#------------------------------------------------------------------------------ #$Date: 2022-04-03 20:23:05 +0100 (Sun, 03 Apr 2022) $ #$Revision: 274242 $ #$URL: svn://www.crystallography.net/cod/cif/4/51/93/4519386.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519386 loop_ _publ_author_name 'Navarro, Miquel' 'Alf\'erez, Macarena G.' 'de Sousa, Morgane' 'Miranda-Pizarro, Juan' 'Campos, Jes\'us' _publ_section_title ; Dicoordinate Au(I)--Ethylene Complexes as Hydroamination Catalysts ; _journal_issue 7 _journal_name_full 'ACS Catalysis' _journal_page_first 4227 _journal_page_last 4241 _journal_paper_doi 10.1021/acscatal.1c05823 _journal_volume 12 _journal_year 2022 _chemical_formula_sum 'C46 H67 Au Cl P' _chemical_formula_weight 883.38 _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.6694(2) _cell_length_b 18.1472(4) _cell_length_c 18.8940(4) _cell_measurement_reflns_used 9843 _cell_measurement_temperature 193(2) _cell_measurement_theta_max 30.10 _cell_measurement_theta_min 2.49 _cell_volume 4344.00(15) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT A' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 193(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0297 _diffrn_reflns_av_unetI/netI 0.0490 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 25 _diffrn_reflns_limit_k_min -25 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -26 _diffrn_reflns_number 48475 _diffrn_reflns_point_group_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.543 _diffrn_reflns_theta_min 2.156 _exptl_absorpt_coefficient_mu 3.514 _exptl_absorpt_correction_T_max 0.7461 _exptl_absorpt_correction_T_min 0.6011 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS, Bruker (2006). APEX 2. Version 2.1. Bruker Analytical X-ray Solutions, Madison, Wisconsin, USA. ; _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.351 _exptl_crystal_description prism _exptl_crystal_F_000 1816 _exptl_crystal_size_max 0.20 _exptl_crystal_size_mid 0.17 _exptl_crystal_size_min 0.10 _refine_diff_density_max 0.849 _refine_diff_density_min -0.466 _refine_diff_density_rms 0.065 _refine_ls_abs_structure_details ; Flack x determined using 5062 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.004(2) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.862 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 454 _refine_ls_number_reflns 13243 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.862 _refine_ls_R_factor_all 0.0267 _refine_ls_R_factor_gt 0.0217 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0393 _refine_ls_wR_factor_ref 0.0404 _reflns_Friedel_coverage 0.821 _reflns_Friedel_fraction_full 0.991 _reflns_Friedel_fraction_max 0.992 _reflns_number_gt 12142 _reflns_number_total 13243 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cs1c05823_si_006.cif _cod_data_source_block jcm4319a _cod_database_code 4519386 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; jcm4319a.res created by SHELXL-2014/7 TITL jcm4319a_0m in P2(1)2(1)2(1) CELL 0.71073 12.6694 18.1472 18.8940 90.000 90.000 90.000 ZERR 4.00 0.0002 0.0004 0.0004 0.000 0.000 0.000 LATT -1 SYMM x+1/2, -y+1/2, -z SYMM -x, y+1/2, -z+1/2 SYMM -x+1/2, -y, z+1/2 SFAC C H P CL AU UNIT 184 268 4 4 4 TEMP -80 ACTA L.S. 24 FMAP 2 CONF omit -6 1 2 ! 858.75 1925.22 17.43 0.117 2.0 omit 1 0 1 ! 568.89 977.64 12.41 0.083 10.5 omit 0 1 1 ! 32143.53 59203.48 9.80 0.648 13.0 WGHT 0.000000 FVAR 0.08594 AU1 5 0.737330 0.358710 0.967040 11.00000 0.02016 0.01739 = 0.02590 0.00637 0.00106 0.00135 CL1 4 0.818723 0.256604 1.013961 11.00000 0.03260 0.02734 = 0.05566 0.02076 -0.00274 0.00840 P1 3 0.637771 0.450697 0.923823 11.00000 0.01572 0.01382 = 0.01865 0.00221 0.00253 -0.00066 C1 1 0.702700 0.531202 0.882727 11.00000 0.01403 0.01398 = 0.01242 -0.00137 0.00033 -0.00147 C2 1 0.644883 0.592955 0.857672 11.00000 0.01559 0.01566 = 0.01852 0.00009 0.00053 0.00183 C3 1 0.692451 0.641830 0.810858 11.00000 0.02318 0.01916 = 0.03100 0.01006 0.00566 0.00426 AFIX 43 H1 2 0.653108 0.682555 0.793476 11.00000 -1.20000 AFIX 0 C4 1 0.795756 0.632493 0.789029 11.00000 0.02601 0.02771 = 0.03805 0.01672 0.00993 0.00246 AFIX 43 H2 2 0.825551 0.664658 0.754757 11.00000 -1.20000 AFIX 0 C5 1 0.854819 0.576443 0.817247 11.00000 0.01543 0.02317 = 0.03480 0.00915 0.00882 0.00197 AFIX 43 H3 2 0.927044 0.571900 0.804459 11.00000 -1.20000 AFIX 0 C6 1 0.810743 0.525985 0.864391 11.00000 0.01580 0.01602 = 0.01693 -0.00218 0.00075 0.00015 C7 1 0.885756 0.470193 0.893223 11.00000 0.01112 0.01624 = 0.02001 0.00129 0.00016 -0.00243 C8 1 0.921345 0.475609 0.962757 11.00000 0.01988 0.01829 = 0.02105 -0.00169 0.00353 0.00193 AFIX 43 H24 2 0.893250 0.512593 0.992947 11.00000 -1.20000 AFIX 0 C9 1 0.998073 0.427122 0.988603 11.00000 0.02420 0.02043 = 0.02050 0.00110 -0.00316 -0.00047 C10 1 1.037013 0.373536 0.943224 11.00000 0.01897 0.01748 = 0.02627 0.00146 -0.00486 0.00343 AFIX 43 H14 2 1.088952 0.340252 0.960347 11.00000 -1.20000 AFIX 0 C11 1 1.002556 0.366687 0.873045 11.00000 0.01546 0.01333 = 0.02404 -0.00049 0.00217 0.00034 C12 1 1.047692 0.305916 0.826528 11.00000 0.02245 0.01658 = 0.02418 -0.00058 0.00180 0.00317 C13 1 0.993695 0.302122 0.753877 11.00000 0.05456 0.03754 = 0.03597 -0.01216 -0.00606 0.01978 AFIX 137 H6 2 0.917603 0.295095 0.760308 11.00000 -1.50000 H5 2 1.022673 0.260706 0.726851 11.00000 -1.50000 H4 2 1.006341 0.348143 0.728097 11.00000 -1.50000 AFIX 0 C14 1 1.165779 0.320113 0.814767 11.00000 0.02868 0.03297 = 0.05672 -0.01600 0.01429 0.00093 AFIX 137 H8 2 1.175077 0.366629 0.789166 11.00000 -1.50000 H9 2 1.196038 0.279695 0.786989 11.00000 -1.50000 H7 2 1.201649 0.323084 0.860632 11.00000 -1.50000 AFIX 0 C15 1 1.031908 0.231676 0.863120 11.00000 0.05895 0.01913 = 0.04211 -0.00079 0.01655 0.00330 AFIX 137 H10 2 1.070717 0.231217 0.907985 11.00000 -1.50000 H12 2 1.058291 0.192173 0.832497 11.00000 -1.50000 H11 2 0.956589 0.224006 0.872353 11.00000 -1.50000 AFIX 0 C16 1 0.926871 0.416203 0.848824 11.00000 0.01634 0.01756 = 0.01904 0.00134 -0.00060 0.00018 AFIX 43 H13 2 0.902929 0.413091 0.801270 11.00000 -1.20000 AFIX 0 C17 1 1.035888 0.434666 1.065367 11.00000 0.03742 0.02793 = 0.02326 -0.00300 -0.01101 0.00513 C18 1 1.107495 0.370769 1.086971 11.00000 0.09631 0.04645 = 0.03651 -0.00701 -0.03594 0.02648 AFIX 137 H16 2 1.070748 0.324006 1.078859 11.00000 -1.50000 H17 2 1.125385 0.375250 1.137249 11.00000 -1.50000 H15 2 1.172284 0.372065 1.058663 11.00000 -1.50000 AFIX 0 C19 1 1.097266 0.506853 1.072541 11.00000 0.04838 0.04153 = 0.03221 -0.00598 -0.01684 -0.00278 AFIX 137 H20 2 1.160335 0.504961 1.042566 11.00000 -1.50000 H19 2 1.118345 0.513806 1.121997 11.00000 -1.50000 H18 2 1.052445 0.548048 1.057656 11.00000 -1.50000 AFIX 0 C20 1 0.941587 0.435348 1.115305 11.00000 0.06649 0.06661 = 0.01941 -0.00021 -0.00181 -0.00895 AFIX 137 H22 2 0.897450 0.478426 1.105184 11.00000 -1.50000 H21 2 0.966528 0.437728 1.164350 11.00000 -1.50000 H23 2 0.900081 0.390328 1.108527 11.00000 -1.50000 AFIX 0 C21 1 0.534096 0.613268 0.878163 11.00000 0.01659 0.01355 = 0.02063 0.00570 0.00103 0.00102 C22 1 0.519190 0.663785 0.933124 11.00000 0.01779 0.01743 = 0.02289 -0.00157 -0.00220 0.00239 AFIX 43 H45 2 0.578794 0.682798 0.957562 11.00000 -1.20000 AFIX 0 C23 1 0.418025 0.686776 0.952707 11.00000 0.02178 0.01895 = 0.02338 0.00002 0.00201 0.00309 C24 1 0.333476 0.657233 0.915388 11.00000 0.01391 0.02714 = 0.02572 -0.00292 0.00231 0.00429 AFIX 43 H35 2 0.264114 0.671516 0.928681 11.00000 -1.20000 AFIX 0 C25 1 0.345019 0.607980 0.859742 11.00000 0.01416 0.01837 = 0.02333 0.00328 0.00092 0.00035 C26 1 0.447455 0.587685 0.841002 11.00000 0.01896 0.01576 = 0.01778 0.00184 0.00273 0.00237 AFIX 43 H25 2 0.457946 0.555613 0.801890 11.00000 -1.20000 AFIX 0 C27 1 0.247226 0.578207 0.821778 11.00000 0.01686 0.02769 = 0.02794 -0.00255 -0.00199 -0.00076 C28 1 0.187921 0.642142 0.786063 11.00000 0.03419 0.04390 = 0.04798 -0.00083 -0.01796 0.00678 AFIX 137 H26 2 0.169627 0.679289 0.821656 11.00000 -1.50000 H28 2 0.123287 0.623407 0.763969 11.00000 -1.50000 H27 2 0.233065 0.664464 0.749809 11.00000 -1.50000 AFIX 0 C29 1 0.174557 0.540685 0.875388 11.00000 0.03021 0.04955 = 0.04314 -0.00213 0.00550 -0.01548 AFIX 137 H30 2 0.213449 0.501661 0.899992 11.00000 -1.50000 H31 2 0.113900 0.519232 0.850662 11.00000 -1.50000 H29 2 0.149740 0.577111 0.909876 11.00000 -1.50000 AFIX 0 C30 1 0.275534 0.521292 0.765146 11.00000 0.02644 0.03954 = 0.03519 -0.01054 -0.00601 -0.00512 AFIX 137 H33 2 0.319642 0.544494 0.728829 11.00000 -1.50000 H34 2 0.210750 0.502436 0.743347 11.00000 -1.50000 H32 2 0.314345 0.480485 0.786983 11.00000 -1.50000 AFIX 0 C31 1 0.396692 0.742445 1.012301 11.00000 0.02633 0.02720 = 0.02876 -0.01047 0.00059 0.00609 C32 1 0.338141 0.809224 0.982629 11.00000 0.04881 0.02997 = 0.04851 -0.01156 -0.00268 0.01483 AFIX 137 H37 2 0.382389 0.833764 0.947210 11.00000 -1.50000 H36 2 0.322353 0.843706 1.021118 11.00000 -1.50000 H38 2 0.272115 0.793049 0.960521 11.00000 -1.50000 AFIX 0 C33 1 0.329271 0.705486 1.069860 11.00000 0.04501 0.05080 = 0.03383 -0.01082 0.01139 0.00574 AFIX 137 H39 2 0.260481 0.691929 1.050034 11.00000 -1.50000 H41 2 0.319096 0.739846 1.109290 11.00000 -1.50000 H40 2 0.365244 0.661116 1.086959 11.00000 -1.50000 AFIX 0 C34 1 0.498876 0.769736 1.046842 11.00000 0.03697 0.04222 = 0.04524 -0.02354 -0.00323 0.00216 AFIX 137 H43 2 0.537966 0.727668 1.066094 11.00000 -1.50000 H42 2 0.481746 0.804099 1.085169 11.00000 -1.50000 H44 2 0.542279 0.794897 1.011356 11.00000 -1.50000 AFIX 0 C35 1 0.558353 0.412551 0.850189 11.00000 0.01969 0.01621 = 0.02724 -0.00083 -0.00303 -0.00073 AFIX 13 H56 2 0.496086 0.445469 0.842557 11.00000 -1.20000 AFIX 0 C36 1 0.517872 0.335119 0.866470 11.00000 0.04499 0.02679 = 0.03687 -0.00212 0.00254 -0.01704 AFIX 23 H54 2 0.578338 0.303138 0.879040 11.00000 -1.20000 H55 2 0.470103 0.337291 0.907883 11.00000 -1.20000 AFIX 0 C37 1 0.458984 0.301252 0.804103 11.00000 0.04231 0.03099 = 0.04916 -0.00653 -0.00397 -0.01825 AFIX 23 H53 2 0.436484 0.250613 0.816442 11.00000 -1.20000 H46 2 0.394924 0.330663 0.793986 11.00000 -1.20000 AFIX 0 C38 1 0.528071 0.298964 0.739086 11.00000 0.06367 0.05013 = 0.04668 -0.02010 -0.00608 -0.01918 AFIX 23 H47 2 0.487848 0.278285 0.698792 11.00000 -1.20000 H48 2 0.589825 0.266817 0.747887 11.00000 -1.20000 AFIX 0 C39 1 0.565330 0.376735 0.721047 11.00000 0.10629 0.07318 = 0.03046 -0.01052 -0.00267 -0.05211 AFIX 23 H49 2 0.612478 0.374739 0.679307 11.00000 -1.20000 H50 2 0.503564 0.407536 0.708598 11.00000 -1.20000 AFIX 0 C40 1 0.623869 0.411888 0.782609 11.00000 0.06304 0.04803 = 0.02319 -0.00970 0.00819 -0.03398 AFIX 23 H52 2 0.642901 0.463128 0.769940 11.00000 -1.20000 H51 2 0.690115 0.384383 0.791233 11.00000 -1.20000 AFIX 0 C41 1 0.554949 0.487712 0.995901 11.00000 0.02136 0.01910 = 0.02416 0.00644 0.00714 0.00134 AFIX 13 H67 2 0.510735 0.528734 0.976669 11.00000 -1.20000 AFIX 0 C42 1 0.482230 0.429753 1.028534 11.00000 0.03206 0.02855 = 0.02847 0.00278 0.01273 -0.00771 AFIX 23 H65 2 0.430013 0.413485 0.992822 11.00000 -1.20000 H66 2 0.524395 0.386321 1.042883 11.00000 -1.20000 AFIX 0 C43 1 0.424489 0.460755 1.093000 11.00000 0.03795 0.04493 = 0.04289 0.00482 0.02338 -0.00573 AFIX 23 H58 2 0.376362 0.500615 1.077563 11.00000 -1.20000 H57 2 0.381120 0.421362 1.114638 11.00000 -1.20000 AFIX 0 C44 1 0.499940 0.490675 1.147649 11.00000 0.05463 0.04778 = 0.02635 -0.00222 0.01667 0.00280 AFIX 23 H59 2 0.543613 0.449975 1.166615 11.00000 -1.20000 H60 2 0.459472 0.512255 1.187393 11.00000 -1.20000 AFIX 0 C45 1 0.571147 0.549142 1.115636 11.00000 0.04732 0.04225 = 0.02927 -0.01163 0.01438 -0.00351 AFIX 23 H62 2 0.622438 0.566015 1.151691 11.00000 -1.20000 H61 2 0.528023 0.592063 1.101149 11.00000 -1.20000 AFIX 0 C46 1 0.630700 0.519269 1.051411 11.00000 0.03132 0.03778 = 0.02930 -0.01101 0.01008 -0.00674 AFIX 23 H64 2 0.680087 0.480202 1.066930 11.00000 -1.20000 H63 2 0.672757 0.559415 1.029885 11.00000 -1.20000 AFIX 0 HKLF 4 1 1 0 0 0 1 0 0 0 1 REM jcm4319a_0m in P2(1)2(1)2(1) REM R1 = 0.0217 for 12142 Fo > 4sig(Fo) and 0.0267 for all 13243 data REM 454 parameters refined using 0 restraints END WGHT 0.0000 0.0000 REM Highest difference peak 0.849, deepest hole -0.466, 1-sigma level 0.065 Q1 1 0.7813 0.3565 0.9280 11.00000 0.05 0.54 Q2 1 0.8150 0.2428 0.9752 11.00000 0.05 0.42 Q3 1 0.6771 0.3621 0.9414 11.00000 0.05 0.40 Q4 1 0.8090 0.2496 1.0355 11.00000 0.05 0.40 Q5 1 0.7775 0.3625 1.0101 11.00000 0.05 0.39 Q6 1 0.6827 0.3592 0.9998 11.00000 0.05 0.36 Q7 1 0.7371 0.3532 1.0211 11.00000 0.05 0.34 Q8 1 0.7263 0.3789 1.0139 11.00000 0.05 0.32 Q9 1 0.8512 0.2718 1.0240 11.00000 0.05 0.32 Q10 1 0.5861 0.4604 0.9546 11.00000 0.05 0.32 Q11 1 0.7645 0.4034 0.9411 11.00000 0.05 0.31 Q12 1 0.5996 0.3405 0.7222 11.00000 0.05 0.30 Q13 1 0.5360 0.3777 0.7245 11.00000 0.05 0.30 Q14 1 0.7759 0.2623 0.9969 11.00000 0.05 0.29 Q15 1 0.6464 0.3762 0.7877 11.00000 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1.76 7 -9 0 19.98 1.77 8 9 0 75.63 4.86 8 -9 0 75.11 5.04 -8 9 0 71.96 4.42 -8 -9 0 73.68 5.13 -8 -9 0 72.49 4.71 8 -9 0 70.21 4.58 9 -9 0 8.18 1.31 -9 9 0 10.31 1.26 9 9 0 9.46 1.58 -9 -9 0 9.31 1.33 -9 -9 0 7.54 1.27 10 9 0 130.56 8.09 10 -9 0 127.56 7.84 -10 -9 0 134.96 8.81 -10 9 0 132.55 7.56 -10 -9 0 131.03 8.67 -10 -9 0 130.93 7.93 11 -9 0 0.80 0.92 -11 9 0 -0.14 0.73 11 9 0 1.36 1.13 -11 -9 0 -0.18 0.90 -11 -9 0 -0.27 0.58 -11 -9 0 -0.29 0.65 -12 -9 0 81.28 5.64 -12 -9 0 83.72 5.71 -12 -9 0 86.82 5.56 12 9 0 75.79 5.59 12 -9 0 86.29 5.50 13 9 0 1.34 1.34 13 -9 0 0.26 1.08 -13 -9 0 1.47 0.65 -13 -9 0 0.91 0.62 14 -9 0 63.21 4.77 14 9 0 68.67 5.12 15 9 0 1.06 1.59 15 -9 0 1.95 1.37 16 9 0 27.02 3.38 16 -9 0 26.39 3.10 0 -10 0 337.46 21.22 0 -10 0 340.70 18.66 1 -10 0 1.21 0.51 1 -10 0 2.52 0.67 -1 -10 0 3.09 0.65 -1 -10 0 1.91 0.64 -2 -10 0 399.09 24.51 -2 -10 0 400.70 21.54 2 -10 0 379.84 24.41 -2 10 0 389.17 20.96 2 -10 0 391.25 21.45 3 -10 0 3.10 0.62 3 10 0 2.23 0.75 3 -10 0 2.19 0.67 -3 10 0 2.76 0.68 -3 -10 0 2.88 0.74 -3 -10 0 1.86 0.66 4 -10 0 136.46 8.95 4 10 0 139.59 8.08 -4 -10 0 139.44 8.03 4 -10 0 138.76 7.93 -4 -10 0 139.01 9.08 -4 10 0 140.10 7.75 -5 -10 0 15.69 1.54 5 10 0 15.32 1.57 -5 -10 0 15.73 1.59 -5 10 0 16.56 1.42 5 -10 0 15.37 1.46 5 -10 0 15.96 1.50 6 -10 0 66.90 4.61 6 10 0 67.14 4.40 -6 -10 0 66.38 4.27 -6 -10 0 67.07 4.75 -6 10 0 65.86 4.05 6 -10 0 68.25 4.19 -7 -10 0 31.72 2.42 7 -10 0 27.15 2.19 7 -10 0 28.36 2.32 -7 10 0 28.28 2.14 -7 -10 0 27.89 2.46 7 10 0 29.40 2.50 -8 10 0 81.76 4.74 8 -10 0 79.59 5.39 -8 -10 0 76.24 4.96 8 -10 0 75.80 4.84 8 10 0 78.18 5.14 -8 -10 0 75.16 5.44 -9 -10 0 5.19 1.05 -9 10 0 7.44 1.16 -9 -10 0 6.48 1.29 9 -10 0 5.55 1.18 9 10 0 5.88 1.39 10 -10 0 14.58 1.78 10 10 0 13.74 1.92 -10 -10 0 15.90 1.80 -10 10 0 15.86 1.63 -10 -10 0 17.90 1.99 11 -10 0 8.76 1.50 11 10 0 8.12 1.70 -11 10 0 8.55 1.31 -11 -10 0 8.23 1.40 -11 -10 0 7.98 1.28 -11 -10 0 9.79 1.61 12 -10 0 21.54 2.36 -12 -10 0 22.54 2.12 12 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0 122.49 7.19 7 11 0 114.46 7.26 7 -11 0 115.32 7.02 8 11 0 11.77 1.72 -8 -11 0 13.82 1.68 -8 -11 0 13.08 1.64 8 -11 0 12.05 1.52 -8 11 0 12.99 1.49 -9 -11 0 65.37 4.46 9 -11 0 60.95 4.31 -9 -11 0 66.65 4.85 -9 11 0 69.56 4.22 9 11 0 70.25 4.74 10 -11 0 24.14 2.31 10 11 0 24.76 2.51 -10 -11 0 23.61 2.35 -10 11 0 26.62 2.15 -10 -11 0 24.71 2.45 -11 -11 0 34.38 3.11 -11 -11 0 34.39 3.00 11 -11 0 36.00 2.91 -11 -11 0 32.38 2.94 11 11 0 39.78 3.34 -11 11 0 34.98 2.71 12 11 0 12.85 2.15 -12 -11 0 8.45 1.68 -12 -11 0 10.73 1.48 12 -11 0 9.76 1.70 -12 -11 0 9.85 1.52 -13 -11 0 11.17 1.44 13 -11 0 10.42 1.79 13 11 0 10.44 2.16 14 11 0 5.12 1.87 14 -11 0 4.52 1.55 15 -11 0 6.56 1.76 15 11 0 7.69 2.09 16 -11 0 3.03 1.61 16 11 0 3.98 1.96 0 -12 0 18.92 1.82 0 -12 0 21.20 1.78 -1 -12 0 7.82 1.11 1 -12 0 8.34 1.12 -1 -12 0 7.36 1.18 1 -12 0 7.00 1.04 2 -12 0 30.13 2.33 -2 12 0 30.31 2.23 -2 -12 0 32.31 2.47 2 -12 0 33.24 2.53 -2 -12 0 31.87 2.60 -3 -12 0 23.88 2.05 -3 12 0 25.85 1.89 3 -12 0 22.91 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0.76 0.89 13 12 0 55.09 4.55 13 -12 0 58.85 4.32 14 12 0 0.55 1.48 14 -12 0 0.14 1.27 15 -12 0 25.02 2.93 15 12 0 25.96 3.33 16 -12 0 -0.39 1.28 16 12 0 0.93 1.75 0 -13 0 0.23 0.69 0 -13 0 0.37 0.56 1 -13 0 57.37 4.19 1 -13 0 59.40 3.82 -1 -13 0 59.04 4.26 -1 -13 0 56.50 3.80 -2 -13 0 23.57 2.24 -2 13 0 26.99 2.06 2 -13 0 24.65 2.16 -2 -13 0 23.93 2.10 2 -13 0 23.71 2.04 3 -13 0 38.72 3.01 3 13 0 43.61 3.00 -3 -13 0 36.08 3.07 -3 -13 0 38.92 2.91 3 -13 0 34.72 2.74 -3 13 0 40.94 2.69 -4 13 0 28.56 2.28 4 -13 0 32.99 2.60 4 13 0 32.09 2.52 -4 -13 0 30.48 2.66 4 -13 0 31.55 2.42 -4 -13 0 27.03 2.40 -5 -13 0 50.67 4.04 5 -13 0 50.23 3.93 5 13 0 57.30 3.86 5 -13 0 54.94 3.60 -5 -13 0 54.03 3.75 -5 13 0 55.17 3.51 -6 -13 0 10.44 1.53 -6 -13 0 7.66 1.42 6 13 0 9.92 1.61 6 -13 0 9.13 1.31 6 -13 0 8.30 1.31 -6 13 0 11.01 1.31 -7 -13 0 6.83 1.33 -7 -13 0 11.68 1.58 7 13 0 9.81 1.61 -7 13 0 9.17 1.32 7 -13 0 9.10 1.41 7 -13 0 10.83 1.46 8 -13 0 29.19 2.42 -8 13 0 27.20 2.29 -8 -13 0 26.75 2.63 8 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0.90 -5 -14 0 0.60 0.71 5 -14 0 -0.66 0.77 5 -14 0 -0.99 0.55 -5 14 0 0.86 0.69 -5 -14 0 1.03 0.85 -6 -14 0 124.87 7.72 -6 -14 0 126.47 8.60 6 -14 0 129.42 8.48 -6 14 0 125.78 7.36 6 -14 0 128.42 7.57 6 14 0 122.86 7.76 -7 -14 0 0.07 0.89 7 -14 0 1.05 0.90 -7 -14 0 0.10 0.76 7 14 0 0.50 0.97 -7 14 0 0.60 0.82 -8 -14 0 106.52 7.38 8 -14 0 105.07 6.54 -8 -14 0 109.00 6.74 -8 14 0 108.32 6.37 8 14 0 98.70 6.75 -9 -14 0 0.06 0.98 -9 14 0 -0.76 0.81 9 14 0 -0.75 0.98 9 -14 0 0.26 0.93 -9 -14 0 0.27 0.84 -10 -14 0 36.22 3.24 -10 -14 0 36.86 3.40 10 -14 0 36.77 3.10 10 14 0 38.33 3.37 11 -14 0 3.69 1.30 -11 -14 0 2.14 1.33 -11 -14 0 1.54 1.01 11 14 0 2.78 1.38 12 -14 0 25.69 2.68 -12 -14 0 22.09 2.72 -12 -14 0 24.47 2.85 12 14 0 23.71 3.02 -12 -14 0 23.59 2.53 13 14 0 -0.07 1.53 13 -14 0 2.22 1.38 14 -14 0 5.25 1.67 14 14 0 4.88 2.00 15 -14 0 -0.45 1.40 15 14 0 2.00 1.82 0 -15 0 1.08 0.64 0 -15 0 0.06 0.73 1 -15 0 66.07 4.77 1 -15 0 66.99 4.35 -1 -15 0 61.27 4.33 -1 -15 0 65.02 4.78 -2 15 0 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3 -14 12.40 2.73 15 3 -14 5.97 1.48 15 -3 14 6.32 2.14 -15 -3 -14 4.53 2.03 15 3 14 5.25 2.06 0 -4 14 108.30 6.37 0 -4 -14 112.27 6.28 0 4 -14 111.21 7.35 0 4 -14 107.46 6.54 0 -4 -14 108.19 6.37 0 4 -14 105.96 6.30 1 4 -14 15.78 1.54 1 -4 14 16.45 1.58 -1 -4 -14 17.14 1.59 -1 -4 -14 14.57 1.61 1 4 -14 14.39 1.68 1 4 -14 14.63 1.61 -1 -4 14 17.92 1.47 1 4 14 15.22 1.33 -1 4 -14 17.23 1.76 1 -4 -14 17.46 1.45 -1 4 -14 16.61 1.58 -1 4 -14 17.02 1.82 2 4 -14 141.42 9.33 2 -4 14 140.20 8.30 -2 -4 -14 135.65 8.32 -2 -4 -14 131.37 8.15 2 4 -14 136.71 8.00 2 -4 -14 147.87 8.08 2 4 14 148.58 8.18 -2 4 -14 151.03 8.50 -2 4 -14 150.31 9.57 -2 4 -14 147.19 8.22 -2 -4 14 144.48 8.10 3 -4 14 31.61 2.55 -3 -4 -14 31.59 2.57 3 4 -14 31.82 2.29 3 4 -14 32.98 2.65 -3 -4 -14 31.76 2.62 3 -4 -14 34.47 2.20 -3 4 -14 36.56 2.78 -3 4 -14 35.10 2.61 3 4 14 36.04 2.50 -3 -4 14 33.29 2.30 -3 4 -14 36.98 3.01 -4 -4 -14 111.32 6.59 -4 -4 -14 109.27 6.53 4 4 -14 108.95 6.08 4 -4 14 112.41 6.54 4 -4 -14 104.20 6.01 -4 4 -14 109.35 7.47 -4 4 -14 96.22 6.57 -4 4 -14 105.76 6.43 4 4 14 106.42 6.41 5 4 -14 6.26 0.87 5 -4 14 7.98 1.33 -5 -4 -14 4.93 1.25 -5 4 -14 4.17 1.14 -5 4 -14 2.84 1.09 5 4 14 3.59 1.01 5 -4 -14 4.65 0.59 -6 -4 -14 73.81 4.92 6 4 -14 71.23 4.24 6 -4 14 75.25 4.85 6 4 14 72.75 4.76 -6 4 -14 72.17 4.79 6 -4 -14 73.08 4.07 -6 4 -14 69.22 4.87 7 4 -14 6.23 0.90 -7 -4 -14 6.15 1.40 7 -4 14 7.27 1.49 -7 4 -14 5.01 1.49 7 4 14 6.61 1.39 -7 4 -14 7.15 1.55 8 -4 14 54.45 4.15 8 4 -14 57.79 3.42 -8 -4 -14 63.49 4.35 8 4 14 53.15 4.06 -8 4 -14 53.56 4.23 -8 4 -14 52.38 4.09 -9 -4 -14 9.46 1.88 9 4 -14 8.71 1.08 9 -4 14 8.13 1.74 9 4 14 11.05 1.82 -9 4 -14 8.32 1.75 -9 4 -14 7.73 1.76 10 -4 14 24.93 2.83 -10 -4 -14 28.61 2.96 -10 4 -14 34.43 3.21 10 4 14 33.89 3.07 -10 4 -14 31.61 3.29 11 4 -14 11.90 1.64 11 -4 14 11.52 2.13 -11 -4 -14 13.05 2.29 -11 4 -14 13.08 2.23 -11 4 -14 13.62 2.27 11 4 14 14.59 2.16 12 4 -14 16.84 1.99 -12 -4 -14 16.92 2.61 12 -4 14 18.73 2.67 12 4 14 17.38 2.58 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21.28 1.55 3 5 14 19.77 1.71 -4 -5 -14 6.41 1.28 4 5 -14 5.99 0.93 4 -5 14 6.26 1.21 4 -5 -14 5.27 0.69 -4 5 -14 4.77 1.20 -4 5 -14 5.41 1.24 -4 5 -14 5.71 1.20 4 5 14 6.55 1.09 -5 -5 -14 8.93 1.54 5 5 -14 8.92 1.11 5 -5 14 9.11 1.46 -5 5 -14 10.58 1.55 -5 5 -14 8.60 1.52 5 -5 -14 10.65 0.85 5 5 14 7.64 1.30 6 5 -14 19.60 1.64 -6 -5 -14 21.49 2.32 6 -5 14 23.91 2.23 6 -5 -14 19.56 1.26 -6 5 -14 21.14 2.37 6 5 14 18.05 1.98 -6 5 -14 19.27 2.19 -7 -5 -14 2.85 1.18 7 -5 14 2.46 1.05 7 5 -14 3.50 0.80 -7 5 -14 1.46 1.09 -7 5 -14 0.57 1.15 7 5 14 1.83 1.05 8 -5 14 23.67 2.40 8 5 -14 18.33 1.74 -8 -5 -14 23.84 2.67 -8 5 -14 25.57 2.57 -8 5 -14 24.75 2.71 8 5 14 28.92 2.42 9 5 -14 10.36 1.24 9 -5 14 8.53 1.75 -9 -5 -14 9.01 1.78 -9 5 -14 7.62 1.72 9 5 14 8.70 1.69 -9 5 -14 7.91 1.71 10 -5 14 49.11 4.01 -10 -5 -14 48.20 3.94 10 5 -14 43.56 3.12 10 5 14 48.57 3.92 -10 5 -14 52.63 4.02 -10 5 -14 49.89 3.96 11 -5 14 4.88 1.68 -11 -5 -14 2.37 1.57 11 5 -14 2.68 1.18 -11 5 -14 3.82 1.59 11 5 14 4.03 1.55 -11 5 -14 2.99 1.62 12 5 -14 40.07 3.07 12 -5 14 40.31 3.76 -12 -5 -14 34.85 3.53 -12 5 -14 33.67 3.60 -12 5 -14 36.09 3.62 12 5 14 36.33 3.59 13 -5 14 4.88 1.90 13 5 -14 3.36 1.32 -13 -5 -14 7.16 2.01 13 5 14 4.91 1.71 -13 5 -14 3.94 1.92 -13 5 -14 3.38 1.81 14 5 -14 16.14 2.33 -14 -5 -14 19.80 3.07 14 -5 14 18.45 2.96 14 5 14 22.86 3.11 -14 5 -14 22.56 3.17 15 5 -14 2.48 1.41 15 -5 14 2.53 1.85 -15 -5 -14 0.02 1.72 15 5 14 0.23 1.76 -15 5 -14 2.04 2.25 0 -6 -14 79.10 4.64 0 -6 14 76.74 4.70 0 6 -14 75.15 4.64 0 6 -14 71.87 5.35 1 6 -14 15.30 1.56 -1 -6 -14 16.83 1.60 1 -6 14 15.34 1.57 1 6 -14 14.99 1.69 1 6 14 14.00 1.26 1 -6 -14 13.40 1.38 -1 6 -14 11.77 1.64 -1 6 -14 12.43 1.55 -1 6 -14 12.93 1.69 -1 -6 14 13.68 1.48 2 6 -14 53.27 3.36 2 -6 14 52.83 3.51 -2 -6 -14 54.05 3.51 2 6 -14 54.34 3.87 -2 6 -14 48.91 3.63 2 6 14 50.70 3.28 -2 6 -14 49.22 3.46 -2 -6 14 47.91 3.30 2 -6 -14 51.27 3.18 -2 6 -14 50.11 3.97 3 6 -14 20.78 1.94 3 6 -14 18.59 1.69 -3 -6 -14 22.23 2.00 3 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14.76 2.17 -10 6 -14 14.03 2.26 11 -6 14 35.50 3.45 11 6 -14 33.23 2.98 -11 -6 -14 28.36 3.35 -11 6 -14 36.69 3.42 -11 6 -14 35.41 3.47 11 6 14 33.67 3.33 12 6 -14 4.79 1.41 12 -6 14 5.21 1.85 -12 -6 -14 5.93 1.94 -12 6 -14 5.55 1.84 -12 6 -14 6.73 1.90 12 6 14 3.98 1.71 -13 -6 -14 27.73 3.39 13 6 -14 24.99 2.61 13 -6 14 27.47 3.33 -13 6 -14 24.79 3.24 -13 6 -14 20.93 3.01 13 6 14 23.04 3.10 14 6 -14 2.86 1.35 14 -6 14 4.17 1.94 -14 -6 -14 0.69 1.79 -14 6 -14 3.19 1.93 14 6 14 3.00 1.86 0 7 -14 0.69 0.75 0 -7 14 1.41 0.76 0 7 -14 1.75 0.80 0 -7 -14 0.44 0.67 1 -7 14 168.62 10.57 1 7 -14 172.47 12.02 1 7 -14 172.33 10.32 -1 -7 -14 181.96 10.53 -1 7 -14 203.63 12.20 -1 7 -14 192.75 10.47 -1 -7 14 196.23 10.59 1 -7 -14 195.75 10.41 2 7 -14 35.61 2.48 2 7 -14 33.89 2.77 2 -7 14 36.59 2.63 -2 -7 -14 33.68 2.57 -2 -7 14 32.15 2.40 2 -7 -14 29.82 2.19 2 7 14 31.16 2.29 -2 7 -14 32.81 2.55 -2 7 -14 29.27 2.83 -3 -7 -14 111.42 6.63 3 -7 14 111.17 6.66 3 7 -14 108.31 6.33 3 7 -14 103.08 7.33 3 7 14 110.28 6.44 -3 7 -14 110.30 6.58 -3 7 -14 108.51 6.79 -3 -7 14 107.99 6.38 3 -7 -14 108.42 6.17 -4 -7 -14 5.34 1.24 4 7 -14 5.28 1.00 4 7 -14 7.64 1.08 4 -7 14 5.74 1.25 4 7 14 2.97 0.90 4 -7 -14 3.12 0.59 -4 7 -14 3.18 1.23 -4 7 -14 2.99 1.10 5 -7 14 75.70 5.33 5 7 -14 78.35 4.97 -5 -7 -14 77.62 5.42 5 7 14 87.84 5.33 -5 7 -14 86.08 5.41 -5 7 -14 91.31 5.60 5 -7 -14 87.73 4.72 -6 -7 -14 3.87 1.33 6 -7 14 3.44 1.24 6 7 -14 3.47 0.92 -6 7 -14 6.83 1.43 6 -7 -14 6.13 0.58 6 7 14 8.12 1.33 -6 7 -14 5.47 1.47 -7 -7 -14 89.74 6.04 7 7 -14 94.28 5.39 7 -7 14 91.05 5.98 7 7 14 85.83 5.80 -7 7 -14 99.89 5.98 -7 7 -14 84.25 5.97 8 -7 14 4.30 1.33 -8 -7 -14 4.16 1.49 8 7 -14 4.12 1.02 -8 7 -14 2.99 1.43 -8 7 -14 3.92 1.56 8 7 14 3.52 1.26 9 -7 14 54.15 4.17 -9 -7 -14 55.05 4.18 9 7 -14 54.89 3.49 9 7 14 52.58 4.05 -9 7 -14 45.33 4.12 -9 7 -14 49.99 4.05 10 -7 14 4.21 1.53 10 7 -14 3.74 1.10 -10 -7 -14 4.15 1.66 -10 7 -14 3.62 1.44 10 7 14 4.61 1.57 -10 7 -14 3.20 1.54 -11 -7 -14 26.39 3.15 11 7 -14 23.43 2.55 11 -7 14 26.79 3.02 11 7 14 24.87 2.88 -11 7 -14 21.14 2.85 -11 7 -14 24.25 2.96 12 7 -14 2.76 1.35 -12 -7 -14 0.86 1.43 12 -7 14 2.27 1.61 -12 7 -14 0.71 1.50 12 7 14 4.18 1.70 -12 7 -14 2.50 1.67 -13 -7 -14 9.97 2.33 13 -7 14 6.49 2.05 13 7 -14 10.01 1.88 -13 7 -14 8.97 2.14 -13 7 -14 6.40 2.28 13 7 14 9.39 2.16 14 7 -14 2.16 1.27 14 -7 14 1.61 1.60 -14 -7 -14 2.40 1.95 -14 7 -14 2.10 1.83 14 7 14 1.42 1.71 0 8 -14 26.54 2.49 0 8 -14 25.27 2.16 0 -8 -14 27.98 2.08 0 -8 14 24.60 2.21 1 8 -14 7.18 1.22 1 -8 14 8.04 1.24 1 8 -14 8.97 1.24 -1 -8 -14 6.74 1.13 -1 8 -14 3.75 1.06 -1 -8 14 4.17 1.00 -1 8 -14 2.44 1.06 1 -8 -14 4.38 0.86 2 8 -14 67.70 4.81 2 8 -14 64.24 4.16 2 -8 14 65.95 4.34 -2 -8 -14 63.96 4.24 -2 -8 14 63.18 4.18 2 -8 -14 68.05 3.97 -2 8 -14 63.24 4.26 3 -8 14 7.29 1.34 3 8 -14 8.28 1.18 -3 -8 -14 7.03 1.27 3 8 -14 8.04 1.24 3 -8 14 7.96 1.29 -3 8 -14 2.95 1.08 -3 -8 14 3.14 0.92 4 8 -14 37.46 2.60 4 8 -14 38.42 3.02 -4 -8 -14 36.90 2.86 4 -8 14 39.85 3.16 4 -8 14 36.34 2.83 4 -8 -14 32.08 2.21 4 8 14 31.34 2.61 -4 8 -14 31.00 2.77 5 -8 14 19.06 2.23 5 -8 14 19.88 2.19 5 8 -14 17.37 1.65 -5 -8 -14 15.98 2.06 -5 8 -14 16.52 2.07 5 -8 -14 18.24 1.29 -5 8 -14 19.77 2.31 5 8 14 18.70 1.86 6 -8 14 31.91 2.94 -6 -8 -14 34.04 3.03 6 8 -14 32.35 2.51 -6 8 -14 35.03 3.10 -6 8 -14 35.55 2.97 6 -8 -14 34.41 2.03 6 8 14 34.00 2.77 -7 -8 -14 28.45 2.86 7 -8 14 28.14 2.64 7 8 -14 28.12 2.24 -7 8 -14 26.51 2.71 7 8 14 28.11 2.55 -7 8 -14 28.03 2.75 8 -8 14 40.23 3.42 -8 -8 -14 40.83 3.42 8 8 -14 39.39 2.81 -8 8 -14 37.15 3.48 8 8 14 37.10 3.20 -8 8 -14 37.63 3.44 9 8 -14 24.99 2.10 9 -8 14 22.84 2.61 -9 -8 -14 22.48 2.78 -9 8 -14 17.66 2.48 -9 8 -14 18.86 2.53 9 8 14 19.94 2.43 -10 -8 -14 17.72 2.55 10 -8 14 15.90 2.29 10 8 -14 16.09 1.82 10 8 14 16.93 2.34 -10 8 -14 16.44 2.46 -10 8 -14 14.14 2.37 11 -8 14 18.84 2.53 11 8 -14 15.15 2.22 -11 -8 -14 17.65 2.68 -11 8 -14 19.87 2.70 -11 8 -14 15.48 2.48 11 8 14 17.10 2.43 12 -8 14 3.90 1.79 -12 -8 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17.61 1.31 -5 9 -14 18.04 2.25 -6 -9 -14 27.15 2.66 6 9 -14 27.82 2.20 6 -9 14 28.63 2.68 -6 9 -14 24.97 2.54 6 9 14 26.59 2.38 6 -9 -14 22.66 1.61 -7 -9 -14 1.18 1.12 7 9 -14 1.11 0.92 7 -9 14 1.10 1.23 7 -9 -14 1.92 0.40 -7 9 -14 1.40 1.23 7 9 14 1.40 1.06 8 9 -14 22.83 2.13 8 -9 14 24.41 2.57 -8 -9 -14 21.92 2.77 -8 9 -14 28.16 2.75 8 9 14 23.87 2.53 9 -9 14 0.69 1.27 9 9 -14 1.48 1.01 -9 -9 -14 -1.03 1.16 9 9 14 1.35 1.25 -9 9 -14 0.23 1.49 10 -9 14 26.50 3.07 -10 -9 -14 28.28 3.21 10 9 -14 27.82 2.35 10 9 14 26.17 2.96 -10 9 -14 23.77 2.96 -11 -9 -14 3.05 1.76 11 9 -14 3.38 1.44 11 -9 14 2.09 1.41 -11 9 -14 0.97 1.51 11 9 14 1.43 1.47 12 -9 14 21.32 2.88 12 9 -14 17.59 2.54 -12 -9 -14 21.20 3.02 12 9 14 21.73 2.84 -12 9 -14 21.49 3.11 13 -9 14 1.16 1.63 13 9 -14 -1.73 1.22 -13 -9 -14 0.30 1.53 13 9 14 0.00 1.49 -13 9 -14 -0.04 1.60 -14 -9 -14 31.40 3.68 14 -9 14 28.28 3.60 14 9 -14 28.88 3.30 14 9 14 28.95 3.55 -14 9 -14 27.84 3.77 0 -10 14 69.53 4.52 0 -10 14 66.47 4.82 0 -10 -14 69.40 4.31 0 10 -14 67.98 4.43 1 -10 14 3.39 0.98 1 10 -14 2.83 1.01 1 -10 14 4.25 1.13 -1 -10 -14 3.30 0.97 -1 -10 14 5.14 0.94 1 -10 -14 5.17 0.96 -1 -10 14 7.05 1.24 -1 10 -14 6.45 1.39 2 10 -14 85.37 5.18 -2 -10 -14 85.23 5.27 2 -10 14 82.58 5.91 2 -10 14 82.33 5.39 -2 10 -14 86.26 5.33 -2 -10 14 80.21 5.28 2 -10 -14 83.06 4.98 3 -10 14 0.72 0.83 3 10 -14 0.96 0.80 3 -10 14 1.20 0.99 -3 -10 -14 0.89 0.89 -3 10 -14 1.93 1.04 -3 -10 14 -0.03 0.79 3 -10 -14 0.37 0.59 4 10 -14 68.11 4.52 4 -10 14 65.76 5.26 -4 -10 -14 71.87 4.76 4 -10 14 69.46 4.81 -4 10 -14 73.26 4.81 4 -10 -14 75.52 4.21 5 10 -14 1.83 0.91 -5 -10 -14 2.32 1.22 5 -10 14 4.97 1.37 -5 10 -14 5.66 1.41 5 10 14 4.68 1.15 5 -10 -14 4.66 0.71 6 -10 14 81.69 5.40 -6 -10 -14 70.24 5.24 6 10 -14 80.03 4.97 -6 10 -14 80.78 5.37 6 -10 -14 79.68 4.54 6 10 14 84.33 5.27 7 -10 14 9.47 1.79 -7 -10 -14 6.72 1.71 7 10 -14 7.62 1.38 -7 10 -14 8.58 1.76 7 -10 -14 9.12 0.85 7 10 14 10.18 1.66 8 -10 14 24.96 2.82 8 10 -14 21.69 2.19 -8 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8.22 1.27 -8 -8 -15 8.02 1.85 -8 8 -15 5.69 1.64 -8 8 -15 7.87 1.83 8 8 15 9.44 1.69 9 8 -15 12.34 1.61 -9 -8 -15 13.80 2.30 9 -8 15 13.05 2.15 -9 8 -15 14.41 2.22 9 8 15 14.19 2.09 -9 8 -15 15.50 2.29 10 8 -15 13.52 1.74 -10 -8 -15 15.43 2.41 10 -8 15 17.95 2.49 10 8 15 19.32 2.46 -10 8 -15 17.40 2.57 -10 8 -15 18.15 2.55 11 8 -15 9.04 1.74 11 -8 15 7.28 1.98 -11 -8 -15 9.38 2.20 -11 8 -15 5.29 1.83 -11 8 -15 5.59 1.87 11 8 15 4.49 1.69 12 -8 15 14.03 2.38 12 8 -15 15.08 2.21 -12 -8 -15 14.94 2.66 12 8 15 10.75 2.19 -12 8 -15 10.11 2.28 -12 8 -15 12.68 2.42 -13 -8 -15 10.34 2.42 13 8 -15 6.11 1.74 13 -8 15 9.72 2.25 13 8 15 10.13 2.27 -13 8 -15 11.80 2.57 -13 8 -15 11.16 2.40 0 9 -15 124.83 7.50 0 -9 -15 130.54 7.47 0 -9 15 126.97 7.62 1 -9 15 1.23 0.88 -1 -9 -15 1.12 0.86 1 9 -15 0.54 0.81 1 -9 -15 1.54 0.74 -1 9 -15 2.21 0.99 -1 -9 15 1.82 0.88 -2 -9 -15 110.18 6.52 2 9 -15 107.67 6.43 2 -9 15 112.24 6.66 2 -9 -15 104.55 6.22 -2 -9 15 102.22 6.46 -2 9 -15 107.10 6.55 3 9 -15 5.34 1.18 3 -9 15 5.21 1.30 -3 -9 -15 4.59 1.19 -3 9 -15 2.52 1.12 3 -9 -15 3.59 0.75 4 -9 15 84.30 5.54 4 9 -15 78.11 5.17 -4 -9 -15 81.78 5.47 4 -9 15 83.68 6.10 4 -9 -15 88.43 4.92 -4 9 -15 90.58 5.56 5 -9 15 2.72 1.21 5 -9 15 2.85 1.15 5 9 -15 2.77 0.98 -5 -9 -15 2.14 1.11 -5 9 -15 3.29 1.26 5 9 15 3.07 1.16 5 -9 -15 3.20 0.60 -6 -9 -15 91.05 6.19 6 -9 15 88.18 6.14 6 9 -15 95.80 5.77 6 -9 -15 94.85 5.35 -6 9 -15 103.39 6.26 6 9 15 99.21 6.06 7 9 -15 3.65 1.07 7 -9 15 4.53 1.37 -7 -9 -15 4.59 1.54 7 9 15 4.08 1.31 -7 9 -15 3.02 1.39 8 9 -15 32.56 2.55 -8 -9 -15 27.61 3.22 8 -9 15 35.34 3.25 -8 9 -15 34.85 3.37 8 9 15 33.25 2.97 9 9 -15 0.98 0.93 9 -9 15 2.69 1.44 -9 -9 -15 1.37 1.56 -9 9 -15 0.17 1.30 9 9 15 0.72 1.17 10 -9 15 20.47 2.62 -10 -9 -15 22.92 2.84 10 9 -15 23.26 2.16 -10 9 -15 15.00 2.53 10 9 15 14.37 2.34 -11 -9 -15 2.17 1.74 11 -9 15 1.16 1.54 11 9 15 -0.55 1.30 -11 9 -15 3.09 1.70 12 -9 15 13.63 2.44 12 9 -15 13.52 2.18 -12 -9 -15 16.69 2.62 -12 9 -15 13.51 2.71 12 9 15 7.33 2.07 13 9 -15 0.89 1.50 13 -9 15 0.05 1.64 -13 -9 -15 0.74 1.84 -13 9 -15 1.49 1.75 13 9 15 0.21 1.31 0 10 -15 2.70 1.05 0 -10 15 2.25 0.97 0 -10 -15 2.44 0.88 1 -10 15 35.96 2.97 1 10 -15 35.96 2.76 1 -10 15 40.08 2.91 -1 -10 -15 35.52 2.73 -1 -10 15 33.18 2.81 -1 10 -15 33.39 2.80 1 -10 -15 34.16 2.52 -2 -10 -15 2.19 1.05 2 -10 15 4.13 1.10 2 10 -15 3.60 1.15 2 -10 15 4.48 1.12 2 -10 -15 2.15 0.77 -2 10 -15 2.98 1.13 -2 -10 15 2.33 0.98 -3 -10 -15 35.21 2.88 3 -10 15 34.42 2.93 3 -10 15 36.45 3.15 3 10 -15 37.48 2.73 -3 10 -15 32.26 2.86 3 -10 -15 33.75 2.38 4 10 -15 11.04 1.46 -4 -10 -15 9.76 1.63 4 -10 15 9.80 1.65 4 -10 15 10.91 1.71 -4 10 -15 6.24 1.51 4 -10 -15 9.59 1.06 -5 -10 -15 19.34 2.29 5 -10 15 21.56 2.42 5 10 -15 20.75 2.01 -5 10 -15 18.88 2.33 5 -10 -15 19.18 1.51 6 10 -15 17.74 1.92 -6 -10 -15 17.76 2.28 6 -10 15 14.82 2.16 6 -10 -15 17.24 1.29 -6 10 -15 15.73 2.23 7 10 -15 14.69 1.81 7 -10 15 12.98 2.07 -7 -10 -15 14.95 2.17 -7 10 -15 17.17 2.46 7 10 15 19.63 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1.65 12 11 15 2.19 1.57 0 -12 15 1.07 0.99 0 -12 15 0.63 0.79 0 -12 -15 0.15 0.83 0 12 -15 1.16 1.01 1 12 -15 67.05 4.73 1 -12 15 68.88 4.89 -1 -12 -15 71.79 4.72 1 -12 15 72.03 5.28 -1 -12 15 77.91 4.96 1 -12 -15 77.60 4.61 -1 -12 15 70.71 5.10 -1 12 -15 74.49 4.87 2 -12 15 0.98 0.91 2 -12 15 -0.03 1.00 2 12 -15 1.15 1.13 -2 -12 -15 1.05 0.96 -2 -12 15 0.28 0.93 -2 12 -15 -0.11 0.99 2 -12 -15 0.63 0.76 3 12 -15 90.95 5.62 -3 -12 -15 90.03 5.67 3 -12 15 88.52 6.40 3 -12 15 95.20 5.82 -3 12 -15 83.28 5.76 3 -12 -15 80.52 5.20 4 -12 15 1.37 1.20 -4 -12 -15 0.97 1.13 4 12 -15 0.55 0.91 4 -12 -15 0.76 0.67 -4 12 -15 1.51 1.18 5 12 -15 67.87 4.41 -5 -12 -15 71.70 4.70 5 -12 15 70.30 4.71 5 -12 -15 59.36 3.89 -5 12 -15 56.78 4.57 6 -12 15 6.35 1.60 -6 -12 -15 4.26 1.49 6 12 -15 6.46 1.40 6 -12 -15 5.57 0.84 -6 12 -15 3.01 1.46 7 -12 15 33.49 3.20 7 12 -15 37.85 2.94 -7 -12 -15 39.70 3.48 -7 12 -15 28.13 3.32 -8 -12 -15 4.83 1.72 8 12 -15 5.10 1.40 8 -12 15 5.52 1.77 -8 12 -15 6.93 2.07 9 -12 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2.03 0 1 -24 12.63 1.94 0 -1 -24 13.50 1.92 1 1 -24 1.70 1.29 1 1 -24 1.01 1.34 -1 -1 -24 1.11 1.36 -1 -1 -24 1.50 1.28 -1 1 -24 1.08 1.32 1 -1 -24 -0.18 1.23 -1 1 -24 1.73 1.39 2 1 -24 15.90 2.17 -2 -1 -24 15.68 2.25 -2 -1 -24 13.65 2.30 -2 1 -24 19.40 2.41 2 -1 -24 18.66 2.20 -2 1 -24 15.02 2.32 -3 -1 -24 0.89 1.52 -3 -1 -24 0.88 1.46 3 -1 -24 0.69 1.03 -3 1 -24 0.80 1.45 -3 1 -24 0.99 1.53 -4 -1 -24 5.09 1.74 -4 -1 -24 3.36 1.76 -4 1 -24 4.83 1.87 -4 1 -24 8.68 2.08 -5 -1 -24 3.40 1.72 -5 -1 -24 1.16 1.72 -5 1 -24 2.25 1.77 -5 1 -24 5.22 1.85 -6 -1 -24 15.65 2.70 -6 -1 -24 12.28 2.45 -6 1 -24 10.47 2.26 -6 1 -24 12.70 2.42 -7 -1 -24 2.08 1.78 -7 -1 -24 2.88 1.86 -7 1 -24 1.92 1.82 -7 1 -24 2.30 1.78 -8 -1 -24 4.33 2.10 -8 1 -24 6.98 2.47 -8 1 -24 7.21 2.23 0 -2 -24 0.09 1.23 0 2 -24 -0.37 1.15 0 2 -24 -0.30 1.35 1 2 -24 1.79 1.42 -1 -2 -24 -0.10 1.24 -1 -2 -24 0.36 1.21 1 2 -24 -0.12 1.20 -1 2 -24 1.25 1.32 1 -2 -24 3.09 1.28 -1 2 -24 0.96 1.38 -2 -2 -24 0.54 1.32 -2 -2 -24 0.55 1.36 -2 2 -24 0.94 1.46 2 -2 -24 -0.16 0.99 -2 2 -24 1.95 1.42 -3 -2 -24 4.43 1.73 -3 -2 -24 5.06 1.64 -3 2 -24 4.45 1.73 -3 2 -24 4.46 1.74 3 -2 -24 3.38 1.28 -4 -2 -24 4.79 1.80 -4 -2 -24 1.16 1.65 -4 2 -24 5.16 1.84 -4 2 -24 2.74 1.48 4 -2 -24 2.87 1.27 -5 -2 -24 4.66 1.91 -5 -2 -24 5.51 1.92 -5 2 -24 4.21 1.91 -5 2 -24 2.72 1.57 -6 -2 -24 2.01 1.76 -6 2 -24 2.03 1.92 -6 2 -24 3.16 1.91 -7 -2 -24 1.11 1.82 -7 2 -24 0.43 1.78 -7 2 -24 0.51 1.93 -8 -2 -24 10.55 2.48 -8 2 -24 8.52 2.35 -8 2 -24 10.18 2.55 0 3 -24 16.44 2.46 0 3 -24 18.99 2.30 0 -3 -24 15.93 2.18 -1 -3 -24 0.05 1.22 1 3 -24 -0.49 1.22 -1 3 -24 1.86 1.50 1 -3 -24 1.06 1.20 -1 3 -24 1.73 1.40 -2 -3 -24 18.85 2.47 -2 3 -24 18.87 2.56 -2 3 -24 16.10 2.26 2 -3 -24 17.88 2.10 -3 -3 -24 4.56 1.61 -3 3 -24 1.49 1.36 -3 3 -24 3.01 1.70 3 -3 -24 5.90 1.40 -4 -3 -24 25.62 3.05 4 -3 -24 26.59 2.48 -4 3 -24 27.33 3.26 -4 3 -24 25.40 2.99 -5 -3 -24 2.28 1.70 -5 3 -24 1.73 1.54 -5 3 -24 1.75 1.80 -6 -3 -24 13.90 2.64 -6 3 -24 19.30 2.91 -6 3 -24 20.85 2.95 -7 -3 -24 5.73 2.02 -7 3 -24 1.17 1.73 -7 3 -24 3.09 2.01 -8 -3 -24 8.25 2.40 -8 3 -24 10.60 2.54 -8 3 -24 9.05 2.37 0 4 -24 0.66 1.23 0 -4 -24 2.85 1.32 -1 -4 -24 22.65 2.64 1 4 -24 25.35 2.55 -1 4 -24 27.28 3.02 1 -4 -24 23.12 2.51 -1 4 -24 21.55 2.68 2 4 -24 2.69 1.25 -2 -4 -24 -0.35 1.37 -2 4 -24 0.73 1.48 2 -4 -24 2.41 1.16 -2 4 -24 3.18 1.60 -3 -4 -24 27.38 3.04 -3 4 -24 25.70 3.22 3 -4 -24 27.75 2.60 -3 4 -24 23.99 3.02 -4 -4 -24 2.48 1.70 -4 4 -24 3.93 1.80 -4 4 -24 1.95 1.51 4 -4 -24 4.22 1.21 -5 -4 -24 32.44 3.57 -5 4 -24 32.01 3.61 -5 4 -24 34.06 3.79 -6 -4 -24 -0.64 1.63 -6 4 -24 -1.13 1.43 -6 4 -24 0.98 1.77 -7 -4 -24 11.41 2.56 -7 4 -24 16.10 2.69 -7 4 -24 15.79 2.80 0 -5 -24 1.33 1.24 0 5 -24 2.13 1.44 1 5 -24 0.06 1.22 -1 -5 -24 -1.45 1.23 1 -5 -24 0.15 1.03 -1 5 -24 0.26 1.35 2 5 -24 -0.16 1.27 -2 -5 -24 -0.20 1.28 -2 5 -24 1.04 1.54 -2 5 -24 1.02 1.51 2 -5 -24 2.31 1.21 -3 -5 -24 1.49 1.58 -3 5 -24 2.03 1.70 3 -5 -24 1.57 1.15 -3 5 -24 4.00 1.61 -4 -5 -24 3.09 1.68 4 -5 -24 4.22 1.16 -4 5 -24 4.44 1.87 -4 5 -24 1.06 1.73 -5 -5 -24 1.88 1.63 -5 5 -24 5.85 2.13 -5 5 -24 4.15 1.76 -6 -5 -24 4.75 1.88 -6 5 -24 5.27 1.89 -6 5 -24 6.69 2.20 -7 -5 -24 11.95 2.49 -7 5 -24 8.86 2.30 -7 5 -24 13.74 2.68 0 6 -24 6.06 1.67 0 -6 -24 6.06 1.56 -1 -6 -24 7.16 1.74 1 6 -24 7.93 1.77 -1 6 -24 10.77 2.05 1 -6 -24 11.37 1.75 -2 -6 -24 2.52 1.49 2 6 -24 2.59 1.36 2 -6 -24 2.20 1.24 -2 6 -24 2.00 1.61 -3 -6 -24 3.14 1.68 -3 6 -24 5.46 1.87 3 -6 -24 5.07 1.34 -4 -6 -24 2.65 1.54 -4 6 -24 1.95 1.59 -4 6 -24 1.68 1.78 4 -6 -24 1.20 0.97 -5 -6 -24 4.57 1.86 -5 6 -24 5.30 2.08 -5 6 -24 3.88 1.80 -6 -6 -24 7.77 2.12 -6 6 -24 7.86 2.13 -6 6 -24 10.48 2.44 -7 -6 -24 12.99 2.57 -7 6 -24 9.68 2.50 -7 6 -24 10.52 2.41 0 7 -24 31.67 3.22 0 -7 -24 32.62 3.08 -1 -7 -24 1.22 1.35 1 7 -24 1.51 1.40 -1 7 -24 2.99 1.60 1 -7 -24 1.07 1.19 2 7 -24 25.49 2.87 -2 -7 -24 27.34 3.05 -2 7 -24 31.37 3.37 2 -7 -24 34.39 2.86 3 7 -24 2.25 1.33 -3 -7 -24 2.17 1.62 -3 7 -24 0.48 1.40 3 -7 -24 2.41 1.12 -4 -7 -24 31.34 3.35 -4 7 -24 26.59 3.19 -5 -7 -24 1.89 1.65 -5 7 -24 5.44 1.94 -6 -7 -24 19.07 2.92 -6 7 -24 19.41 2.89 0 -8 -24 -0.04 1.17 0 8 -24 0.35 1.40 1 8 -24 11.79 2.10 -1 -8 -24 9.25 1.86 1 -8 -24 13.25 1.87 -1 8 -24 10.48 2.23 -2 -8 -24 1.78 1.48 2 8 -24 0.69 1.38 2 -8 -24 0.07 1.17 -2 8 -24 0.30 1.65 -3 -8 -24 12.72 2.25 3 8 -24 13.69 2.06 3 -8 -24 13.53 1.74 -3 8 -24 10.65 2.36 -4 -8 -24 2.36 1.70 -4 8 -24 1.94 1.81 -5 -8 -24 14.67 2.55 -5 8 -24 16.43 2.78 -6 -8 -24 1.78 1.86 -6 8 -24 2.56 2.10 0 9 -24 1.64 1.59 0 -9 -24 0.38 1.09 -1 -9 -24 1.73 1.37 1 9 -24 0.83 1.50 1 -9 -24 2.30 1.27 -1 9 -24 2.34 1.47 2 9 -24 2.26 1.50 -2 -9 -24 2.19 1.56 2 -9 -24 2.72 1.31 -2 9 -24 2.10 1.74 3 9 -24 2.37 1.48 -3 -9 -24 3.00 1.67 3 -9 -24 1.25 1.08 -3 9 -24 1.40 1.51 -4 -9 -24 3.57 1.78 -4 9 -24 1.96 1.64 -5 -9 -24 2.44 1.75 -5 9 -24 2.98 1.81 0 10 -24 5.54 1.90 0 -10 -24 6.07 1.51 1 10 -24 23.01 2.86 -1 -10 -24 23.25 2.72 1 -10 -24 23.81 2.60 -1 10 -24 24.41 3.09 -2 -10 -24 9.21 1.95 2 10 -24 4.26 1.73 -2 10 -24 4.99 2.00 2 -10 -24 5.09 1.43 3 10 -24 21.49 2.62 -3 -10 -24 19.16 2.65 -3 10 -24 18.99 2.96 3 -10 -24 19.88 2.15 -4 -10 -24 -0.37 1.63 4 10 -24 1.42 1.53 -4 10 -24 2.14 1.70 0 -11 -24 40.67 3.42 0 11 -24 36.12 3.74 1 11 -24 0.37 1.38 -1 -11 -24 1.08 1.48 -1 11 -24 2.78 1.84 1 -11 -24 -0.10 1.31 2 11 -24 26.08 3.07 -2 -11 -24 29.41 3.16 -2 11 -24 25.45 3.33 2 -11 -24 29.18 2.81 -3 -11 -24 0.85 1.52 3 11 -24 -1.50 1.36 -3 11 -24 0.16 1.81 0 0 -25 1.98 1.39 -1 0 -25 3.76 1.49 -1 0 -25 0.73 1.50 1 0 -25 2.45 1.39 -2 0 -25 2.17 1.49 2 0 -25 1.38 1.30 -2 0 -25 0.82 1.41 -3 0 -25 0.80 1.58 -3 0 -25 1.51 1.56 -4 0 -25 2.61 1.75 -4 0 -25 2.28 1.74 -5 0 -25 6.52 2.09 -5 0 -25 5.60 2.08 -6 0 -25 0.43 1.72 -6 0 -25 3.35 2.01 0 1 -25 2.64 1.47 0 -1 -25 2.08 1.50 0 1 -25 2.86 1.60 -1 -1 -25 20.54 2.51 1 1 -25 15.02 2.25 -1 -1 -25 14.04 2.26 -1 1 -25 16.67 2.37 1 -1 -25 14.39 2.07 -1 1 -25 13.42 2.30 -2 -1 -25 5.54 1.83 -2 -1 -25 6.20 1.79 -2 1 -25 7.58 1.92 -2 1 -25 3.85 1.67 2 -1 -25 6.40 1.46 -3 -1 -25 13.09 2.22 -3 -1 -25 14.88 2.37 -3 1 -25 8.41 2.09 3 -1 -25 13.30 1.92 -3 1 -25 11.13 2.25 -4 -1 -25 4.53 1.84 -4 -1 -25 5.83 1.76 -4 1 -25 3.64 1.88 -4 1 -25 6.83 2.01 -5 -1 -25 14.62 2.47 -5 -1 -25 16.14 2.71 -5 1 -25 14.13 2.61 -5 1 -25 12.99 2.40 -6 -1 -25 2.43 1.88 -6 -1 -25 2.71 1.75 -6 1 -25 3.16 1.91 -6 1 -25 1.76 1.92 0 2 -25 25.01 2.71 0 -2 -25 23.83 2.69 0 2 -25 20.94 2.78 -1 -2 -25 8.66 1.78 -1 -2 -25 13.06 2.01 -1 2 -25 6.94 1.76 1 -2 -25 5.32 1.61 -1 2 -25 7.61 2.00 -2 -2 -25 35.89 3.38 -2 -2 -25 35.49 3.24 -2 2 -25 33.57 3.37 2 -2 -25 31.55 2.93 -2 2 -25 28.15 3.22 -3 -2 -25 1.40 1.52 -3 -2 -25 1.99 1.66 -3 2 -25 6.43 1.96 3 -2 -25 6.37 1.54 -3 2 -25 7.28 1.92 -4 -2 -25 10.90 2.20 -4 2 -25 8.92 2.18 -4 2 -25 14.37 2.50 -5 -2 -25 3.84 1.84 -5 2 -25 3.66 1.77 -5 2 -25 6.99 2.13 -6 -2 -25 23.46 3.19 -6 2 -25 23.85 3.14 -6 2 -25 21.73 3.18 0 3 -25 4.53 1.54 0 -3 -25 1.58 1.37 0 3 -25 2.99 1.61 -1 -3 -25 5.34 1.71 1 -3 -25 5.17 1.52 -1 3 -25 6.19 1.87 -1 3 -25 5.79 1.75 -2 -3 -25 3.05 1.67 -2 3 -25 4.11 1.89 -2 3 -25 3.93 1.71 2 -3 -25 2.80 1.21 -3 -3 -25 4.37 1.67 3 -3 -25 3.71 1.32 -3 3 -25 2.48 1.74 -3 3 -25 3.19 1.75 -4 -3 -25 1.26 1.67 -4 3 -25 0.66 1.63 -4 3 -25 -0.08 1.39 4 -3 -25 -0.91 1.00 -5 -3 -25 4.59 1.89 -5 3 -25 7.28 1.98 -5 3 -25 6.94 2.14 -6 -3 -25 4.98 2.00 -6 3 -25 3.75 2.11 -6 3 -25 4.35 2.13 0 -4 -25 2.72 1.44 0 4 -25 2.61 1.48 -1 -4 -25 1.59 1.46 1 4 -25 -0.29 1.21 -1 4 -25 2.02 1.52 1 -4 -25 1.85 1.12 -2 -4 -25 1.20 1.47 2 -4 -25 4.43 1.39 -2 4 -25 3.24 1.71 -2 4 -25 2.62 1.67 -3 -4 -25 4.37 1.70 -3 4 -25 3.40 1.84 -3 4 -25 3.85 1.79 3 -4 -25 2.51 1.32 -4 -4 -25 5.05 1.81 -4 4 -25 4.89 1.96 4 -4 -25 5.39 1.29 -4 4 -25 4.67 2.02 -5 -4 -25 8.75 2.15 -5 4 -25 5.37 2.13 -5 4 -25 7.89 2.25 -6 -4 -25 0.56 1.78 -6 4 -25 0.57 1.88 -6 4 -25 0.81 1.65 0 -5 -25 4.90 1.57 0 5 -25 3.93 1.57 1 5 -25 13.46 2.09 -1 -5 -25 10.87 2.06 -1 5 -25 11.42 2.13 1 -5 -25 12.36 1.84 -2 -5 -25 6.18 1.84 -2 5 -25 3.45 1.81 2 -5 -25 4.13 1.44 -3 -5 -25 26.42 3.12 3 -5 -25 27.91 2.64 -3 5 -25 27.01 3.39 -3 5 -25 28.97 3.36 -4 -5 -25 7.65 2.04 -4 5 -25 10.28 2.33 -4 5 -25 7.61 2.24 -5 -5 -25 18.44 2.83 -5 5 -25 18.85 2.97 -5 5 -25 14.31 2.53 0 6 -25 11.19 2.10 0 -6 -25 11.08 1.94 1 6 -25 0.37 1.47 -1 -6 -25 -0.70 1.24 1 -6 -25 -0.13 1.09 -1 6 -25 1.28 1.53 -2 -6 -25 15.23 2.34 2 -6 -25 12.94 1.97 -2 6 -25 16.91 2.55 -3 -6 -25 3.97 1.71 -3 6 -25 4.89 1.76 3 -6 -25 3.86 1.28 -4 -6 -25 22.19 2.90 -4 6 -25 19.38 2.95 -5 -6 -25 4.34 1.90 -5 6 -25 4.59 1.85 -5 6 -25 7.13 2.30 0 -7 -25 -1.32 1.07 0 7 -25 0.73 1.27 1 7 -25 1.69 1.47 -1 -7 -25 0.36 1.28 -1 7 -25 0.69 1.54 1 -7 -25 0.87 1.27 -2 -7 -25 0.42 1.42 2 7 -25 -0.13 1.35 2 -7 -25 1.45 1.27 -2 7 -25 -0.67 1.61 -3 -7 -25 -1.21 1.46 3 -7 -25 1.79 1.10 -3 7 -25 0.49 1.42 -4 -7 -25 0.90 1.59 -4 7 -25 1.59 1.92 0 -8 -25 9.88 1.82 0 8 -25 15.01 2.37 1 8 -25 9.45 2.01 -1 -8 -25 8.52 1.88 1 -8 -25 6.69 1.68 -1 8 -25 7.28 1.88 2 8 -25 15.43 2.31 -2 -8 -25 14.01 2.38 2 -8 -25 15.21 2.02 -2 8 -25 11.40 2.43 -3 -8 -25 5.98 1.87 -3 8 -25 7.19 1.96 3 -8 -25 3.94 1.26 0 -9 -25 3.71 1.52 0 9 -25 5.38 1.86 -1 -9 -25 25.88 2.92 1 9 -25 25.24 3.02 1 -9 -25 25.40 2.74 -2 -9 -25 3.50 1.65 2 9 -25 2.87 1.61 -2 9 -25 1.15 1.55 2 -9 -25 1.95 1.29 0 0 -26 14.31 2.31 1 0 -26 23.65 2.79 -1 0 -26 25.51 2.95 2 0 -26 5.90 1.53 -2 0 -26 4.38 1.91 -2 0 -26 5.18 1.78 -3 0 -26 9.23 2.09 -3 0 -26 8.22 2.09 -4 0 -26 4.34 1.93 -4 0 -26 4.46 1.97 0 1 -26 4.97 1.72 0 -1 -26 5.58 1.69 -1 -1 -26 9.10 2.04 1 1 -26 6.83 1.81 -1 1 -26 10.27 2.00 1 -1 -26 9.70 1.91 -1 1 -26 10.34 2.17 -2 -1 -26 12.53 2.21 -2 -1 -26 11.59 2.20 -2 1 -26 13.19 2.36 -2 1 -26 13.00 2.34 2 -1 -26 10.80 1.91 -3 -1 -26 1.12 1.63 -3 -1 -26 -2.39 1.38 -3 1 -26 -1.35 1.50 -3 1 -26 2.55 1.72 -4 -1 -26 1.24 1.75 -4 -1 -26 1.14 1.72 -4 1 -26 4.35 1.97 -4 1 -26 5.51 2.01 0 -2 -26 0.83 1.35 0 2 -26 2.12 1.57 -1 -2 -26 -0.44 1.45 -1 2 -26 1.36 1.48 1 -2 -26 0.92 1.30 -1 2 -26 -0.90 1.53 -2 -2 -26 3.81 1.77 -2 2 -26 3.85 1.66 2 -2 -26 3.07 1.37 -2 2 -26 3.80 1.73 -3 -2 -26 3.13 1.71 3 -2 -26 0.09 1.24 -3 2 -26 3.13 1.82 -3 2 -26 1.34 1.67 -4 -2 -26 4.00 1.90 -4 2 -26 3.62 1.89 -4 2 -26 3.16 1.94 0 3 -26 8.55 1.92 0 -3 -26 6.08 1.68 -1 -3 -26 4.53 1.72 -1 3 -26 5.11 1.98 1 -3 -26 7.48 1.61 -1 3 -26 5.68 1.78 -2 -3 -26 11.97 2.23 2 -3 -26 11.03 1.96 -2 3 -26 11.21 2.21 -2 3 -26 10.01 2.17 -3 -3 -26 12.28 2.29 -3 3 -26 10.36 2.30 3 -3 -26 9.47 1.77 -3 3 -26 8.72 2.24 -4 -3 -26 15.12 2.55 -4 3 -26 11.13 2.44 -4 3 -26 16.63 2.74 0 -4 -26 3.99 1.59 0 4 -26 3.07 1.57 -1 -4 -26 7.46 1.86 1 -4 -26 8.65 1.73 -1 4 -26 9.68 2.02 -2 -4 -26 10.01 2.11 -2 4 -26 7.40 2.02 2 -4 -26 9.09 1.79 -2 4 -26 6.56 2.08 -3 -4 -26 13.30 2.43 3 -4 -26 10.78 1.82 -3 4 -26 8.38 2.22 -3 4 -26 11.65 2.37 -4 4 -26 7.17 2.19 0 -5 -26 2.43 1.51 0 5 -26 1.47 1.52 -1 -5 -26 3.39 1.50 -1 5 -26 1.46 1.65 1 -5 -26 0.73 1.27 -2 -5 -26 4.75 1.83 -2 5 -26 3.70 1.82 2 -5 -26 3.83 1.46 -3 -5 -26 2.04 1.72 3 -5 -26 1.16 1.17 -3 5 -26 -0.63 1.42 0 6 -26 1.72 1.58 0 -6 -26 4.05 1.42 -1 -6 -26 2.16 1.55 1 -6 -26 6.31 1.63 -1 6 -26 2.47 1.72 -2 -6 -26 5.36 1.87 -2 6 -26 7.59 2.14 2 -6 -26 3.62 1.48 0 7 -26 13.13 2.33 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 62566 loop_ _space_group_symop_operation_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Au1 Au 0.73733(2) 0.35871(2) 0.96704(2) 0.02115(3) Uani 1 1 d . . . . . Cl1 Cl 0.81872(6) 0.25660(4) 1.01396(5) 0.0385(2) Uani 1 1 d . . . . . P1 P 0.63777(5) 0.45070(4) 0.92382(4) 0.01606(15) Uani 1 1 d . . . . . C1 C 0.70270(19) 0.53120(14) 0.88273(14) 0.0135(5) Uani 1 1 d . . . . . C2 C 0.6449(2) 0.59296(15) 0.85767(14) 0.0166(6) Uani 1 1 d . . . . . C3 C 0.6925(2) 0.64183(19) 0.81086(15) 0.0244(6) Uani 1 1 d . . . . . H1 H 0.6531 0.6826 0.7935 0.029 Uiso 1 1 calc R U . . . C4 C 0.7958(2) 0.63249(19) 0.78903(17) 0.0306(7) Uani 1 1 d . . . . . H2 H 0.8256 0.6647 0.7548 0.037 Uiso 1 1 calc R U . . . C5 C 0.8548(2) 0.57644(17) 0.81725(16) 0.0245(6) Uani 1 1 d . . . . . H3 H 0.9270 0.5719 0.8045 0.029 Uiso 1 1 calc R U . . . C6 C 0.8107(2) 0.52598(15) 0.86439(15) 0.0163(6) Uani 1 1 d . . . . . C7 C 0.88576(19) 0.47019(14) 0.89322(15) 0.0158(5) Uani 1 1 d . . . . . C8 C 0.92135(19) 0.47561(15) 0.96276(16) 0.0197(5) Uani 1 1 d . . . . . H24 H 0.8933 0.5126 0.9929 0.024 Uiso 1 1 calc R U . . . C9 C 0.9981(2) 0.42712(17) 0.98860(15) 0.0217(6) Uani 1 1 d . . . . . C10 C 1.0370(2) 0.37354(15) 0.94322(15) 0.0209(6) Uani 1 1 d . . . . . H14 H 1.0890 0.3403 0.9603 0.025 Uiso 1 1 calc R U . . . C11 C 1.00256(19) 0.36669(15) 0.87305(14) 0.0176(5) Uani 1 1 d . . . . . C12 C 1.0477(2) 0.30592(16) 0.82653(16) 0.0211(6) Uani 1 1 d . . . . . C13 C 0.9937(3) 0.3021(2) 0.7539(2) 0.0427(10) Uani 1 1 d . . . . . H6 H 0.9176 0.2951 0.7603 0.064 Uiso 1 1 calc R U . . . H5 H 1.0227 0.2607 0.7269 0.064 Uiso 1 1 calc R U . . . H4 H 1.0063 0.3481 0.7281 0.064 Uiso 1 1 calc R U . . . C14 C 1.1658(2) 0.3201(2) 0.8148(2) 0.0395(9) Uani 1 1 d . . . . . H8 H 1.1751 0.3666 0.7892 0.059 Uiso 1 1 calc R U . . . H9 H 1.1960 0.2797 0.7870 0.059 Uiso 1 1 calc R U . . . H7 H 1.2016 0.3231 0.8606 0.059 Uiso 1 1 calc R U . . . C15 C 1.0319(3) 0.23168(18) 0.86312(18) 0.0401(9) Uani 1 1 d . . . . . H10 H 1.0707 0.2312 0.9080 0.060 Uiso 1 1 calc R U . . . H12 H 1.0583 0.1922 0.8325 0.060 Uiso 1 1 calc R U . . . H11 H 0.9566 0.2240 0.8724 0.060 Uiso 1 1 calc R U . . . C16 C 0.9269(2) 0.41620(16) 0.84882(15) 0.0176(6) Uani 1 1 d . . . . . H13 H 0.9029 0.4131 0.8013 0.021 Uiso 1 1 calc R U . . . C17 C 1.0359(3) 0.43467(19) 1.06537(17) 0.0295(8) Uani 1 1 d . . . . . C18 C 1.1075(3) 0.3708(2) 1.0870(2) 0.0598(12) Uani 1 1 d . . . . . H16 H 1.0707 0.3240 1.0789 0.090 Uiso 1 1 calc R U . . . H17 H 1.1254 0.3752 1.1372 0.090 Uiso 1 1 calc R U . . . H15 H 1.1723 0.3721 1.0587 0.090 Uiso 1 1 calc R U . . . C19 C 1.0973(3) 0.5069(2) 1.07254(19) 0.0407(9) Uani 1 1 d . . . . . H20 H 1.1603 0.5050 1.0426 0.061 Uiso 1 1 calc R U . . . H19 H 1.1183 0.5138 1.1220 0.061 Uiso 1 1 calc R U . . . H18 H 1.0524 0.5480 1.0577 0.061 Uiso 1 1 calc R U . . . C20 C 0.9416(3) 0.4353(3) 1.11530(17) 0.0508(11) Uani 1 1 d . . . . . H22 H 0.8974 0.4784 1.1052 0.076 Uiso 1 1 calc R U . . . H21 H 0.9665 0.4377 1.1643 0.076 Uiso 1 1 calc R U . . . H23 H 0.9001 0.3903 1.1085 0.076 Uiso 1 1 calc R U . . . C21 C 0.5341(2) 0.61327(15) 0.87816(14) 0.0169(6) Uani 1 1 d . . . . . C22 C 0.5192(2) 0.66378(15) 0.93312(15) 0.0194(6) Uani 1 1 d . . . . . H45 H 0.5788 0.6828 0.9576 0.023 Uiso 1 1 calc R U . . . C23 C 0.4180(2) 0.68678(15) 0.95271(15) 0.0214(6) Uani 1 1 d . . . . . C24 C 0.3335(2) 0.65723(15) 0.91539(15) 0.0223(6) Uani 1 1 d . . . . . H35 H 0.2641 0.6715 0.9287 0.027 Uiso 1 1 calc R U . . . C25 C 0.3450(2) 0.60798(15) 0.85974(15) 0.0186(6) Uani 1 1 d . . . . . C26 C 0.4475(2) 0.58768(15) 0.84100(15) 0.0175(6) Uani 1 1 d . . . . . H25 H 0.4579 0.5556 0.8019 0.021 Uiso 1 1 calc R U . . . C27 C 0.2472(2) 0.57821(15) 0.82178(14) 0.0242(6) Uani 1 1 d . . . . . C28 C 0.1879(3) 0.6421(2) 0.78606(19) 0.0420(8) Uani 1 1 d . . . . . H26 H 0.1696 0.6793 0.8217 0.063 Uiso 1 1 calc R U . . . H28 H 0.1233 0.6234 0.7640 0.063 Uiso 1 1 calc R U . . . H27 H 0.2331 0.6645 0.7498 0.063 Uiso 1 1 calc R U . . . C29 C 0.1746(3) 0.5407(2) 0.87539(19) 0.0410(9) Uani 1 1 d . . . . . H30 H 0.2134 0.5017 0.9000 0.061 Uiso 1 1 calc R U . . . H31 H 0.1139 0.5192 0.8507 0.061 Uiso 1 1 calc R U . . . H29 H 0.1497 0.5771 0.9099 0.061 Uiso 1 1 calc R U . . . C30 C 0.2755(3) 0.52129(18) 0.76515(16) 0.0337(7) Uani 1 1 d . . . . . H33 H 0.3196 0.5445 0.7288 0.051 Uiso 1 1 calc R U . . . H34 H 0.2107 0.5024 0.7433 0.051 Uiso 1 1 calc R U . . . H32 H 0.3143 0.4805 0.7870 0.051 Uiso 1 1 calc R U . . . C31 C 0.3967(2) 0.74245(18) 1.01230(16) 0.0274(7) Uani 1 1 d . . . . . C32 C 0.3381(3) 0.80922(18) 0.98263(19) 0.0424(9) Uani 1 1 d . . . . . H37 H 0.3824 0.8338 0.9472 0.064 Uiso 1 1 calc R U . . . H36 H 0.3224 0.8437 1.0211 0.064 Uiso 1 1 calc R U . . . H38 H 0.2721 0.7930 0.9605 0.064 Uiso 1 1 calc R U . . . C33 C 0.3293(3) 0.7055(2) 1.06986(18) 0.0432(9) Uani 1 1 d . . . . . H39 H 0.2605 0.6919 1.0500 0.065 Uiso 1 1 calc R U . . . H41 H 0.3191 0.7398 1.1093 0.065 Uiso 1 1 calc R U . . . H40 H 0.3652 0.6611 1.0870 0.065 Uiso 1 1 calc R U . . . C34 C 0.4989(2) 0.7697(2) 1.04684(19) 0.0415(9) Uani 1 1 d . . . . . H43 H 0.5380 0.7277 1.0661 0.062 Uiso 1 1 calc R U . . . H42 H 0.4817 0.8041 1.0852 0.062 Uiso 1 1 calc R U . . . H44 H 0.5423 0.7949 1.0114 0.062 Uiso 1 1 calc R U . . . C35 C 0.5584(2) 0.41255(16) 0.85019(16) 0.0210(6) Uani 1 1 d . . . . . H56 H 0.4961 0.4455 0.8426 0.025 Uiso 1 1 calc R U . . . C36 C 0.5179(3) 0.33512(18) 0.86647(18) 0.0362(8) Uani 1 1 d . . . . . H54 H 0.5783 0.3031 0.8790 0.043 Uiso 1 1 calc R U . . . H55 H 0.4701 0.3373 0.9079 0.043 Uiso 1 1 calc R U . . . C37 C 0.4590(3) 0.3013(2) 0.80410(19) 0.0408(9) Uani 1 1 d . . . . . H53 H 0.4365 0.2506 0.8164 0.049 Uiso 1 1 calc R U . . . H46 H 0.3949 0.3307 0.7940 0.049 Uiso 1 1 calc R U . . . C38 C 0.5281(3) 0.2990(3) 0.7391(2) 0.0535(12) Uani 1 1 d . . . . . H47 H 0.4878 0.2783 0.6988 0.064 Uiso 1 1 calc R U . . . H48 H 0.5898 0.2668 0.7479 0.064 Uiso 1 1 calc R U . . . C39 C 0.5653(4) 0.3767(3) 0.7210(2) 0.0700(15) Uani 1 1 d . . . . . H49 H 0.6125 0.3747 0.6793 0.084 Uiso 1 1 calc R U . . . H50 H 0.5036 0.4075 0.7086 0.084 Uiso 1 1 calc R U . . . C40 C 0.6239(3) 0.4119(2) 0.78261(17) 0.0448(10) Uani 1 1 d . . . . . H52 H 0.6429 0.4631 0.7699 0.054 Uiso 1 1 calc R U . . . H51 H 0.6901 0.3844 0.7912 0.054 Uiso 1 1 calc R U . . . C41 C 0.5549(2) 0.48771(16) 0.99590(15) 0.0215(6) Uani 1 1 d . . . . . H67 H 0.5107 0.5287 0.9767 0.026 Uiso 1 1 calc R U . . . C42 C 0.4822(2) 0.42975(17) 1.02853(18) 0.0297(7) Uani 1 1 d . . . . . H65 H 0.4300 0.4135 0.9928 0.036 Uiso 1 1 calc R U . . . H66 H 0.5244 0.3863 1.0429 0.036 Uiso 1 1 calc R U . . . C43 C 0.4245(3) 0.4608(2) 1.0930(2) 0.0419(9) Uani 1 1 d . . . . . H58 H 0.3764 0.5006 1.0776 0.050 Uiso 1 1 calc R U . . . H57 H 0.3811 0.4214 1.1146 0.050 Uiso 1 1 calc R U . . . C44 C 0.4999(3) 0.4907(2) 1.14765(18) 0.0429(9) Uani 1 1 d . . . . . H59 H 0.5436 0.4500 1.1666 0.052 Uiso 1 1 calc R U . . . H60 H 0.4595 0.5123 1.1874 0.052 Uiso 1 1 calc R U . . . C45 C 0.5711(3) 0.5491(2) 1.11564(18) 0.0396(9) Uani 1 1 d . . . . . H62 H 0.6224 0.5660 1.1517 0.048 Uiso 1 1 calc R U . . . H61 H 0.5280 0.5921 1.1011 0.048 Uiso 1 1 calc R U . . . C46 C 0.6307(2) 0.51927(19) 1.05141(17) 0.0328(8) Uani 1 1 d . . . . . H64 H 0.6801 0.4802 1.0669 0.039 Uiso 1 1 calc R U . . . H63 H 0.6728 0.5594 1.0299 0.039 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Au1 0.02016(5) 0.01739(4) 0.02590(5) 0.00637(4) 0.00106(5) 0.00135(4) Cl1 0.0326(4) 0.0273(4) 0.0557(6) 0.0208(4) -0.0027(4) 0.0084(3) P1 0.0157(3) 0.0138(3) 0.0186(4) 0.0022(3) 0.0025(3) -0.0007(3) C1 0.0140(12) 0.0140(12) 0.0124(13) -0.0014(10) 0.0003(10) -0.0015(9) C2 0.0156(13) 0.0157(13) 0.0185(14) 0.0001(11) 0.0005(11) 0.0018(10) C3 0.0232(13) 0.0192(13) 0.0310(16) 0.0101(15) 0.0057(12) 0.0043(13) C4 0.0260(15) 0.0277(18) 0.0381(18) 0.0167(15) 0.0099(13) 0.0025(13) C5 0.0154(14) 0.0232(15) 0.0348(18) 0.0092(14) 0.0088(12) 0.0020(11) C6 0.0158(13) 0.0160(13) 0.0169(14) -0.0022(11) 0.0007(11) 0.0001(10) C7 0.0111(12) 0.0162(13) 0.0200(15) 0.0013(11) 0.0002(11) -0.0024(10) C8 0.0199(13) 0.0183(13) 0.0211(15) -0.0017(13) 0.0035(13) 0.0019(10) C9 0.0242(15) 0.0204(14) 0.0205(15) 0.0011(12) -0.0032(11) -0.0005(12) C10 0.0190(13) 0.0175(15) 0.0263(15) 0.0015(11) -0.0049(11) 0.0034(10) C11 0.0155(12) 0.0133(13) 0.0240(14) -0.0005(12) 0.0022(10) 0.0003(10) C12 0.0224(15) 0.0166(14) 0.0242(16) -0.0006(12) 0.0018(12) 0.0032(11) C13 0.055(2) 0.038(2) 0.036(2) -0.0122(17) -0.0061(18) 0.0198(18) C14 0.0287(18) 0.0330(19) 0.057(2) -0.0160(17) 0.0143(17) 0.0009(14) C15 0.059(2) 0.0191(16) 0.042(2) -0.0008(15) 0.0166(19) 0.0033(16) C16 0.0163(13) 0.0176(15) 0.0190(15) 0.0013(12) -0.0006(11) 0.0002(10) C17 0.0374(19) 0.0279(18) 0.0233(17) -0.0030(14) -0.0110(14) 0.0051(14) C18 0.096(3) 0.046(3) 0.037(2) -0.0070(19) -0.036(2) 0.026(2) C19 0.048(2) 0.042(2) 0.032(2) -0.0060(17) -0.0168(17) -0.0028(17) C20 0.066(3) 0.067(3) 0.0194(18) -0.0002(19) -0.0018(18) -0.009(2) C21 0.0166(13) 0.0135(12) 0.0206(15) 0.0057(11) 0.0010(11) 0.0010(10) C22 0.0178(14) 0.0174(13) 0.0229(15) -0.0016(11) -0.0022(12) 0.0024(10) C23 0.0218(14) 0.0189(13) 0.0234(16) 0.0000(12) 0.0020(12) 0.0031(10) C24 0.0139(12) 0.0271(16) 0.0257(16) -0.0029(12) 0.0023(11) 0.0043(10) C25 0.0142(13) 0.0184(13) 0.0233(15) 0.0033(12) 0.0009(11) 0.0003(10) C26 0.0190(13) 0.0158(13) 0.0178(14) 0.0018(11) 0.0027(11) 0.0024(10) C27 0.0169(14) 0.0277(14) 0.0279(14) -0.0025(12) -0.0020(13) -0.0008(12) C28 0.0342(17) 0.044(2) 0.048(2) -0.001(2) -0.0180(15) 0.0068(18) C29 0.0302(18) 0.050(2) 0.043(2) -0.0021(18) 0.0055(16) -0.0155(16) C30 0.0264(17) 0.0395(18) 0.0352(17) -0.0105(14) -0.0060(15) -0.0051(14) C31 0.0263(16) 0.0272(16) 0.0288(18) -0.0105(13) 0.0006(13) 0.0061(12) C32 0.049(2) 0.0300(18) 0.049(2) -0.0116(17) -0.0027(18) 0.0148(15) C33 0.045(2) 0.051(2) 0.034(2) -0.0108(18) 0.0114(17) 0.0057(18) C34 0.0370(19) 0.042(2) 0.045(2) -0.0235(18) -0.0032(17) 0.0022(15) C35 0.0197(14) 0.0162(15) 0.0272(17) -0.0008(13) -0.0030(12) -0.0007(11) C36 0.045(2) 0.0268(18) 0.037(2) -0.0021(15) 0.0025(16) -0.0170(15) C37 0.042(2) 0.031(2) 0.049(2) -0.0065(18) -0.0040(18) -0.0182(16) C38 0.064(3) 0.050(3) 0.047(3) -0.020(2) -0.006(2) -0.019(2) C39 0.106(4) 0.073(3) 0.030(2) -0.011(2) -0.003(2) -0.052(3) C40 0.063(3) 0.048(2) 0.0232(17) -0.0097(17) 0.0082(17) -0.034(2) C41 0.0214(15) 0.0191(14) 0.0242(16) 0.0064(12) 0.0071(12) 0.0013(11) C42 0.0321(15) 0.0286(16) 0.0285(17) 0.0028(16) 0.0127(16) -0.0077(12) C43 0.038(2) 0.045(2) 0.043(2) 0.0048(18) 0.0234(18) -0.0057(16) C44 0.055(2) 0.048(2) 0.0264(19) -0.0022(17) 0.0167(18) 0.0028(19) C45 0.047(2) 0.042(2) 0.0293(19) -0.0116(16) 0.0144(17) -0.0035(17) C46 0.0313(17) 0.0378(19) 0.0293(19) -0.0110(15) 0.0101(14) -0.0067(14) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag P1 Au1 Cl1 172.48(3) . . ? C41 P1 C1 105.99(12) . . ? C41 P1 C35 112.43(13) . . ? C1 P1 C35 102.82(13) . . ? C41 P1 Au1 108.75(10) . . ? C1 P1 Au1 119.37(8) . . ? C35 P1 Au1 107.49(10) . . ? C6 C1 C2 118.0(2) . . ? C6 C1 P1 118.7(2) . . ? C2 C1 P1 122.30(19) . . ? C3 C2 C1 119.5(2) . . ? C3 C2 C21 114.4(2) . . ? C1 C2 C21 126.1(2) . . ? C4 C3 C2 121.5(3) . . ? C5 C4 C3 119.4(3) . . ? C4 C5 C6 121.1(3) . . ? C5 C6 C1 120.0(3) . . ? C5 C6 C7 115.1(2) . . ? C1 C6 C7 124.9(3) . . ? C16 C7 C8 119.8(2) . . ? C16 C7 C6 119.8(2) . . ? C8 C7 C6 120.2(2) . . ? C7 C8 C9 120.7(3) . . ? C10 C9 C8 118.2(3) . . ? C10 C9 C17 122.4(3) . . ? C8 C9 C17 119.4(3) . . ? C9 C10 C11 122.4(3) . . ? C16 C11 C10 117.9(3) . . ? C16 C11 C12 122.5(3) . . ? C10 C11 C12 119.6(2) . . ? C11 C12 C15 109.2(2) . . ? C11 C12 C13 112.4(2) . . ? C15 C12 C13 107.9(3) . . ? C11 C12 C14 109.2(2) . . ? C15 C12 C14 110.0(3) . . ? C13 C12 C14 108.2(3) . . ? C7 C16 C11 121.0(3) . . ? C20 C17 C18 107.9(3) . . ? C20 C17 C19 109.7(3) . . ? C18 C17 C19 108.9(3) . . ? C20 C17 C9 110.0(3) . . ? C18 C17 C9 111.7(3) . . ? C19 C17 C9 108.6(3) . . ? C26 C21 C22 119.3(2) . . ? C26 C21 C2 121.9(2) . . ? C22 C21 C2 118.6(2) . . ? C21 C22 C23 121.1(3) . . ? C24 C23 C22 117.2(3) . . ? C24 C23 C31 119.3(2) . . ? C22 C23 C31 123.5(3) . . ? C25 C24 C23 123.5(2) . . ? C24 C25 C26 117.4(3) . . ? C24 C25 C27 119.8(2) . . ? C26 C25 C27 122.8(2) . . ? C21 C26 C25 121.4(3) . . ? C29 C27 C30 107.7(3) . . ? C29 C27 C25 109.5(2) . . ? C30 C27 C25 112.1(2) . . ? C29 C27 C28 109.4(3) . . ? C30 C27 C28 108.5(2) . . ? C25 C27 C28 109.6(2) . . ? C32 C31 C33 109.6(3) . . ? C32 C31 C23 109.8(3) . . ? C33 C31 C23 109.2(3) . . ? C32 C31 C34 108.1(3) . . ? C33 C31 C34 108.0(3) . . ? C23 C31 C34 112.1(2) . . ? C40 C35 C36 110.2(3) . . ? C40 C35 P1 109.7(2) . . ? C36 C35 P1 112.0(2) . . ? C37 C36 C35 112.3(3) . . ? C38 C37 C36 110.9(3) . . ? C37 C38 C39 109.6(4) . . ? C40 C39 C38 111.6(4) . . ? C39 C40 C35 112.3(3) . . ? C42 C41 C46 111.0(3) . . ? C42 C41 P1 113.0(2) . . ? C46 C41 P1 106.55(19) . . ? C43 C42 C41 110.9(3) . . ? C44 C43 C42 112.0(3) . . ? C43 C44 C45 110.8(3) . . ? C44 C45 C46 111.2(3) . . ? C45 C46 C41 111.5(3) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Au1 P1 2.2460(7) . ? Au1 Cl1 2.2984(7) . ? P1 C41 1.846(3) . ? P1 C1 1.848(3) . ? P1 C35 1.851(3) . ? C1 C6 1.415(4) . ? C1 C2 1.420(4) . ? C2 C3 1.390(4) . ? C2 C21 1.502(4) . ? C3 C4 1.383(4) . ? C4 C5 1.371(4) . ? C5 C6 1.394(4) . ? C6 C7 1.492(4) . ? C7 C16 1.391(4) . ? C7 C8 1.392(4) . ? C8 C9 1.399(4) . ? C9 C10 1.387(4) . ? C9 C17 1.534(4) . ? C10 C11 1.401(4) . ? C11 C16 1.392(4) . ? C11 C12 1.522(4) . ? C12 C15 1.527(4) . ? C12 C13 1.535(5) . ? C12 C14 1.534(4) . ? C17 C20 1.522(5) . ? C17 C18 1.528(5) . ? C17 C19 1.529(5) . ? C21 C26 1.383(4) . ? C21 C22 1.398(4) . ? C22 C23 1.398(4) . ? C23 C24 1.390(4) . ? C23 C31 1.537(4) . ? C24 C25 1.388(4) . ? C25 C26 1.395(4) . ? C25 C27 1.530(4) . ? C27 C29 1.529(4) . ? C27 C30 1.530(4) . ? C27 C28 1.538(4) . ? C31 C32 1.527(4) . ? C31 C33 1.537(5) . ? C31 C34 1.532(4) . ? C35 C40 1.523(4) . ? C35 C36 1.527(4) . ? C36 C37 1.524(4) . ? C37 C38 1.509(5) . ? C38 C39 1.527(6) . ? C39 C40 1.520(5) . ? C41 C42 1.528(4) . ? C41 C46 1.533(4) . ? C42 C43 1.528(4) . ? C43 C44 1.508(5) . ? C44 C45 1.518(5) . ? C45 C46 1.528(4) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C41 P1 C1 C6 137.6(2) . . . . ? C35 P1 C1 C6 -104.2(2) . . . . ? Au1 P1 C1 C6 14.6(2) . . . . ? C41 P1 C1 C2 -53.6(3) . . . . ? C35 P1 C1 C2 64.5(2) . . . . ? Au1 P1 C1 C2 -176.67(18) . . . . ? C6 C1 C2 C3 6.3(4) . . . . ? P1 C1 C2 C3 -162.6(2) . . . . ? C6 C1 C2 C21 -172.2(3) . . . . ? P1 C1 C2 C21 19.0(4) . . . . ? C1 C2 C3 C4 -1.2(5) . . . . ? C21 C2 C3 C4 177.4(3) . . . . ? C2 C3 C4 C5 -3.9(5) . . . . ? C3 C4 C5 C6 3.9(5) . . . . ? C4 C5 C6 C1 1.3(5) . . . . ? C4 C5 C6 C7 -177.3(3) . . . . ? C2 C1 C6 C5 -6.4(4) . . . . ? P1 C1 C6 C5 162.9(2) . . . . ? C2 C1 C6 C7 172.1(2) . . . . ? P1 C1 C6 C7 -18.6(4) . . . . ? C5 C6 C7 C16 -68.9(3) . . . . ? C1 C6 C7 C16 112.5(3) . . . . ? C5 C6 C7 C8 105.8(3) . . . . ? C1 C6 C7 C8 -72.7(4) . . . . ? C16 C7 C8 C9 -0.1(4) . . . . ? C6 C7 C8 C9 -174.8(2) . . . . ? C7 C8 C9 C10 -0.3(4) . . . . ? C7 C8 C9 C17 179.8(3) . . . . ? C8 C9 C10 C11 0.2(4) . . . . ? C17 C9 C10 C11 -179.9(3) . . . . ? C9 C10 C11 C16 0.3(4) . . . . ? C9 C10 C11 C12 -179.2(3) . . . . ? C16 C11 C12 C15 -124.5(3) . . . . ? C10 C11 C12 C15 55.0(4) . . . . ? C16 C11 C12 C13 -4.9(4) . . . . ? C10 C11 C12 C13 174.6(3) . . . . ? C16 C11 C12 C14 115.2(3) . . . . ? C10 C11 C12 C14 -65.3(4) . . . . ? C8 C7 C16 C11 0.7(4) . . . . ? C6 C7 C16 C11 175.5(2) . . . . ? C10 C11 C16 C7 -0.8(4) . . . . ? C12 C11 C16 C7 178.7(3) . . . . ? C10 C9 C17 C20 -127.7(3) . . . . ? C8 C9 C17 C20 52.2(4) . . . . ? C10 C9 C17 C18 -7.9(4) . . . . ? C8 C9 C17 C18 171.9(3) . . . . ? C10 C9 C17 C19 112.3(3) . . . . ? C8 C9 C17 C19 -67.9(4) . . . . ? C3 C2 C21 C26 91.3(3) . . . . ? C1 C2 C21 C26 -90.2(4) . . . . ? C3 C2 C21 C22 -83.9(3) . . . . ? C1 C2 C21 C22 94.6(3) . . . . ? C26 C21 C22 C23 2.3(4) . . . . ? C2 C21 C22 C23 177.6(3) . . . . ? C21 C22 C23 C24 0.1(4) . . . . ? C21 C22 C23 C31 -179.6(3) . . . . ? C22 C23 C24 C25 -1.3(4) . . . . ? C31 C23 C24 C25 178.5(3) . . . . ? C23 C24 C25 C26 0.0(4) . . . . ? C23 C24 C25 C27 179.9(3) . . . . ? C22 C21 C26 C25 -3.7(4) . . . . ? C2 C21 C26 C25 -178.8(2) . . . . ? C24 C25 C26 C21 2.5(4) . . . . ? C27 C25 C26 C21 -177.4(3) . . . . ? C24 C25 C27 C29 -57.0(4) . . . . ? C26 C25 C27 C29 122.9(3) . . . . ? C24 C25 C27 C30 -176.5(3) . . . . ? C26 C25 C27 C30 3.4(4) . . . . ? C24 C25 C27 C28 63.0(3) . . . . ? C26 C25 C27 C28 -117.1(3) . . . . ? C24 C23 C31 C32 -59.2(4) . . . . ? C22 C23 C31 C32 120.5(3) . . . . ? C24 C23 C31 C33 61.0(4) . . . . ? C22 C23 C31 C33 -119.3(3) . . . . ? C24 C23 C31 C34 -179.3(3) . . . . ? C22 C23 C31 C34 0.4(4) . . . . ? C41 P1 C35 C40 157.3(2) . . . . ? C1 P1 C35 C40 43.7(3) . . . . ? Au1 P1 C35 C40 -83.1(2) . . . . ? C41 P1 C35 C36 -80.1(2) . . . . ? C1 P1 C35 C36 166.4(2) . . . . ? Au1 P1 C35 C36 39.6(2) . . . . ? C40 C35 C36 C37 -53.6(4) . . . . ? P1 C35 C36 C37 -176.0(2) . . . . ? C35 C36 C37 C38 57.1(4) . . . . ? C36 C37 C38 C39 -57.6(5) . . . . ? C37 C38 C39 C40 57.2(5) . . . . ? C38 C39 C40 C35 -55.5(5) . . . . ? C36 C35 C40 C39 52.7(5) . . . . ? P1 C35 C40 C39 176.5(3) . . . . ? C1 P1 C41 C42 171.2(2) . . . . ? C35 P1 C41 C42 59.6(3) . . . . ? Au1 P1 C41 C42 -59.3(2) . . . . ? C1 P1 C41 C46 -66.7(2) . . . . ? C35 P1 C41 C46 -178.2(2) . . . . ? Au1 P1 C41 C46 62.8(2) . . . . ? C46 C41 C42 C43 54.1(3) . . . . ? P1 C41 C42 C43 173.7(2) . . . . ? C41 C42 C43 C44 -55.8(4) . . . . ? C42 C43 C44 C45 56.5(4) . . . . ? C43 C44 C45 C46 -56.0(4) . . . . ? C44 C45 C46 C41 55.3(4) . . . . ? C42 C41 C46 C45 -54.4(4) . . . . ? P1 C41 C46 C45 -177.8(2) . . . . ?