0.9600 . ? C28 H28C 0.9600 . ? C29 H29A 0.9600 . ? C29 H29B 0.9600 . ? C29 H29C 0.9600 . ? C27 H27A 0.9600 . ? C27 H27B 0.9600 . ? C27 H27C 0.9600 . ? C19 H19A 0.9700 . ? C19 H19B 0.9700 . ? C19 C18 1.522(5) . ? C18 H18A 0.9700 . ? C18 H18B 0.9700 . ? C18 C17 1.520(6) . ? C22 H22A 0.9700 . ? C22 H22B 0.9700 . ? C22 C23 1.543(5) . ? C17 H17A 0.9700 . ? C17 H17B 0.9700 . ? N11 C39 1.282(7) . ? N11 C41 1.551(7) . ? N11 C43 1.487(7) . ? C24 H24A 0.9700 . ? C24 H24B 0.9700 . ? C24 C25 1.507(6) . ? C24 C23 1.520(7) . ? C25 H25A 0.9700 . ? C25 H25B 0.9700 . ? C23 H23A 0.9700 . ? C23 H23B 0.9700 . ? C36 H36A 0.9600 . ? C36 H36B 0.9600 . ? C36 H36C 0.9600 . ? C39 C42 1.495(7) . ? C42 H42A 0.9600 . ? C42 H42B 0.9600 . ? C42 H42C 0.9600 . ? C41 H41A 0.9600 . ? C41 H41B 0.9600 . ? C41 H41C 0.9600 . ? C43 H43A 0.9600 . ? C43 H43B 0.9600 . ? C43 H43C 0.9600 . ? loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -2.0945 10.1780 0.3522 0.0941 0.3943 -0.9141 3.9720 -8.8148 -3.5561 -0.0789 0.0189 0.9967 -10.0937 -1.7952 -1.4367 0.9724 -0.2331 -0.0095 10.0937 1.7952 1.4367 -0.9724 0.2331 0.0095 2.3540 -10.0743 -1.0692 -0.0754 -0.3159 0.9458 -1.9224 10.2040 -0.1070 0.1059 0.4428 -0.8904 -2.1372 10.1666 0.4650 0.0913 0.3822 -0.9196 -3.2733 0.2768 8.2957 -0.2026 -0.8445 -0.4957 3.1121 0.5841 -8.3074 0.2116 0.8822 0.4207