#------------------------------------------------------------------------------ #$Date: 2022-04-03 20:22:39 +0100 (Sun, 03 Apr 2022) $ #$Revision: 274241 $ #$URL: svn://www.crystallography.net/cod/cif/4/51/93/4519385.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519385 loop_ _publ_author_name 'Navarro, Miquel' 'Alf\'erez, Macarena G.' 'de Sousa, Morgane' 'Miranda-Pizarro, Juan' 'Campos, Jes\'us' _publ_section_title ; Dicoordinate Au(I)--Ethylene Complexes as Hydroamination Catalysts ; _journal_issue 7 _journal_name_full 'ACS Catalysis' _journal_page_first 4227 _journal_page_last 4241 _journal_paper_doi 10.1021/acscatal.1c05823 _journal_volume 12 _journal_year 2022 _chemical_formula_moiety 'C63 H81 Au N2 O P, F3 Sb0.5' _chemical_formula_sum 'C63 H81 Au F3 N2 O P Sb0.5' _chemical_formula_weight 1228.10 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _audit_creation_date 2022-02-15 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408) ; _cell_angle_alpha 68.369(2) _cell_angle_beta 80.530(2) _cell_angle_gamma 65.864(2) _cell_formula_units_Z 2 _cell_length_a 15.5190(7) _cell_length_b 15.6380(8) _cell_length_c 17.4595(10) _cell_measurement_reflns_used 9895 _cell_measurement_temperature 193.0 _cell_measurement_theta_max 29.50 _cell_measurement_theta_min 2.27 _cell_volume 3594.0(3) _computing_cell_refinement 'SAINT V8.40B (?, 2016)' _computing_data_reduction 'SAINT V8.40B (?, 2016)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'olex2.solve 1.3 (Bourhis et al., 2015)' _diffrn_ambient_temperature 193.0 _diffrn_measured_fraction_theta_full 0.994 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0756 _diffrn_reflns_av_unetI/netI 0.0333 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_h_min -21 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_number 240470 _diffrn_reflns_point_group_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 29.622 _diffrn_reflns_theta_min 1.893 _diffrn_source_current 1.4 _diffrn_source_power 0.07 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 2.294 _exptl_absorpt_correction_T_max 0.7459 _exptl_absorpt_correction_T_min 0.4864 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0946 before and 0.0661 after correction. The Ratio of minimum to maximum transmission is 0.6521. The \l/2 correction factor is Not present. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.135 _exptl_crystal_description needle _exptl_crystal_F_000 1255 _exptl_crystal_size_max 0.15 _exptl_crystal_size_mid 0.14 _exptl_crystal_size_min 0.10 _refine_diff_density_max 1.293 _refine_diff_density_min -2.432 _refine_diff_density_rms 0.140 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.097 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 716 _refine_ls_number_reflns 20146 _refine_ls_number_restraints 102 _refine_ls_restrained_S_all 1.096 _refine_ls_R_factor_all 0.0824 _refine_ls_R_factor_gt 0.0575 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0677P)^2^+16.6372P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1475 _refine_ls_wR_factor_ref 0.1680 _reflns_Friedel_coverage 0.000 _reflns_number_gt 15637 _reflns_number_total 20146 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cs1c05823_si_007.cif _cod_data_source_block jcm00722a_0m_sq _cod_original_formula_sum 'C63 H81 Au F3 N2 O P Sb0.50' _cod_database_code 4519385 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.786 _shelx_estimated_absorpt_t_min 0.670 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances C53-C54A \\sim C53-C55A \\sim C53-C56A \\sim C53-C54B \\sim C53-C55B \\sim C53-C56B with sigma of 0.02 C54A-C55A \\sim C55A-C56A \\sim C56A-C54A \\sim C54B-C55B \\sim C55B-C56B \\sim C56B-C54B with sigma of 0.02 3. Rigid body (RIGU) restrains C17, C18A, C19A, C20A, C18B, C19B, C20B with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C53, C54A, C55A, C56A, C55B, C54B, C56B with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001 4. Others Sof(C18B)=Sof(H18D)=Sof(H18E)=Sof(H18F)=Sof(C19B)=Sof(H19D)=Sof(H19E)= Sof(H19F)=Sof(C20B)=Sof(H20D)=Sof(H20E)=Sof(H20F)=1-FVAR(1) Sof(C18A)=Sof(H18A)=Sof(H18B)=Sof(H18C)=Sof(C19A)=Sof(H19A)=Sof(H19B)= Sof(H19C)=Sof(C20A)=Sof(H20A)=Sof(H20B)=Sof(H20C)=FVAR(1) Sof(C55B)=Sof(H55D)=Sof(H55E)=Sof(H55F)=Sof(C54B)=Sof(H54D)=Sof(H54E)= Sof(H54F)=Sof(C56B)=Sof(H56D)=Sof(H56E)=Sof(H56F)=1-FVAR(2) Sof(C54A)=Sof(H54A)=Sof(H54B)=Sof(H54C)=Sof(C55A)=Sof(H55A)=Sof(H55B)= Sof(H55C)=Sof(C56A)=Sof(H56A)=Sof(H56B)=Sof(H56C)=FVAR(2) 5.a Secondary CH2 refined with riding coordinates: C62(H62A,H62B), C63(H63A,H63B) 5.b Me refined with riding coordinates: C15(H15A,H15B,H15C), C18B(H18D,H18E,H18F), C19B(H19D,H19E,H19F), C20B(H20D, H20E,H20F), C54A(H54A,H54B,H54C), C55A(H55A,H55B,H55C), C56A(H56A,H56B,H56C), C55B(H55D,H55E,H55F), C54B(H54D,H54E,H54F), C56B(H56D,H56E,H56F) 5.c Aromatic/amide H refined with riding coordinates: N1(H1), N2(H2), C2(H2A), C4(H4), C5(H5), C8(H8), C9(H9), C11(H11), C12(H12), C22(H22), C24(H24), C25(H25), C28(H28), C29(H29), C31(H31), C32(H32), C42(H42), C44(H44), C45(H45), C48(H48), C49(H49), C51(H51), C52(H52) 5.d Idealised Me refined as rotating group: C14(H14A,H14B,H14C), C16(H16A,H16B,H16C), C34(H34A,H34B,H34C), C35(H35A,H35B, H35C), C36(H36A,H36B,H36C), C38(H38A,H38B,H38C), C39(H39A,H39B,H39C), C40(H40A, H40B,H40C), C58(H58A,H58B,H58C), C59(H59A,H59B,H59C), C60(H60A,H60B,H60C), C18A(H18A,H18B,H18C), C19A(H19A,H19B,H19C), C20A(H20A,H20B,H20C) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL jcm00722a_0m_a.res in P-1 jcm00722a_0m_sq.res created by SHELXL-2018/3 at 10:47:44 on 15-Feb-2022 REM Old TITL jcm00722a_0m in P-1 #2 REM SHELXT solution in P-1: R1 0.141, Rweak 0.013, Alpha 0.046 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C120 N18 O2 F6 P4 Sb Au2 CELL 0.71073 15.519 15.638 17.4595 68.369 80.53 65.864 ZERR 2 0.0007 0.0008 0.001 0.002 0.002 0.002 LATT 1 SFAC C H Au F N O P Sb UNIT 126 162 2 6 4 2 2 1 RIGU C17 C18A > C20B RIGU 0.001 0.001 C53 C54A > C56B SADI C53 C54A C53 C55A C53 C56A C53 C54B C53 C55B C53 C56B SADI C54A C55A C55A C56A C56A C54A C54B C55B C55B C56B C56B C54B L.S. 24 PLAN 41 SIZE 0.11 0.14 0.19 TEMP -80.15 CONF MORE -1 ABIN BOND $H fmap 2 53 acta OMIT -1 2 4 OMIT -7 0 2 OMIT 0 3 0 OMIT 2 2 3 OMIT 1 1 2 OMIT 2 1 1 OMIT 4 0 0 OMIT -2 -5 1 OMIT -1 -2 5 OMIT -1 -1 4 OMIT 3 0 1 OMIT 3 1 1 OMIT -2 0 1 OMIT -1 4 2 OMIT 0 0 5 OMIT -1 3 5 OMIT 2 2 2 OMIT -1 -1 1 OMIT -2 -5 2 OMIT 2 1 4 OMIT -1 0 3 OMIT 3 -2 1 OMIT 2 2 5 OMIT 1 -3 4 OMIT 4 2 7 OMIT -4 0 6 OMIT 1 1 8 OMIT -1 -1 3 OMIT 0 5 1 OMIT -4 2 2 OMIT -5 0 1 OMIT 3 2 5 OMIT -3 2 0 OMIT -2 -1 1 OMIT 2 4 4 OMIT 0 -1 1 OMIT -2 -2 1 OMIT 3 -1 6 OMIT 3 3 1 OMIT 1 -1 8 OMIT -5 1 3 OMIT -1 7 3 OMIT 2 0 3 OMIT 2 1 2 OMIT 3 2 7 OMIT 2 0 2 OMIT -1 0 2 OMIT -4 -2 2 OMIT -3 -4 1 OMIT 2 4 9 OMIT 1 -4 4 OMIT 3 3 2 OMIT 2 1 5 OMIT -1 3 1 OMIT -4 -3 2 OMIT 3 1 0 OMIT 4 3 8 OMIT 3 9 2 OMIT -2 1 1 OMIT -1 2 3 OMIT 1 4 2 OMIT -3 -3 1 OMIT 1 3 2 OMIT -2 2 1 OMIT 0 1 5 OMIT 0 2 3 REM REM REM WGHT 0.067700 16.637201 FVAR 0.35583 0.66331 0.39206 AU1 3 0.277662 0.580695 0.329810 11.00000 0.03682 0.02944 = 0.04066 -0.01502 0.00376 -0.00880 P1 7 0.336759 0.443195 0.297911 11.00000 0.02676 0.02336 = 0.02837 -0.00961 0.00159 -0.00694 O1 6 0.227783 0.709450 0.360863 11.00000 0.05727 0.02398 = 0.03671 -0.01636 -0.00117 -0.01079 N1 5 0.175223 0.876650 0.328735 11.00000 0.07055 0.04068 = 0.07866 -0.03175 0.00135 -0.01238 AFIX 43 H1 2 0.186661 0.876481 0.376523 11.00000 -1.20000 AFIX 0 N2 5 0.181119 0.820715 0.230674 11.00000 0.07826 0.04104 = 0.05252 -0.01689 -0.00342 -0.01455 AFIX 43 H2 2 0.184576 0.779062 0.206393 11.00000 -1.20000 AFIX 0 C1 1 0.269584 0.362659 0.336279 11.00000 0.03063 0.02664 = 0.03653 -0.01254 0.00321 -0.00886 C2 1 0.319543 0.260620 0.351768 11.00000 0.03207 0.03270 = 0.04606 -0.01560 0.00246 -0.00848 AFIX 43 H2A 2 0.385179 0.237331 0.338874 11.00000 -1.20000 AFIX 0 C3 1 0.276339 0.192242 0.385377 11.00000 0.03904 0.02854 = 0.06725 -0.01935 0.00149 -0.01243 C4 1 0.181192 0.229057 0.404147 11.00000 0.04392 0.03524 = 0.09365 -0.02048 0.01283 -0.02128 AFIX 43 H4 2 0.149394 0.184458 0.427790 11.00000 -1.20000 AFIX 0 C5 1 0.131599 0.329119 0.389245 11.00000 0.03280 0.03425 = 0.08784 -0.01764 0.01084 -0.01257 AFIX 43 H5 2 0.066211 0.351486 0.403180 11.00000 -1.20000 AFIX 0 C6 1 0.173036 0.398961 0.354661 11.00000 0.03185 0.03110 = 0.05105 -0.01414 0.00419 -0.01174 C7 1 0.111283 0.505811 0.339260 11.00000 0.02962 0.03216 = 0.05654 -0.01251 0.00181 -0.01197 C8 1 0.068576 0.537794 0.404690 11.00000 0.03952 0.03639 = 0.05499 -0.02026 -0.00681 -0.00302 AFIX 43 H8 2 0.084178 0.492888 0.459237 11.00000 -1.20000 AFIX 0 C9 1 0.003394 0.633858 0.392972 11.00000 0.04432 0.04344 = 0.07014 -0.03149 -0.00189 -0.00510 AFIX 43 H9 2 -0.025272 0.653417 0.439437 11.00000 -1.20000 AFIX 0 C10 1 -0.020384 0.701406 0.314741 11.00000 0.03735 0.03157 = 0.07351 -0.02023 -0.00223 -0.00546 C11 1 0.024624 0.669410 0.248701 11.00000 0.05953 0.04006 = 0.07088 -0.00639 0.01254 0.00238 AFIX 43 H11 2 0.010021 0.714057 0.193948 11.00000 -1.20000 AFIX 0 C12 1 0.090337 0.573425 0.261816 11.00000 0.05142 0.04070 = 0.06261 -0.01292 0.01342 0.00082 AFIX 43 H12 2 0.121592 0.554183 0.215780 11.00000 -1.20000 AFIX 0 C13 1 0.330520 0.080857 0.402484 11.00000 0.05098 0.02529 = 0.10893 -0.02462 0.01067 -0.01388 C14 1 0.432745 0.056861 0.370091 11.00000 0.04972 0.03716 = 0.14902 -0.03890 0.00994 -0.00318 AFIX 137 H14A 2 0.433009 0.092510 0.310698 11.00000 -1.50000 H14B 2 0.464229 -0.014867 0.380551 11.00000 -1.50000 H14C 2 0.466321 0.077605 0.398325 11.00000 -1.50000 AFIX 0 C15 1 0.279700 0.044761 0.358026 11.00000 0.06444 0.06490 = 0.20571 -0.08224 0.01222 -0.02183 AFIX 33 H15A 2 0.313512 -0.026717 0.368303 11.00000 -1.50000 H15B 2 0.214721 0.057599 0.379204 11.00000 -1.50000 H15C 2 0.278931 0.080717 0.298630 11.00000 -1.50000 AFIX 0 C16 1 0.329026 0.028239 0.496936 11.00000 0.11573 0.03416 = 0.11952 0.00108 0.00995 -0.00526 AFIX 137 H16A 2 0.350080 0.060482 0.524596 11.00000 -1.50000 H16B 2 0.371411 -0.041853 0.510515 11.00000 -1.50000 H16C 2 0.264641 0.032799 0.515451 11.00000 -1.50000 AFIX 0 C17 1 -0.096047 0.807874 0.299965 11.00000 0.05268 0.03319 = 0.09728 -0.02016 0.00573 0.00309 C21 1 0.453263 0.360011 0.340757 11.00000 0.02899 0.02591 = 0.03352 -0.00947 0.00104 -0.00978 C22 1 0.523602 0.313802 0.292042 11.00000 0.03328 0.02543 = 0.03473 -0.01094 0.00307 -0.00757 AFIX 43 H22 2 0.508440 0.323246 0.238212 11.00000 -1.20000 AFIX 0 C23 1 0.616193 0.253713 0.319835 11.00000 0.02976 0.02624 = 0.04357 -0.01181 0.00720 -0.00546 C24 1 0.636205 0.241334 0.398802 11.00000 0.03084 0.03528 = 0.04102 -0.00929 0.00060 -0.00627 AFIX 43 H24 2 0.698458 0.202265 0.419094 11.00000 -1.20000 AFIX 0 C25 1 0.565885 0.285644 0.448407 11.00000 0.03051 0.03746 = 0.03887 -0.00910 -0.00251 -0.00900 AFIX 43 H25 2 0.580943 0.274402 0.502762 11.00000 -1.20000 AFIX 0 C26 1 0.473304 0.346492 0.420769 11.00000 0.02872 0.02889 = 0.03313 -0.01074 0.00154 -0.00813 C27 1 0.402825 0.394915 0.475610 11.00000 0.03066 0.03712 = 0.02645 -0.01036 0.00367 -0.01353 C28 1 0.403698 0.478025 0.485433 11.00000 0.03432 0.04086 = 0.03985 -0.01905 0.00683 -0.01846 AFIX 43 H28 2 0.449581 0.504247 0.455974 11.00000 -1.20000 AFIX 0 C29 1 0.339626 0.524704 0.537037 11.00000 0.04214 0.04151 = 0.04470 -0.01976 0.00435 -0.01958 AFIX 43 H29 2 0.343901 0.580473 0.543658 11.00000 -1.20000 AFIX 0 C30 1 0.270396 0.491332 0.578473 11.00000 0.03391 0.03644 = 0.03801 -0.01631 0.00007 -0.01161 C31 1 0.267816 0.407615 0.569497 11.00000 0.03769 0.04199 = 0.04233 -0.01912 0.01138 -0.01915 AFIX 43 H31 2 0.221185 0.382444 0.598738 11.00000 -1.20000 AFIX 0 C32 1 0.333074 0.359631 0.517866 11.00000 0.04678 0.03396 = 0.03911 -0.01621 0.00628 -0.01948 AFIX 43 H32 2 0.329653 0.303195 0.511768 11.00000 -1.20000 AFIX 0 C33 1 0.689296 0.207654 0.262082 11.00000 0.04083 0.03782 = 0.04775 -0.01605 0.00709 -0.00054 C34 1 0.663416 0.133805 0.245483 11.00000 0.05966 0.07358 = 0.09782 -0.05727 0.00801 -0.01163 AFIX 137 H34A 2 0.599575 0.166448 0.223194 11.00000 -1.50000 H34B 2 0.665379 0.079120 0.296928 11.00000 -1.50000 H34C 2 0.708360 0.107526 0.205467 11.00000 -1.50000 AFIX 0 C35 1 0.693824 0.290292 0.182014 11.00000 0.06048 0.06712 = 0.05285 -0.01546 0.02171 -0.00193 AFIX 137 H35A 2 0.732729 0.260742 0.141145 11.00000 -1.50000 H35B 2 0.721735 0.330747 0.192701 11.00000 -1.50000 H35C 2 0.629909 0.332337 0.160893 11.00000 -1.50000 AFIX 0 C36 1 0.788902 0.152533 0.300118 11.00000 0.03573 0.06595 = 0.07431 -0.03009 0.00856 -0.00136 AFIX 137 H36A 2 0.786836 0.102072 0.353472 11.00000 -1.50000 H36B 2 0.809335 0.200312 0.307923 11.00000 -1.50000 H36C 2 0.833551 0.120344 0.263024 11.00000 -1.50000 AFIX 0 C37 1 0.196005 0.548496 0.630957 11.00000 0.03828 0.04938 = 0.04867 -0.02796 0.00548 -0.01329 C38 1 0.129276 0.496241 0.677269 11.00000 0.04607 0.07373 = 0.08551 -0.05061 0.02769 -0.02528 AFIX 137 H38A 2 0.093160 0.493673 0.637661 11.00000 -1.50000 H38B 2 0.085769 0.532998 0.712064 11.00000 -1.50000 H38C 2 0.165995 0.428455 0.711860 11.00000 -1.50000 AFIX 0 C39 1 0.139459 0.651795 0.575022 11.00000 0.05134 0.05365 = 0.07372 -0.02825 0.00710 0.00209 AFIX 137 H39A 2 0.182633 0.683053 0.541294 11.00000 -1.50000 H39B 2 0.098741 0.691969 0.608510 11.00000 -1.50000 H39C 2 0.100408 0.647219 0.539061 11.00000 -1.50000 AFIX 0 C40 1 0.246123 0.556574 0.695212 11.00000 0.05687 0.08076 = 0.05459 -0.04384 0.01301 -0.02615 AFIX 137 H40A 2 0.278364 0.490125 0.734314 11.00000 -1.50000 H40B 2 0.199537 0.598506 0.724877 11.00000 -1.50000 H40C 2 0.292497 0.586253 0.667510 11.00000 -1.50000 AFIX 0 C41 1 0.353815 0.466756 0.186055 11.00000 0.03230 0.03449 = 0.02831 -0.01056 -0.00047 -0.00658 C42 1 0.331545 0.408764 0.154315 11.00000 0.04074 0.04551 = 0.04331 -0.02185 0.00655 -0.01733 AFIX 43 H42 2 0.309755 0.359203 0.191015 11.00000 -1.20000 AFIX 0 C43 1 0.340063 0.420819 0.070897 11.00000 0.04739 0.07456 = 0.04286 -0.03345 0.00799 -0.02537 C44 1 0.368863 0.494974 0.020210 11.00000 0.07547 0.08085 = 0.03353 -0.02225 0.00414 -0.03780 AFIX 43 H44 2 0.374357 0.506052 -0.037342 11.00000 -1.20000 AFIX 0 C45 1 0.390403 0.554788 0.050153 11.00000 0.07495 0.05649 = 0.03184 -0.01198 0.00656 -0.02892 AFIX 43 H45 2 0.409376 0.606097 0.012574 11.00000 -1.20000 AFIX 0 C46 1 0.384793 0.541175 0.133793 11.00000 0.03985 0.04177 = 0.03440 -0.01365 0.00000 -0.01244 C47 1 0.412689 0.606848 0.159407 11.00000 0.04119 0.03745 = 0.03375 -0.00857 0.00395 -0.01592 C48 1 0.376666 0.709213 0.119645 11.00000 0.05860 0.04040 = 0.03917 -0.00741 -0.00987 -0.01375 AFIX 43 H48 2 0.332894 0.736529 0.076610 11.00000 -1.20000 AFIX 0 C49 1 0.402047 0.772093 0.140314 11.00000 0.05781 0.03223 = 0.04870 -0.00546 -0.00479 -0.01406 AFIX 43 H49 2 0.376221 0.841410 0.110729 11.00000 -1.20000 AFIX 0 C50 1 0.465273 0.736613 0.204134 11.00000 0.03995 0.03864 = 0.04111 -0.01334 0.00223 -0.01476 C51 1 0.502910 0.634442 0.242068 11.00000 0.03855 0.03974 = 0.04395 -0.01074 -0.00210 -0.01252 AFIX 43 H51 2 0.547700 0.607265 0.284259 11.00000 -1.20000 AFIX 0 C52 1 0.478579 0.570479 0.221611 11.00000 0.03828 0.03411 = 0.04548 -0.00350 -0.00277 -0.01301 AFIX 43 H52 2 0.506515 0.500939 0.249742 11.00000 -1.20000 AFIX 0 C53 1 0.319508 0.352005 0.039236 11.00000 0.10140 0.11233 = 0.07063 -0.06190 0.01775 -0.06193 SB1 8 0.000000 1.000000 0.500000 10.50000 0.04818 0.05233 = 0.05897 -0.02399 0.00489 -0.02272 F1 4 0.049170 1.083545 0.503656 11.00000 0.11720 0.15866 = 0.50966 -0.20086 0.01393 -0.07251 F2 4 0.003557 0.943387 0.610264 11.00000 0.14836 0.20260 = 0.07609 -0.00662 0.01484 0.06703 F3 4 0.122147 0.908692 0.490598 11.00000 0.06152 0.08025 = 0.08005 -0.03409 0.00292 -0.00703 C57 1 0.493345 0.804411 0.231172 11.00000 0.06112 0.03940 = 0.05688 -0.01308 -0.00588 -0.01364 C58 1 0.440168 0.912746 0.185392 11.00000 0.12649 0.04587 = 0.09627 -0.01928 -0.03530 -0.02510 AFIX 137 H58A 2 0.454169 0.926494 0.126249 11.00000 -1.50000 H58B 2 0.459497 0.953473 0.204854 11.00000 -1.50000 H58C 2 0.372214 0.928808 0.195264 11.00000 -1.50000 AFIX 0 C59 1 0.598977 0.777319 0.218248 11.00000 0.07510 0.07324 = 0.10322 -0.04359 -0.00250 -0.03978 AFIX 137 H59A 2 0.632361 0.709868 0.255349 11.00000 -1.50000 H59B 2 0.616923 0.824402 0.230040 11.00000 -1.50000 H59C 2 0.615928 0.780176 0.161000 11.00000 -1.50000 AFIX 0 C60 1 0.470072 0.783882 0.324198 11.00000 0.09093 0.07130 = 0.06522 -0.03467 -0.00591 -0.02358 AFIX 137 H60A 2 0.401537 0.804964 0.333009 11.00000 -1.50000 H60B 2 0.493419 0.821082 0.344427 11.00000 -1.50000 H60C 2 0.500506 0.712583 0.354143 11.00000 -1.50000 AFIX 0 C61 1 0.197750 0.794023 0.310232 11.00000 0.04232 0.02894 = 0.04728 -0.01609 0.00412 -0.00830 C62 1 0.130496 0.965097 0.262003 11.00000 0.07198 0.03126 = 0.10099 -0.01689 -0.00584 -0.01395 AFIX 23 H62A 2 0.155899 1.016478 0.254181 11.00000 -1.20000 H62B 2 0.061229 0.992740 0.270694 11.00000 -1.20000 AFIX 0 C63 1 0.156667 0.926409 0.188816 11.00000 0.08029 0.05029 = 0.06618 -0.00439 0.00078 -0.02248 AFIX 23 H63A 2 0.102516 0.955303 0.151840 11.00000 -1.20000 H63B 2 0.210949 0.940683 0.156689 11.00000 -1.20000 AFIX 0 PART 1 C18A 1 -0.184815 0.804786 0.320336 21.00000 0.05104 0.04926 = 0.23977 -0.02622 0.00408 -0.00595 AFIX 137 H18A 2 -0.213431 0.811242 0.271452 21.00000 -1.50000 H18B 2 -0.224456 0.859611 0.340652 21.00000 -1.50000 H18C 2 -0.179551 0.741311 0.363362 21.00000 -1.50000 AFIX 0 C19A 1 -0.083330 0.881779 0.209719 21.00000 0.06859 0.03361 = 0.12741 0.00054 -0.01510 0.00478 AFIX 137 H19A 2 -0.021602 0.886610 0.205429 21.00000 -1.50000 H19B 2 -0.133331 0.947847 0.201107 21.00000 -1.50000 H19C 2 -0.087326 0.855805 0.167761 21.00000 -1.50000 AFIX 0 C20A 1 -0.065682 0.850076 0.357865 21.00000 0.12288 0.04881 = 0.14164 -0.05486 0.01533 -0.02217 AFIX 137 H20A 2 -0.061962 0.805352 0.415047 21.00000 -1.50000 H20B 2 -0.112689 0.916422 0.354237 21.00000 -1.50000 H20C 2 -0.003878 0.854192 0.339618 21.00000 -1.50000 AFIX 0 PART 2 C18B 1 -0.184678 0.809265 0.253900 -21.00000 0.06039 0.03561 = 0.07822 -0.00649 -0.01173 0.01151 AFIX 33 H18D 2 -0.205125 0.755399 0.289064 -21.00000 -1.50000 H18E 2 -0.237919 0.873239 0.245383 -21.00000 -1.50000 H18F 2 -0.162297 0.799963 0.200585 -21.00000 -1.50000 AFIX 0 C19B 1 -0.061220 0.877569 0.258707 -21.00000 0.06963 0.04456 = 0.18746 -0.02527 0.03581 -0.00976 AFIX 33 H19D 2 -0.111289 0.943475 0.250770 -21.00000 -1.50000 H19E 2 -0.010001 0.869690 0.290078 -21.00000 -1.50000 H19F 2 -0.036742 0.870826 0.204913 -21.00000 -1.50000 AFIX 0 C20B 1 -0.146101 0.822998 0.382613 -21.00000 0.05186 0.05701 = 0.11190 -0.05248 0.00180 -0.00018 AFIX 33 H20D 2 -0.171001 0.770823 0.411635 -21.00000 -1.50000 H20E 2 -0.100388 0.819352 0.417474 -21.00000 -1.50000 H20F 2 -0.198101 0.888244 0.370224 -21.00000 -1.50000 AFIX 0 PART 1 C54A 1 0.283121 0.278757 0.105441 31.00000 0.11484 0.11473 = 0.09759 -0.06707 0.02623 -0.07331 AFIX 33 H54A 2 0.271491 0.237248 0.081041 31.00000 -1.50000 H54B 2 0.330243 0.236462 0.148691 31.00000 -1.50000 H54C 2 0.224140 0.315282 0.129326 31.00000 -1.50000 AFIX 0 C55A 1 0.411887 0.295397 0.000945 31.00000 0.12605 0.12170 = 0.12361 -0.08086 0.04821 -0.06747 AFIX 33 H55A 2 0.434965 0.343094 -0.041709 31.00000 -1.50000 H55B 2 0.459381 0.252880 0.043860 31.00000 -1.50000 H55C 2 0.400134 0.254172 -0.023696 31.00000 -1.50000 AFIX 0 C56A 1 0.246812 0.412730 -0.031099 31.00000 0.13997 0.22011 = 0.09598 -0.04520 -0.01432 -0.07487 AFIX 33 H56A 2 0.269130 0.460514 -0.074502 31.00000 -1.50000 H56B 2 0.239545 0.367538 -0.054002 31.00000 -1.50000 H56C 2 0.185798 0.448531 -0.009263 31.00000 -1.50000 AFIX 0 PART 2 C55B 1 0.392284 0.249767 0.075410 -31.00000 0.14242 0.12563 = 0.12657 -0.06157 -0.00290 -0.04210 AFIX 33 H55D 2 0.388035 0.229426 0.135681 -31.00000 -1.50000 H55E 2 0.381087 0.202924 0.057269 -31.00000 -1.50000 H55F 2 0.455341 0.250070 0.056946 -31.00000 -1.50000 AFIX 0 C54B 1 0.220532 0.354219 0.068920 -31.00000 0.11505 0.17421 = 0.09487 -0.09111 0.03177 -0.09136 AFIX 33 H54D 2 0.173859 0.421527 0.044717 -31.00000 -1.50000 H54E 2 0.207612 0.307521 0.051935 -31.00000 -1.50000 H54F 2 0.216674 0.335028 0.129138 -31.00000 -1.50000 AFIX 0 C56B 1 0.323914 0.386413 -0.054833 -31.00000 0.11234 0.16305 = 0.07168 -0.07882 0.01841 -0.07293 AFIX 33 H56D 2 0.275740 0.453327 -0.076971 -31.00000 -1.50000 H56E 2 0.386542 0.387567 -0.074102 -31.00000 -1.50000 H56F 2 0.312288 0.340421 -0.073778 -31.00000 -1.50000 AFIX 0 HKLF 4 REM jcm00722a_0m_a.res in P-1 REM wR2 = 0.1680, GooF = S = 1.097, Restrained GooF = 1.096 for all data REM R1 = 0.0575 for 15637 Fo > 4sig(Fo) and 0.0824 for all 20146 data REM 716 parameters refined using 102 restraints END WGHT 0.0675 16.6621 REM Highest difference peak 1.293, deepest hole -2.432, 1-sigma level 0.140 Q1 1 0.9086 0.1631 0.0057 11.00000 0.05 1.29 Q2 1 0.5327 0.6745 0.3328 11.00000 0.05 1.21 Q3 1 0.2390 0.5190 0.3682 11.00000 0.05 1.08 Q4 1 0.3445 0.5645 0.3832 11.00000 0.05 1.06 Q5 1 0.5250 0.6992 0.3268 11.00000 0.05 1.05 Q6 1 0.2837 0.5013 0.3244 11.00000 0.05 0.99 Q7 1 0.3628 0.5408 0.3598 11.00000 0.05 0.96 Q8 1 0.2801 0.4974 0.3878 11.00000 0.05 0.89 Q9 1 0.3195 0.6411 0.2938 11.00000 0.05 0.88 Q10 1 0.3371 0.5017 0.3207 11.00000 0.05 0.86 Q11 1 0.1957 0.6364 0.2903 11.00000 0.05 0.85 Q12 1 0.2485 0.6246 0.2410 11.00000 0.05 0.84 Q13 1 0.3659 0.5573 0.2984 11.00000 0.05 0.80 Q14 1 0.2709 0.6591 0.3350 11.00000 0.05 0.78 Q15 1 0.3013 0.6442 0.3455 11.00000 0.05 0.78 Q16 1 0.3205 0.5807 0.2581 11.00000 0.05 0.77 Q17 1 0.0329 1.0366 0.5732 11.00000 0.05 0.76 Q18 1 0.2425 0.6373 0.3805 11.00000 0.05 0.75 Q19 1 0.2297 0.6633 0.3386 11.00000 0.05 0.75 Q20 1 0.2138 0.5921 0.2749 11.00000 0.05 0.74 Q21 1 0.1821 0.7202 0.3196 11.00000 0.05 0.68 Q22 1 0.2346 0.5714 0.4021 11.00000 0.05 0.66 Q23 1 0.3177 0.6201 0.3586 11.00000 0.05 0.65 Q24 1 -0.0161 0.9227 0.5614 11.00000 0.05 0.60 Q25 1 0.0931 0.8004 0.3190 11.00000 0.05 0.59 Q26 1 0.1583 0.5653 0.3835 11.00000 0.05 0.58 Q27 1 0.1455 0.6740 0.3380 11.00000 0.05 0.57 Q28 1 0.1407 0.5928 0.3772 11.00000 0.05 0.54 Q29 1 0.1802 0.6184 0.2405 11.00000 0.05 0.54 Q30 1 0.2343 0.7331 0.2998 11.00000 0.05 0.54 Q31 1 0.0416 1.0066 0.5659 11.00000 0.05 0.53 Q32 1 0.3935 0.5743 0.2925 11.00000 0.05 0.52 Q33 1 0.2657 0.7206 0.3112 11.00000 0.05 0.51 Q34 1 0.4033 0.4648 0.1782 11.00000 0.05 0.51 Q35 1 0.2818 0.6820 0.3825 11.00000 0.05 0.50 Q36 1 0.4586 0.3165 0.1993 11.00000 0.05 0.50 Q37 1 0.0173 0.9593 0.6165 11.00000 0.05 0.50 Q38 1 0.1827 0.2200 0.0238 11.00000 0.05 0.50 Q39 1 0.2882 0.4461 0.4198 11.00000 0.05 0.49 Q40 1 0.3654 0.4247 0.8018 11.00000 0.05 0.49 Q41 1 0.2027 0.7303 0.2962 11.00000 0.05 0.49 ; _shelx_res_checksum 26900 _shelx_hkl_file ; -2 0 0 772.12 24.10 -2 0 0 780.32 21.60 -2 0 0 673.53 21.90 -2 0 0 758.62 23.40 -2 0 0 716.03 20.50 -2 0 0 802.12 22.40 -2 0 0 747.13 23.40 -2 0 0 729.33 20.70 -2 0 0 778.92 19.90 -2 0 0 695.83 19.60 2 0 0 710.93 23.60 2 0 0 740.23 21.40 2 0 0 673.53 21.80 2 0 0 760.02 23.40 2 0 0 729.53 20.60 2 0 0 720.93 20.60 2 0 0 707.53 20.10 2 0 0 787.22 20.40 2 0 0 736.13 20.80 2 0 0 773.32 23.50 2 0 0 756.92 20.90 -3 0 0 4493.85 113.29 -3 0 0 4213.78 111.79 -3 0 0 4676.33 117.19 -3 0 0 4821.92 117.39 3 0 0 4502.15 117.69 3 0 0 4322.57 113.09 -4 0 0 560.34 24.20 -4 0 0 530.55 16.60 -4 0 0 521.95 21.50 -4 0 0 519.95 16.50 -4 0 0 542.95 18.60 -4 0 0 530.25 18.70 -4 0 0 572.04 19.10 -4 0 0 557.74 23.30 -4 0 0 582.34 20.30 -4 0 0 620.64 24.10 4 0 0 542.45 21.30 4 0 0 551.54 19.10 4 0 0 552.34 18.30 4 0 0 563.24 23.40 4 0 0 557.44 20.00 4 0 0 560.84 23.30 4 0 0 555.04 18.90 4 0 0 559.64 19.00 4 0 0 545.05 24.00 -5 0 0 751.02 28.80 -5 0 0 731.93 21.60 -5 0 0 732.63 31.50 -5 0 0 746.03 26.40 -5 0 0 734.63 24.90 -5 0 0 779.12 31.10 -5 0 0 743.53 24.70 -5 0 0 738.73 25.00 -5 0 0 771.62 21.90 5 0 0 808.22 28.90 5 0 0 749.53 26.40 5 0 0 752.82 30.40 5 0 0 712.93 24.70 5 0 0 752.72 25.50 5 0 0 748.73 31.70 5 0 0 777.72 31.00 5 0 0 762.12 25.30 5 0 0 707.43 24.10 5 0 0 718.43 24.30 5 0 0 734.83 25.00 -6 0 0 66.19 5.10 -6 0 0 65.59 8.00 -6 0 0 73.59 8.10 -6 0 0 70.69 11.80 -6 0 0 76.09 8.30 -6 0 0 82.39 8.30 -6 0 0 73.49 10.50 -6 0 0 84.29 14.40 -6 0 0 66.79 9.20 -6 0 0 71.29 5.30 6 0 0 72.19 8.50 6 0 0 61.29 7.50 6 0 0 68.39 12.20 6 0 0 62.39 11.30 6 0 0 69.99 7.90 6 0 0 67.59 8.10 6 0 0 78.89 12.00 6 0 0 68.39 8.50 6 0 0 82.19 10.50 6 0 0 68.69 8.00 6 0 0 89.79 13.30 6 0 0 76.59 8.90 -7 0 0 1273.97 33.00 -7 0 0 1304.57 46.80 -7 0 0 1281.27 49.20 -7 0 0 1256.67 40.40 -7 0 0 1234.48 40.30 -7 0 0 1298.17 42.80 -7 0 0 1266.67 40.70 -7 0 0 1297.87 51.19 -7 0 0 1239.58 40.00 7 0 0 1288.67 41.50 7 0 0 1228.58 48.20 7 0 0 1365.76 60.79 7 0 0 1306.07 41.10 7 0 0 1300.77 50.09 7 0 0 1246.28 40.30 7 0 0 1273.37 40.30 7 0 0 1233.08 50.29 7 0 0 1288.27 40.80 7 0 0 1205.48 44.70 7 0 0 1249.28 42.40 -8 0 0 327.67 17.40 -8 0 0 338.67 17.90 -8 0 0 376.56 25.70 -8 0 0 379.46 27.40 -8 0 0 318.57 22.40 -8 0 0 316.67 18.10 -8 0 0 340.37 18.20 8 0 0 323.27 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32.50 8 -3 0 401.56 28.20 8 -3 0 342.27 23.90 8 -3 0 400.36 25.10 8 -3 0 381.86 30.00 8 -3 0 345.07 26.90 8 -3 0 417.36 26.20 8 -3 0 423.06 25.80 8 -3 0 387.46 17.10 -8 3 0 383.36 25.30 -8 3 0 377.56 28.20 -8 3 0 382.96 25.50 -8 3 0 442.76 31.80 -8 3 0 389.26 24.30 -8 3 0 416.36 24.50 -8 3 0 410.96 23.80 7 -3 0 1957.60 67.29 7 -3 0 1913.81 65.99 7 -3 0 1931.41 55.09 7 -3 0 1956.30 66.39 7 -3 0 2050.39 65.59 7 -3 0 1836.62 68.19 7 -3 0 1954.50 65.09 7 -3 0 1932.81 65.29 7 -3 0 1947.21 70.29 7 -3 0 1984.90 72.39 7 -3 0 2041.90 66.49 -7 3 0 1999.70 65.29 -7 3 0 2073.39 74.29 -7 3 0 2154.28 71.19 -7 3 0 2030.10 66.39 -7 3 0 1971.00 63.89 -7 3 0 1959.40 62.99 -7 3 0 1969.70 64.59 6 -3 0 2458.85 78.69 6 -3 0 2336.07 64.19 6 -3 0 2316.77 79.39 6 -3 0 2380.26 74.59 6 -3 0 2455.45 75.19 6 -3 0 2403.66 75.59 6 -3 0 2528.05 76.39 6 -3 0 2418.66 74.19 6 -3 0 2285.77 74.29 6 -3 0 2399.36 80.29 6 -3 0 2383.56 73.79 -6 3 0 2351.56 72.99 -6 3 0 2438.86 77.69 -6 3 0 2367.26 73.59 -6 3 0 2424.96 72.89 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16.70 7 16 -3 -1.10 16.10 7 16 -3 21.20 17.50 7 16 -3 -12.10 15.70 7 16 -3 13.80 20.00 7 16 -3 -12.30 11.80 7 16 -3 5.30 17.30 -7 -16 3 15.30 17.10 -7 -16 3 -2.30 28.40 -7 -16 3 -5.80 14.10 -7 -16 3 -5.30 14.70 6 16 -3 101.49 25.50 6 16 -3 81.29 23.90 6 16 -3 81.19 25.00 6 16 -3 162.68 32.70 6 16 -3 96.09 26.40 6 16 -3 91.59 26.50 -6 -16 3 107.29 23.10 -6 -16 3 112.49 36.50 -6 -16 3 69.29 22.80 -6 -16 3 100.09 25.10 5 16 -3 19.00 17.60 5 16 -3 -13.20 16.90 5 16 -3 4.40 17.00 5 16 -3 -24.90 14.30 5 16 -3 4.80 17.00 5 16 -3 8.50 19.70 -5 -16 3 -10.90 20.90 -5 -16 3 -5.30 17.10 -5 -16 3 7.80 19.30 -5 -16 3 11.50 16.70 -5 -16 3 -44.40 18.20 4 16 -3 313.47 39.50 4 16 -3 243.58 35.70 4 16 -3 201.68 32.10 4 16 -3 225.08 37.30 4 16 -3 230.48 33.30 4 16 -3 236.68 36.00 -4 -16 3 242.08 38.80 -4 -16 3 242.28 35.20 -4 -16 3 216.88 32.00 -4 -16 3 269.57 45.80 -4 -16 3 227.68 54.99 3 16 -3 67.49 22.90 3 16 -3 54.79 22.40 3 16 -3 97.79 38.50 3 16 -3 103.79 27.10 3 16 -3 68.39 27.10 3 16 -3 71.49 26.40 -3 -16 3 96.99 31.60 -3 -16 3 135.19 30.50 -3 -16 3 67.19 37.80 -3 -16 3 75.69 27.60 -3 -16 3 70.39 24.00 2 16 -3 44.60 23.30 2 16 -3 27.30 20.60 2 16 -3 14.40 21.60 2 16 -3 35.00 21.40 2 16 -3 10.60 23.00 -2 -16 3 39.10 21.20 -2 -16 3 35.20 10.80 -2 -16 3 -5.60 22.40 -2 -16 3 16.30 22.40 -2 -16 3 14.90 22.40 1 16 -3 245.88 38.10 1 16 -3 247.48 38.10 1 16 -3 203.58 35.50 1 16 -3 281.67 38.70 1 16 -3 240.18 40.70 1 16 -3 290.77 23.90 -1 -16 3 359.86 43.60 -1 -16 3 222.18 36.90 -1 -16 3 331.67 27.50 -1 -16 3 335.87 40.30 -1 -16 3 209.08 36.50 0 16 -3 3.20 18.10 0 16 -3 26.50 22.90 0 16 -3 11.20 10.20 0 16 -3 -48.80 19.20 0 16 -3 -11.70 20.40 0 -16 3 -19.60 21.10 0 -16 3 -4.10 34.40 0 -16 3 41.80 22.80 0 -16 3 10.30 12.70 0 -16 3 -1.00 20.90 -1 16 -3 52.19 16.60 -1 16 -3 33.90 27.00 -1 16 -3 71.09 23.70 -1 16 -3 62.09 24.80 -1 16 -3 34.90 22.90 1 -16 3 69.59 30.30 1 -16 3 54.09 27.30 1 -16 3 81.29 19.10 1 -16 3 84.19 26.60 1 -16 3 85.39 29.50 -2 16 -3 -27.90 19.90 -2 16 -3 -0.10 21.30 -2 16 -3 -53.59 19.50 2 -16 3 -17.80 20.50 2 -16 3 -17.60 18.40 2 -16 3 -15.40 14.20 2 -16 3 -4.70 25.90 -3 16 -3 35.00 14.40 -3 16 -3 48.80 29.00 -3 16 -3 -10.80 22.90 -3 16 -3 14.20 23.10 3 -16 3 67.89 21.30 3 -16 3 95.39 29.70 3 -16 3 49.40 20.50 3 -16 3 55.39 30.10 -4 16 -3 23.10 27.00 4 -16 3 -19.00 15.80 17 15 -3 99.69 19.30 17 15 -3 75.79 17.80 17 15 -3 50.79 16.40 17 15 -3 57.89 17.10 17 15 -3 55.59 13.00 17 15 -3 108.19 24.20 -17 -15 3 183.58 51.09 -17 -15 3 101.89 37.40 16 15 -3 -18.10 16.80 16 15 -3 -17.20 13.90 16 15 -3 4.00 10.80 16 15 -3 -12.50 13.20 16 15 -3 17.10 14.90 16 15 -3 29.10 9.40 16 15 -3 13.00 13.30 16 15 -3 -12.10 11.00 -16 -15 3 59.49 35.90 -16 -15 3 14.40 28.60 15 15 -3 31.00 17.40 15 15 -3 34.30 15.00 15 15 -3 43.30 16.70 15 15 -3 7.60 17.50 15 15 -3 8.20 10.90 15 15 -3 14.80 13.70 -15 -15 3 62.69 32.20 -15 -15 3 59.29 35.60 14 15 -3 142.69 19.90 14 15 -3 109.89 30.30 14 15 -3 129.79 21.80 14 15 -3 139.89 22.30 14 15 -3 215.48 43.20 14 15 -3 159.28 23.50 14 15 -3 190.38 23.90 14 15 -3 147.09 23.10 -14 -15 3 167.18 19.20 -14 -15 3 157.88 18.00 -14 -15 3 236.28 52.59 -14 -15 3 124.69 14.60 -14 -15 3 180.08 42.80 13 15 -3 6.90 12.50 13 15 -3 -5.20 13.30 13 15 -3 14.10 13.50 13 15 -3 -17.60 13.10 13 15 -3 -19.80 17.40 13 15 -3 -25.70 15.60 13 15 -3 -9.80 16.00 13 15 -3 -8.50 11.20 -13 -15 3 35.00 13.80 -13 -15 3 -28.40 13.60 -13 -15 3 41.00 31.00 -13 -15 3 -8.10 10.40 -13 -15 3 61.39 31.50 12 15 -3 99.79 18.40 12 15 -3 60.39 17.70 12 15 -3 83.89 21.00 12 15 -3 74.79 19.10 12 15 -3 52.09 18.30 12 15 -3 69.19 18.10 12 15 -3 9.90 20.10 12 15 -3 71.89 20.30 -12 -15 3 66.69 38.10 -12 -15 3 84.29 34.90 -12 -15 3 62.59 17.80 -12 -15 3 54.09 22.70 -12 -15 3 30.60 14.30 11 15 -3 19.40 14.70 11 15 -3 47.50 16.00 11 15 -3 9.30 16.60 11 15 -3 34.70 17.80 11 15 -3 10.80 14.50 11 15 -3 7.30 15.90 11 15 -3 23.50 15.80 -11 -15 3 -15.00 14.70 -11 -15 3 39.60 17.50 -11 -15 3 29.20 31.40 -11 -15 3 46.10 27.90 -11 -15 3 9.40 12.50 10 15 -3 111.09 23.80 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90.39 23.20 -7 -15 3 126.59 36.10 -7 -15 3 128.89 21.60 -7 -15 3 84.59 20.60 -7 -15 3 66.29 16.90 -7 -15 3 79.39 19.80 -7 -15 3 111.89 24.80 6 15 -3 118.99 23.70 6 15 -3 164.98 27.20 6 15 -3 107.69 24.60 6 15 -3 116.09 23.30 6 15 -3 115.19 25.80 6 15 -3 131.79 24.70 6 15 -3 161.28 27.10 -6 -15 3 159.98 37.80 -6 -15 3 131.09 22.50 -6 -15 3 158.48 24.40 -6 -15 3 87.69 23.50 -6 -15 3 107.69 27.70 -6 -15 3 150.98 24.10 5 15 -3 37.00 19.40 5 15 -3 76.79 20.30 5 15 -3 57.89 20.40 5 15 -3 12.90 15.60 5 15 -3 44.70 19.50 5 15 -3 44.00 21.40 5 15 -3 50.39 21.10 -5 -15 3 48.20 28.00 -5 -15 3 46.50 17.20 -5 -15 3 18.20 17.60 -5 -15 3 52.59 19.80 -5 -15 3 17.30 14.70 -5 -15 3 26.70 21.10 4 15 -3 75.69 21.70 4 15 -3 64.69 20.50 4 15 -3 86.99 24.40 4 15 -3 64.09 23.40 4 15 -3 73.09 21.40 4 15 -3 54.99 22.50 4 15 -3 71.19 23.60 -4 -15 3 26.20 18.20 -4 -15 3 108.39 22.50 -4 -15 3 35.20 22.50 -4 -15 3 47.10 20.80 -4 -15 3 82.29 28.90 -4 -15 3 62.69 18.70 -4 -15 3 66.49 22.80 3 15 -3 180.38 31.30 3 15 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11.40 25.70 5 -15 3 18.80 26.90 5 -15 3 50.69 24.10 5 -15 3 15.60 14.20 5 -15 3 -17.50 17.60 5 -15 3 3.00 24.20 18 14 -3 -2.80 11.70 18 14 -3 -12.70 8.90 18 14 -3 -45.20 16.50 18 14 -3 -19.90 7.40 -18 -14 3 3.00 25.60 -18 -14 3 -42.40 29.90 17 14 -3 -7.40 9.30 17 14 -3 22.90 12.70 17 14 -3 13.70 10.20 17 14 -3 -11.00 13.00 -17 -14 3 24.40 33.10 -17 -14 3 -17.30 25.50 16 14 -3 110.89 18.00 16 14 -3 80.79 13.90 16 14 -3 93.79 14.30 16 14 -3 101.99 19.50 16 14 -3 117.39 20.50 16 14 -3 118.79 19.20 16 14 -3 93.19 14.90 16 14 -3 91.39 15.50 -16 -14 3 126.79 36.70 -16 -14 3 143.19 43.10 15 14 -3 77.59 18.70 15 14 -3 32.10 12.50 15 14 -3 8.20 11.20 15 14 -3 40.60 13.10 15 14 -3 40.70 13.70 15 14 -3 24.90 15.60 -15 -14 3 44.80 32.40 -15 -14 3 46.30 27.00 14 14 -3 107.69 22.10 14 14 -3 90.69 27.60 14 14 -3 126.39 17.90 14 14 -3 93.09 18.70 14 14 -3 84.49 16.90 14 14 -3 98.59 19.80 14 14 -3 88.59 18.10 14 14 -3 125.79 18.90 -14 -14 3 141.39 39.70 -14 -14 3 81.09 13.70 -14 -14 3 131.99 42.10 -14 -14 3 88.89 12.10 -14 -14 3 99.09 11.00 -14 -14 3 85.19 11.60 13 14 -3 39.80 16.20 13 14 -3 23.00 24.90 13 14 -3 9.00 11.50 13 14 -3 33.10 13.20 13 14 -3 40.80 15.00 13 14 -3 -12.00 13.00 -13 -14 3 5.90 17.40 -13 -14 3 25.80 12.70 -13 -14 3 23.80 31.00 -13 -14 3 2.90 10.60 -13 -14 3 38.20 27.20 -13 -14 3 14.60 12.30 12 14 -3 258.97 27.50 12 14 -3 198.58 25.70 12 14 -3 238.58 28.50 12 14 -3 278.67 26.10 12 14 -3 253.67 27.70 12 14 -3 275.37 28.50 12 14 -3 197.98 25.70 12 14 -3 191.28 31.60 -12 -14 3 272.47 46.70 -12 -14 3 190.68 23.00 -12 -14 3 244.68 26.60 -12 -14 3 199.88 24.40 -12 -14 3 197.48 47.70 11 14 -3 -0.80 14.00 11 14 -3 5.40 12.80 11 14 -3 28.70 17.30 11 14 -3 11.50 14.10 11 14 -3 31.80 13.90 11 14 -3 23.40 13.40 11 14 -3 18.80 14.90 11 14 -3 12.50 13.60 -11 -14 3 34.70 31.20 -11 -14 3 22.30 14.70 -11 -14 3 10.70 14.00 -11 -14 3 20.00 13.20 -11 -14 3 17.40 26.40 -11 -14 3 -3.70 11.10 10 14 -3 57.99 17.90 10 14 -3 74.99 18.10 10 14 -3 90.39 17.90 10 14 -3 46.70 18.20 10 14 -3 81.79 18.50 10 14 -3 44.30 17.40 10 14 -3 69.59 18.90 10 14 -3 73.79 20.20 -10 -14 3 71.69 17.50 -10 -14 3 46.20 44.30 -10 -14 3 83.69 18.60 -10 -14 3 116.49 36.80 -10 -14 3 62.19 17.50 -10 -14 3 76.29 19.30 9 14 -3 121.29 22.40 9 14 -3 149.99 25.50 9 14 -3 138.09 21.40 9 14 -3 116.49 20.90 9 14 -3 98.99 21.30 9 14 -3 122.59 21.70 9 14 -3 124.19 21.00 -9 -14 3 120.19 14.90 -9 -14 3 125.99 23.10 -9 -14 3 113.79 21.90 -9 -14 3 165.98 38.10 -9 -14 3 167.88 23.70 -9 -14 3 109.99 22.30 8 14 -3 193.38 25.10 8 14 -3 261.27 27.30 8 14 -3 284.87 31.10 8 14 -3 190.38 25.40 8 14 -3 270.87 27.90 8 14 -3 205.68 29.60 8 14 -3 212.18 30.00 -8 -14 3 242.68 27.10 -8 -14 3 197.98 26.80 -8 -14 3 152.58 52.69 -8 -14 3 214.98 28.20 -8 -14 3 233.08 43.40 -8 -14 3 157.78 18.60 7 14 -3 117.29 22.50 7 14 -3 147.19 25.40 7 14 -3 119.19 23.20 7 14 -3 161.18 23.80 7 14 -3 127.39 22.10 7 14 -3 76.09 19.50 7 14 -3 87.49 20.40 -7 -14 3 77.99 17.30 -7 -14 3 107.39 20.60 -7 -14 3 105.99 21.50 -7 -14 3 143.59 25.60 -7 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34.60 9 12 -3 613.54 37.10 9 12 -3 628.64 38.70 9 12 -3 682.73 37.40 9 12 -3 605.14 36.00 -9 -12 3 627.94 37.10 -9 -12 3 665.63 38.10 -9 -12 3 682.43 37.50 -9 -12 3 684.03 51.19 -9 -12 3 623.14 37.80 8 12 -3 67.09 15.20 8 12 -3 49.99 15.30 8 12 -3 46.00 14.30 8 12 -3 35.40 14.80 8 12 -3 44.70 14.50 8 12 -3 59.79 15.30 8 12 -3 55.49 13.80 -8 -12 3 74.99 27.90 -8 -12 3 53.79 15.30 -8 -12 3 50.39 15.40 -8 -12 3 64.99 14.70 -8 -12 3 85.59 17.70 -8 -12 3 47.10 9.90 -8 -12 3 58.59 22.60 -8 -12 3 76.09 11.40 7 12 -3 213.78 35.30 7 12 -3 175.08 22.30 7 12 -3 141.79 21.30 7 12 -3 140.99 19.80 7 12 -3 189.88 23.90 7 12 -3 152.88 20.30 7 12 -3 168.38 24.90 -7 -12 3 150.38 19.00 -7 -12 3 146.69 22.00 -7 -12 3 189.28 22.00 -7 -12 3 169.48 23.00 -7 -12 3 159.88 34.20 6 12 -3 415.86 30.00 6 12 -3 288.87 30.60 6 12 -3 353.76 29.00 6 12 -3 393.56 29.90 6 12 -3 353.46 28.70 6 12 -3 353.76 31.00 6 12 -3 361.36 32.80 -6 -12 3 351.96 28.80 -6 -12 3 394.86 29.50 -6 -12 3 312.47 26.40 -6 -12 3 329.77 30.20 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32.60 18.30 12 17 -4 -4.30 18.60 12 17 -4 29.50 17.80 12 17 -4 56.69 23.40 12 17 -4 -6.10 20.70 12 17 -4 -5.90 21.00 -12 -17 4 -8.70 26.80 -12 -17 4 48.00 34.60 -12 -17 4 24.10 20.10 11 17 -4 13.10 19.80 11 17 -4 44.00 20.10 11 17 -4 49.20 19.60 11 17 -4 -15.20 18.20 -11 -17 4 1.40 23.40 -11 -17 4 4.30 18.60 -11 -17 4 -2.70 31.30 -11 -17 4 -5.80 21.10 10 17 -4 -10.20 13.50 10 17 -4 -2.50 19.50 10 17 -4 12.50 17.70 10 17 -4 -5.60 16.30 10 17 -4 -22.00 18.20 10 17 -4 -19.30 19.30 10 17 -4 -24.80 17.30 -10 -17 4 -28.40 23.00 -10 -17 4 49.60 27.90 -10 -17 4 -32.30 17.20 -10 -17 4 43.50 32.20 9 17 -4 105.89 26.40 9 17 -4 80.39 25.60 9 17 -4 42.40 26.00 9 17 -4 83.99 23.30 9 17 -4 110.39 30.70 9 17 -4 125.99 26.80 9 17 -4 48.40 20.40 -9 -17 4 65.29 29.40 -9 -17 4 103.89 26.50 -9 -17 4 22.60 33.90 -9 -17 4 115.49 42.70 -9 -17 4 95.69 24.60 -9 -17 4 58.69 12.80 8 17 -4 50.19 23.50 8 17 -4 28.60 21.20 8 17 -4 21.20 21.90 8 17 -4 28.50 22.30 8 17 -4 -6.60 19.50 -8 -17 4 12.40 17.10 -8 -17 4 12.90 26.70 -8 -17 4 -10.50 21.60 -8 -17 4 -4.40 22.80 -8 -17 4 -25.80 17.60 -8 -17 4 26.00 20.80 7 17 -4 100.99 27.40 7 17 -4 63.39 25.30 7 17 -4 19.70 23.10 7 17 -4 25.60 23.10 7 17 -4 95.59 27.20 7 17 -4 53.99 22.60 -7 -17 4 86.49 37.30 -7 -17 4 67.89 26.00 -7 -17 4 60.29 22.80 -7 -17 4 72.29 26.10 -7 -17 4 37.30 18.20 6 17 -4 18.60 23.70 6 17 -4 -4.10 18.40 6 17 -4 -14.40 19.40 6 17 -4 -8.50 17.40 6 17 -4 10.70 21.00 -6 -17 4 -47.20 20.30 -6 -17 4 -5.10 22.70 -6 -17 4 53.79 23.50 -6 -17 4 -3.50 19.20 -6 -17 4 22.80 30.10 5 17 -4 171.18 32.60 5 17 -4 179.48 34.00 5 17 -4 218.88 34.80 5 17 -4 141.89 32.60 5 17 -4 147.59 32.00 -5 -17 4 195.68 30.60 -5 -17 4 226.98 36.90 -5 -17 4 195.98 42.10 -5 -17 4 159.68 32.90 4 17 -4 -10.80 17.80 4 17 -4 -12.70 21.90 4 17 -4 32.00 23.60 4 17 -4 17.00 24.50 4 17 -4 4.00 23.10 -4 -17 4 39.30 26.50 -4 -17 4 22.30 20.80 -4 -17 4 62.29 41.60 -4 -17 4 20.50 27.30 -4 -17 4 12.20 24.20 3 17 -4 84.49 27.90 3 17 -4 61.19 25.60 3 17 -4 31.20 27.70 3 17 -4 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30.30 18.10 9 16 -4 104.29 21.90 9 16 -4 92.49 35.90 9 16 -4 89.59 25.00 -9 -16 4 64.19 21.30 -9 -16 4 69.99 35.70 -9 -16 4 57.79 15.10 -9 -16 4 45.10 28.10 -9 -16 4 53.89 21.50 8 16 -4 8.50 18.50 8 16 -4 -9.30 16.40 8 16 -4 0.90 16.20 8 16 -4 10.50 17.80 8 16 -4 4.40 15.90 8 16 -4 32.50 17.60 -8 -16 4 33.40 19.40 -8 -16 4 -15.30 21.60 -8 -16 4 24.90 18.60 -8 -16 4 -29.60 24.70 -8 -16 4 -20.00 12.80 -8 -16 4 8.10 15.30 7 16 -4 71.29 24.30 7 16 -4 97.39 26.10 7 16 -4 82.09 23.50 7 16 -4 99.19 24.90 7 16 -4 110.69 26.10 -7 -16 4 66.59 18.60 -7 -16 4 84.89 20.50 -7 -16 4 120.79 27.80 -7 -16 4 107.29 37.70 -7 -16 4 88.39 25.60 6 16 -4 -11.80 15.80 6 16 -4 27.80 18.90 6 16 -4 -29.00 16.20 6 16 -4 -30.70 18.80 6 16 -4 -31.60 16.80 6 16 -4 -15.90 15.30 -6 -16 4 1.60 17.20 -6 -16 4 -0.10 25.10 -6 -16 4 -17.00 20.50 -6 -16 4 10.00 17.20 -6 -16 4 -16.50 16.20 5 16 -4 27.30 20.30 5 16 -4 66.39 25.00 5 16 -4 4.10 19.70 5 16 -4 37.90 22.20 5 16 -4 47.10 20.30 5 16 -4 6.90 18.30 -5 -16 4 30.60 21.40 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33.30 0 -16 4 177.28 34.10 0 -16 4 196.58 25.00 0 -16 4 177.68 36.50 0 -16 4 185.28 33.70 0 -16 4 196.18 35.60 -1 16 -4 3.60 28.00 -1 16 -4 17.50 13.70 -1 16 -4 18.90 24.00 1 -16 4 50.59 24.70 1 -16 4 16.30 26.40 1 -16 4 35.80 15.90 1 -16 4 55.79 29.90 1 -16 4 24.10 22.90 -2 16 -4 -58.59 28.20 -2 16 -4 13.00 27.70 -2 16 -4 28.40 27.70 -2 16 -4 -4.60 12.70 -2 16 -4 -9.30 23.30 2 -16 4 26.30 27.60 2 -16 4 -1.40 23.50 2 -16 4 -17.20 26.50 2 -16 4 -3.00 15.20 -3 16 -4 -25.70 21.50 -3 16 -4 -9.50 13.70 -3 16 -4 39.30 26.30 -3 16 -4 22.80 30.40 3 -16 4 19.50 28.30 3 -16 4 24.80 27.00 3 -16 4 -35.70 27.00 3 -16 4 22.80 21.40 17 15 -4 64.99 11.90 17 15 -4 66.89 17.60 17 15 -4 27.60 14.80 17 15 -4 43.70 14.40 17 15 -4 44.40 9.80 17 15 -4 31.80 11.30 -17 -15 4 6.20 29.80 -17 -15 4 35.10 38.00 16 15 -4 -11.00 15.90 16 15 -4 -27.60 19.50 16 15 -4 26.00 14.80 16 15 -4 40.60 12.10 16 15 -4 11.40 15.10 16 15 -4 12.90 14.50 16 15 -4 18.70 10.20 16 15 -4 19.60 16.60 -16 -15 4 13.20 26.50 -16 -15 4 19.00 34.80 15 15 -4 -12.70 18.80 15 15 -4 17.50 14.90 15 15 -4 53.19 15.10 15 15 -4 6.40 14.60 15 15 -4 7.00 19.50 15 15 -4 59.79 13.70 -15 -15 4 21.90 28.30 -15 -15 4 47.90 10.40 -15 -15 4 94.09 42.70 -15 -15 4 28.70 8.60 14 15 -4 -16.60 10.60 14 15 -4 6.20 13.20 14 15 -4 17.60 14.00 14 15 -4 29.00 27.40 -14 -15 4 0.50 31.30 -14 -15 4 3.70 12.90 -14 -15 4 0.50 27.30 -14 -15 4 -6.50 11.50 -14 -15 4 -4.60 12.10 13 15 -4 133.09 22.70 13 15 -4 128.09 31.40 13 15 -4 112.09 24.90 13 15 -4 139.49 23.90 13 15 -4 146.49 25.10 13 15 -4 138.79 24.50 13 15 -4 145.09 43.20 -13 -15 4 157.18 44.50 -13 -15 4 205.28 43.10 -13 -15 4 124.89 24.40 -13 -15 4 148.39 21.70 12 15 -4 -46.50 16.30 12 15 -4 14.40 14.50 12 15 -4 0.00 11.60 12 15 -4 4.70 12.80 12 15 -4 27.50 18.00 12 15 -4 -30.00 15.10 12 15 -4 -16.50 13.60 -12 -15 4 -13.10 12.50 -12 -15 4 1.10 28.30 -12 -15 4 -16.40 24.30 -12 -15 4 -14.40 13.10 11 15 -4 50.09 16.10 11 15 -4 19.00 16.20 11 15 -4 45.50 19.80 11 15 -4 30.70 15.80 11 15 -4 29.30 17.10 -11 -15 4 8.30 12.80 -11 -15 4 57.59 33.70 -11 -15 4 18.60 16.60 -11 -15 4 42.50 28.10 -11 -15 4 32.40 18.30 10 15 -4 25.20 19.80 10 15 -4 38.00 18.80 10 15 -4 33.40 18.00 10 15 -4 48.40 17.10 10 15 -4 65.69 18.10 10 15 -4 34.40 19.80 -10 -15 4 57.49 18.50 -10 -15 4 42.50 18.30 -10 -15 4 65.89 33.70 -10 -15 4 69.59 19.30 -10 -15 4 66.29 30.30 9 15 -4 63.59 19.60 9 15 -4 12.60 18.30 9 15 -4 65.89 21.60 9 15 -4 5.80 14.70 9 15 -4 20.20 17.10 9 15 -4 29.10 16.70 9 15 -4 71.59 17.30 -9 -15 4 39.30 18.60 -9 -15 4 27.80 9.90 -9 -15 4 3.60 17.90 -9 -15 4 6.40 22.90 -9 -15 4 76.79 33.80 8 15 -4 19.50 16.90 8 15 -4 53.29 17.60 8 15 -4 45.40 19.70 8 15 -4 41.20 19.20 8 15 -4 62.19 17.60 8 15 -4 45.10 19.40 8 15 -4 33.80 18.50 -8 -15 4 28.80 24.70 -8 -15 4 43.60 18.30 -8 -15 4 48.60 32.30 -8 -15 4 37.90 32.10 -8 -15 4 44.50 19.90 7 15 -4 -1.00 18.10 7 15 -4 -5.30 15.40 7 15 -4 -16.40 16.10 7 15 -4 5.40 18.20 7 15 -4 29.30 16.80 7 15 -4 -28.50 12.20 7 15 -4 -0.90 15.50 -7 -15 4 -25.70 12.40 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35.90 -2 15 -4 3.70 22.40 -2 15 -4 -9.90 17.00 -2 15 -4 -19.90 21.00 -2 15 -4 24.80 14.90 2 -15 4 49.00 28.80 2 -15 4 20.50 16.30 2 -15 4 13.40 22.60 2 -15 4 54.39 24.40 2 -15 4 -2.40 17.70 -3 15 -4 63.09 28.70 -3 15 -4 28.30 28.90 -3 15 -4 66.79 17.80 -3 15 -4 57.09 27.80 -3 15 -4 93.99 31.00 3 -15 4 53.99 28.40 3 -15 4 85.39 27.50 3 -15 4 39.20 18.80 3 -15 4 62.99 23.70 3 -15 4 53.29 28.10 -4 15 -4 -49.70 20.60 -4 15 -4 -9.50 14.60 -4 15 -4 -14.10 20.50 4 -15 4 -17.40 16.00 4 -15 4 -4.90 29.00 4 -15 4 -24.90 21.00 4 -15 4 13.20 24.80 4 -15 4 -1.20 18.60 -5 15 -4 117.59 23.40 -5 15 -4 58.79 30.30 -5 15 -4 133.39 37.70 -5 15 -4 110.39 32.60 5 -15 4 121.99 32.70 5 -15 4 146.69 34.50 5 -15 4 116.99 33.00 5 -15 4 125.79 23.60 5 -15 4 130.99 28.10 17 14 -4 13.20 19.90 17 14 -4 40.20 10.70 17 14 -4 27.00 12.70 17 14 -4 32.30 14.50 17 14 -4 39.80 8.00 17 14 -4 32.60 8.30 -17 -14 4 50.09 40.10 -17 -14 4 67.89 33.60 16 14 -4 -0.50 12.70 16 14 -4 21.50 8.70 16 14 -4 -18.40 16.90 16 14 -4 -24.40 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36.10 11.60 -1 -1 10 30.70 11.70 -1 -1 10 35.20 9.00 -1 -1 10 32.80 11.20 -1 -1 10 34.60 6.40 -1 -1 10 27.30 11.60 -1 -1 10 26.80 11.90 0 1 -10 70.79 16.80 0 1 -10 64.69 13.20 0 1 -10 69.19 13.90 0 1 -10 59.89 14.30 0 1 -10 59.59 15.00 0 1 -10 67.69 13.40 0 1 -10 63.89 12.80 0 -1 10 43.40 12.00 0 -1 10 53.19 9.10 0 -1 10 52.19 11.20 0 -1 10 64.09 14.20 0 -1 10 59.99 13.30 0 -1 10 62.09 14.10 0 -1 10 65.39 14.60 0 -1 10 47.00 12.50 0 -1 10 71.39 14.30 -1 1 -10 2014.80 71.49 -1 1 -10 1916.01 68.79 -1 1 -10 2059.79 69.49 -1 1 -10 2104.39 74.39 -1 1 -10 1982.40 73.09 -1 1 -10 1967.90 68.49 -1 1 -10 2011.40 74.59 1 -1 10 1973.50 69.19 1 -1 10 2148.39 70.79 1 -1 10 1945.81 67.29 1 -1 10 1976.10 77.09 1 -1 10 2001.10 73.29 1 -1 10 2015.50 73.39 1 -1 10 2020.00 64.69 1 -1 10 2081.69 75.39 -2 1 -10 76.49 13.60 -2 1 -10 49.60 14.40 -2 1 -10 50.19 13.70 -2 1 -10 50.49 13.00 -2 1 -10 89.79 15.10 -2 1 -10 77.09 15.60 -2 1 -10 83.89 14.80 2 -1 10 51.99 14.10 2 -1 10 89.19 17.60 2 -1 10 100.59 14.30 2 -1 10 64.89 13.90 2 -1 10 55.69 12.80 2 -1 10 103.39 16.70 2 -1 10 58.79 12.80 2 -1 10 64.09 12.30 -3 1 -10 596.34 31.80 -3 1 -10 532.65 34.50 -3 1 -10 526.45 33.30 -3 1 -10 553.04 35.90 -3 1 -10 540.95 31.70 -3 1 -10 548.35 30.80 -3 1 -10 504.55 33.60 3 -1 10 572.64 33.30 3 -1 10 531.15 31.90 3 -1 10 560.64 35.90 3 -1 10 528.65 31.60 3 -1 10 564.34 31.60 3 -1 10 539.45 33.10 3 -1 10 595.04 35.80 -4 1 -10 108.39 19.00 -4 1 -10 100.09 16.20 -4 1 -10 88.99 17.10 -4 1 -10 84.39 16.30 -4 1 -10 112.79 17.60 -4 1 -10 120.19 22.10 -4 1 -10 90.39 17.60 -4 1 -10 99.69 18.00 4 -1 10 85.29 17.70 4 -1 10 116.39 17.00 4 -1 10 96.99 17.90 4 -1 10 110.29 19.30 4 -1 10 79.79 15.40 4 -1 10 102.49 17.30 4 -1 10 105.09 16.20 4 -1 10 109.79 18.20 -5 1 -10 388.56 29.10 -5 1 -10 318.47 28.20 -5 1 -10 274.37 26.60 -5 1 -10 343.97 32.10 -5 1 -10 415.86 32.30 -5 1 -10 332.47 27.00 -5 1 -10 346.17 27.50 -5 1 -10 349.96 42.50 5 -1 10 319.67 27.40 5 -1 10 357.76 29.50 5 -1 10 298.67 26.40 5 -1 10 290.17 25.60 5 -1 10 306.37 27.60 5 -1 10 329.97 29.70 5 -1 10 308.67 28.60 5 -1 10 327.47 26.60 -6 1 -10 460.05 32.10 -6 1 -10 479.15 33.40 -6 1 -10 464.45 33.00 -6 1 -10 444.66 34.30 -6 1 -10 394.76 30.40 -6 1 -10 393.46 30.60 -6 1 -10 401.46 35.90 -6 1 -10 338.97 26.80 6 -1 10 399.06 30.50 6 -1 10 383.16 30.90 6 -1 10 358.36 33.60 6 -1 10 367.06 29.00 6 -1 10 403.76 29.80 6 -1 10 397.46 30.00 6 -1 10 446.66 33.10 6 -1 10 404.86 30.50 -7 1 -10 48.90 15.30 -7 1 -10 37.50 15.10 -7 1 -10 4.40 12.00 -7 1 -10 10.70 16.10 -7 1 -10 20.40 14.30 -7 1 -10 38.40 14.70 -7 1 -10 17.60 12.40 -7 1 -10 29.50 17.40 7 -1 10 19.00 12.90 7 -1 10 32.90 13.10 7 -1 10 21.00 13.50 7 -1 10 10.70 11.40 7 -1 10 23.80 14.10 7 -1 10 19.90 14.30 7 -1 10 26.10 14.40 -8 1 -10 462.25 42.00 -8 1 -10 436.46 33.80 -8 1 -10 446.36 34.50 -8 1 -10 419.26 33.70 -8 1 -10 462.75 34.30 -8 1 -10 548.45 41.50 -8 1 -10 537.05 34.40 -8 1 -10 514.75 37.70 8 -1 10 439.76 33.60 8 -1 10 452.35 32.50 8 -1 10 424.76 35.80 8 -1 10 485.25 35.60 8 -1 10 452.55 33.50 8 -1 10 498.65 36.10 8 -1 10 515.85 34.70 -9 1 -10 105.69 26.40 -9 1 -10 77.69 18.10 -9 1 -10 88.39 24.50 -9 1 -10 137.69 22.50 -9 1 -10 77.29 19.70 -9 1 -10 128.59 23.10 -9 1 -10 78.99 22.80 -9 1 -10 89.09 17.20 -9 1 -10 67.69 21.90 9 -1 10 75.39 20.00 9 -1 10 80.69 17.50 9 -1 10 62.39 17.50 9 -1 10 96.89 19.20 9 -1 10 103.79 19.20 9 -1 10 137.59 23.40 9 -1 10 122.79 22.10 -10 1 -10 46.20 23.10 -10 1 -10 33.70 21.30 -10 1 -10 58.59 18.70 -10 1 -10 31.00 16.80 -10 1 -10 40.20 15.30 -10 1 -10 50.39 17.10 -10 1 -10 39.90 16.70 -10 1 -10 35.00 15.00 -10 1 -10 20.70 19.00 10 -1 10 28.10 15.50 10 -1 10 48.90 17.40 10 -1 10 31.20 15.50 10 -1 10 51.49 18.70 10 -1 10 14.00 17.40 10 -1 10 67.69 17.00 10 -1 10 45.30 16.30 -11 1 -10 48.40 25.30 -11 1 -10 21.90 14.70 -11 1 -10 64.49 25.00 -11 1 -10 45.70 16.50 -11 1 -10 61.89 22.10 -11 1 -10 42.30 18.80 -11 1 -10 77.09 21.20 -11 1 -10 24.50 17.90 -11 1 -10 68.39 28.50 11 -1 10 44.20 22.10 11 -1 10 73.69 17.90 11 -1 10 67.69 18.20 11 -1 10 36.80 20.30 11 -1 10 52.49 19.60 11 -1 10 37.20 19.20 11 -1 10 63.49 19.80 -12 1 -10 161.78 26.60 -12 1 -10 217.68 33.60 -12 1 -10 232.78 38.00 -12 1 -10 143.99 20.70 -12 1 -10 126.19 27.10 -12 1 -10 142.99 24.50 -12 1 -10 154.18 21.40 -12 1 -10 183.28 34.50 -12 1 -10 169.38 37.70 12 -1 10 179.68 27.80 12 -1 10 157.78 25.00 12 -1 10 180.28 28.00 12 -1 10 182.48 28.20 12 -1 10 179.98 30.10 12 -1 10 188.78 27.10 12 -1 10 183.48 27.10 -13 1 -10 -15.40 24.90 -13 1 -10 -7.60 10.70 -13 1 -10 -18.40 14.00 -13 1 -10 5.30 12.20 -13 1 -10 -19.00 15.10 -13 1 -10 16.10 21.00 -13 1 -10 12.10 23.80 13 -1 10 -9.00 18.60 13 -1 10 -7.30 18.50 13 -1 10 -12.20 13.70 13 -1 10 -6.80 15.90 13 -1 10 -19.50 13.10 13 -1 10 -9.60 15.00 13 -1 10 16.20 16.60 13 -1 10 -4.10 15.50 -14 1 -10 34.40 19.60 -14 1 -10 19.00 10.30 -14 1 -10 47.10 32.00 -14 1 -10 29.60 24.60 -14 1 -10 59.19 20.60 -14 1 -10 9.50 10.70 14 -1 10 68.19 21.00 14 -1 10 31.40 20.70 14 -1 10 17.00 17.80 14 -1 10 1.60 15.10 14 -1 10 38.10 21.80 14 -1 10 41.20 24.10 14 -1 10 28.00 23.30 14 -1 10 38.20 19.80 -15 1 -10 7.20 21.60 -15 1 -10 9.50 29.10 -15 1 -10 18.20 28.60 15 -1 10 -22.40 15.90 15 -1 10 3.10 18.30 15 -1 10 -28.80 14.80 15 -1 10 -3.50 17.30 15 -1 10 27.80 22.30 15 -1 10 -4.90 19.20 15 -1 10 1.30 23.60 -16 1 -10 34.90 32.10 -16 1 -10 22.70 26.50 -16 1 -10 55.49 33.80 -16 1 -10 -10.10 21.70 16 -1 10 -0.90 21.20 16 -1 10 -5.50 20.10 16 -1 10 -7.50 17.00 16 -1 10 20.50 34.60 16 -1 10 -51.79 22.40 16 -1 10 -2.10 16.80 -17 1 -10 11.20 23.90 -17 1 -10 27.00 27.70 -17 1 -10 112.59 41.30 17 -1 10 12.00 25.20 17 -1 10 10.40 23.20 17 -1 10 11.60 22.60 17 -1 10 0.20 21.40 17 -1 10 18.40 27.00 17 -1 10 42.40 22.70 17 0 -10 21.10 16.60 17 0 -10 19.10 17.60 17 0 -10 36.60 15.80 17 0 -10 4.90 18.60 17 0 -10 33.20 19.30 -17 0 10 -5.30 17.90 16 0 -10 1.40 12.40 16 0 -10 -0.30 15.60 16 0 -10 -8.00 14.20 16 0 -10 22.60 15.80 16 0 -10 10.50 17.90 16 0 -10 -41.90 18.90 16 0 -10 24.70 16.40 -16 0 10 28.90 19.90 -16 0 10 19.70 15.00 -16 0 10 6.20 12.70 15 0 -10 108.39 25.10 15 0 -10 77.19 19.80 15 0 -10 76.49 18.60 15 0 -10 110.09 22.60 15 0 -10 49.00 22.00 15 0 -10 70.09 20.70 -15 0 10 70.59 15.80 -15 0 10 63.39 23.00 -15 0 10 92.69 18.90 -15 0 10 53.19 18.90 14 0 -10 37.80 17.10 14 0 -10 45.60 18.80 14 0 -10 65.99 18.60 14 0 -10 45.50 16.10 14 0 -10 60.29 17.70 14 0 -10 54.19 18.50 14 0 -10 26.60 15.80 -14 0 10 9.90 21.40 -14 0 10 42.30 14.10 -14 0 10 18.50 13.70 -14 0 10 23.70 18.00 13 0 -10 12.90 15.50 13 0 -10 -3.90 14.20 13 0 -10 -4.80 12.10 13 0 -10 8.50 15.40 13 0 -10 18.10 13.00 13 0 -10 18.50 15.90 13 0 -10 -2.10 9.70 -13 0 10 15.00 14.20 -13 0 10 -1.10 11.50 -13 0 10 -2.40 10.30 -13 0 10 -25.90 9.60 -13 0 10 -14.60 16.20 12 0 -10 416.36 32.70 12 0 -10 310.37 31.10 12 0 -10 298.97 23.20 12 0 -10 294.37 39.30 12 0 -10 340.97 30.60 12 0 -10 376.56 30.70 12 0 -10 335.77 32.50 12 0 -10 350.66 32.50 -12 0 10 323.77 30.20 -12 0 10 298.17 32.30 -12 0 10 308.37 36.60 -12 0 10 384.06 29.90 -12 0 10 397.16 41.90 -12 0 10 385.56 31.90 11 0 -10 139.99 21.80 11 0 -10 148.89 23.80 11 0 -10 146.89 23.10 11 0 -10 163.08 23.90 11 0 -10 138.19 21.40 11 0 -10 159.48 15.80 11 0 -10 238.08 25.70 -11 0 10 173.18 22.80 -11 0 10 157.58 21.90 -11 0 10 114.69 27.10 -11 0 10 217.58 34.10 -11 0 10 156.18 22.00 -11 0 10 161.58 15.70 -11 0 10 148.99 22.10 -11 0 10 179.08 16.70 10 0 -10 381.56 31.30 10 0 -10 370.66 30.60 10 0 -10 383.06 30.60 10 0 -10 335.07 19.50 10 0 -10 310.87 28.10 10 0 -10 408.16 31.80 10 0 -10 328.37 30.20 10 0 -10 350.26 30.40 -10 0 10 340.97 28.50 -10 0 10 323.47 37.40 -10 0 10 385.46 29.50 -10 0 10 301.87 36.30 -10 0 10 397.56 38.40 -10 0 10 394.76 28.90 -10 0 10 404.36 25.70 9 0 -10 233.48 25.50 9 0 -10 289.77 25.60 9 0 -10 213.68 16.90 9 0 -10 274.97 26.70 9 0 -10 244.58 25.50 9 0 -10 273.47 26.70 9 0 -10 259.47 25.40 9 0 -10 261.57 25.70 -9 0 10 257.47 22.20 -9 0 10 234.68 30.90 -9 0 10 244.58 26.10 -9 0 10 233.38 21.70 -9 0 10 197.98 23.70 -9 0 10 253.17 24.20 -9 0 10 275.87 25.00 8 0 -10 555.04 36.30 8 0 -10 572.44 35.90 8 0 -10 622.64 52.09 8 0 -10 664.93 36.80 8 0 -10 669.53 38.40 8 0 -10 570.34 35.90 8 0 -10 588.64 35.10 -8 0 10 568.74 33.90 -8 0 10 620.34 32.30 -8 0 10 630.94 42.10 -8 0 10 627.44 35.70 -8 0 10 579.04 35.00 -8 0 10 629.64 35.40 -8 0 10 560.44 32.20 7 0 -10 29.40 12.30 7 0 -10 40.10 14.00 7 0 -10 26.70 12.30 7 0 -10 18.70 12.50 7 0 -10 23.70 11.20 7 0 -10 45.20 12.90 7 0 -10 25.60 12.80 -7 0 10 37.40 12.40 -7 0 10 31.90 11.40 -7 0 10 27.70 11.20 -7 0 10 24.10 10.90 -7 0 10 25.10 12.80 -7 0 10 23.00 10.50 -7 0 10 31.40 11.70 6 0 -10 139.79 19.60 6 0 -10 136.99 19.30 6 0 -10 166.68 21.80 6 0 -10 168.58 20.20 6 0 -10 133.99 19.50 6 0 -10 162.88 21.60 -6 0 10 136.59 19.60 -6 0 10 151.58 19.70 -6 0 10 138.59 19.00 -6 0 10 120.99 18.30 -6 0 10 139.99 18.00 -6 0 10 171.18 23.10 -6 0 10 172.68 21.50 5 0 -10 378.46 27.90 5 0 -10 377.76 28.50 5 0 -10 367.86 26.50 5 0 -10 363.36 28.10 5 0 -10 378.86 27.00 5 0 -10 368.86 27.00 5 0 -10 325.57 25.60 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1447.96 55.39 -2 0 -10 1609.04 60.99 -2 0 -10 1553.74 60.29 -2 0 -10 1557.14 60.19 -2 0 -10 1480.95 55.19 2 0 10 1617.04 57.79 2 0 10 1466.85 58.49 2 0 10 1541.95 56.79 2 0 10 1557.34 57.09 2 0 10 1591.34 57.99 2 0 10 1510.75 60.19 2 0 10 1510.35 53.49 2 0 10 1577.94 61.79 -3 0 -10 1282.97 50.49 -3 0 -10 1216.58 49.20 -3 0 -10 1324.67 54.19 -3 0 -10 1312.87 50.39 -3 0 -10 1260.17 54.99 -3 0 -10 1241.68 54.09 -3 0 -10 1228.98 52.39 3 0 10 1212.58 50.09 3 0 10 1288.27 50.69 3 0 10 1302.57 55.09 3 0 10 1262.57 49.70 3 0 10 1234.48 53.19 3 0 10 1318.57 52.89 3 0 10 1202.48 49.40 3 0 10 1240.48 51.09 -4 0 -10 323.67 26.90 -4 0 -10 285.67 23.40 -4 0 -10 295.47 27.30 -4 0 -10 330.87 27.30 -4 0 -10 285.17 24.20 -4 0 -10 345.77 28.30 -4 0 -10 301.87 24.50 4 0 10 332.27 25.50 4 0 10 350.06 27.60 4 0 10 326.27 24.90 4 0 10 302.37 25.60 4 0 10 367.56 29.20 4 0 10 319.87 25.60 4 0 10 316.97 24.60 -5 0 -10 113.69 21.60 -5 0 -10 124.49 19.90 -5 0 -10 151.88 20.10 -5 0 -10 92.09 18.30 -5 0 -10 135.39 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9 9 1.6948 -0.0864 20 9 10 1.0499 -0.0187 20 9 11 -0.8094 0.1447 20 9 12 -1.0447 0.2504 20 10 0 1.1243 -0.1879 20 10 1 -0.3978 -0.2962 20 10 2 0.7564 -0.1390 20 10 3 1.2943 0.1567 20 10 4 2.2284 0.3227 20 10 5 -0.3970 0.0235 20 10 6 0.5094 -0.1248 20 10 7 0.2292 -0.2979 20 10 8 1.5665 -0.1379 20 10 9 1.8008 0.0780 20 10 10 -0.3223 0.1371 20 10 11 -2.5215 -0.0621 20 10 12 -0.2137 -0.0266 20 11 0 0.9369 -0.5409 20 11 1 -0.1177 -0.3604 20 11 2 0.6928 -0.2196 20 11 3 0.9680 -0.2385 20 11 4 0.4154 -0.1681 20 11 5 -0.0294 0.1721 20 11 6 2.1683 0.4352 20 11 7 3.2196 0.2484 20 11 8 4.6000 -0.0326 20 11 9 3.4987 -0.1267 20 11 10 -0.2851 -0.0732 20 11 11 -1.1434 -0.0714 20 11 12 3.2164 -0.0826 20 12 0 -0.9547 0.9681 20 12 1 0.4210 0.5279 20 12 2 1.7349 0.0536 20 12 3 1.7371 0.1317 20 12 4 -0.3660 0.1043 20 12 5 -1.4850 -0.0349 20 12 6 -1.2723 -0.5033 20 12 7 1.8582 -0.4577 20 12 8 2.7979 -0.1790 20 12 9 0.6203 0.0539 20 12 10 -0.3073 0.1109 20 12 11 1.5579 0.1862 20 12 12 4.2510 0.2178 20 13 0 -3.2948 -1.3334 20 13 1 -2.3951 -0.8594 20 13 2 -1.5244 -0.4068 20 13 3 1.6587 0.0679 20 13 4 3.6361 0.0653 20 13 5 3.4666 0.3431 20 13 6 0.5539 0.4076 20 13 7 0.5019 0.4671 20 13 8 -1.6929 0.1667 20 13 9 -1.0465 -0.0738 20 13 10 3.3434 -0.2264 20 13 11 5.5468 -0.2399 20 13 12 4.3610 -0.5693 20 14 1 -1.1162 0.2332 20 14 2 0.1000 0.0502 20 14 3 2.1999 0.0251 20 14 4 0.4471 -0.0684 20 14 5 -2.6646 -0.2348 20 14 6 -4.3188 -0.3455 20 14 7 -1.9142 -0.1168 20 14 8 -1.6828 -0.0238 20 14 9 -0.0708 -0.0191 20 14 10 1.4174 -0.1411 20 14 11 1.7840 0.0220 20 15 4 -0.5886 0.4601 20 15 5 -2.9239 -0.0219 20 15 6 -2.8809 0.1051 20 15 7 -1.5143 0.1816 20 15 8 -1.8706 -0.0976 20 15 9 -1.1205 0.0832 21 5 0 -2.1241 1.5908 21 5 1 -1.3997 0.8169 21 5 2 0.4190 0.2645 21 5 3 2.0108 -0.0351 21 5 4 3.3461 -0.2925 21 5 5 2.4107 -0.0311 21 6 0 2.2564 -0.7674 21 6 1 2.5725 -0.5441 21 6 2 1.9155 -0.0118 21 6 3 -0.0225 0.3397 21 6 4 1.6554 0.2591 21 6 5 1.4686 0.2108 21 6 6 3.4024 0.2317 21 6 7 3.7711 0.4884 21 7 0 0.9954 -0.1836 21 7 1 2.3007 -0.0420 21 7 2 3.3429 -0.1696 21 7 3 1.0621 -0.1616 21 7 4 -1.3408 -0.0696 21 7 5 -5.5911 0.0037 21 7 6 -4.2981 0.3443 21 7 7 -1.1335 0.5838 21 7 8 2.0044 0.8534 21 8 0 0.2550 0.3472 21 8 1 -1.6164 0.1728 21 8 2 -2.3622 0.2034 21 8 3 -3.1839 0.2332 21 8 4 -3.3827 0.0769 21 8 5 -3.3200 -0.2199 21 8 6 -3.1606 -0.2922 21 8 7 -3.3558 -0.6776 21 8 8 -3.8918 -0.9088 21 9 0 0.5529 -1.1571 21 9 1 1.4670 -0.7256 21 9 2 -0.0996 -0.2252 21 9 3 -2.6338 -0.0291 21 9 4 -4.4550 0.0608 21 9 5 -1.3578 0.2227 21 9 6 1.6837 0.4449 21 9 7 4.5024 0.4390 21 9 8 1.3468 -0.0301 21 9 9 -0.9938 -0.4161 21 10 0 0.1497 1.3164 21 10 1 0.8042 0.8457 21 10 2 -0.7194 0.2213 21 10 3 -1.1135 0.0318 21 10 4 -1.5726 -0.0604 21 10 5 2.4782 -0.1964 21 10 6 4.7820 -0.4957 21 10 7 6.0679 -0.4330 21 10 8 2.0256 -0.2089 21 10 9 1.4390 0.3915 21 11 1 -3.5308 -0.5347 21 11 2 -4.4278 0.1366 21 11 3 -2.5548 0.3816 21 11 4 0.2158 0.2347 21 11 5 5.0163 0.2861 21 11 6 4.6634 0.2338 21 11 7 2.5943 0.0908 21 11 8 0.5359 -0.0989 21 11 9 1.1552 -0.2271 21 12 2 -0.6924 0.4518 21 12 3 -2.0812 -0.0859 21 12 4 -1.6691 -0.1765 21 12 5 -0.5036 -0.2437 21 12 6 -1.3639 -0.1609 21 12 7 -0.5526 0.1212 21 12 8 1.8908 0.6052 21 13 5 2.1656 -0.1837 21 13 6 0.9377 0.1639 21 13 7 -0.2381 0.3036 0 0 0 0.0 0.0 ; _shelx_fab_checksum 7530 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Au1 Au 0.27766(2) 0.58070(2) 0.32981(2) 0.03651(7) Uani 1 1 d . . . . . P1 P 0.33676(8) 0.44319(9) 0.29791(8) 0.0270(2) Uani 1 1 d . . . . . O1 O 0.2278(3) 0.7094(3) 0.3609(2) 0.0390(8) Uani 1 1 d . . . . . N1 N 0.1752(5) 0.8766(4) 0.3287(5) 0.0630(16) Uani 1 1 d . . . . . H1 H 0.186661 0.876481 0.376523 0.076 Uiso 1 1 calc R U . . . N2 N 0.1811(5) 0.8207(4) 0.2307(4) 0.0594(15) Uani 1 1 d . . . . . H2 H 0.184576 0.779062 0.206393 0.071 Uiso 1 1 calc R U . . . C1 C 0.2696(4) 0.3627(4) 0.3363(3) 0.0319(10) Uani 1 1 d . . . . . C2 C 0.3195(4) 0.2606(4) 0.3518(4) 0.0379(11) Uani 1 1 d . . . . . H2A H 0.385179 0.237331 0.338874 0.046 Uiso 1 1 calc R U . . . C3 C 0.2763(4) 0.1922(4) 0.3854(4) 0.0444(13) Uani 1 1 d . . . . . C4 C 0.1812(5) 0.2291(5) 0.4041(5) 0.0576(19) Uani 1 1 d . . . . . H4 H 0.149394 0.184458 0.427790 0.069 Uiso 1 1 calc R U . . . C5 C 0.1316(4) 0.3291(5) 0.3892(5) 0.0541(17) Uani 1 1 d . . . . . H5 H 0.066211 0.351486 0.403180 0.065 Uiso 1 1 calc R U . . . C6 C 0.1730(4) 0.3990(4) 0.3547(4) 0.0386(11) Uani 1 1 d . . . . . C7 C 0.1113(4) 0.5058(4) 0.3393(4) 0.0404(12) Uani 1 1 d . . . . . C8 C 0.0686(4) 0.5378(4) 0.4047(4) 0.0453(13) Uani 1 1 d . . . . . H8 H 0.084178 0.492888 0.459237 0.054 Uiso 1 1 calc R U . . . C9 C 0.0034(5) 0.6339(5) 0.3930(5) 0.0527(16) Uani 1 1 d . . . . . H9 H -0.025272 0.653417 0.439437 0.063 Uiso 1 1 calc R U . . . C10 C -0.0204(4) 0.7014(4) 0.3147(5) 0.0491(15) Uani 1 1 d . . . . . C11 C 0.0246(6) 0.6694(5) 0.2487(5) 0.070(2) Uani 1 1 d . . . . . H11 H 0.010021 0.714057 0.193948 0.084 Uiso 1 1 calc R U . . . C12 C 0.0903(5) 0.5734(5) 0.2618(5) 0.0611(19) Uani 1 1 d . . . . . H12 H 0.121592 0.554183 0.215780 0.073 Uiso 1 1 calc R U . . . C13 C 0.3305(5) 0.0809(5) 0.4025(6) 0.063(2) Uani 1 1 d . . . . . C14 C 0.4327(6) 0.0569(6) 0.3701(8) 0.082(3) Uani 1 1 d . . . . . H14A H 0.433009 0.092510 0.310698 0.124 Uiso 1 1 calc R U . . . H14B H 0.464229 -0.014867 0.380551 0.124 Uiso 1 1 calc R U . . . H14C H 0.466321 0.077605 0.398325 0.124 Uiso 1 1 calc R U . . . C15 C 0.2797(7) 0.0448(7) 0.3580(9) 0.103(4) Uani 1 1 d . . . . . H15A H 0.313512 -0.026717 0.368303 0.155 Uiso 1 1 calc R U . . . H15B H 0.214721 0.057599 0.379204 0.155 Uiso 1 1 calc R U . . . H15C H 0.278931 0.080717 0.298630 0.155 Uiso 1 1 calc R U . . . C16 C 0.3290(9) 0.0282(6) 0.4969(8) 0.108(4) Uani 1 1 d . . . . . H16A H 0.350080 0.060482 0.524596 0.161 Uiso 1 1 calc R U . . . H16B H 0.371411 -0.041853 0.510515 0.161 Uiso 1 1 calc R U . . . H16C H 0.264641 0.032799 0.515451 0.161 Uiso 1 1 calc R U . . . C17 C -0.0960(6) 0.8079(5) 0.3000(6) 0.069(2) Uani 1 1 d . . . . . C21 C 0.4533(3) 0.3600(4) 0.3408(3) 0.0300(9) Uani 1 1 d . . . . . C22 C 0.5236(4) 0.3138(4) 0.2920(3) 0.0326(10) Uani 1 1 d . . . . . H22 H 0.508440 0.323246 0.238212 0.039 Uiso 1 1 calc R U . . . C23 C 0.6162(4) 0.2537(4) 0.3198(4) 0.0360(11) Uani 1 1 d . . . . . C24 C 0.6362(4) 0.2413(4) 0.3988(4) 0.0391(12) Uani 1 1 d . . . . . H24 H 0.698458 0.202265 0.419094 0.047 Uiso 1 1 calc R U . . . C25 C 0.5659(4) 0.2856(4) 0.4484(4) 0.0379(11) Uani 1 1 d . . . . . H25 H 0.580943 0.274402 0.502762 0.045 Uiso 1 1 calc R U . . . C26 C 0.4733(3) 0.3465(4) 0.4208(3) 0.0314(10) Uani 1 1 d . . . . . C27 C 0.4028(4) 0.3949(4) 0.4756(3) 0.0318(10) Uani 1 1 d . . . . . C28 C 0.4037(4) 0.4780(4) 0.4854(3) 0.0361(11) Uani 1 1 d . . . . . H28 H 0.449581 0.504247 0.455974 0.043 Uiso 1 1 calc R U . . . C29 C 0.3396(4) 0.5247(4) 0.5370(4) 0.0405(12) Uani 1 1 d . . . . . H29 H 0.343901 0.580473 0.543658 0.049 Uiso 1 1 calc R U . . . C30 C 0.2704(4) 0.4913(4) 0.5785(3) 0.0356(11) Uani 1 1 d . . . . . C31 C 0.2678(4) 0.4076(4) 0.5695(4) 0.0393(12) Uani 1 1 d . . . . . H31 H 0.221185 0.382444 0.598738 0.047 Uiso 1 1 calc R U . . . C32 C 0.3331(4) 0.3596(4) 0.5179(3) 0.0382(11) Uani 1 1 d . . . . . H32 H 0.329653 0.303195 0.511768 0.046 Uiso 1 1 calc R U . . . C33 C 0.6893(4) 0.2077(5) 0.2621(4) 0.0476(14) Uani 1 1 d . . . . . C34 C 0.6634(6) 0.1338(7) 0.2455(6) 0.074(2) Uani 1 1 d . . . . . H34A H 0.599575 0.166448 0.223194 0.111 Uiso 1 1 calc R U . . . H34B H 0.665379 0.079120 0.296928 0.111 Uiso 1 1 calc R U . . . H34C H 0.708360 0.107526 0.205467 0.111 Uiso 1 1 calc R U . . . C35 C 0.6938(6) 0.2903(6) 0.1820(5) 0.072(2) Uani 1 1 d . . . . . H35A H 0.732729 0.260742 0.141145 0.108 Uiso 1 1 calc R U . . . H35B H 0.721735 0.330747 0.192701 0.108 Uiso 1 1 calc R U . . . H35C H 0.629909 0.332337 0.160893 0.108 Uiso 1 1 calc R U . . . C36 C 0.7889(5) 0.1525(6) 0.3001(5) 0.064(2) Uani 1 1 d . . . . . H36A H 0.786836 0.102072 0.353472 0.096 Uiso 1 1 calc R U . . . H36B H 0.809335 0.200312 0.307923 0.096 Uiso 1 1 calc R U . . . H36C H 0.833551 0.120344 0.263024 0.096 Uiso 1 1 calc R U . . . C37 C 0.1960(4) 0.5485(5) 0.6310(4) 0.0439(13) Uani 1 1 d . . . . . C38 C 0.1293(5) 0.4962(6) 0.6773(6) 0.064(2) Uani 1 1 d . . . . . H38A H 0.093160 0.493673 0.637661 0.096 Uiso 1 1 calc R U . . . H38B H 0.085769 0.532998 0.712064 0.096 Uiso 1 1 calc R U . . . H38C H 0.165995 0.428455 0.711860 0.096 Uiso 1 1 calc R U . . . C39 C 0.1395(5) 0.6518(6) 0.5750(5) 0.066(2) Uani 1 1 d . . . . . H39A H 0.182633 0.683053 0.541294 0.099 Uiso 1 1 calc R U . . . H39B H 0.098741 0.691969 0.608510 0.099 Uiso 1 1 calc R U . . . H39C H 0.100408 0.647219 0.539061 0.099 Uiso 1 1 calc R U . . . C40 C 0.2461(5) 0.5566(6) 0.6952(5) 0.0594(18) Uani 1 1 d . . . . . H40A H 0.278364 0.490125 0.734314 0.089 Uiso 1 1 calc R U . . . H40B H 0.199537 0.598506 0.724877 0.089 Uiso 1 1 calc R U . . . H40C H 0.292497 0.586253 0.667510 0.089 Uiso 1 1 calc R U . . . C41 C 0.3538(4) 0.4668(4) 0.1861(3) 0.0338(10) Uani 1 1 d . . . . . C42 C 0.3315(4) 0.4088(5) 0.1543(4) 0.0416(12) Uani 1 1 d . . . . . H42 H 0.309755 0.359203 0.191015 0.050 Uiso 1 1 calc R U . . . C43 C 0.3401(5) 0.4208(6) 0.0709(4) 0.0511(15) Uani 1 1 d . . . . . C44 C 0.3689(6) 0.4950(6) 0.0202(4) 0.0602(18) Uani 1 1 d . . . . . H44 H 0.374357 0.506052 -0.037342 0.072 Uiso 1 1 calc R U . . . C45 C 0.3904(6) 0.5548(6) 0.0502(4) 0.0549(16) Uani 1 1 d . . . . . H45 H 0.409376 0.606097 0.012574 0.066 Uiso 1 1 calc R U . . . C46 C 0.3848(4) 0.5412(4) 0.1338(3) 0.0395(12) Uani 1 1 d . . . . . C47 C 0.4127(4) 0.6068(4) 0.1594(3) 0.0387(11) Uani 1 1 d . . . . . C48 C 0.3767(5) 0.7092(5) 0.1196(4) 0.0485(14) Uani 1 1 d . . . . . H48 H 0.332894 0.736529 0.076610 0.058 Uiso 1 1 calc R U . . . C49 C 0.4020(5) 0.7721(5) 0.1403(4) 0.0493(14) Uani 1 1 d . . . . . H49 H 0.376221 0.841410 0.110729 0.059 Uiso 1 1 calc R U . . . C50 C 0.4653(4) 0.7366(4) 0.2041(4) 0.0403(12) Uani 1 1 d . . . . . C51 C 0.5029(4) 0.6344(4) 0.2421(4) 0.0424(12) Uani 1 1 d . . . . . H51 H 0.547700 0.607265 0.284259 0.051 Uiso 1 1 calc R U . . . C52 C 0.4786(4) 0.5705(4) 0.2216(4) 0.0423(12) Uani 1 1 d . . . . . H52 H 0.506515 0.500939 0.249742 0.051 Uiso 1 1 calc R U . . . C53 C 0.3195(7) 0.3520(8) 0.0392(5) 0.080(2) Uani 1 1 d D . . . . Sb1 Sb 0.000000 1.000000 0.500000 0.05099(15) Uani 1 2 d S . P . . F1 F 0.0492(7) 1.0835(8) 0.5037(11) 0.230(7) Uani 1 1 d . . . . . F2 F 0.0036(7) 0.9434(8) 0.6103(5) 0.203(6) Uani 1 1 d . . . . . F3 F 0.1221(3) 0.9087(4) 0.4906(3) 0.0791(14) Uani 1 1 d . . . . . C57 C 0.4933(5) 0.8044(5) 0.2312(5) 0.0547(16) Uani 1 1 d . . . . . C58 C 0.4402(9) 0.9127(6) 0.1854(7) 0.089(3) Uani 1 1 d . . . . . H58A H 0.454169 0.926494 0.126249 0.134 Uiso 1 1 calc R U . . . H58B H 0.459497 0.953473 0.204854 0.134 Uiso 1 1 calc R U . . . H58C H 0.372214 0.928808 0.195264 0.134 Uiso 1 1 calc R U . . . C59 C 0.5990(6) 0.7773(7) 0.2182(7) 0.075(2) Uani 1 1 d . . . . . H59A H 0.632361 0.709868 0.255349 0.113 Uiso 1 1 calc R U . . . H59B H 0.616923 0.824402 0.230040 0.113 Uiso 1 1 calc R U . . . H59C H 0.615928 0.780176 0.161000 0.113 Uiso 1 1 calc R U . . . C60 C 0.4701(7) 0.7839(7) 0.3242(5) 0.074(2) Uani 1 1 d . . . . . H60A H 0.401537 0.804964 0.333009 0.111 Uiso 1 1 calc R U . . . H60B H 0.493419 0.821082 0.344427 0.111 Uiso 1 1 calc R U . . . H60C H 0.500506 0.712583 0.354143 0.111 Uiso 1 1 calc R U . . . C61 C 0.1978(4) 0.7940(4) 0.3102(4) 0.0409(12) Uani 1 1 d . . . . . C62 C 0.1305(6) 0.9651(5) 0.2620(6) 0.071(2) Uani 1 1 d . . . . . H62A H 0.155899 1.016478 0.254181 0.085 Uiso 1 1 calc R U . . . H62B H 0.061229 0.992740 0.270694 0.085 Uiso 1 1 calc R U . . . C63 C 0.1567(7) 0.9264(6) 0.1888(5) 0.071(2) Uani 1 1 d . . . . . H63A H 0.102516 0.955303 0.151840 0.086 Uiso 1 1 calc R U . . . H63B H 0.210949 0.940683 0.156689 0.086 Uiso 1 1 calc R U . . . C18A C -0.1848(11) 0.8048(12) 0.3203(19) 0.126(10) Uani 0.66(2) 1 d . . P A 1 H18A H -0.213431 0.811242 0.271452 0.188 Uiso 0.66(2) 1 calc R U P A 1 H18B H -0.224456 0.859611 0.340652 0.188 Uiso 0.66(2) 1 calc R U P A 1 H18C H -0.179551 0.741311 0.363362 0.188 Uiso 0.66(2) 1 calc R U P A 1 C19A C -0.0833(13) 0.8818(12) 0.2097(13) 0.092(5) Uani 0.66(2) 1 d . . P A 1 H19A H -0.021602 0.886610 0.205429 0.137 Uiso 0.66(2) 1 calc R U P A 1 H19B H -0.133331 0.947847 0.201107 0.137 Uiso 0.66(2) 1 calc R U P A 1 H19C H -0.087326 0.855805 0.167761 0.137 Uiso 0.66(2) 1 calc R U P A 1 C20A C -0.0657(14) 0.8501(11) 0.3579(13) 0.103(6) Uani 0.66(2) 1 d . . P A 1 H20A H -0.061962 0.805352 0.415047 0.155 Uiso 0.66(2) 1 calc R U P A 1 H20B H -0.112689 0.916422 0.354237 0.155 Uiso 0.66(2) 1 calc R U P A 1 H20C H -0.003878 0.854192 0.339618 0.155 Uiso 0.66(2) 1 calc R U P A 1 C18B C -0.1847(19) 0.8093(19) 0.254(2) 0.071(6) Uani 0.34(2) 1 d . . P A 2 H18D H -0.205125 0.755399 0.289064 0.106 Uiso 0.34(2) 1 calc R U P A 2 H18E H -0.237919 0.873239 0.245383 0.106 Uiso 0.34(2) 1 calc R U P A 2 H18F H -0.162297 0.799963 0.200585 0.106 Uiso 0.34(2) 1 calc R U P A 2 C19B C -0.061(3) 0.878(3) 0.259(4) 0.114(14) Uani 0.34(2) 1 d . . P A 2 H19D H -0.111289 0.943475 0.250770 0.171 Uiso 0.34(2) 1 calc R U P A 2 H19E H -0.010001 0.869690 0.290078 0.171 Uiso 0.34(2) 1 calc R U P A 2 H19F H -0.036742 0.870826 0.204913 0.171 Uiso 0.34(2) 1 calc R U P A 2 C20B C -0.1461(18) 0.8230(19) 0.3826(19) 0.074(7) Uani 0.34(2) 1 d . . P A 2 H20D H -0.171001 0.770823 0.411635 0.111 Uiso 0.34(2) 1 calc R U P A 2 H20E H -0.100388 0.819352 0.417474 0.111 Uiso 0.34(2) 1 calc R U P A 2 H20F H -0.198101 0.888244 0.370224 0.111 Uiso 0.34(2) 1 calc R U P A 2 C54A C 0.283(2) 0.2788(18) 0.1054(13) 0.093(6) Uani 0.392(15) 1 d D . P B 1 H54A H 0.271491 0.237248 0.081041 0.139 Uiso 0.392(15) 1 calc R U P B 1 H54B H 0.330243 0.236462 0.148691 0.139 Uiso 0.392(15) 1 calc R U P B 1 H54C H 0.224140 0.315282 0.129326 0.139 Uiso 0.392(15) 1 calc R U P B 1 C55A C 0.4119(16) 0.295(2) 0.0009(19) 0.111(8) Uani 0.392(15) 1 d D . P B 1 H55A H 0.434965 0.343094 -0.041709 0.166 Uiso 0.392(15) 1 calc R U P B 1 H55B H 0.459381 0.252880 0.043860 0.166 Uiso 0.392(15) 1 calc R U P B 1 H55C H 0.400134 0.254172 -0.023696 0.166 Uiso 0.392(15) 1 calc R U P B 1 C56A C 0.247(2) 0.413(3) -0.0311(16) 0.151(14) Uani 0.392(15) 1 d D . P B 1 H56A H 0.269130 0.460514 -0.074502 0.226 Uiso 0.392(15) 1 calc R U P B 1 H56B H 0.239545 0.367538 -0.054002 0.226 Uiso 0.392(15) 1 calc R U P B 1 H56C H 0.185798 0.448531 -0.009263 0.226 Uiso 0.392(15) 1 calc R U P B 1 C55B C 0.3923(15) 0.2498(13) 0.0754(13) 0.129(6) Uani 0.608(15) 1 d D . P B 2 H55D H 0.388035 0.229426 0.135681 0.193 Uiso 0.608(15) 1 calc R U P B 2 H55E H 0.381087 0.202924 0.057269 0.193 Uiso 0.608(15) 1 calc R U P B 2 H55F H 0.455341 0.250070 0.056946 0.193 Uiso 0.608(15) 1 calc R U P B 2 C54B C 0.2205(11) 0.3542(17) 0.0689(11) 0.106(5) Uani 0.608(15) 1 d D . P B 2 H54D H 0.173859 0.421527 0.044717 0.158 Uiso 0.608(15) 1 calc R U P B 2 H54E H 0.207612 0.307521 0.051935 0.158 Uiso 0.608(15) 1 calc R U P B 2 H54F H 0.216674 0.335028 0.129138 0.158 Uiso 0.608(15) 1 calc R U P B 2 C56B C 0.3239(13) 0.3864(15) -0.0548(8) 0.099(5) Uani 0.608(15) 1 d D . P B 2 H56D H 0.275740 0.453327 -0.076971 0.148 Uiso 0.608(15) 1 calc R U P B 2 H56E H 0.386542 0.387567 -0.074102 0.148 Uiso 0.608(15) 1 calc R U P B 2 H56F H 0.312288 0.340421 -0.073778 0.148 Uiso 0.608(15) 1 calc R U P B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Au1 0.03682(11) 0.02944(10) 0.04066(12) -0.01502(8) 0.00376(8) -0.00880(7) P1 0.0268(5) 0.0234(5) 0.0284(6) -0.0096(4) 0.0016(4) -0.0069(4) O1 0.057(2) 0.0240(17) 0.037(2) -0.0164(15) -0.0012(17) -0.0108(16) N1 0.071(4) 0.041(3) 0.079(4) -0.032(3) 0.001(3) -0.012(3) N2 0.078(4) 0.041(3) 0.053(3) -0.017(3) -0.003(3) -0.015(3) C1 0.031(2) 0.027(2) 0.037(3) -0.0125(19) 0.0032(19) -0.0089(18) C2 0.032(2) 0.033(3) 0.046(3) -0.016(2) 0.002(2) -0.008(2) C3 0.039(3) 0.029(3) 0.067(4) -0.019(3) 0.001(3) -0.012(2) C4 0.044(3) 0.035(3) 0.094(6) -0.020(3) 0.013(3) -0.021(3) C5 0.033(3) 0.034(3) 0.088(5) -0.018(3) 0.011(3) -0.013(2) C6 0.032(2) 0.031(3) 0.051(3) -0.014(2) 0.004(2) -0.012(2) C7 0.030(2) 0.032(3) 0.057(3) -0.013(2) 0.002(2) -0.012(2) C8 0.040(3) 0.036(3) 0.055(4) -0.020(3) -0.007(3) -0.003(2) C9 0.044(3) 0.043(3) 0.070(4) -0.031(3) -0.002(3) -0.005(3) C10 0.037(3) 0.032(3) 0.074(4) -0.020(3) -0.002(3) -0.005(2) C11 0.060(4) 0.040(4) 0.071(5) -0.006(3) 0.013(4) 0.002(3) C12 0.051(4) 0.041(3) 0.063(4) -0.013(3) 0.013(3) 0.001(3) C13 0.051(4) 0.025(3) 0.109(6) -0.025(3) 0.011(4) -0.014(3) C14 0.050(4) 0.037(4) 0.149(9) -0.039(5) 0.010(5) -0.003(3) C15 0.064(5) 0.065(5) 0.206(13) -0.082(7) 0.012(7) -0.022(4) C16 0.116(9) 0.034(4) 0.120(9) 0.001(5) 0.010(7) -0.005(5) C17 0.053(4) 0.033(3) 0.097(6) -0.020(3) 0.006(4) 0.003(3) C21 0.029(2) 0.026(2) 0.034(2) -0.0095(18) 0.0010(18) -0.0098(18) C22 0.033(2) 0.025(2) 0.035(3) -0.0109(19) 0.0031(19) -0.0076(19) C23 0.030(2) 0.026(2) 0.044(3) -0.012(2) 0.007(2) -0.0055(19) C24 0.031(2) 0.035(3) 0.041(3) -0.009(2) 0.001(2) -0.006(2) C25 0.031(2) 0.037(3) 0.039(3) -0.009(2) -0.003(2) -0.009(2) C26 0.029(2) 0.029(2) 0.033(2) -0.0107(19) 0.0015(18) -0.0081(18) C27 0.031(2) 0.037(3) 0.026(2) -0.0104(19) 0.0037(18) -0.014(2) C28 0.034(3) 0.041(3) 0.040(3) -0.019(2) 0.007(2) -0.018(2) C29 0.042(3) 0.042(3) 0.045(3) -0.020(2) 0.004(2) -0.020(2) C30 0.034(2) 0.036(3) 0.038(3) -0.016(2) 0.000(2) -0.012(2) C31 0.038(3) 0.042(3) 0.042(3) -0.019(2) 0.011(2) -0.019(2) C32 0.047(3) 0.034(3) 0.039(3) -0.016(2) 0.006(2) -0.019(2) C33 0.041(3) 0.038(3) 0.048(3) -0.016(3) 0.007(2) -0.001(2) C34 0.060(5) 0.074(5) 0.098(7) -0.057(5) 0.008(4) -0.012(4) C35 0.060(4) 0.067(5) 0.053(4) -0.015(4) 0.022(3) -0.002(4) C36 0.036(3) 0.066(5) 0.074(5) -0.030(4) 0.009(3) -0.001(3) C37 0.038(3) 0.049(3) 0.049(3) -0.028(3) 0.005(2) -0.013(2) C38 0.046(4) 0.074(5) 0.086(6) -0.051(4) 0.028(4) -0.025(3) C39 0.051(4) 0.054(4) 0.074(5) -0.028(4) 0.007(4) 0.002(3) C40 0.057(4) 0.081(5) 0.055(4) -0.044(4) 0.013(3) -0.026(4) C41 0.032(2) 0.034(2) 0.028(2) -0.011(2) -0.0005(19) -0.007(2) C42 0.041(3) 0.046(3) 0.043(3) -0.022(3) 0.007(2) -0.017(2) C43 0.047(3) 0.075(5) 0.043(3) -0.033(3) 0.008(3) -0.025(3) C44 0.075(5) 0.081(5) 0.034(3) -0.022(3) 0.004(3) -0.038(4) C45 0.075(5) 0.056(4) 0.032(3) -0.012(3) 0.007(3) -0.029(4) C46 0.040(3) 0.042(3) 0.034(3) -0.014(2) 0.000(2) -0.012(2) C47 0.041(3) 0.037(3) 0.034(3) -0.009(2) 0.004(2) -0.016(2) C48 0.059(4) 0.040(3) 0.039(3) -0.007(2) -0.010(3) -0.014(3) C49 0.058(4) 0.032(3) 0.049(3) -0.005(2) -0.005(3) -0.014(3) C50 0.040(3) 0.039(3) 0.041(3) -0.013(2) 0.002(2) -0.015(2) C51 0.039(3) 0.040(3) 0.044(3) -0.011(2) -0.002(2) -0.013(2) C52 0.038(3) 0.034(3) 0.045(3) -0.003(2) -0.003(2) -0.013(2) C53 0.101(6) 0.112(6) 0.071(4) -0.062(5) 0.018(4) -0.062(5) Sb1 0.0482(3) 0.0523(3) 0.0590(4) -0.0240(3) 0.0049(3) -0.0227(3) F1 0.117(7) 0.159(8) 0.51(2) -0.201(12) 0.014(10) -0.073(6) F2 0.148(7) 0.203(10) 0.076(5) -0.007(5) 0.015(5) 0.067(7) F3 0.062(3) 0.080(3) 0.080(3) -0.034(3) 0.003(2) -0.007(2) C57 0.061(4) 0.039(3) 0.057(4) -0.013(3) -0.006(3) -0.014(3) C58 0.126(9) 0.046(4) 0.096(7) -0.019(4) -0.035(6) -0.025(5) C59 0.075(5) 0.073(5) 0.103(7) -0.044(5) -0.002(5) -0.040(5) C60 0.091(6) 0.071(5) 0.065(5) -0.035(4) -0.006(4) -0.024(5) C61 0.042(3) 0.029(2) 0.047(3) -0.016(2) 0.004(2) -0.008(2) C62 0.072(5) 0.031(3) 0.101(7) -0.017(4) -0.006(5) -0.014(3) C63 0.080(6) 0.050(4) 0.066(5) -0.004(4) 0.001(4) -0.022(4) C18A 0.051(7) 0.049(8) 0.24(3) -0.026(13) 0.004(11) -0.006(6) C19A 0.069(9) 0.034(6) 0.127(10) 0.001(8) -0.015(9) 0.005(6) C20A 0.123(14) 0.049(7) 0.142(13) -0.055(9) 0.015(10) -0.022(8) C18B 0.060(12) 0.036(10) 0.078(15) -0.006(11) -0.012(11) 0.012(8) C19B 0.07(2) 0.045(12) 0.19(4) -0.03(2) 0.04(2) -0.010(13) C20B 0.052(13) 0.057(13) 0.112(13) -0.052(12) 0.002(10) 0.000(10) C54A 0.115(15) 0.115(13) 0.098(11) -0.067(7) 0.026(9) -0.073(11) C55A 0.126(11) 0.122(15) 0.124(19) -0.081(13) 0.048(11) -0.067(9) C56A 0.140(13) 0.22(3) 0.096(13) -0.045(14) -0.014(11) -0.075(15) C55B 0.142(10) 0.126(9) 0.127(12) -0.062(8) -0.003(10) -0.042(7) C54B 0.115(7) 0.174(16) 0.095(10) -0.091(10) 0.032(7) -0.091(8) C56B 0.112(12) 0.163(14) 0.072(5) -0.079(6) 0.018(5) -0.073(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Au1 P1 177.54(12) . . ? C1 P1 Au1 115.64(16) . . ? C1 P1 C41 106.9(2) . . ? C21 P1 Au1 113.14(17) . . ? C21 P1 C1 102.5(2) . . ? C21 P1 C41 104.5(2) . . ? C41 P1 Au1 113.09(18) . . ? C61 O1 Au1 123.6(4) . . ? C61 N1 H1 123.8 . . ? C61 N1 C62 112.3(7) . . ? C62 N1 H1 123.8 . . ? C61 N2 H2 124.0 . . ? C61 N2 C63 112.0(6) . . ? C63 N2 H2 124.0 . . ? C2 C1 P1 117.5(4) . . ? C6 C1 P1 122.2(4) . . ? C6 C1 C2 120.1(5) . . ? C1 C2 H2A 118.9 . . ? C3 C2 C1 122.2(5) . . ? C3 C2 H2A 118.9 . . ? C2 C3 C13 122.4(5) . . ? C4 C3 C2 117.0(5) . . ? C4 C3 C13 120.6(5) . . ? C3 C4 H4 119.4 . . ? C5 C4 C3 121.2(6) . . ? C5 C4 H4 119.4 . . ? C4 C5 H5 118.6 . . ? C4 C5 C6 122.8(6) . . ? C6 C5 H5 118.6 . . ? C1 C6 C7 125.5(5) . . ? C5 C6 C1 116.7(5) . . ? C5 C6 C7 117.9(5) . . ? C8 C7 C6 119.7(6) . . ? C12 C7 C6 122.5(6) . . ? C12 C7 C8 117.6(6) . . ? C7 C8 H8 119.2 . . ? C7 C8 C9 121.6(6) . . ? C9 C8 H8 119.2 . . ? C8 C9 H9 119.6 . . ? C10 C9 C8 120.8(6) . . ? C10 C9 H9 119.6 . . ? C9 C10 C11 117.3(6) . . ? C9 C10 C17 121.8(7) . . ? C11 C10 C17 120.8(7) . . ? C10 C11 H11 119.6 . . ? C12 C11 C10 120.9(7) . . ? C12 C11 H11 119.6 . . ? C7 C12 C11 121.6(7) . . ? C7 C12 H12 119.2 . . ? C11 C12 H12 119.2 . . ? C3 C13 C14 112.1(6) . . ? C3 C13 C15 108.3(7) . . ? C3 C13 C16 107.7(7) . . ? C14 C13 C15 108.3(8) . . ? C14 C13 C16 110.1(8) . . ? C16 C13 C15 110.5(8) . . ? C13 C14 H14A 109.5 . . ? C13 C14 H14B 109.5 . . ? C13 C14 H14C 109.5 . . ? H14A C14 H14B 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C13 C15 H15A 109.5 . . ? C13 C15 H15B 109.5 . . ? C13 C15 H15C 109.5 . . ? H15A C15 H15B 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C13 C16 H16A 109.5 . . ? C13 C16 H16B 109.5 . . ? C13 C16 H16C 109.5 . . ? H16A C16 H16B 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C10 C17 C19A 111.1(9) . . ? C10 C17 C20A 104.7(8) . . ? C10 C17 C18B 103.9(10) . . ? C10 C17 C20B 111.9(11) . . ? C18A C17 C10 110.3(9) . . ? C18A C17 C19A 116.5(14) . . ? C18A C17 C20A 112.1(16) . . ? C20A C17 C19A 101.2(12) . . ? C19B C17 C10 112.2(17) . . ? C19B C17 C18B 116(3) . . ? C19B C17 C20B 111(3) . . ? C20B C17 C18B 101.0(16) . . ? C22 C21 P1 119.5(4) . . ? C22 C21 C26 120.2(5) . . ? C26 C21 P1 120.2(4) . . ? C21 C22 H22 118.9 . . ? C21 C22 C23 122.2(5) . . ? C23 C22 H22 118.9 . . ? C22 C23 C33 118.9(5) . . ? C24 C23 C22 117.6(5) . . ? C24 C23 C33 123.6(5) . . ? C23 C24 H24 119.7 . . ? C23 C24 C25 120.6(5) . . ? C25 C24 H24 119.7 . . ? C24 C25 H25 118.9 . . ? C24 C25 C26 122.2(5) . . ? C26 C25 H25 118.9 . . ? C21 C26 C25 117.3(5) . . ? C21 C26 C27 123.3(4) . . ? C25 C26 C27 119.3(5) . . ? C28 C27 C26 120.4(5) . . ? C28 C27 C32 117.7(5) . . ? C32 C27 C26 121.9(5) . . ? C27 C28 H28 118.9 . . ? C27 C28 C29 122.1(5) . . ? C29 C28 H28 118.9 . . ? C28 C29 H29 119.6 . . ? C30 C29 C28 120.8(5) . . ? C30 C29 H29 119.6 . . ? C29 C30 C31 118.2(5) . . ? C29 C30 C37 119.9(5) . . ? C31 C30 C37 121.9(5) . . ? C30 C31 H31 119.4 . . ? C30 C31 C32 121.1(5) . . ? C32 C31 H31 119.4 . . ? C27 C32 C31 120.0(5) . . ? C27 C32 H32 120.0 . . ? C31 C32 H32 120.0 . . ? C23 C33 C35 109.0(5) . . ? C23 C33 C36 111.4(6) . . ? C34 C33 C23 109.7(6) . . ? C34 C33 C35 110.8(7) . . ? C34 C33 C36 107.9(6) . . ? C35 C33 C36 107.9(6) . . ? C33 C34 H34A 109.5 . . ? C33 C34 H34B 109.5 . . ? C33 C34 H34C 109.5 . . ? H34A C34 H34B 109.5 . . ? H34A C34 H34C 109.5 . . ? H34B C34 H34C 109.5 . . ? C33 C35 H35A 109.5 . . ? C33 C35 H35B 109.5 . . ? C33 C35 H35C 109.5 . . ? H35A C35 H35B 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? C33 C36 H36A 109.5 . . ? C33 C36 H36B 109.5 . . ? C33 C36 H36C 109.5 . . ? H36A C36 H36B 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? C38 C37 C30 112.3(5) . . ? C38 C37 C40 107.5(6) . . ? C39 C37 C30 108.9(5) . . ? C39 C37 C38 109.4(6) . . ? C39 C37 C40 109.4(6) . . ? C40 C37 C30 109.3(5) . . ? C37 C38 H38A 109.5 . . ? C37 C38 H38B 109.5 . . ? C37 C38 H38C 109.5 . . ? H38A C38 H38B 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? C37 C39 H39A 109.5 . . ? C37 C39 H39B 109.5 . . ? C37 C39 H39C 109.5 . . ? H39A C39 H39B 109.5 . . ? H39A C39 H39C 109.5 . . ? H39B C39 H39C 109.5 . . ? C37 C40 H40A 109.5 . . ? C37 C40 H40B 109.5 . . ? C37 C40 H40C 109.5 . . ? H40A C40 H40B 109.5 . . ? H40A C40 H40C 109.5 . . ? H40B C40 H40C 109.5 . . ? C42 C41 P1 117.1(4) . . ? C42 C41 C46 120.4(5) . . ? C46 C41 P1 122.4(4) . . ? C41 C42 H42 118.8 . . ? C43 C42 C41 122.3(6) . . ? C43 C42 H42 118.8 . . ? C42 C43 C53 120.6(7) . . ? C44 C43 C42 116.7(6) . . ? C44 C43 C53 122.7(6) . . ? C43 C44 H44 119.0 . . ? C43 C44 C45 122.1(6) . . ? C45 C44 H44 119.0 . . ? C44 C45 H45 119.3 . . ? C46 C45 C44 121.5(6) . . ? C46 C45 H45 119.3 . . ? C41 C46 C47 126.0(5) . . ? C45 C46 C41 116.9(6) . . ? C45 C46 C47 117.0(6) . . ? C48 C47 C46 120.6(5) . . ? C48 C47 C52 116.3(6) . . ? C52 C47 C46 123.1(5) . . ? C47 C48 H48 118.8 . . ? C49 C48 C47 122.4(6) . . ? C49 C48 H48 118.8 . . ? C48 C49 H49 119.2 . . ? C48 C49 C50 121.6(6) . . ? C50 C49 H49 119.2 . . ? C49 C50 C57 123.5(5) . . ? C51 C50 C49 115.8(6) . . ? C51 C50 C57 120.7(6) . . ? C50 C51 H51 118.4 . . ? C52 C51 C50 123.1(6) . . ? C52 C51 H51 118.4 . . ? C47 C52 H52 119.6 . . ? C51 C52 C47 120.7(5) . . ? C51 C52 H52 119.6 . . ? C43 C53 C55A 107.3(12) . . ? C43 C53 C56A 111.0(18) . . ? C54A C53 C43 113.8(10) . . ? C54A C53 C55A 109.9(11) . . ? C54A C53 C56A 108.3(11) . . ? C55A C53 C56A 106.3(11) . . ? C55B C53 C43 106.8(11) . . ? C55B C53 C54B 110.5(10) . . ? C55B C53 C56B 111.0(9) . . ? C54B C53 C43 108.4(8) . . ? C56B C53 C43 110.8(9) . . ? C56B C53 C54B 109.3(8) . . ? F1 Sb1 F1 180.0(3) 2_576 . ? F1 Sb1 F2 88.4(7) 2_576 . ? F1 Sb1 F2 88.4(7) . 2_576 ? F1 Sb1 F2 91.6(7) . . ? F1 Sb1 F2 91.6(7) 2_576 2_576 ? F1 Sb1 F3 90.4(4) 2_576 . ? F1 Sb1 F3 90.4(4) . 2_576 ? F1 Sb1 F3 89.6(4) . . ? F1 Sb1 F3 89.6(4) 2_576 2_576 ? F2 Sb1 F2 180.0 2_576 . ? F2 Sb1 F3 90.4(3) 2_576 2_576 ? F2 Sb1 F3 90.5(3) . . ? F2 Sb1 F3 89.5(3) . 2_576 ? F2 Sb1 F3 89.6(3) 2_576 . ? F3 Sb1 F3 180.0 2_576 . ? C50 C57 C60 107.8(6) . . ? C58 C57 C50 112.0(6) . . ? C58 C57 C59 110.9(8) . . ? C58 C57 C60 108.8(7) . . ? C59 C57 C50 108.6(6) . . ? C59 C57 C60 108.7(7) . . ? C57 C58 H58A 109.5 . . ? C57 C58 H58B 109.5 . . ? C57 C58 H58C 109.5 . . ? H58A C58 H58B 109.5 . . ? H58A C58 H58C 109.5 . . ? H58B C58 H58C 109.5 . . ? C57 C59 H59A 109.5 . . ? C57 C59 H59B 109.5 . . ? C57 C59 H59C 109.5 . . ? H59A C59 H59B 109.5 . . ? H59A C59 H59C 109.5 . . ? H59B C59 H59C 109.5 . . ? C57 C60 H60A 109.5 . . ? C57 C60 H60B 109.5 . . ? C57 C60 H60C 109.5 . . ? H60A C60 H60B 109.5 . . ? H60A C60 H60C 109.5 . . ? H60B C60 H60C 109.5 . . ? O1 C61 N1 123.6(6) . . ? O1 C61 N2 128.1(5) . . ? N2 C61 N1 108.3(6) . . ? N1 C62 H62A 111.4 . . ? N1 C62 H62B 111.4 . . ? N1 C62 C63 101.8(6) . . ? H62A C62 H62B 109.3 . . ? C63 C62 H62A 111.4 . . ? C63 C62 H62B 111.4 . . ? N2 C63 C62 101.3(6) . . ? N2 C63 H63A 111.5 . . ? N2 C63 H63B 111.5 . . ? C62 C63 H63A 111.5 . . ? C62 C63 H63B 111.5 . . ? H63A C63 H63B 109.3 . . ? C17 C18A H18A 109.5 . . ? C17 C18A H18B 109.5 . . ? C17 C18A H18C 109.5 . . ? H18A C18A H18B 109.5 . . ? H18A C18A H18C 109.5 . . ? H18B C18A H18C 109.5 . . ? C17 C19A H19A 109.5 . . ? C17 C19A H19B 109.5 . . ? C17 C19A H19C 109.5 . . ? H19A C19A H19B 109.5 . . ? H19A C19A H19C 109.5 . . ? H19B C19A H19C 109.5 . . ? C17 C20A H20A 109.5 . . ? C17 C20A H20B 109.5 . . ? C17 C20A H20C 109.5 . . ? H20A C20A H20B 109.5 . . ? H20A C20A H20C 109.5 . . ? H20B C20A H20C 109.5 . . ? C17 C18B H18D 109.5 . . ? C17 C18B H18E 109.5 . . ? C17 C18B H18F 109.5 . . ? H18D C18B H18E 109.5 . . ? H18D C18B H18F 109.5 . . ? H18E C18B H18F 109.5 . . ? C17 C19B H19D 109.5 . . ? C17 C19B H19E 109.5 . . ? C17 C19B H19F 109.5 . . ? H19D C19B H19E 109.5 . . ? H19D C19B H19F 109.5 . . ? H19E C19B H19F 109.5 . . ? C17 C20B H20D 109.5 . . ? C17 C20B H20E 109.5 . . ? C17 C20B H20F 109.5 . . ? H20D C20B H20E 109.5 . . ? H20D C20B H20F 109.5 . . ? H20E C20B H20F 109.5 . . ? C53 C54A H54A 109.5 . . ? C53 C54A H54B 109.5 . . ? C53 C54A H54C 109.5 . . ? H54A C54A H54B 109.5 . . ? H54A C54A H54C 109.5 . . ? H54B C54A H54C 109.5 . . ? C53 C55A H55A 109.5 . . ? C53 C55A H55B 109.5 . . ? C53 C55A H55C 109.5 . . ? H55A C55A H55B 109.5 . . ? H55A C55A H55C 109.5 . . ? H55B C55A H55C 109.5 . . ? C53 C56A H56A 109.5 . . ? C53 C56A H56B 109.5 . . ? C53 C56A H56C 109.5 . . ? H56A C56A H56B 109.5 . . ? H56A C56A H56C 109.5 . . ? H56B C56A H56C 109.5 . . ? C53 C55B H55D 109.5 . . ? C53 C55B H55E 109.5 . . ? C53 C55B H55F 109.5 . . ? H55D C55B H55E 109.5 . . ? H55D C55B H55F 109.5 . . ? H55E C55B H55F 109.5 . . ? C53 C54B H54D 109.5 . . ? C53 C54B H54E 109.5 . . ? C53 C54B H54F 109.5 . . ? H54D C54B H54E 109.5 . . ? H54D C54B H54F 109.5 . . ? H54E C54B H54F 109.5 . . ? C53 C56B H56D 109.5 . . ? C53 C56B H56E 109.5 . . ? C53 C56B H56F 109.5 . . ? H56D C56B H56E 109.5 . . ? H56D C56B H56F 109.5 . . ? H56E C56B H56F 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Au1 P1 2.2084(12) . ? Au1 O1 2.083(3) . ? P1 C1 1.829(5) . ? P1 C21 1.823(5) . ? P1 C41 1.844(5) . ? O1 C61 1.232(7) . ? N1 H1 0.8800 . ? N1 C61 1.341(8) . ? N1 C62 1.430(10) . ? N2 H2 0.8800 . ? N2 C61 1.331(9) . ? N2 C63 1.448(10) . ? C1 C2 1.400(7) . ? C1 C6 1.397(7) . ? C2 H2A 0.9500 . ? C2 C3 1.390(8) . ? C3 C4 1.380(9) . ? C3 C13 1.527(8) . ? C4 H4 0.9500 . ? C4 C5 1.375(9) . ? C5 H5 0.9500 . ? C5 C6 1.390(8) . ? C6 C7 1.492(8) . ? C7 C8 1.377(9) . ? C7 C12 1.364(10) . ? C8 H8 0.9500 . ? C8 C9 1.386(8) . ? C9 H9 0.9500 . ? C9 C10 1.379(10) . ? C10 C11 1.394(11) . ? C10 C17 1.550(8) . ? C11 H11 0.9500 . ? C11 C12 1.385(9) . ? C12 H12 0.9500 . ? C13 C14 1.534(11) . ? C13 C15 1.559(13) . ? C13 C16 1.549(14) . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 C18A 1.381(18) . ? C17 C19A 1.61(2) . ? C17 C20A 1.61(2) . ? C17 C18B 1.69(3) . ? C17 C19B 1.33(4) . ? C17 C20B 1.57(3) . ? C21 C22 1.393(7) . ? C21 C26 1.402(7) . ? C22 H22 0.9500 . ? C22 C23 1.404(7) . ? C23 C24 1.389(8) . ? C23 C33 1.521(8) . ? C24 H24 0.9500 . ? C24 C25 1.391(8) . ? C25 H25 0.9500 . ? C25 C26 1.405(7) . ? C26 C27 1.483(7) . ? C27 C28 1.378(7) . ? C27 C32 1.395(7) . ? C28 H28 0.9500 . ? C28 C29 1.389(8) . ? C29 H29 0.9500 . ? C29 C30 1.369(8) . ? C30 C31 1.392(8) . ? C30 C37 1.544(8) . ? C31 H31 0.9500 . ? C31 C32 1.406(8) . ? C32 H32 0.9500 . ? C33 C34 1.498(11) . ? C33 C35 1.529(10) . ? C33 C36 1.549(10) . ? C34 H34A 0.9800 . ? C34 H34B 0.9800 . ? C34 H34C 0.9800 . ? C35 H35A 0.9800 . ? C35 H35B 0.9800 . ? C35 H35C 0.9800 . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C37 C38 1.524(10) . ? C37 C39 1.514(10) . ? C37 C40 1.533(9) . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? C39 H39A 0.9800 . ? C39 H39B 0.9800 . ? C39 H39C 0.9800 . ? C40 H40A 0.9800 . ? C40 H40B 0.9800 . ? C40 H40C 0.9800 . ? C41 C42 1.392(8) . ? C41 C46 1.396(8) . ? C42 H42 0.9500 . ? C42 C43 1.389(8) . ? C43 C44 1.366(10) . ? C43 C53 1.531(10) . ? C44 H44 0.9500 . ? C44 C45 1.391(10) . ? C45 H45 0.9500 . ? C45 C46 1.389(8) . ? C46 C47 1.486(8) . ? C47 C48 1.391(8) . ? C47 C52 1.408(8) . ? C48 H48 0.9500 . ? C48 C49 1.370(9) . ? C49 H49 0.9500 . ? C49 C50 1.404(9) . ? C50 C51 1.384(8) . ? C50 C57 1.533(9) . ? C51 H51 0.9500 . ? C51 C52 1.374(9) . ? C52 H52 0.9500 . ? C53 C54A 1.518(14) . ? C53 C55A 1.539(15) . ? C53 C56A 1.550(15) . ? C53 C55B 1.498(14) . ? C53 C54B 1.529(13) . ? C53 C56B 1.527(12) . ? Sb1 F1 1.785(7) 2_576 ? Sb1 F1 1.785(7) . ? Sb1 F2 1.798(8) 2_576 ? Sb1 F2 1.798(8) . ? Sb1 F3 1.875(5) 2_576 ? Sb1 F3 1.875(5) . ? C57 C58 1.505(11) . ? C57 C59 1.516(11) . ? C57 C60 1.546(11) . ? C58 H58A 0.9800 . ? C58 H58B 0.9800 . ? C58 H58C 0.9800 . ? C59 H59A 0.9800 . ? C59 H59B 0.9800 . ? C59 H59C 0.9800 . ? C60 H60A 0.9800 . ? C60 H60B 0.9800 . ? C60 H60C 0.9800 . ? C62 H62A 0.9900 . ? C62 H62B 0.9900 . ? C62 C63 1.537(13) . ? C63 H63A 0.9900 . ? C63 H63B 0.9900 . ? C18A H18A 0.9800 . ? C18A H18B 0.9800 . ? C18A H18C 0.9800 . ? C19A H19A 0.9800 . ? C19A H19B 0.9800 . ? C19A H19C 0.9800 . ? C20A H20A 0.9800 . ? C20A H20B 0.9800 . ? C20A H20C 0.9800 . ? C18B H18D 0.9800 . ? C18B H18E 0.9800 . ? C18B H18F 0.9800 . ? C19B H19D 0.9800 . ? C19B H19E 0.9800 . ? C19B H19F 0.9800 . ? C20B H20D 0.9800 . ? C20B H20E 0.9800 . ? C20B H20F 0.9800 . ? C54A H54A 0.9800 . ? C54A H54B 0.9800 . ? C54A H54C 0.9800 . ? C55A H55A 0.9800 . ? C55A H55B 0.9800 . ? C55A H55C 0.9800 . ? C56A H56A 0.9800 . ? C56A H56B 0.9800 . ? C56A H56C 0.9800 . ? C55B H55D 0.9800 . ? C55B H55E 0.9800 . ? C55B H55F 0.9800 . ? C54B H54D 0.9800 . ? C54B H54E 0.9800 . ? C54B H54F 0.9800 . ? C56B H56D 0.9800 . ? C56B H56E 0.9800 . ? C56B H56F 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Au1 P1 C1 C2 -151.7(4) . . . . ? Au1 P1 C1 C6 24.5(5) . . . . ? Au1 P1 C21 C22 -136.9(4) . . . . ? Au1 P1 C21 C26 40.0(4) . . . . ? Au1 P1 C41 C42 -140.0(4) . . . . ? Au1 P1 C41 C46 38.0(5) . . . . ? Au1 O1 C61 N1 -172.5(5) . . . . ? Au1 O1 C61 N2 8.1(9) . . . . ? P1 C1 C2 C3 176.3(5) . . . . ? P1 C1 C6 C5 -175.3(5) . . . . ? P1 C1 C6 C7 5.6(9) . . . . ? P1 C21 C22 C23 176.1(4) . . . . ? P1 C21 C26 C25 -176.6(4) . . . . ? P1 C21 C26 C27 1.8(7) . . . . ? P1 C41 C42 C43 178.9(5) . . . . ? P1 C41 C46 C45 -176.9(5) . . . . ? P1 C41 C46 C47 3.4(8) . . . . ? N1 C62 C63 N2 19.6(9) . . . . ? C1 P1 C21 C22 97.9(4) . . . . ? C1 P1 C21 C26 -85.2(4) . . . . ? C1 P1 C41 C42 -11.6(5) . . . . ? C1 P1 C41 C46 166.4(4) . . . . ? C1 C2 C3 C4 -0.8(10) . . . . ? C1 C2 C3 C13 -179.9(7) . . . . ? C1 C6 C7 C8 -116.7(7) . . . . ? C1 C6 C7 C12 67.2(9) . . . . ? C2 C1 C6 C5 0.8(9) . . . . ? C2 C1 C6 C7 -178.4(6) . . . . ? C2 C3 C4 C5 0.7(12) . . . . ? C2 C3 C13 C14 -6.0(11) . . . . ? C2 C3 C13 C15 -125.4(8) . . . . ? C2 C3 C13 C16 115.2(9) . . . . ? C3 C4 C5 C6 0.2(13) . . . . ? C4 C3 C13 C14 174.9(8) . . . . ? C4 C3 C13 C15 55.5(11) . . . . ? C4 C3 C13 C16 -63.9(10) . . . . ? C4 C5 C6 C1 -0.9(11) . . . . ? C4 C5 C6 C7 178.3(7) . . . . ? C5 C6 C7 C8 64.1(8) . . . . ? C5 C6 C7 C12 -111.9(8) . . . . ? C6 C1 C2 C3 0.0(9) . . . . ? C6 C7 C8 C9 -173.5(6) . . . . ? C6 C7 C12 C11 172.6(7) . . . . ? C7 C8 C9 C10 -0.6(10) . . . . ? C8 C7 C12 C11 -3.5(11) . . . . ? C8 C9 C10 C11 -0.9(11) . . . . ? C8 C9 C10 C17 177.4(7) . . . . ? C9 C10 C11 C12 0.1(12) . . . . ? C9 C10 C17 C18A -70.2(17) . . . . ? C9 C10 C17 C19A 159.0(11) . . . . ? C9 C10 C17 C20A 50.6(11) . . . . ? C9 C10 C17 C18B -113.6(13) . . . . ? C9 C10 C17 C19B 120(3) . . . . ? C9 C10 C17 C20B -5.4(15) . . . . ? C10 C11 C12 C7 2.1(14) . . . . ? C11 C10 C17 C18A 108.1(17) . . . . ? C11 C10 C17 C19A -22.7(14) . . . . ? C11 C10 C17 C20A -131.1(11) . . . . ? C11 C10 C17 C18B 64.7(14) . . . . ? C11 C10 C17 C19B -61(3) . . . . ? C11 C10 C17 C20B 172.8(13) . . . . ? C12 C7 C8 C9 2.8(10) . . . . ? C13 C3 C4 C5 179.9(8) . . . . ? C17 C10 C11 C12 -178.2(8) . . . . ? C21 P1 C1 C2 -28.2(5) . . . . ? C21 P1 C1 C6 148.0(5) . . . . ? C21 P1 C41 C42 96.5(5) . . . . ? C21 P1 C41 C46 -85.5(5) . . . . ? C21 C22 C23 C24 0.0(8) . . . . ? C21 C22 C23 C33 -178.8(5) . . . . ? C21 C26 C27 C28 -100.9(6) . . . . ? C21 C26 C27 C32 78.1(7) . . . . ? C22 C21 C26 C25 0.2(7) . . . . ? C22 C21 C26 C27 178.6(5) . . . . ? C22 C23 C24 C25 1.3(8) . . . . ? C22 C23 C33 C34 -65.9(7) . . . . ? C22 C23 C33 C35 55.6(8) . . . . ? C22 C23 C33 C36 174.5(6) . . . . ? C23 C24 C25 C26 -1.9(9) . . . . ? C24 C23 C33 C34 115.4(7) . . . . ? C24 C23 C33 C35 -123.1(7) . . . . ? C24 C23 C33 C36 -4.1(9) . . . . ? C24 C25 C26 C21 1.1(8) . . . . ? C24 C25 C26 C27 -177.4(5) . . . . ? C25 C26 C27 C28 77.4(7) . . . . ? C25 C26 C27 C32 -103.5(6) . . . . ? C26 C21 C22 C23 -0.7(8) . . . . ? C26 C27 C28 C29 -179.2(5) . . . . ? C26 C27 C32 C31 179.8(5) . . . . ? C27 C28 C29 C30 -2.2(9) . . . . ? C28 C27 C32 C31 -1.1(8) . . . . ? C28 C29 C30 C31 2.0(9) . . . . ? C28 C29 C30 C37 -176.0(6) . . . . ? C29 C30 C31 C32 -1.4(9) . . . . ? C29 C30 C37 C38 -175.8(6) . . . . ? C29 C30 C37 C39 62.8(8) . . . . ? C29 C30 C37 C40 -56.6(8) . . . . ? C30 C31 C32 C27 1.0(9) . . . . ? C31 C30 C37 C38 6.3(9) . . . . ? C31 C30 C37 C39 -115.0(7) . . . . ? C31 C30 C37 C40 125.5(6) . . . . ? C32 C27 C28 C29 1.7(9) . . . . ? C33 C23 C24 C25 180.0(6) . . . . ? C37 C30 C31 C32 176.5(6) . . . . ? C41 P1 C1 C2 81.4(5) . . . . ? C41 P1 C1 C6 -102.4(5) . . . . ? C41 P1 C21 C22 -13.5(5) . . . . ? C41 P1 C21 C26 163.4(4) . . . . ? C41 C42 C43 C44 -2.0(10) . . . . ? C41 C42 C43 C53 176.9(7) . . . . ? C41 C46 C47 C48 -131.1(6) . . . . ? C41 C46 C47 C52 51.5(9) . . . . ? C42 C41 C46 C45 1.1(8) . . . . ? C42 C41 C46 C47 -178.7(5) . . . . ? C42 C43 C44 C45 1.1(12) . . . . ? C42 C43 C53 C54A 4.5(15) . . . . ? C42 C43 C53 C55A -117.3(14) . . . . ? C42 C43 C53 C56A 126.9(14) . . . . ? C42 C43 C53 C55B -64.8(12) . . . . ? C42 C43 C53 C54B 54.3(12) . . . . ? C42 C43 C53 C56B 174.2(9) . . . . ? C43 C44 C45 C46 0.8(13) . . . . ? C44 C43 C53 C54A -176.7(14) . . . . ? C44 C43 C53 C55A 61.5(15) . . . . ? C44 C43 C53 C56A -54.3(16) . . . . ? C44 C43 C53 C55B 114.1(12) . . . . ? C44 C43 C53 C54B -126.8(11) . . . . ? C44 C43 C53 C56B -6.9(12) . . . . ? C44 C45 C46 C41 -1.9(10) . . . . ? C44 C45 C46 C47 177.9(7) . . . . ? C45 C46 C47 C48 49.2(8) . . . . ? C45 C46 C47 C52 -128.2(7) . . . . ? C46 C41 C42 C43 0.9(9) . . . . ? C46 C47 C48 C49 -178.7(6) . . . . ? C46 C47 C52 C51 179.0(5) . . . . ? C47 C48 C49 C50 -1.0(11) . . . . ? C48 C47 C52 C51 1.6(9) . . . . ? C48 C49 C50 C51 2.6(10) . . . . ? C48 C49 C50 C57 -178.1(7) . . . . ? C49 C50 C51 C52 -2.2(9) . . . . ? C49 C50 C57 C58 4.0(10) . . . . ? C49 C50 C57 C59 -118.8(8) . . . . ? C49 C50 C57 C60 123.6(7) . . . . ? C50 C51 C52 C47 0.1(9) . . . . ? C51 C50 C57 C58 -176.7(7) . . . . ? C51 C50 C57 C59 60.5(8) . . . . ? C51 C50 C57 C60 -57.1(8) . . . . ? C52 C47 C48 C49 -1.1(10) . . . . ? C53 C43 C44 C45 -177.8(8) . . . . ? C57 C50 C51 C52 178.4(6) . . . . ? C61 N1 C62 C63 -17.4(9) . . . . ? C61 N2 C63 C62 -17.3(9) . . . . ? C62 N1 C61 O1 -172.2(7) . . . . ? C62 N1 C61 N2 7.3(9) . . . . ? C63 N2 C61 O1 -173.2(7) . . . . ? C63 N2 C61 N1 7.4(9) . . . . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 -0.147 -0.107 0.000 1079.3 232.5 '1 CD2Cl2'