#------------------------------------------------------------------------------ #$Date: 2022-04-03 20:26:58 +0100 (Sun, 03 Apr 2022) $ #$Revision: 274249 $ #$URL: svn://www.crystallography.net/cod/cif/4/51/93/4519393.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519393 loop_ _publ_author_name 'de Vries, Folkert' 'Otten, Edwin' _publ_section_title ; Reversible On/Off Switching of Lactide Cyclopolymerization with a Redox-Active Formazanate Ligand ; _journal_issue 7 _journal_name_full 'ACS Catalysis' _journal_page_first 4125 _journal_page_last 4130 _journal_paper_doi 10.1021/acscatal.1c05689 _journal_volume 12 _journal_year 2022 _chemical_formula_sum 'C59 H52 N8 O2 Zn2' _chemical_formula_weight 1035.82 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_method SHELXL-2018/1 _cell_angle_alpha 80.7300(10) _cell_angle_beta 73.2480(10) _cell_angle_gamma 67.2520(10) _cell_formula_units_Z 1 _cell_length_a 9.1508(3) _cell_length_b 10.8692(4) _cell_length_c 14.2352(5) _cell_measurement_reflns_used 9902 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 72.57 _cell_measurement_theta_min 5.34 _cell_volume 1248.34(8) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX3' _computing_data_reduction 'Bruker SAINT' _computing_structure_refinement 'SHELXL-2018/1 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0320 _diffrn_reflns_av_unetI/netI 0.0202 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 31685 _diffrn_reflns_point_group_measured_fraction_full 0.996 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 72.562 _diffrn_reflns_theta_min 3.247 _exptl_absorpt_coefficient_mu 1.595 _exptl_absorpt_correction_T_max 0.7536 _exptl_absorpt_correction_T_min 0.5011 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS _exptl_crystal_colour 'dark blue' _exptl_crystal_density_diffrn 1.378 _exptl_crystal_description block _exptl_crystal_F_000 538 _exptl_crystal_size_max 0.423 _exptl_crystal_size_mid 0.200 _exptl_crystal_size_min 0.060 _refine_diff_density_max 0.288 _refine_diff_density_min -0.656 _refine_diff_density_rms 0.043 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.043 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 342 _refine_ls_number_reflns 4939 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.043 _refine_ls_R_factor_all 0.0283 _refine_ls_R_factor_gt 0.0270 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0243P)^2^+0.7544P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0672 _refine_ls_wR_factor_ref 0.0681 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4715 _reflns_number_total 4939 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cs1c05689_si_003.cif _cod_data_source_block cu_molan663_0m_a _cod_database_code 4519393 _shelx_shelxl_version_number 2018/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; TITL cu_molan663_0m_a.res in P-1 cu_molan663_0m_a.res created by SHELXL-2018/1 at 11:45:02 on 06-Jan-2022 REM Old TITL cu_molan663_0m in P-1 REM SHELXT solution in P-1 REM R1 0.152, Rweak 0.008, Alpha 0.020, Orientation as input REM Formula found by SHELXT: C30 N4 O Zn CELL 1.54178 9.1508 10.8692 14.2352 80.730 73.248 67.252 ZERR 1.000 0.0003 0.0004 0.0005 0.001 0.001 0.001 LATT 1 SFAC C H N O ZN UNIT 59 52 8 2 2 TEMP -173.150 L.S. 10 BOND $H LIST 4 ACTA OMIT 3 5 4 OMIT 1 2 7 OMIT -3 1 2 FMAP 2 PLAN 20 WGHT 0.024300 0.754400 FVAR 0.57242 ZN1 5 0.884147 0.534048 0.435131 11.00000 0.02090 0.04291 = 0.02229 -0.01638 -0.00777 -0.00767 O1 4 0.888811 0.584130 0.558380 11.00000 0.02100 0.04804 = 0.02511 -0.02176 -0.00721 -0.00377 N1 3 0.758563 0.430381 0.419066 11.00000 0.02033 0.03729 = 0.02016 -0.01131 -0.00743 -0.00613 C1 1 0.777330 0.494874 0.254024 11.00000 0.01920 0.03402 = 0.02186 -0.01071 -0.00755 -0.00615 N2 3 0.741390 0.416123 0.334045 11.00000 0.01994 0.03632 = 0.01900 -0.01073 -0.00748 -0.00574 C2 1 0.756017 0.460728 0.162332 11.00000 0.01967 0.03093 = 0.02037 -0.00952 -0.00819 -0.00510 C3 1 0.685590 0.366888 0.163612 11.00000 0.03245 0.03421 = 0.01986 -0.00266 -0.00942 -0.01416 AFIX 43 H3 2 0.649991 0.322796 0.224059 11.00000 -1.20000 AFIX 0 N3 3 0.815484 0.605083 0.243504 11.00000 0.02007 0.03376 = 0.02516 -0.01379 -0.00894 -0.00476 C4 1 0.667158 0.337481 0.077155 11.00000 0.03406 0.03194 = 0.02400 -0.00475 -0.01095 -0.01526 AFIX 43 H4 2 0.619114 0.273249 0.079625 11.00000 -1.20000 AFIX 0 N4 3 0.852594 0.643354 0.313644 11.00000 0.02043 0.03514 = 0.02997 -0.01582 -0.00995 -0.00444 C5 1 0.717496 0.400005 -0.013053 11.00000 0.02263 0.02917 = 0.02000 -0.00759 -0.00780 -0.00546 C6 1 0.787589 0.492500 -0.013732 11.00000 0.03051 0.03565 = 0.01905 -0.00429 -0.00596 -0.01369 AFIX 43 H6 2 0.822887 0.536692 -0.074200 11.00000 -1.20000 AFIX 0 C8 1 0.696389 0.368308 -0.106733 11.00000 0.03354 0.03624 = 0.02020 -0.00813 -0.00963 -0.01196 AFIX 137 H8A 2 0.704314 0.439880 -0.157219 11.00000 -1.50000 H8B 2 0.588944 0.360940 -0.094282 11.00000 -1.50000 H8C 2 0.782219 0.283541 -0.129468 11.00000 -1.50000 AFIX 0 C7 1 0.807506 0.522203 0.072233 11.00000 0.02793 0.03551 = 0.02514 -0.00828 -0.00644 -0.01470 AFIX 43 H7 2 0.857091 0.585515 0.069302 11.00000 -1.20000 AFIX 0 C9 1 0.706174 0.344301 0.495935 11.00000 0.01891 0.03667 = 0.02089 -0.00786 -0.00884 -0.00476 C10 1 0.656512 0.385071 0.591954 11.00000 0.02355 0.03719 = 0.02391 -0.01095 -0.00921 -0.00541 AFIX 43 H10 2 0.657629 0.468094 0.604076 11.00000 -1.20000 AFIX 0 C11 1 0.605698 0.303972 0.669308 11.00000 0.02604 0.04526 = 0.02052 -0.00898 -0.00835 -0.00684 AFIX 43 H11 2 0.570282 0.332264 0.734507 11.00000 -1.20000 AFIX 0 C12 1 0.606081 0.181787 0.652384 11.00000 0.03316 0.04392 = 0.02764 -0.00099 -0.01255 -0.01230 AFIX 43 H12 2 0.570641 0.126588 0.705667 11.00000 -1.20000 AFIX 0 C13 1 0.658852 0.140447 0.556601 11.00000 0.04078 0.03852 = 0.03214 -0.00639 -0.01514 -0.01249 AFIX 43 H13 2 0.661001 0.056079 0.544892 11.00000 -1.20000 AFIX 0 C14 1 0.708051 0.221165 0.478562 11.00000 0.03189 0.03875 = 0.02484 -0.01096 -0.01140 -0.00788 AFIX 43 H14 2 0.742970 0.192801 0.413406 11.00000 -1.20000 AFIX 0 C15 1 0.880034 0.765968 0.290309 11.00000 0.02071 0.03041 = 0.04297 -0.01921 -0.01263 0.00040 C16 1 0.939173 0.805719 0.356275 11.00000 0.02625 0.04283 = 0.04519 -0.02241 -0.01317 -0.00536 AFIX 43 H16 2 0.956470 0.752334 0.414685 11.00000 -1.20000 AFIX 0 C17 1 0.972368 0.922146 0.336676 11.00000 0.02973 0.04346 = 0.06852 -0.03069 -0.01998 -0.00363 AFIX 43 H17 2 1.013662 0.947856 0.381339 11.00000 -1.20000 AFIX 0 C18 1 0.946077 1.001187 0.252943 11.00000 0.04167 0.02893 = 0.08740 -0.02041 -0.03056 -0.00234 AFIX 43 H18 2 0.968983 1.081267 0.239612 11.00000 -1.20000 AFIX 0 C19 1 0.885631 0.962689 0.188004 11.00000 0.05724 0.02821 = 0.08367 -0.00621 -0.04523 -0.00423 AFIX 43 H19 2 0.866846 1.017213 0.130245 11.00000 -1.20000 AFIX 0 C20 1 0.852470 0.845841 0.206483 11.00000 0.04567 0.02727 = 0.06504 -0.01081 -0.03731 -0.00225 AFIX 43 H20 2 0.810913 0.820659 0.161694 11.00000 -1.20000 AFIX 0 C21 1 0.775845 0.678262 0.620971 11.00000 0.02316 0.03304 = 0.02053 -0.01180 -0.00124 -0.01208 C22 1 0.801821 0.683865 0.711413 11.00000 0.03218 0.03464 = 0.02208 -0.00896 -0.00848 -0.00781 AFIX 43 H22 2 0.897907 0.622615 0.729265 11.00000 -1.20000 AFIX 0 C23 1 0.686790 0.779309 0.775491 11.00000 0.04429 0.03758 = 0.02270 -0.01268 -0.00684 -0.00996 AFIX 43 H23 2 0.705045 0.783323 0.837142 11.00000 -1.20000 AFIX 0 C24 1 0.546364 0.868401 0.750932 11.00000 0.03726 0.02907 = 0.02798 -0.01267 0.00111 -0.01045 AFIX 43 H24 2 0.468098 0.933225 0.795421 11.00000 -1.20000 AFIX 0 C25 1 0.520206 0.862701 0.660841 11.00000 0.02705 0.03251 = 0.03312 -0.00765 -0.00509 -0.00814 AFIX 43 H25 2 0.423745 0.923845 0.643353 11.00000 -1.20000 AFIX 0 C26 1 0.635272 0.767358 0.595878 11.00000 0.02624 0.04159 = 0.02509 -0.01099 -0.00702 -0.01109 AFIX 43 H26 2 0.617051 0.763583 0.534169 11.00000 -1.20000 AFIX 0 PART -1 C27 1 0.866907 0.846480 -0.039655 10.50000 0.03444 0.03918 = 0.03022 0.00140 -0.00555 -0.01347 AFIX 137 H27A 2 0.904735 0.808507 -0.104107 10.50000 -1.50000 H27B 2 0.885782 0.774062 0.011393 10.50000 -1.50000 H27C 2 0.927345 0.903354 -0.038599 10.50000 -1.50000 AFIX 66 C28 1 0.676592 0.933432 -0.019594 10.50000 0.04884 0.04041 = 0.02205 -0.00186 -0.00919 -0.02826 C29 1 0.564620 0.884045 0.046623 10.50000 0.03831 0.02076 = 0.02669 0.00669 -0.01556 -0.01417 AFIX 43 H29 2 0.602070 0.801231 0.082483 10.50000 -1.20000 AFIX 65 C30 1 0.397855 0.955829 0.060371 10.50000 0.04436 0.03028 = 0.02660 0.00323 -0.01124 -0.02323 AFIX 43 H30 2 0.321328 0.922075 0.105627 10.50000 -1.20000 AFIX 65 C31 1 0.343059 1.076998 0.007902 10.50000 0.05674 0.02055 = 0.03427 -0.00018 -0.02924 -0.00619 AFIX 43 H31 2 0.229081 1.126059 0.017299 10.50000 -1.20000 AFIX 65 C32 1 0.455028 1.126386 -0.058314 10.50000 0.07374 0.03248 = 0.03370 0.00466 -0.01825 -0.02390 AFIX 43 H32 2 0.417577 1.209201 -0.094173 10.50000 -1.20000 AFIX 65 C33 1 0.621794 1.054605 -0.072063 10.50000 0.05519 0.03108 = 0.03249 0.00357 -0.01211 -0.01919 AFIX 43 H33 2 0.698321 1.088359 -0.117319 10.50000 -1.20000 PART 0 AFIX 0 HKLF 4 REM cu_molan663_0m_a.res in P-1 REM R1 = 0.0270 for 4715 Fo > 4sig(Fo) and 0.0283 for all 4939 data REM 342 parameters refined using 0 restraints END WGHT 0.0243 0.7544 REM Highest difference peak 0.288, deepest hole -0.656, 1-sigma level 0.043 Q1 1 0.7600 0.4785 0.2068 11.00000 0.05 0.29 Q2 1 0.6836 0.3625 0.5446 11.00000 0.05 0.24 Q3 1 0.9856 0.9470 0.2853 11.00000 0.05 0.23 Q4 1 0.7069 0.3843 -0.0549 11.00000 0.05 0.23 Q5 1 0.6736 0.2959 0.4854 11.00000 0.05 0.21 Q6 1 0.9634 0.9838 0.1969 11.00000 0.05 0.21 Q7 1 0.7696 0.5064 0.1260 11.00000 0.05 0.21 Q8 1 0.7195 0.7372 0.6025 11.00000 0.05 0.21 Q9 1 0.9241 0.7869 0.3182 11.00000 0.05 0.21 Q10 1 0.7603 0.5218 0.0393 11.00000 0.05 0.20 Q11 1 0.9775 0.5324 0.5624 11.00000 0.05 0.20 Q12 1 0.6922 0.4354 0.1629 11.00000 0.05 0.20 Q13 1 0.7649 0.6641 0.6787 11.00000 0.05 0.20 Q14 1 0.7567 0.4361 -0.0139 11.00000 0.05 0.20 Q15 1 0.7220 0.4610 -0.0115 11.00000 0.05 0.19 Q16 1 0.8063 0.6979 0.6569 11.00000 0.05 0.19 Q17 1 0.7758 0.4958 0.4337 11.00000 0.05 0.19 Q18 1 0.5794 0.2553 0.6553 11.00000 0.05 0.19 Q19 1 0.5497 0.8835 0.6977 11.00000 0.05 0.19 Q20 1 0.2453 1.0844 0.0262 11.00000 0.05 0.18 ; _shelx_res_checksum 14985 _shelx_hkl_file ; -1 0 0 218.28 7.80 -1 0 0 223.68 7.80 1 0 0 216.78 7.80 -2 0 0 2385.66 83.99 -2 0 0 2412.16 83.89 2 0 0 2558.24 83.99 -3 0 0 44.00 2.50 -3 0 0 43.90 2.40 3 0 0 46.40 3.00 3 0 0 43.70 2.50 -4 0 0 696.13 25.40 -4 0 0 717.73 25.10 4 0 0 708.63 25.70 4 0 0 693.73 24.90 -5 0 0 382.56 14.70 -5 0 0 422.36 15.00 -5 0 0 402.36 14.50 -5 0 0 399.26 15.60 -5 0 0 385.86 14.40 -5 0 0 382.66 14.90 5 0 0 398.56 23.20 5 0 0 413.56 16.70 5 0 0 376.96 14.90 5 0 0 414.06 16.10 -6 0 0 19.10 1.50 -6 0 0 19.20 1.80 -6 0 0 18.50 1.80 -6 0 0 19.00 1.90 -6 0 0 18.50 1.50 -6 0 0 21.10 3.20 -6 0 0 16.90 1.50 -6 0 0 12.90 2.60 -6 0 0 17.60 1.80 -6 0 0 18.40 1.60 6 0 0 20.60 8.90 6 0 0 26.70 7.60 -7 0 0 9.00 1.30 -7 0 0 9.60 1.10 -7 0 0 10.30 1.20 -7 0 0 7.60 1.30 -7 0 0 8.90 1.20 -7 0 0 9.80 1.30 -7 0 0 9.90 3.40 -7 0 0 7.20 1.20 -7 0 0 9.10 1.40 -8 0 0 96.59 4.20 -8 0 0 90.69 4.10 -8 0 0 95.29 4.40 -8 0 0 95.79 4.60 -8 0 0 90.49 4.40 -8 0 0 94.29 4.40 -8 0 0 96.09 4.00 -8 0 0 103.29 4.60 -9 0 0 114.59 4.80 -9 0 0 112.69 4.70 -9 0 0 121.49 5.10 -10 0 0 17.20 1.10 -9 1 0 33.00 2.10 -9 1 0 38.50 2.20 -9 1 0 45.10 2.70 -9 1 0 44.20 2.10 -8 1 0 202.28 8.30 -8 1 0 198.48 8.20 -8 1 0 203.08 8.10 -8 1 0 218.18 8.00 -8 1 0 207.68 8.50 -7 1 0 3.30 0.90 -7 1 0 3.80 4.30 -7 1 0 -0.60 1.10 -7 1 0 1.60 0.70 -7 1 0 1.90 0.60 -7 1 0 1.00 0.80 -7 1 0 2.00 0.70 -7 1 0 1.50 0.90 6 -1 0 35.30 12.70 -6 1 0 29.30 2.10 -6 1 0 29.20 2.30 -6 1 0 29.60 2.50 -6 1 0 26.90 1.80 -6 1 0 30.20 1.90 -6 1 0 29.00 2.00 -6 1 0 28.40 3.80 -6 1 0 29.60 2.30 -6 1 0 31.20 2.30 5 -1 0 67.59 7.00 -5 1 0 59.09 3.20 -5 1 0 59.09 4.20 -5 1 0 62.59 3.00 -5 1 0 59.09 3.10 -5 1 0 59.99 3.40 -5 1 0 65.69 3.50 4 -1 0 68.29 5.70 4 -1 0 59.29 5.20 -4 1 0 62.09 3.70 -4 1 0 59.29 3.30 3 -1 0 2436.56 80.49 3 -1 0 2253.67 79.39 3 -1 0 2193.08 79.59 -3 1 0 2438.96 79.69 -3 1 0 2296.77 80.19 1 -1 0 639.34 21.90 1 -1 0 627.64 21.90 1 -1 0 660.63 22.40 -1 1 0 644.04 22.60 -1 1 0 676.13 21.90 -1 1 0 643.64 21.90 -1 1 0 578.54 22.10 -1 -1 0 1057.39 40.70 1 1 0 1282.57 40.60 1 1 0 1227.98 40.80 -2 -1 0 32.00 1.70 -2 -1 0 27.80 1.60 -3 -1 0 1.80 0.70 -3 -1 0 0.40 0.60 3 1 0 0.80 0.90 -4 -1 0 590.84 22.30 -4 -1 0 634.14 22.40 4 1 0 615.64 22.20 4 1 0 625.64 22.40 -5 -1 0 320.47 12.90 -5 -1 0 328.97 12.80 5 1 0 322.67 13.40 5 1 0 328.27 13.10 5 1 0 328.97 13.60 -6 -1 0 155.38 7.50 -6 -1 0 149.19 6.30 -6 -1 0 144.19 6.00 -6 -1 0 146.09 6.30 -6 -1 0 131.69 6.00 -6 -1 0 146.39 6.00 -6 -1 0 147.09 6.90 -6 -1 0 143.09 5.90 -6 -1 0 144.29 6.00 -6 -1 0 147.89 6.00 6 1 0 143.99 9.90 6 1 0 133.59 12.30 6 1 0 142.49 11.40 -7 -1 0 13.60 1.60 -7 -1 0 11.80 1.20 -7 -1 0 11.60 1.50 -7 -1 0 10.00 1.40 -7 -1 0 10.80 2.70 -7 -1 0 13.60 1.70 -7 -1 0 12.10 1.20 -7 -1 0 11.90 1.30 -7 -1 0 12.80 3.00 -7 -1 0 12.60 1.60 -8 -1 0 20.10 1.70 -8 -1 0 23.90 1.70 -8 -1 0 20.80 2.30 -8 -1 0 22.40 2.00 -8 -1 0 20.50 2.20 -8 -1 0 22.30 2.00 -9 -1 0 222.78 8.60 -9 -1 0 237.18 9.10 -9 -1 0 236.78 9.00 -9 -1 0 231.58 8.90 -9 -1 0 219.48 8.40 -10 -1 0 59.19 2.60 -10 -1 0 55.59 2.60 -10 -1 0 56.29 2.80 -9 2 0 134.99 5.10 -9 2 0 122.19 4.80 -9 2 0 115.49 5.90 -8 2 0 95.59 4.30 -8 2 0 96.99 4.80 -8 2 0 109.59 4.90 -8 2 0 107.49 4.70 -8 2 0 110.19 4.40 -7 2 0 46.10 4.20 -7 2 0 53.19 2.90 -7 2 0 58.19 3.70 -7 2 0 54.19 3.50 -7 2 0 64.09 8.30 -6 2 0 142.29 6.50 -6 2 0 148.89 5.90 -6 2 0 133.89 5.90 -6 2 0 142.49 6.20 -6 2 0 142.09 6.00 -6 2 0 138.49 6.30 -6 2 0 142.99 8.30 5 -2 0 29.90 2.10 5 -2 0 29.10 7.90 -5 2 0 33.80 2.50 -5 2 0 32.50 2.20 -5 2 0 34.80 2.40 -5 2 0 31.90 3.70 -5 2 0 38.00 2.20 4 -2 0 107.99 8.40 4 -2 0 102.09 3.90 -4 2 0 100.39 4.20 -4 2 0 101.49 4.60 -4 2 0 90.29 5.20 -4 2 0 101.29 4.80 3 -2 0 1056.79 37.10 3 -2 0 1015.30 35.80 -3 2 0 1012.80 36.50 2 -2 0 1614.84 53.99 2 -2 0 1572.64 52.99 -2 2 0 1442.66 53.49 1 -2 0 3362.46 112.69 1 -2 0 3385.56 112.19 -1 2 0 3389.56 111.99 -1 2 0 2936.11 111.89 -1 2 0 3343.17 112.69 0 -2 0 992.60 34.40 0 -2 0 995.30 34.80 0 2 0 986.00 34.80 0 2 0 1011.70 34.40 0 2 0 1019.00 34.70 -1 -2 0 255.87 9.20 1 2 0 257.97 9.30 1 2 0 257.67 9.30 -2 -2 0 1654.23 56.99 2 2 0 1688.33 56.89 2 2 0 1611.54 56.49 -3 -2 0 124.69 5.30 -3 -2 0 132.99 5.60 3 2 0 136.89 5.70 3 2 0 128.59 5.00 -4 -2 0 478.05 18.00 4 2 0 505.25 17.60 4 2 0 497.25 18.30 4 2 0 486.35 18.40 -5 -2 0 662.83 23.90 -5 -2 0 641.44 23.70 5 2 0 581.44 23.10 5 2 0 679.23 29.40 5 2 0 678.93 24.30 -6 -2 0 31.00 2.10 -6 -2 0 41.50 4.40 -6 -2 0 31.40 2.30 -6 -2 0 31.40 2.00 -6 -2 0 32.70 2.40 -6 -2 0 34.20 2.20 -6 -2 0 24.80 3.20 -6 -2 0 32.00 2.20 -6 -2 0 30.10 2.30 -6 -2 0 31.00 2.10 6 2 0 30.10 5.70 6 2 0 33.60 6.00 -7 -2 0 85.39 4.00 -7 -2 0 84.69 4.00 -7 -2 0 86.89 4.10 -7 -2 0 87.19 4.10 -7 -2 0 88.09 4.20 -7 -2 0 85.79 4.40 -7 -2 0 95.99 5.80 7 2 0 81.09 13.10 -8 -2 0 61.19 3.10 -8 -2 0 62.29 3.10 -8 -2 0 62.99 3.10 -8 -2 0 63.19 3.20 -8 -2 0 64.09 3.50 -8 -2 0 66.19 6.30 -8 -2 0 62.99 3.30 -8 -2 0 57.79 3.20 -8 -2 0 56.99 3.40 -9 -2 0 69.69 3.10 -9 -2 0 70.79 3.50 -9 -2 0 68.49 3.20 -9 -2 0 68.99 3.40 -9 -2 0 71.09 3.50 -9 -2 0 71.09 3.20 -9 -2 0 64.19 3.60 -10 -2 0 15.40 1.30 -10 -2 0 15.70 1.30 -10 -2 0 13.80 1.10 -10 -2 0 15.90 1.40 -8 3 0 79.49 3.90 -8 3 0 82.59 3.70 -8 3 0 70.29 3.50 7 -3 0 2.90 1.60 -7 3 0 3.00 0.80 -7 3 0 0.80 0.80 -7 3 0 1.00 0.60 -7 3 0 1.20 0.60 -7 3 0 1.20 0.70 6 -3 0 5.00 1.30 -6 3 0 3.40 1.00 -6 3 0 3.20 0.90 -6 3 0 5.00 0.80 -6 3 0 4.70 1.20 -6 3 0 6.10 3.80 -6 3 0 4.10 1.00 -6 3 0 2.90 0.90 5 -3 0 1.30 0.90 5 -3 0 8.10 19.90 -5 3 0 1.20 0.80 -5 3 0 1.10 0.60 -5 3 0 -0.20 0.90 -5 3 0 2.50 1.50 -5 3 0 0.90 0.60 -5 3 0 3.90 2.20 4 -3 0 3.40 0.90 4 -3 0 4.20 5.10 -4 3 0 1.90 0.50 -4 3 0 1.70 0.70 -4 3 0 2.40 0.60 -4 3 0 2.00 1.70 3 -3 0 2141.29 72.19 3 -3 0 2060.19 72.99 3 -3 0 2194.68 74.69 -3 3 0 2050.39 73.69 -3 3 0 2122.99 72.39 2 -3 0 595.64 20.70 2 -3 0 622.24 22.60 2 -3 0 601.84 21.30 -2 3 0 575.34 21.70 1 -3 0 282.17 10.90 -1 3 0 333.77 11.30 -1 3 0 285.97 10.80 -1 3 0 285.27 12.20 0 -3 0 535.35 19.40 0 -3 0 518.35 18.90 0 3 0 554.14 18.70 0 3 0 515.85 19.50 0 3 0 540.85 19.20 -2 -3 0 2358.36 80.59 -2 -3 0 2415.56 80.19 -2 -3 0 2401.86 80.09 2 3 0 2345.07 80.49 2 3 0 2189.88 80.69 -3 -3 0 26.00 1.50 -3 -3 0 23.70 2.00 3 3 0 21.50 2.20 3 3 0 23.60 2.50 4 3 0 448.86 16.10 4 3 0 457.05 17.10 -5 -3 0 332.67 13.60 5 3 0 345.07 14.10 -6 -3 0 466.75 17.00 -6 -3 0 477.75 17.00 -6 -3 0 479.05 17.10 -6 -3 0 480.35 17.10 -6 -3 0 444.96 17.50 -6 -3 0 484.95 18.60 -6 -3 0 463.65 17.20 -6 -3 0 444.76 16.80 6 3 0 480.95 19.90 -7 -3 0 3.10 1.50 -7 -3 0 5.90 1.10 -7 -3 0 3.90 1.10 -7 -3 0 4.50 1.00 -7 -3 0 4.60 1.10 -7 -3 0 3.90 0.90 -7 -3 0 2.80 0.80 -7 -3 0 3.80 0.80 -7 -3 0 4.40 2.20 7 3 0 6.20 11.90 7 3 0 -6.20 10.30 -8 -3 0 100.19 4.70 -8 -3 0 96.09 4.40 -8 -3 0 114.19 7.10 -8 -3 0 100.19 4.40 -8 -3 0 96.49 4.40 -8 -3 0 94.89 4.40 -8 -3 0 96.09 4.90 -8 -3 0 87.39 4.30 -9 -3 0 55.69 2.70 -9 -3 0 60.69 2.90 -9 -3 0 53.29 2.80 -9 -3 0 55.69 3.00 -9 -3 0 58.29 3.10 -9 -3 0 60.99 3.20 -10 -3 0 18.40 1.40 -10 -3 0 16.50 1.40 -10 -3 0 18.80 1.20 -10 -3 0 16.10 1.20 -10 -3 0 12.50 1.50 -8 4 0 59.49 2.70 -8 4 0 48.30 2.40 -8 4 0 48.50 2.40 -8 4 0 54.49 2.30 7 -4 0 2.60 1.90 -7 4 0 0.80 0.60 -7 4 0 0.80 0.70 6 -4 0 2.10 1.30 -6 4 0 1.80 0.60 -6 4 0 6.40 5.80 -6 4 0 1.80 0.80 -6 4 0 2.50 0.90 -6 4 0 0.70 0.90 5 -4 0 172.88 7.00 -5 4 0 167.68 7.40 -5 4 0 165.98 7.10 -5 4 0 154.68 6.50 -5 4 0 154.18 6.60 -5 4 0 159.38 6.90 -5 4 0 165.58 6.50 -5 4 0 156.88 9.20 4 -4 0 158.58 6.30 4 -4 0 151.68 16.80 -4 4 0 144.09 5.50 -4 4 0 147.39 7.90 -4 4 0 149.59 6.00 -4 4 0 148.39 6.30 -4 4 0 152.88 6.30 -4 4 0 156.48 6.90 -4 4 0 134.99 6.00 3 -4 0 1111.39 40.40 3 -4 0 1165.48 43.30 3 -4 0 1100.19 40.00 -3 4 0 1292.37 42.40 -3 4 0 1124.59 39.90 -3 4 0 1145.99 40.40 -3 4 0 1246.38 41.60 -3 4 0 1111.09 41.80 2 -4 0 159.38 8.90 2 -4 0 161.98 6.00 2 -4 0 157.78 6.20 2 -4 0 153.68 8.70 -2 4 0 154.48 7.10 -2 4 0 162.78 6.00 1 -4 0 368.76 13.30 1 -4 0 363.26 14.80 1 -4 0 362.76 13.00 1 -4 0 383.36 14.40 -1 4 0 345.07 13.40 -1 4 0 381.36 13.80 0 -4 0 56.39 2.60 0 -4 0 55.59 4.00 0 -4 0 47.70 4.40 0 -4 0 55.49 2.40 0 4 0 58.49 2.90 0 4 0 52.19 2.40 0 4 0 56.29 4.30 -1 -4 0 1176.78 40.70 -1 -4 0 1128.19 40.70 -1 -4 0 1161.48 39.90 -1 -4 0 1174.88 40.20 1 4 0 1134.29 41.00 1 4 0 1162.78 40.20 -2 -4 0 351.26 13.00 -2 -4 0 346.67 12.50 -2 -4 0 343.97 12.90 -2 -4 0 330.97 14.00 2 4 0 334.77 13.30 2 4 0 383.16 15.30 2 4 0 346.17 13.00 -3 -4 0 1041.30 36.90 3 4 0 1037.20 36.40 -4 -4 0 31.40 2.70 4 4 0 33.10 3.70 4 4 0 36.30 4.00 -5 -4 0 268.57 10.10 -5 -4 0 266.57 11.40 -5 -4 0 265.77 10.10 -5 -4 0 278.87 10.20 -5 -4 0 259.07 10.30 5 4 0 273.27 10.70 5 4 0 272.07 12.20 -6 -4 0 830.72 30.60 -6 -4 0 832.22 29.00 -6 -4 0 853.41 29.00 -6 -4 0 751.42 28.60 -6 -4 0 825.72 29.00 -6 -4 0 792.62 29.60 -6 -4 0 828.12 29.10 -6 -4 0 834.82 29.30 6 4 0 830.52 31.50 -7 -4 0 108.29 5.40 -7 -4 0 112.59 4.90 -7 -4 0 115.89 6.90 -7 -4 0 112.39 5.20 -7 -4 0 112.69 5.00 -7 -4 0 105.59 4.80 -7 -4 0 112.49 4.90 -7 -4 0 113.79 5.00 7 4 0 90.89 12.90 -8 -4 0 43.70 2.70 -8 -4 0 45.50 2.60 -8 -4 0 43.30 2.90 -8 -4 0 47.40 2.60 -8 -4 0 46.00 5.50 -8 -4 0 43.40 2.50 -8 -4 0 45.10 2.70 -8 -4 0 39.00 2.90 8 4 0 46.20 3.80 -9 -4 0 7.10 1.00 -9 -4 0 8.30 1.20 -9 -4 0 7.80 1.20 -9 -4 0 8.00 1.00 -9 -4 0 8.80 1.10 -9 -4 0 8.90 1.30 -10 -4 0 46.80 2.50 -10 -4 0 49.20 2.50 -10 -4 0 49.20 2.40 -10 -4 0 49.40 2.30 -10 -4 0 41.90 2.20 7 -5 0 1.60 1.80 -7 5 0 1.50 0.70 -7 5 0 -0.70 0.60 -7 5 0 1.40 0.50 -7 5 0 0.80 0.50 6 -5 0 60.19 4.10 -6 5 0 63.59 3.50 -6 5 0 59.09 2.90 -6 5 0 60.49 3.30 -6 5 0 63.39 3.40 5 -5 0 423.96 15.30 -5 5 0 390.36 14.30 -5 5 0 369.06 14.30 -5 5 0 398.46 15.00 -5 5 0 389.66 15.30 -5 5 0 387.56 17.70 -5 5 0 393.36 14.70 4 -5 0 316.17 11.40 4 -5 0 276.97 10.70 -4 5 0 285.07 13.00 -4 5 0 260.37 10.50 -4 5 0 281.97 11.00 -4 5 0 297.47 10.70 -4 5 0 268.87 10.10 -4 5 0 291.77 11.70 3 -5 0 702.43 30.40 3 -5 0 779.52 25.20 3 -5 0 682.13 24.40 -3 5 0 693.93 26.40 -3 5 0 680.73 24.80 -3 5 0 658.23 24.60 -3 5 0 692.33 24.20 -3 5 0 689.13 25.50 -3 5 0 681.23 24.50 2 -5 0 0.70 0.90 2 -5 0 -0.30 4.00 2 -5 0 1.10 0.70 -2 5 0 1.50 0.70 -2 5 0 2.10 0.50 -2 5 0 0.80 0.30 -2 5 0 1.70 1.20 1 -5 0 214.08 8.20 1 -5 0 237.28 8.70 1 -5 0 219.78 8.40 1 -5 0 222.88 11.20 -1 5 0 213.28 8.10 -1 5 0 211.58 8.90 -1 5 0 225.78 10.70 0 -5 0 6.40 2.40 0 -5 0 7.20 0.90 0 5 0 6.50 1.50 0 5 0 8.10 0.90 0 5 0 7.90 0.90 0 5 0 7.70 4.30 -1 -5 0 99.89 5.90 -1 -5 0 99.09 4.10 -1 -5 0 99.89 4.10 -1 -5 0 96.19 4.40 1 5 0 97.49 3.90 1 5 0 101.29 4.70 -2 -5 0 98.19 4.20 -2 -5 0 99.99 4.80 -2 -5 0 105.49 4.40 -2 -5 0 102.89 5.60 2 5 0 94.99 7.70 2 5 0 106.49 5.10 -3 -5 0 22.80 2.30 -3 -5 0 22.20 2.50 3 5 0 24.30 1.90 3 5 0 21.30 4.00 3 5 0 26.50 3.20 -4 -5 0 900.01 33.90 -4 -5 0 932.21 32.90 4 5 0 956.80 34.00 4 5 0 949.40 33.20 4 5 0 950.30 33.50 -5 -5 0 111.59 5.20 -5 -5 0 121.79 5.00 -5 -5 0 118.79 5.20 -5 -5 0 113.49 4.50 -5 -5 0 116.89 6.30 5 5 0 117.29 5.40 5 5 0 119.89 7.90 -6 -5 0 171.58 6.80 -6 -5 0 157.68 6.00 -6 -5 0 166.58 6.70 -6 -5 0 167.28 6.80 -6 -5 0 169.28 8.40 -6 -5 0 162.68 6.80 -6 -5 0 160.08 6.80 6 5 0 166.98 7.20 6 5 0 168.78 11.90 -7 -5 0 86.89 4.20 -7 -5 0 91.59 4.20 -7 -5 0 91.29 4.20 -7 -5 0 90.99 4.20 -7 -5 0 90.29 6.20 -7 -5 0 90.39 4.40 -7 -5 0 86.29 4.80 -7 -5 0 82.79 5.80 7 5 0 86.29 4.70 -8 -5 0 9.70 3.30 -8 -5 0 7.70 1.10 -8 -5 0 5.10 1.00 -8 -5 0 5.20 0.90 -8 -5 0 7.40 1.20 -8 -5 0 6.40 1.00 -8 -5 0 5.20 1.10 8 5 0 6.20 1.90 8 5 0 6.90 1.80 -9 -5 0 33.80 2.10 -9 -5 0 35.60 2.10 -9 -5 0 32.60 1.90 -9 -5 0 35.30 2.10 -9 -5 0 35.40 2.50 -9 -5 0 36.30 2.30 -10 -5 0 109.09 4.70 -10 -5 0 109.79 4.70 -10 -5 0 112.39 4.40 -10 -5 0 106.39 4.30 -10 -5 0 101.19 4.30 -7 6 0 1.00 0.40 -7 6 0 0.90 0.40 -7 6 0 0.80 0.50 -6 6 0 129.19 5.20 -6 6 0 131.19 5.70 -6 6 0 131.69 5.70 -6 6 0 130.99 5.60 5 -6 0 15.20 1.50 5 -6 0 14.50 2.50 -5 6 0 17.50 1.70 -5 6 0 11.20 1.60 -5 6 0 20.50 10.60 -5 6 0 17.40 1.60 -5 6 0 15.60 1.30 4 -6 0 14.10 1.50 4 -6 0 18.90 2.40 -4 6 0 17.10 1.50 -4 6 0 15.20 1.90 -4 6 0 14.50 1.90 -4 6 0 16.60 4.10 -4 6 0 18.20 1.80 -4 6 0 16.00 1.00 3 -6 0 239.98 9.70 3 -6 0 220.68 8.60 -3 6 0 207.08 10.60 -3 6 0 223.98 8.50 -3 6 0 225.48 9.50 -3 6 0 218.98 8.20 -3 6 0 234.68 9.10 2 -6 0 16.20 7.30 2 -6 0 19.80 2.10 2 -6 0 18.20 1.50 2 -6 0 19.90 2.30 -2 6 0 17.60 1.30 -2 6 0 17.90 1.20 -2 6 0 19.50 1.80 -2 6 0 18.20 2.70 -2 6 0 16.60 1.80 -2 6 0 17.40 1.30 1 -6 0 50.29 2.80 1 -6 0 51.99 3.30 1 -6 0 49.60 2.50 1 -6 0 43.40 6.10 1 -6 0 49.99 2.70 -1 6 0 51.49 2.40 -1 6 0 44.10 3.50 -1 6 0 48.20 2.30 -1 6 0 53.29 2.70 -1 6 0 52.39 2.60 -1 6 0 47.60 2.30 0 -6 0 79.69 3.60 0 -6 0 82.09 8.30 0 -6 0 84.69 3.70 0 -6 0 73.29 4.20 0 -6 0 80.49 3.50 0 6 0 78.89 3.40 0 6 0 82.49 3.50 0 6 0 83.19 4.90 0 6 0 81.99 3.50 0 6 0 84.09 3.50 0 6 0 84.89 3.80 -1 -6 0 203.98 7.90 -1 -6 0 211.38 8.30 -1 -6 0 208.68 10.50 -1 -6 0 213.18 8.00 1 6 0 217.08 8.80 1 6 0 204.78 7.70 1 6 0 194.18 7.90 1 6 0 203.68 8.00 -2 -6 0 3.00 0.70 -2 -6 0 1.90 0.60 -2 -6 0 1.00 1.40 -2 -6 0 2.80 3.00 -2 -6 0 0.30 1.20 2 6 0 1.80 0.60 2 6 0 2.20 0.80 2 6 0 2.30 1.90 -3 -6 0 0.60 3.20 -3 -6 0 3.00 1.50 -3 -6 0 0.50 0.60 -3 -6 0 2.70 0.60 -3 -6 0 0.40 1.10 -3 -6 0 0.60 0.70 -3 -6 0 1.70 1.40 3 6 0 0.90 0.60 3 6 0 0.20 0.70 3 6 0 3.10 2.50 -4 -6 0 13.40 1.40 -4 -6 0 15.50 1.50 -4 -6 0 9.70 2.00 -4 -6 0 18.70 1.40 4 6 0 11.90 3.00 4 6 0 14.70 1.60 -5 -6 0 3.60 1.20 -5 -6 0 3.70 0.60 -5 -6 0 2.50 0.90 -5 -6 0 3.70 0.90 -5 -6 0 3.10 0.90 5 6 0 5.90 1.00 5 6 0 2.40 1.00 5 6 0 3.60 3.90 -6 -6 0 256.17 10.00 -6 -6 0 255.37 11.70 -6 -6 0 260.77 10.00 6 6 0 251.67 14.90 6 6 0 253.17 9.70 6 6 0 273.17 10.60 -7 -6 0 50.29 3.50 -7 -6 0 53.09 2.90 -7 -6 0 50.99 2.90 -7 -6 0 50.79 2.90 -7 -6 0 53.69 3.10 -7 -6 0 54.79 2.90 -7 -6 0 46.00 3.30 -7 -6 0 50.69 5.30 -8 -6 0 35.00 4.70 -8 -6 0 40.80 2.50 8 6 0 45.60 3.30 8 6 0 48.50 3.20 -9 -6 0 1.20 0.80 -9 -6 0 0.40 0.50 -9 -6 0 0.90 0.50 -9 -6 0 0.70 0.90 -9 -6 0 1.00 0.50 -9 -6 0 0.30 0.60 9 6 0 2.90 2.40 9 6 0 1.40 1.30 -10 -6 0 42.20 2.30 -10 -6 0 42.40 2.70 -10 -6 0 43.90 2.40 -10 -6 0 43.90 2.10 -10 -6 0 40.90 2.10 6 -7 0 81.09 4.90 -6 7 0 102.89 4.10 -6 7 0 94.69 3.80 -6 7 0 100.19 4.10 5 -7 0 5.00 0.80 5 -7 0 2.10 1.60 -5 7 0 5.50 1.00 -5 7 0 3.30 0.60 -5 7 0 4.90 0.90 -5 7 0 3.40 0.90 4 -7 0 40.90 3.90 4 -7 0 52.99 2.60 -4 7 0 46.50 2.90 -4 7 0 55.99 3.10 -4 7 0 53.49 2.10 -4 7 0 54.79 3.00 -4 7 0 52.09 2.60 -4 7 0 51.59 3.20 -4 7 0 64.59 7.80 3 -7 0 29.40 1.80 3 -7 0 28.90 3.00 -3 7 0 27.40 2.10 -3 7 0 27.60 4.80 -3 7 0 28.30 2.30 -3 7 0 29.70 1.80 -3 7 0 28.80 1.50 2 -7 0 515.05 21.30 2 -7 0 522.05 19.20 -2 7 0 544.05 19.00 -2 7 0 551.34 19.20 -2 7 0 553.24 19.60 -2 7 0 555.64 20.20 -2 7 0 527.65 21.40 1 -7 0 44.00 10.30 1 -7 0 41.40 2.20 1 -7 0 38.80 2.80 1 -7 0 35.40 3.20 1 -7 0 41.40 2.70 -1 7 0 39.90 2.80 -1 7 0 41.40 2.20 -1 7 0 44.00 2.60 -1 7 0 40.30 3.70 -1 7 0 38.50 2.00 -1 7 0 42.20 2.20 -1 7 0 39.30 2.00 0 -7 0 57.49 2.80 0 -7 0 61.59 8.30 0 -7 0 59.79 3.20 0 7 0 58.99 3.70 0 7 0 59.99 2.70 0 7 0 59.49 2.70 0 7 0 64.49 3.00 0 7 0 61.79 2.80 0 7 0 63.09 2.90 0 7 0 59.39 2.70 0 7 0 66.29 6.00 -1 -7 0 90.49 10.70 -1 -7 0 88.79 3.80 -1 -7 0 91.59 4.60 -1 -7 0 87.69 4.00 -1 -7 0 91.89 4.20 1 7 0 93.29 3.90 1 7 0 93.69 4.00 1 7 0 88.09 4.10 1 7 0 92.29 3.80 1 7 0 96.69 6.00 1 7 0 90.69 3.80 1 7 0 92.19 4.10 -2 -7 0 140.29 5.90 -2 -7 0 139.49 6.70 -2 -7 0 141.19 5.60 -2 -7 0 124.69 6.20 -2 -7 0 134.29 5.40 -2 -7 0 121.19 5.90 -2 -7 0 147.59 5.70 -2 -7 0 150.18 11.00 2 7 0 140.89 5.40 2 7 0 145.59 7.70 2 7 0 138.89 5.90 2 7 0 138.49 6.00 2 7 0 141.39 5.50 2 7 0 142.69 5.50 -3 -7 0 202.88 8.10 -3 -7 0 209.88 7.80 -3 -7 0 192.58 7.60 -3 -7 0 177.28 8.00 -3 -7 0 205.98 9.10 -3 -7 0 228.48 12.60 -3 -7 0 207.38 8.20 -3 -7 0 219.48 8.10 3 7 0 208.18 8.50 3 7 0 204.48 7.60 3 7 0 202.58 10.00 3 7 0 215.08 7.90 -4 -7 0 11.10 1.30 -4 -7 0 15.60 1.40 -4 -7 0 14.20 2.70 -4 -7 0 12.70 1.50 -4 -7 0 14.90 1.40 -4 -7 0 11.50 1.40 -4 -7 0 14.90 1.20 4 7 0 10.90 4.50 4 7 0 14.10 1.60 4 7 0 14.50 1.30 -5 -7 0 50.29 2.50 -5 -7 0 48.40 4.60 -5 -7 0 42.50 2.50 -5 -7 0 47.60 2.60 -5 -7 0 43.70 2.20 -5 -7 0 45.40 2.80 5 7 0 48.20 2.50 5 7 0 46.60 3.00 5 7 0 34.00 5.80 -6 -7 0 15.50 1.20 -6 -7 0 14.10 2.20 -6 -7 0 16.50 1.60 -6 -7 0 17.30 1.60 -6 -7 0 10.30 2.70 -6 -7 0 15.30 1.50 -6 -7 0 18.10 1.70 6 7 0 17.90 2.00 -7 -7 0 32.30 2.10 -7 -7 0 27.20 2.30 -7 -7 0 31.30 2.90 -7 -7 0 33.70 2.30 -7 -7 0 32.60 2.20 -7 -7 0 25.10 3.10 -7 -7 0 31.00 2.00 -7 -7 0 30.30 1.50 -7 -7 0 28.60 4.20 7 7 0 27.20 2.00 7 7 0 28.80 2.50 -8 -7 0 74.39 3.90 -8 -7 0 92.69 4.10 -8 -7 0 92.89 4.10 -8 -7 0 93.99 5.00 -8 -7 0 83.59 7.50 -8 -7 0 93.89 4.10 8 7 0 91.49 4.80 8 7 0 90.39 4.60 -9 -7 0 2.90 0.70 -9 -7 0 1.10 0.60 -9 -7 0 2.40 0.60 -9 -7 0 2.30 0.70 -9 -7 0 2.10 0.60 9 7 0 2.90 1.10 9 7 0 4.40 2.00 -10 -7 0 84.09 3.50 -10 -7 0 89.89 3.90 -10 -7 0 87.29 3.90 -10 -7 0 80.09 3.60 -10 -7 0 88.59 3.60 5 -8 0 2.10 1.50 5 -8 0 0.50 0.60 -5 8 0 0.20 0.40 -5 8 0 -0.30 0.40 -5 8 0 0.40 0.40 4 -8 0 2.60 1.90 -4 8 0 1.70 0.50 -4 8 0 2.80 0.70 -4 8 0 2.00 0.70 3 -8 0 72.39 3.30 -3 8 0 69.99 3.30 -3 8 0 70.79 3.70 -3 8 0 69.69 2.90 -3 8 0 69.89 3.50 -3 8 0 77.49 8.10 2 -8 0 17.50 1.40 -2 8 0 17.80 1.40 -2 8 0 14.90 1.10 -2 8 0 14.60 3.90 -2 8 0 14.90 1.70 -2 8 0 15.50 1.60 1 -8 0 113.49 4.80 1 -8 0 98.89 5.60 1 -8 0 109.89 5.20 -1 8 0 124.09 4.80 -1 8 0 116.89 7.00 -1 8 0 109.69 4.30 -1 8 0 110.59 5.30 -1 8 0 115.29 4.60 0 -8 0 6.70 1.10 0 -8 0 7.40 1.00 0 -8 0 8.10 1.40 0 -8 0 6.80 1.50 0 -8 0 3.40 1.60 0 8 0 5.20 0.80 0 8 0 7.20 1.10 0 8 0 7.50 0.80 0 8 0 7.20 0.80 0 8 0 6.90 1.50 -1 -8 0 17.10 2.00 -1 -8 0 15.30 1.50 -1 -8 0 16.10 1.80 -1 -8 0 26.30 11.30 1 8 0 15.50 1.30 1 8 0 18.30 1.30 1 8 0 12.90 5.40 1 8 0 16.80 1.30 1 8 0 19.00 1.50 1 8 0 16.50 1.70 -2 -8 0 41.70 2.70 -2 -8 0 43.10 2.60 -2 -8 0 44.80 9.50 -2 -8 0 42.60 2.30 -2 -8 0 40.40 2.90 -2 -8 0 42.20 2.20 -2 -8 0 36.50 3.00 2 8 0 39.30 5.60 2 8 0 39.50 2.20 2 8 0 40.50 2.10 2 8 0 43.50 2.20 2 8 0 42.50 2.60 2 8 0 43.90 2.60 -3 -8 0 51.89 10.90 -3 -8 0 50.29 2.90 -3 -8 0 49.60 2.40 -3 -8 0 55.79 2.80 -3 -8 0 47.50 5.10 -3 -8 0 50.89 3.10 -3 -8 0 54.19 2.70 -3 -8 0 50.19 2.90 -3 -8 0 47.80 3.20 3 8 0 30.30 7.90 3 8 0 52.79 3.10 3 8 0 47.90 2.50 3 8 0 51.29 2.60 3 8 0 53.49 2.60 3 8 0 54.59 3.20 -4 -8 0 19.40 1.90 -4 -8 0 17.60 1.40 -4 -8 0 15.10 1.50 -4 -8 0 17.50 3.30 -4 -8 0 17.50 1.40 -4 -8 0 16.60 1.60 4 8 0 19.20 6.40 4 8 0 18.20 1.70 4 8 0 18.50 1.80 4 8 0 15.60 2.00 4 8 0 16.10 1.80 -5 -8 0 81.79 3.50 -5 -8 0 78.79 3.70 -5 -8 0 81.79 3.90 -5 -8 0 79.89 4.10 -5 -8 0 72.49 6.10 5 8 0 79.69 4.30 5 8 0 84.19 3.70 -6 -8 0 32.50 2.10 -6 -8 0 34.20 1.80 -6 -8 0 33.20 2.20 -6 -8 0 36.40 4.60 -6 -8 0 34.00 2.40 -6 -8 0 36.00 2.10 6 8 0 33.20 2.60 6 8 0 32.40 2.00 6 8 0 32.80 2.70 -7 -8 0 77.99 7.20 -7 -8 0 77.39 3.70 -7 -8 0 75.69 3.60 -7 -8 0 78.79 4.10 -7 -8 0 78.79 3.80 7 8 0 74.09 4.20 7 8 0 77.49 4.30 -8 -8 0 57.69 3.80 -8 -8 0 59.09 3.20 -8 -8 0 61.19 2.90 -8 -8 0 55.89 2.90 -8 -8 0 59.49 2.90 -8 -8 0 43.80 7.40 8 8 0 62.29 3.70 8 8 0 55.09 2.70 -9 -8 0 25.60 1.80 -9 -8 0 23.90 1.60 -9 -8 0 26.00 2.10 -9 -8 0 26.30 1.60 9 8 0 24.60 1.70 9 8 0 22.40 1.90 9 8 0 23.50 2.80 -10 -8 0 7.10 0.80 -10 -8 0 8.30 0.80 -10 -8 0 7.50 0.90 -10 -8 0 7.10 1.00 10 8 0 5.30 1.40 4 -9 0 10.30 1.80 4 -9 0 13.30 1.00 -4 9 0 14.00 1.10 -4 9 0 10.10 1.20 -4 9 0 12.80 1.00 3 -9 0 64.69 4.80 3 -9 0 64.09 2.80 -3 9 0 60.39 2.80 -3 9 0 63.69 2.50 -3 9 0 63.59 3.20 -3 9 0 60.69 3.10 2 -9 0 67.69 5.40 2 -9 0 77.89 3.50 -2 9 0 76.69 3.20 -2 9 0 79.19 3.50 -2 9 0 79.69 3.80 1 -9 0 24.70 3.90 -1 9 0 25.90 1.70 -1 9 0 26.20 2.00 -1 9 0 18.70 4.30 -1 9 0 25.10 1.70 0 -9 0 12.90 1.80 0 -9 0 10.00 2.20 0 -9 0 14.10 1.30 0 -9 0 16.40 2.30 0 -9 0 14.00 1.50 0 9 0 14.20 1.10 0 9 0 15.50 3.00 0 9 0 14.60 1.10 0 9 0 15.90 1.40 -1 -9 0 14.90 1.30 -1 -9 0 12.10 1.80 -1 -9 0 10.90 1.50 -1 -9 0 16.30 2.80 -1 -9 0 12.20 1.40 -1 -9 0 17.20 2.30 1 9 0 14.40 1.70 1 9 0 11.10 1.20 1 9 0 13.40 1.10 1 9 0 13.10 1.10 -2 -9 0 78.59 3.70 -2 -9 0 79.89 4.20 -2 -9 0 80.09 4.40 -2 -9 0 79.89 3.50 2 9 0 83.19 3.60 2 9 0 77.59 3.90 2 9 0 78.09 4.00 2 9 0 76.69 3.80 -3 -9 0 116.79 5.50 -3 -9 0 110.79 5.50 -3 -9 0 114.59 4.70 -3 -9 0 120.59 5.00 3 9 0 112.69 5.30 3 9 0 120.19 4.90 3 9 0 119.99 4.90 3 9 0 108.69 5.70 3 9 0 114.99 4.70 -4 -9 0 59.09 3.00 -4 -9 0 56.29 2.80 -4 -9 0 58.49 2.90 -4 -9 0 61.49 3.20 -4 -9 0 59.39 7.40 4 9 0 64.19 3.60 4 9 0 57.39 2.90 4 9 0 61.69 3.50 4 9 0 61.79 3.00 -5 -9 0 25.30 1.80 -5 -9 0 22.30 1.70 -5 -9 0 22.10 1.90 -5 -9 0 20.80 1.40 5 9 0 21.10 2.10 5 9 0 22.20 2.00 5 9 0 21.30 1.50 -6 -9 0 64.49 2.90 -6 -9 0 62.39 3.30 -6 -9 0 60.99 7.80 -6 -9 0 62.69 3.50 -6 -9 0 67.69 3.10 6 9 0 63.59 3.80 6 9 0 63.69 3.80 6 9 0 63.59 3.00 -7 -9 0 148.79 6.40 -7 -9 0 145.69 5.90 -7 -9 0 150.28 10.90 -7 -9 0 141.69 5.80 -7 -9 0 150.28 5.60 -7 -9 0 146.79 6.10 7 9 0 139.89 5.70 7 9 0 145.19 6.60 7 9 0 147.89 6.70 -8 -9 0 2.10 0.70 -8 -9 0 0.70 0.70 -8 -9 0 1.30 0.50 -8 -9 0 1.10 0.50 -8 -9 0 1.80 0.70 8 9 0 -0.70 1.30 8 9 0 2.60 0.60 8 9 0 0.20 0.70 -9 -9 0 6.30 0.90 -9 -9 0 6.50 1.20 -9 -9 0 6.80 0.90 -9 -9 0 5.70 0.80 -9 -9 0 5.40 0.70 9 9 0 6.90 1.30 9 9 0 7.30 1.60 9 9 0 8.00 1.00 -10 -9 0 1.90 0.60 -10 -9 0 2.00 0.50 -10 -9 0 1.50 0.40 -10 -9 0 1.80 0.50 3 -10 0 3.10 1.00 3 -10 0 2.80 0.90 3 -10 0 2.00 0.40 -3 10 0 2.40 0.50 2 -10 0 37.80 2.70 2 -10 0 43.20 3.20 2 -10 0 43.60 2.60 -2 10 0 40.80 1.90 1 -10 0 4.50 1.60 1 -10 0 4.60 1.20 0 -10 0 11.50 1.80 0 -10 0 17.00 1.30 0 -10 0 16.50 2.60 0 -10 0 18.00 1.70 0 10 0 14.80 1.00 0 10 0 11.40 4.50 0 10 0 15.80 1.10 -1 -10 0 -0.20 1.10 -1 -10 0 1.90 0.70 -1 -10 0 -1.10 1.30 -1 -10 0 1.80 0.50 1 10 0 1.70 0.40 1 10 0 1.80 0.50 1 10 0 2.90 2.80 -2 -10 0 40.40 2.30 -2 -10 0 43.20 3.10 2 10 0 40.90 2.80 2 10 0 40.60 2.20 2 10 0 40.40 2.20 2 10 0 42.00 2.20 -3 -10 0 5.40 2.20 -3 -10 0 9.20 1.10 -3 -10 0 9.90 1.00 3 10 0 9.20 1.10 3 10 0 7.40 1.30 3 10 0 8.90 1.50 3 10 0 9.30 1.00 3 10 0 9.60 1.00 -4 -10 0 156.38 6.40 -4 -10 0 153.58 6.30 4 10 0 153.68 6.70 4 10 0 160.28 6.90 4 10 0 152.28 6.30 4 10 0 153.78 6.40 4 10 0 164.58 6.70 -5 -10 0 16.40 1.70 -5 -10 0 19.20 1.80 -5 -10 0 19.00 1.30 5 10 0 17.10 2.00 5 10 0 20.30 1.90 5 10 0 20.30 1.40 -6 -10 0 37.00 2.10 -6 -10 0 39.20 2.50 -6 -10 0 37.80 2.30 6 10 0 38.00 2.00 6 10 0 40.20 2.80 6 10 0 36.20 2.60 -7 -10 0 64.79 3.30 -7 -10 0 63.19 3.10 -7 -10 0 69.39 2.80 -7 -10 0 62.39 2.90 -7 -10 0 62.69 2.90 7 10 0 64.69 2.90 7 10 0 64.99 3.50 7 10 0 61.99 3.60 -8 -10 0 10.00 2.10 -8 -10 0 12.80 1.20 -8 -10 0 12.10 1.10 -8 -10 0 9.00 1.00 8 10 0 11.80 1.30 8 10 0 10.70 0.90 8 10 0 11.30 1.10 8 10 0 10.70 1.60 -9 -10 0 4.10 0.60 -9 -10 0 3.70 0.70 -9 -10 0 5.20 0.80 -9 -10 0 6.00 1.00 9 10 0 4.30 0.80 9 10 0 4.90 0.80 2 -11 0 26.20 1.90 2 -11 0 27.30 1.30 -2 11 0 27.80 1.50 -2 11 0 25.70 1.10 1 -11 0 39.40 1.90 1 -11 0 38.10 2.40 -1 11 0 38.50 1.70 0 -11 0 20.40 2.10 0 -11 0 24.30 1.70 0 -11 0 21.30 1.30 0 11 0 22.90 1.30 -1 -11 0 10.40 1.60 -1 -11 0 11.70 1.20 -1 -11 0 10.50 1.00 1 11 0 13.30 1.20 1 11 0 11.20 0.90 -2 -11 0 0.50 1.80 -2 -11 0 0.00 0.40 -2 -11 0 0.90 0.40 2 11 0 0.40 0.30 2 11 0 -0.10 0.30 -3 -11 0 0.20 0.30 -3 -11 0 0.20 0.40 3 11 0 -1.90 1.90 3 11 0 -0.10 0.30 3 11 0 0.10 0.30 3 11 0 -0.50 0.60 -4 -11 0 10.40 1.60 -4 -11 0 8.40 0.90 4 11 0 7.20 1.40 4 11 0 9.50 1.60 4 11 0 8.70 0.90 4 11 0 8.20 1.00 4 11 0 9.70 1.00 -5 -11 0 24.30 1.90 -5 -11 0 25.70 1.50 5 11 0 25.20 1.50 5 11 0 25.80 1.90 5 11 0 25.10 1.60 5 11 0 24.80 2.10 -6 -11 0 6.90 1.00 -6 -11 0 7.80 0.80 6 11 0 6.30 1.10 6 11 0 7.10 1.20 6 11 0 8.20 1.00 6 11 0 7.50 0.80 -7 -11 0 22.70 1.50 -7 -11 0 22.30 1.50 -7 -11 0 24.60 1.20 7 11 0 21.50 1.50 7 11 0 23.80 1.30 7 11 0 21.60 1.70 7 11 0 20.90 2.10 -8 -11 0 8.10 1.20 -8 -11 0 6.70 0.90 -8 -11 0 7.90 1.10 8 11 0 7.50 1.10 8 11 0 7.10 0.90 0 -12 0 5.30 0.60 0 12 0 6.20 0.50 0 12 0 5.00 0.60 -1 -12 0 43.10 2.00 1 12 0 43.40 1.90 -2 -12 0 0.40 0.30 2 12 0 0.80 0.30 2 12 0 -0.10 0.30 -3 -12 0 6.50 0.80 3 12 0 7.40 0.60 3 12 0 6.90 0.70 4 12 0 12.30 1.30 4 12 0 13.40 1.00 4 12 0 11.30 1.20 -5 -12 0 6.40 0.70 5 12 0 6.20 1.00 5 12 0 7.20 1.50 5 12 0 6.50 0.60 -6 -12 0 2.20 0.40 6 12 0 0.50 1.20 6 12 0 2.50 0.40 6 12 0 2.50 1.30 6 12 0 1.80 0.60 -7 -12 0 7.00 1.10 7 12 0 6.70 0.90 7 12 0 7.40 1.30 7 12 0 5.70 0.50 -2 -13 0 5.80 0.80 2 13 0 6.40 0.50 -3 -13 0 -0.20 0.30 3 13 0 0.40 0.30 -4 -13 0 16.90 1.00 4 13 0 16.90 1.10 4 13 0 15.60 0.90 -5 -13 0 0.30 0.30 5 13 0 -0.10 0.30 -5 -13 1 2.10 0.40 4 13 -1 25.20 1.10 -4 -13 1 28.20 1.50 3 13 -1 0.10 0.30 -3 -13 1 0.10 0.30 7 12 -1 6.10 0.90 7 12 -1 5.00 0.50 -7 -12 1 4.70 1.00 6 12 -1 8.00 0.90 6 12 -1 8.80 0.70 -6 -12 1 7.90 0.70 5 12 -1 52.19 2.40 5 12 -1 52.39 2.20 -5 -12 1 49.10 2.30 4 12 -1 23.40 1.40 4 12 -1 25.60 1.30 4 12 -1 26.60 1.60 3 12 -1 1.40 0.30 3 12 -1 1.60 0.40 -3 -12 1 1.70 0.50 2 12 -1 -0.10 0.30 2 12 -1 0.60 0.30 -2 -12 1 0.10 0.40 -2 -12 1 0.60 0.40 1 12 -1 3.50 0.50 -1 -12 1 2.60 0.40 -1 -12 1 3.30 0.80 0 12 -1 0.50 0.20 0 -12 1 0.40 0.30 8 11 -1 0.50 0.60 8 11 -1 0.00 0.40 8 11 -1 0.50 0.50 -8 -11 1 0.30 0.50 -8 -11 1 0.00 0.50 7 11 -1 40.70 2.10 7 11 -1 37.10 2.70 7 11 -1 44.10 2.40 7 11 -1 41.20 1.90 -7 -11 1 41.10 2.70 -7 -11 1 38.50 1.70 6 11 -1 2.20 1.00 6 11 -1 1.20 0.40 6 11 -1 1.90 0.70 6 11 -1 1.50 0.60 -6 -11 1 1.30 0.70 -6 -11 1 1.80 0.40 5 11 -1 -0.70 0.80 5 11 -1 0.30 1.30 5 11 -1 0.10 0.50 5 11 -1 0.00 0.30 -5 -11 1 -0.40 0.70 -5 -11 1 0.30 0.50 4 11 -1 60.79 2.90 4 11 -1 64.79 2.90 4 11 -1 60.09 3.20 4 11 -1 62.09 4.60 4 11 -1 65.49 2.90 -4 -11 1 65.69 3.30 -4 -11 1 62.09 2.90 3 11 -1 0.20 0.40 3 11 -1 0.30 0.30 3 11 -1 0.00 1.50 3 11 -1 1.20 0.70 -3 -11 1 0.40 0.50 -3 -11 1 0.40 0.50 2 11 -1 6.40 0.70 2 11 -1 6.90 0.80 -2 -11 1 7.20 0.90 -2 -11 1 6.40 0.80 1 11 -1 8.80 1.10 1 11 -1 7.10 0.70 -1 -11 1 7.40 1.00 -1 -11 1 7.70 0.90 0 11 -1 16.60 1.10 0 -11 1 19.50 2.40 0 -11 1 17.60 1.60 0 -11 1 17.60 1.20 -1 11 -1 8.80 0.70 1 -11 1 8.10 0.80 1 -11 1 7.50 1.30 -2 11 -1 18.90 1.20 -2 11 -1 17.80 0.80 2 -11 1 18.80 1.10 9 10 -1 6.30 1.20 9 10 -1 4.10 0.80 -9 -10 1 3.20 0.60 -9 -10 1 5.10 0.90 -9 -10 1 4.90 0.90 8 10 -1 0.80 0.50 8 10 -1 0.50 0.70 8 10 -1 0.90 1.30 8 10 -1 1.00 0.50 -8 -10 1 0.20 0.50 -8 -10 1 0.40 0.70 -8 -10 1 1.10 0.50 -8 -10 1 1.40 0.60 7 10 -1 3.50 0.60 7 10 -1 2.20 1.60 7 10 -1 2.80 0.80 -7 -10 1 1.60 0.80 -7 -10 1 2.10 0.60 -7 -10 1 4.40 1.00 -7 -10 1 3.20 0.70 -7 -10 1 3.70 0.70 -7 -10 1 3.00 1.00 6 10 -1 24.40 2.20 6 10 -1 20.10 1.40 6 10 -1 22.20 2.20 -6 -10 1 20.60 1.60 -6 -10 1 22.20 1.70 -6 -10 1 23.60 1.90 5 10 -1 105.89 5.00 5 10 -1 106.49 5.10 5 10 -1 103.69 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7 -4 81.89 3.40 -4 7 -4 82.09 4.50 -4 7 -4 80.49 3.90 -4 7 -4 74.69 8.40 -4 7 -4 83.39 3.50 4 -7 4 76.69 5.10 4 -7 4 85.99 4.60 4 -7 4 84.59 3.80 -5 7 -4 66.29 2.90 -5 7 -4 70.69 3.70 -5 7 -4 75.59 3.80 -5 7 -4 72.39 3.40 5 -7 4 71.99 3.30 5 -7 4 55.09 4.70 -6 7 -4 0.10 0.50 -6 7 -4 0.00 0.40 -6 7 -4 0.00 0.50 -6 7 -4 -0.30 0.40 6 -7 4 -1.20 0.70 6 -7 4 -0.20 1.90 -9 -6 4 0.70 0.50 -9 -6 4 0.70 0.60 -9 -6 4 0.00 0.50 -9 -6 4 0.50 0.50 8 6 -4 3.40 1.60 -8 -6 4 2.80 0.90 -8 -6 4 3.10 0.80 -8 -6 4 2.50 0.90 -8 -6 4 4.00 0.80 -8 -6 4 4.90 1.20 -8 -6 4 3.60 1.00 7 6 -4 183.88 8.20 -7 -6 4 181.38 8.10 -7 -6 4 177.58 7.50 -7 -6 4 176.58 7.50 -7 -6 4 182.28 7.50 -7 -6 4 187.78 7.60 6 6 -4 59.59 3.40 6 6 -4 61.99 4.00 -6 -6 4 71.49 5.20 -6 -6 4 66.19 3.50 -6 -6 4 65.79 3.60 -6 -6 4 61.49 3.50 -6 -6 4 62.59 3.70 -6 -6 4 70.99 3.70 5 6 -4 382.66 15.70 -5 -6 4 399.36 15.10 -5 -6 4 406.26 14.40 -5 -6 4 404.96 15.00 -5 -6 4 409.76 15.90 -5 -6 4 421.06 15.10 -5 -6 4 391.46 15.10 4 6 -4 270.47 10.80 4 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2.00 -9 -5 4 6.20 0.90 -9 -5 4 7.40 1.10 -9 -5 4 7.70 1.00 -9 -5 4 8.40 1.40 -9 -5 4 6.50 1.00 8 5 -4 46.30 3.70 -8 -5 4 39.50 2.60 -8 -5 4 45.00 2.60 -8 -5 4 33.10 2.50 -8 -5 4 42.10 2.50 -8 -5 4 39.80 2.50 7 5 -4 427.66 16.60 -7 -5 4 482.35 17.90 -7 -5 4 397.16 15.90 -7 -5 4 410.96 15.90 6 5 -4 3.50 1.80 -6 -5 4 2.80 1.00 -6 -5 4 5.40 1.20 -6 -5 4 5.90 1.20 -6 -5 4 4.20 1.00 -6 -5 4 3.10 1.00 -6 -5 4 4.50 2.20 5 5 -4 128.29 5.80 5 5 -4 142.39 11.00 5 5 -4 133.99 12.10 5 5 -4 150.68 6.80 -5 -5 4 150.98 5.70 -5 -5 4 155.08 6.50 -5 -5 4 147.19 7.10 -5 -5 4 148.59 6.40 -5 -5 4 164.88 8.00 4 5 -4 202.08 8.30 4 5 -4 206.18 8.00 4 5 -4 204.58 8.90 4 5 -4 203.08 10.50 -4 -5 4 219.38 8.00 -4 -5 4 216.48 8.70 -4 -5 4 221.98 8.50 -4 -5 4 215.38 8.50 -4 -5 4 212.48 8.40 -4 -5 4 219.28 8.50 -4 -5 4 218.68 9.00 3 5 -4 157.68 7.80 3 5 -4 144.49 6.20 3 5 -4 146.09 5.90 3 5 -4 150.58 7.50 -3 -5 4 155.98 6.00 -3 -5 4 156.08 6.50 -3 -5 4 149.49 6.40 -3 -5 4 152.58 6.40 -3 -5 4 152.58 6.60 2 5 -4 18.90 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7.30 -4 5 -4 26.70 4.00 -4 5 -4 29.90 1.70 -4 5 -4 33.30 2.20 -4 5 -4 35.00 2.30 -4 5 -4 29.40 1.80 -4 5 -4 37.30 2.60 4 -5 4 30.70 2.50 4 -5 4 31.90 2.60 4 -5 4 28.30 2.20 4 -5 4 29.70 2.10 -5 5 -4 126.09 5.00 -5 5 -4 128.79 5.40 -5 5 -4 120.09 8.80 -5 5 -4 130.29 6.50 -5 5 -4 142.69 6.00 -5 5 -4 134.39 5.50 5 -5 4 127.99 5.50 5 -5 4 137.89 6.20 5 -5 4 131.09 6.20 5 -5 4 133.39 5.80 -6 5 -4 54.79 3.10 -6 5 -4 48.70 2.50 -6 5 -4 43.10 2.70 -6 5 -4 47.10 3.20 -6 5 -4 44.80 2.50 6 -5 4 46.70 2.60 -7 5 -4 0.50 0.40 -7 5 -4 0.10 0.50 7 -5 4 -1.00 1.20 -8 5 -4 2.20 0.50 -8 5 -4 1.80 0.50 -8 5 -4 2.40 0.40 -9 -4 4 34.50 2.10 -9 -4 4 35.00 2.00 -9 -4 4 34.30 2.10 -9 -4 4 35.80 2.00 -8 -4 4 68.59 3.60 -8 -4 4 78.39 3.80 -8 -4 4 77.09 3.80 -8 -4 4 75.69 3.70 -8 -4 4 64.99 3.70 -8 -4 4 70.89 4.60 7 4 -4 355.06 14.60 -7 -4 4 371.56 14.00 -7 -4 4 370.56 14.20 -7 -4 4 363.76 14.40 -7 -4 4 395.76 14.30 -7 -4 4 383.56 14.30 6 4 -4 22.10 2.80 -6 -4 4 20.00 2.70 -6 -4 4 23.50 2.20 -6 -4 4 27.60 2.20 -6 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623.54 23.50 2 -4 4 576.64 20.30 2 -4 4 556.24 20.50 2 -4 4 555.44 20.20 -3 4 -4 11.60 1.40 -3 4 -4 12.60 2.30 -3 4 -4 11.00 1.10 -3 4 -4 10.20 1.10 -3 4 -4 11.40 1.00 -3 4 -4 12.30 1.20 3 -4 4 11.50 1.40 3 -4 4 10.00 5.30 3 -4 4 10.80 1.40 3 -4 4 10.30 1.20 3 -4 4 12.50 1.40 -4 4 -4 203.98 8.00 -4 4 -4 203.38 7.80 -4 4 -4 217.78 8.60 -4 4 -4 210.68 8.00 -4 4 -4 219.88 10.30 -4 4 -4 206.18 8.10 4 -4 4 202.38 8.10 4 -4 4 206.18 8.20 4 -4 4 226.38 20.30 4 -4 4 207.88 8.10 4 -4 4 208.88 8.50 -5 4 -4 7.50 2.60 -5 4 -4 13.90 1.40 -5 4 -4 13.80 1.60 -5 4 -4 13.60 1.40 -5 4 -4 13.60 1.00 -5 4 -4 14.30 1.20 5 -4 4 16.30 2.00 5 -4 4 12.20 1.70 5 -4 4 14.10 1.80 -6 4 -4 29.30 5.40 -6 4 -4 28.50 3.00 -6 4 -4 32.00 2.80 -6 4 -4 30.10 2.30 -6 4 -4 26.90 2.00 -6 4 -4 26.20 2.30 6 -4 4 35.60 2.70 6 -4 4 24.10 2.20 6 -4 4 32.50 3.60 6 -4 4 28.20 2.50 -7 4 -4 0.30 1.00 -7 4 -4 3.30 0.80 -7 4 -4 1.40 0.60 -7 4 -4 0.50 0.50 7 -4 4 1.60 1.10 -8 4 -4 10.80 1.00 -8 4 -4 10.80 1.40 -8 4 -4 10.30 1.20 8 -4 4 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213.58 8.70 -1 -3 4 223.58 8.60 0 3 -4 63.49 3.50 0 3 -4 65.59 3.70 0 3 -4 63.19 3.20 0 -3 4 66.69 4.10 -1 3 -4 872.31 30.80 1 -3 4 890.01 31.60 -2 3 -4 620.84 21.20 2 -3 4 566.34 20.40 2 -3 4 577.14 20.50 2 -3 4 590.04 21.80 2 -3 4 553.14 20.60 -3 3 -4 49.99 2.60 -3 3 -4 54.79 3.60 -3 3 -4 50.49 2.40 -3 3 -4 51.99 2.50 3 -3 4 52.69 6.30 3 -3 4 50.59 2.50 3 -3 4 48.90 2.50 3 -3 4 51.89 2.70 -4 3 -4 204.18 7.40 -4 3 -4 213.98 9.90 -4 3 -4 193.88 7.50 -4 3 -4 194.38 7.20 -4 3 -4 194.38 7.80 -4 3 -4 190.28 7.60 4 -3 4 189.28 7.40 4 -3 4 184.08 7.40 4 -3 4 186.98 12.20 4 -3 4 189.18 7.50 4 -3 4 188.28 7.70 -5 3 -4 334.07 12.70 -5 3 -4 331.37 14.70 -5 3 -4 315.57 12.40 -5 3 -4 329.37 12.10 -5 3 -4 333.87 11.90 5 -3 4 331.67 12.20 5 -3 4 333.57 12.60 5 -3 4 332.57 12.20 5 -3 4 328.97 12.30 -6 3 -4 128.89 5.60 -6 3 -4 114.49 4.40 -6 3 -4 109.99 5.50 -6 3 -4 131.79 5.20 -6 3 -4 120.39 5.30 -6 3 -4 121.89 8.70 6 -3 4 123.69 5.50 6 -3 4 122.89 5.60 6 -3 4 122.19 5.20 6 -3 4 116.09 5.30 -7 3 -4 24.00 7.10 -7 3 -4 28.20 2.30 -7 3 -4 31.70 1.90 -7 3 -4 30.20 2.00 -7 3 -4 31.60 2.30 -7 3 -4 33.90 2.70 7 -3 4 29.30 3.20 7 -3 4 34.00 2.70 -8 3 -4 0.90 0.50 -8 3 -4 0.40 0.50 8 -3 4 -0.30 1.10 -9 3 -4 12.30 1.10 -9 3 -4 14.10 1.30 -9 3 -4 14.10 1.00 -9 -2 4 4.70 1.50 -9 -2 4 4.90 0.80 -9 -2 4 4.40 0.90 -9 -2 4 5.60 0.90 -8 -2 4 69.49 3.30 -8 -2 4 66.09 3.20 -8 -2 4 59.69 3.40 -8 -2 4 56.19 3.10 -8 -2 4 66.89 3.30 -8 -2 4 62.89 3.20 -8 -2 4 62.49 3.10 -7 -2 4 205.78 8.10 -7 -2 4 199.58 8.10 -7 -2 4 195.68 8.10 -7 -2 4 211.18 8.40 -7 -2 4 200.08 8.20 -7 -2 4 199.88 8.40 -6 -2 4 20.90 2.00 -6 -2 4 24.00 2.10 -6 -2 4 21.50 1.90 -6 -2 4 24.90 2.10 -6 -2 4 21.90 1.80 -6 -2 4 21.00 2.00 -6 -2 4 19.10 1.80 -6 -2 4 23.40 1.90 5 2 -4 6.20 4.10 5 2 -4 4.80 4.80 -5 -2 4 10.60 1.40 -5 -2 4 9.10 1.30 -5 -2 4 8.10 1.30 -5 -2 4 8.70 1.30 -5 -2 4 8.70 1.30 -5 -2 4 9.10 1.50 -5 -2 4 7.50 1.60 4 2 -4 156.88 7.20 4 2 -4 152.98 8.50 -4 -2 4 154.78 6.20 -4 -2 4 157.58 6.80 -4 -2 4 151.48 6.40 -4 -2 4 160.48 6.50 -4 -2 4 155.28 6.50 3 2 -4 70.59 3.80 3 2 -4 70.49 4.70 -3 -2 4 72.69 3.50 -3 -2 4 63.79 3.20 2 2 -4 207.48 8.00 -2 -2 4 197.28 7.80 -2 -2 4 201.98 10.60 -2 -2 4 217.48 8.00 1 2 -4 616.54 21.50 1 2 -4 610.64 20.90 1 2 -4 521.05 21.70 -1 -2 4 610.74 20.80 -1 -2 4 591.94 21.90 0 2 -4 90.89 3.80 0 2 -4 85.39 5.90 0 2 -4 94.59 4.20 0 -2 4 80.39 5.40 0 -2 4 86.99 3.60 0 -2 4 94.79 4.70 -1 2 -4 447.06 16.00 -1 2 -4 422.56 17.60 1 -2 4 468.45 16.50 -2 2 -4 662.03 22.20 2 -2 4 629.34 22.50 2 -2 4 607.74 21.60 2 -2 4 575.94 21.70 -3 2 -4 375.36 13.90 3 -2 4 350.56 12.90 3 -2 4 355.86 14.20 3 -2 4 350.56 12.80 -4 2 -4 94.49 4.50 -4 2 -4 102.99 4.20 -4 2 -4 103.79 4.60 -4 2 -4 102.09 4.10 -4 2 -4 108.19 5.70 -4 2 -4 101.39 4.40 4 -2 4 101.99 4.20 4 -2 4 102.89 4.30 4 -2 4 103.99 7.70 -5 2 -4 209.38 8.30 -5 2 -4 203.78 8.10 -5 2 -4 209.48 8.10 -5 2 -4 209.68 7.60 -5 2 -4 212.98 10.10 -5 2 -4 205.08 7.80 5 -2 4 198.48 8.00 5 -2 4 215.98 13.70 5 -2 4 203.08 7.90 5 -2 4 198.98 8.00 -6 2 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5 -0.60 0.50 -4 -8 5 0.90 0.80 -4 -8 5 0.30 1.20 3 8 -5 44.20 3.10 3 8 -5 40.30 2.40 3 8 -5 41.60 2.40 3 8 -5 35.40 2.50 -3 -8 5 44.70 2.50 -3 -8 5 38.80 2.60 -3 -8 5 41.20 2.70 -3 -8 5 41.20 3.40 -3 -8 5 41.60 3.10 2 8 -5 37.60 2.30 2 8 -5 41.70 2.40 2 8 -5 36.50 2.80 2 8 -5 36.40 2.30 -2 -8 5 35.80 2.50 -2 -8 5 38.60 2.90 -2 -8 5 39.30 3.10 -2 -8 5 38.00 2.30 -2 -8 5 40.90 2.40 1 8 -5 68.49 3.40 1 8 -5 72.49 3.40 1 8 -5 68.49 3.30 1 8 -5 67.59 3.80 1 8 -5 67.49 4.10 -1 -8 5 74.09 4.00 -1 -8 5 67.69 3.30 -1 -8 5 67.89 4.20 0 8 -5 10.70 1.30 0 8 -5 10.80 1.10 0 8 -5 11.20 1.10 0 -8 5 11.60 2.00 0 -8 5 11.50 1.50 0 -8 5 12.50 1.40 0 -8 5 4.00 3.30 0 -8 5 12.90 1.80 -1 8 -5 1.10 0.50 -1 8 -5 1.20 2.40 -1 8 -5 1.20 0.60 -1 8 -5 1.50 0.50 1 -8 5 2.80 2.70 1 -8 5 2.60 1.00 1 -8 5 1.40 0.60 1 -8 5 1.00 1.50 1 -8 5 2.50 1.10 -2 8 -5 124.89 5.20 -2 8 -5 115.19 5.00 -2 8 -5 146.29 9.40 2 -8 5 112.69 5.40 2 -8 5 125.49 5.20 2 -8 5 118.29 6.00 2 -8 5 126.89 5.60 -3 8 -5 6.40 0.90 -3 8 -5 5.40 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5 -7 18.10 1.30 -5 5 -7 16.80 1.70 5 -5 7 16.80 2.10 5 -5 7 19.90 2.10 5 -5 7 19.60 2.00 5 -5 7 21.10 1.80 -6 5 -7 36.50 1.80 -6 5 -7 40.50 2.80 -6 5 -7 36.20 2.20 6 -5 7 36.50 2.90 6 -5 7 40.00 2.90 6 -5 7 36.30 4.10 6 -5 7 42.10 2.30 -7 5 -7 17.50 1.50 -7 5 -7 16.30 1.20 7 -5 7 13.10 1.40 7 -5 7 12.00 2.20 -8 -4 7 6.40 0.90 -8 -4 7 6.50 0.90 -8 -4 7 4.90 0.90 -8 -4 7 5.20 0.80 7 4 -7 20.10 3.00 -7 -4 7 16.50 1.70 -7 -4 7 18.80 2.30 -7 -4 7 17.10 1.70 -7 -4 7 19.30 1.60 6 4 -7 71.69 4.40 -6 -4 7 70.19 3.80 -6 -4 7 70.39 3.80 -6 -4 7 68.89 3.80 -6 -4 7 73.09 3.70 -6 -4 7 65.09 3.80 -6 -4 7 73.29 4.10 5 4 -7 32.80 2.90 5 4 -7 28.10 2.20 -5 -4 7 29.40 2.50 -5 -4 7 30.90 2.30 -5 -4 7 33.30 2.50 -5 -4 7 30.00 2.50 -5 -4 7 30.30 2.60 -5 -4 7 29.50 2.50 4 4 -7 48.10 2.60 4 4 -7 48.90 3.30 -4 -4 7 48.80 3.00 -4 -4 7 48.60 2.60 -4 -4 7 48.20 2.90 -4 -4 7 47.80 3.20 -4 -4 7 43.30 3.00 -4 -4 7 44.70 3.00 -4 -4 7 45.40 3.70 3 4 -7 3.80 0.80 3 4 -7 3.00 0.90 3 4 -7 2.60 1.00 3 4 -7 5.50 4.40 3 4 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2.10 2 -4 7 20.10 5.50 2 -4 7 23.70 1.90 2 -4 7 28.00 2.30 2 -4 7 23.70 1.80 2 -4 7 26.00 2.20 -3 4 -7 353.66 12.30 -3 4 -7 338.97 12.30 -3 4 -7 339.97 12.50 -3 4 -7 340.17 13.70 -3 4 -7 311.67 12.30 -3 4 -7 319.17 12.20 3 -4 7 341.57 13.00 3 -4 7 330.17 12.90 3 -4 7 328.37 12.70 3 -4 7 327.37 18.30 3 -4 7 327.87 12.50 -4 4 -7 36.70 2.90 -4 4 -7 33.90 4.20 -4 4 -7 38.00 2.10 -4 4 -7 33.50 2.30 -4 4 -7 32.10 2.00 -4 4 -7 39.50 2.30 4 -4 7 39.80 2.80 4 -4 7 36.60 2.60 4 -4 7 35.40 2.40 4 -4 7 33.70 2.30 -5 4 -7 64.79 3.40 -5 4 -7 57.39 2.90 -5 4 -7 63.29 3.20 -5 4 -7 69.69 3.30 -5 4 -7 64.69 3.00 -5 4 -7 70.49 5.90 5 -4 7 62.59 3.40 5 -4 7 64.69 3.80 5 -4 7 65.59 3.30 -6 4 -7 19.60 1.80 -6 4 -7 17.20 5.10 -6 4 -7 14.60 1.20 -6 4 -7 18.50 1.70 -6 4 -7 15.50 1.00 6 -4 7 18.50 1.70 6 -4 7 16.10 2.00 6 -4 7 17.60 2.20 6 -4 7 13.20 1.80 -7 4 -7 45.90 3.00 -7 4 -7 37.40 2.00 -7 4 -7 42.00 2.20 -7 4 -7 42.50 2.50 7 -4 7 35.40 4.00 7 -4 7 40.80 2.80 7 -4 7 41.30 3.20 7 -4 7 46.20 2.50 -8 4 -7 20.50 1.30 -8 4 -7 22.50 1.40 -8 4 -7 25.50 1.70 8 -4 7 21.00 2.40 -8 -3 7 12.50 1.30 -8 -3 7 14.70 1.30 -8 -3 7 10.80 1.20 -8 -3 7 12.60 1.20 7 3 -7 1.20 2.30 -7 -3 7 1.60 0.80 -7 -3 7 2.10 0.80 -7 -3 7 1.40 0.80 -7 -3 7 1.80 0.70 -7 -3 7 1.70 0.70 6 3 -7 97.79 4.70 6 3 -7 121.99 5.80 -6 -3 7 112.49 4.90 -6 -3 7 102.89 5.30 -6 -3 7 104.19 4.90 -6 -3 7 105.49 5.30 -6 -3 7 104.59 4.90 -6 -3 7 104.89 5.10 -5 -3 7 162.78 6.50 -5 -3 7 151.58 6.60 -5 -3 7 153.78 6.90 -5 -3 7 156.58 7.10 -5 -3 7 154.48 7.10 4 3 -7 11.10 1.80 4 3 -7 11.70 1.90 -4 -3 7 12.30 1.40 -4 -3 7 11.60 1.70 -4 -3 7 11.90 1.50 -4 -3 7 10.10 1.50 -4 -3 7 12.20 1.30 -4 -3 7 10.70 1.60 3 3 -7 7.00 1.30 3 3 -7 7.00 1.20 3 3 -7 10.60 3.60 3 3 -7 4.00 4.80 -3 -3 7 6.20 1.10 -3 -3 7 7.00 1.30 -3 -3 7 7.10 1.20 -3 -3 7 9.80 1.20 -3 -3 7 6.80 1.10 -3 -3 7 7.00 1.60 -3 -3 7 6.30 1.70 2 3 -7 146.39 6.40 2 3 -7 150.58 6.20 2 3 -7 141.99 8.40 2 3 -7 154.78 7.20 -2 -3 7 150.78 6.00 -2 -3 7 156.18 6.10 -2 -3 7 140.59 6.50 -2 -3 7 135.49 6.40 -2 -3 7 145.99 6.40 1 3 -7 202.88 10.10 1 3 -7 186.58 7.20 1 3 -7 186.58 9.10 1 3 -7 180.98 7.20 1 3 -7 191.38 7.90 -1 -3 7 172.78 7.60 -1 -3 7 190.18 7.50 -1 -3 7 176.18 7.80 -1 -3 7 187.98 7.30 -1 -3 7 174.28 7.50 0 3 -7 38.90 2.20 0 3 -7 41.60 2.70 0 3 -7 40.10 4.30 0 -3 7 39.40 2.50 0 -3 7 39.00 2.30 0 -3 7 29.80 2.70 0 -3 7 35.30 2.20 0 -3 7 41.20 2.40 -1 3 -7 78.09 3.70 -1 3 -7 70.59 3.90 -1 3 -7 71.89 3.30 -1 3 -7 69.69 5.20 1 -3 7 76.39 3.90 1 -3 7 70.89 3.60 1 -3 7 72.29 3.60 1 -3 7 79.29 3.80 -2 3 -7 30.60 1.90 -2 3 -7 26.90 2.40 -2 3 -7 34.10 4.40 -2 3 -7 26.60 2.80 -2 3 -7 30.60 1.90 -2 3 -7 28.20 1.70 -2 3 -7 29.00 1.70 2 -3 7 27.60 2.20 2 -3 7 29.80 1.90 2 -3 7 30.90 2.10 2 -3 7 27.70 1.90 2 -3 7 29.80 1.90 -3 3 -7 57.79 2.70 -3 3 -7 61.29 2.90 -3 3 -7 57.99 2.90 -3 3 -7 46.60 2.80 -3 3 -7 55.79 2.70 -3 3 -7 46.30 5.30 3 -3 7 57.99 2.90 3 -3 7 49.40 6.00 3 -3 7 56.19 3.10 3 -3 7 55.39 2.90 3 -3 7 56.69 3.50 3 -3 7 55.39 2.80 -4 3 -7 127.79 5.30 -4 3 -7 128.59 5.40 -4 3 -7 124.39 5.50 -4 3 -7 132.19 5.30 -4 3 -7 121.69 5.20 -4 3 -7 123.69 6.80 4 -3 7 123.39 14.50 4 -3 7 134.49 5.80 4 -3 7 131.39 5.50 4 -3 7 123.69 5.50 4 -3 7 136.79 5.70 -5 3 -7 8.30 1.10 -5 3 -7 10.90 1.00 -5 3 -7 8.90 1.30 -5 3 -7 9.70 2.70 -5 3 -7 13.40 1.30 5 -3 7 10.20 1.50 5 -3 7 11.00 1.50 5 -3 7 10.70 1.40 5 -3 7 9.10 1.30 -6 3 -7 1.80 3.20 -6 3 -7 4.00 1.00 -6 3 -7 5.10 1.10 -6 3 -7 4.70 0.90 6 -3 7 5.40 1.40 6 -3 7 5.80 1.10 6 -3 7 3.30 1.00 -7 3 -7 71.39 4.30 -7 3 -7 71.69 3.60 -7 3 -7 77.39 3.40 -7 3 -7 68.69 3.10 7 -3 7 66.89 3.50 7 -3 7 68.89 3.90 7 -3 7 75.39 3.50 7 -3 7 64.49 4.10 -8 3 -7 135.29 6.10 -8 3 -7 139.39 5.30 -8 3 -7 139.19 5.50 -8 3 -7 127.79 5.10 8 -3 7 135.69 5.90 -8 -2 7 28.90 1.80 -8 -2 7 32.10 2.20 -8 -2 7 31.90 1.80 -8 -2 7 31.60 2.00 -8 -2 7 23.50 1.80 -7 -2 7 20.50 1.60 -7 -2 7 20.50 1.90 -7 -2 7 21.20 1.70 -7 -2 7 20.50 1.80 -7 -2 7 18.90 1.70 6 2 -7 102.99 5.30 -6 -2 7 108.69 5.10 -6 -2 7 97.99 5.00 -6 -2 7 99.69 5.20 -6 -2 7 97.89 4.70 -6 -2 7 100.99 4.60 -6 -2 7 109.29 4.70 5 2 -7 177.78 7.80 -5 -2 7 193.38 7.70 -5 -2 7 190.18 8.30 -5 -2 7 183.08 8.10 -5 -2 7 198.48 7.60 -5 -2 7 181.78 7.70 -5 -2 7 195.38 8.00 4 2 -7 28.70 10.50 4 2 -7 33.60 2.40 -4 -2 7 36.10 2.40 -4 -2 7 36.20 2.60 -4 -2 7 35.60 2.60 -4 -2 7 35.90 2.40 -4 -2 7 38.20 2.10 -4 -2 7 34.70 2.20 -4 -2 7 34.50 2.70 3 2 -7 9.70 3.00 3 2 -7 6.40 1.20 3 2 -7 7.70 1.50 3 2 -7 11.20 4.40 -3 -2 7 7.00 1.00 -3 -2 7 6.90 1.10 -3 -2 7 8.90 1.20 -3 -2 7 7.10 1.10 -3 -2 7 8.10 1.90 -3 -2 7 10.00 1.80 2 2 -7 44.50 3.60 2 2 -7 43.10 2.50 2 2 -7 44.50 4.90 -2 -2 7 43.50 2.60 -2 -2 7 44.10 2.70 -2 -2 7 41.80 2.80 -2 -2 7 39.80 2.90 -2 -2 7 38.20 2.80 1 2 -7 538.25 19.10 1 2 -7 535.45 20.10 1 2 -7 520.05 19.00 -1 -2 7 522.95 18.70 -1 -2 7 505.55 19.00 -1 -2 7 542.95 19.30 -1 -2 7 501.45 19.00 0 2 -7 196.68 7.90 0 2 -7 180.68 8.40 0 -2 7 192.48 7.50 0 -2 7 192.08 7.50 -1 2 -7 5.70 2.10 -1 2 -7 5.00 1.10 -1 2 -7 6.80 0.90 -1 2 -7 3.60 0.90 1 -2 7 3.40 0.90 1 -2 7 5.20 1.00 1 -2 7 3.90 0.80 -2 2 -7 197.78 8.40 -2 2 -7 214.18 8.10 -2 2 -7 203.18 8.00 -2 2 -7 212.58 8.10 -2 2 -7 209.38 8.00 -2 2 -7 216.08 9.40 2 -2 7 196.88 7.90 2 -2 7 219.18 8.30 2 -2 7 218.08 8.10 2 -2 7 234.68 8.10 -3 2 -7 174.08 7.40 -3 2 -7 166.28 6.60 -3 2 -7 167.68 6.60 -3 2 -7 168.98 6.50 -3 2 -7 157.38 6.50 3 -2 7 165.88 6.60 3 -2 7 166.98 6.50 3 -2 7 169.28 6.60 3 -2 7 171.28 6.80 -4 2 -7 189.68 7.10 -4 2 -7 179.18 6.90 -4 2 -7 183.88 7.10 -4 2 -7 178.98 8.20 -4 2 -7 175.88 7.20 -4 2 -7 169.28 6.90 4 -2 7 178.38 11.30 4 -2 7 179.58 7.10 4 -2 7 169.98 7.00 4 -2 7 182.78 7.30 -5 2 -7 152.38 6.00 -5 2 -7 145.89 6.10 -5 2 -7 154.48 6.60 -5 2 -7 152.58 6.20 -5 2 -7 153.18 7.90 -5 2 -7 147.39 6.10 -5 2 -7 147.99 5.70 5 -2 7 154.48 6.50 5 -2 7 148.29 6.20 -6 2 -7 6.80 1.00 -6 2 -7 5.60 2.80 -6 2 -7 8.40 1.20 -6 2 -7 7.50 1.20 -6 2 -7 6.70 1.40 -6 2 -7 8.10 0.90 6 -2 7 11.80 1.60 6 -2 7 8.30 1.20 6 -2 7 8.40 1.40 6 -2 7 7.30 1.10 -7 2 -7 4.00 4.40 -7 2 -7 3.90 0.90 -7 2 -7 2.60 1.00 -7 2 -7 3.50 0.80 -7 2 -7 2.80 0.60 -7 2 -7 3.20 0.50 7 -2 7 4.00 1.30 7 -2 7 3.80 0.90 7 -2 7 2.90 1.00 7 -2 7 3.60 1.10 -8 2 -7 124.89 5.00 -8 2 -7 128.69 5.30 -8 2 -7 124.39 6.00 -8 2 -7 126.09 5.00 8 -2 7 128.39 5.70 8 -2 7 127.09 6.50 8 -2 7 113.19 5.20 8 -2 7 113.99 5.80 -9 2 -7 26.30 1.50 -9 2 -7 27.30 1.70 -9 2 -7 21.10 2.40 -9 2 -7 23.00 1.30 9 -2 7 18.90 2.10 -8 -1 7 99.09 4.50 -8 -1 7 118.19 4.50 -8 -1 7 107.09 4.60 -8 -1 7 121.09 4.50 -7 -1 7 0.20 0.70 -7 -1 7 0.20 0.50 -7 -1 7 0.10 0.70 -7 -1 7 1.00 0.90 -7 -1 7 -0.30 0.60 6 1 -7 45.60 5.00 -6 -1 7 47.60 2.80 -6 -1 7 48.40 2.60 -6 -1 7 45.60 3.00 -6 -1 7 44.40 2.80 -6 -1 7 46.90 3.10 5 1 -7 45.00 2.80 -5 -1 7 43.10 2.90 -5 -1 7 43.50 2.50 -5 -1 7 41.80 3.10 -5 -1 7 41.30 2.60 -5 -1 7 40.40 2.70 -5 -1 7 38.50 2.80 4 1 -7 514.95 19.00 4 1 -7 507.75 22.80 -4 -1 7 507.05 19.10 -4 -1 7 540.45 19.40 -4 -1 7 538.55 19.80 -4 -1 7 510.25 19.10 -4 -1 7 531.35 19.60 -4 -1 7 561.34 19.10 3 1 -7 66.59 6.80 -3 -1 7 70.89 3.30 -3 -1 7 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121.59 5.70 -2 5 -9 3.90 1.00 -2 5 -9 4.00 0.80 -2 5 -9 3.60 0.80 -2 5 -9 6.00 3.00 2 -5 9 5.00 1.10 2 -5 9 2.00 1.10 2 -5 9 4.70 1.50 2 -5 9 4.60 1.20 -3 5 -9 70.69 3.50 -3 5 -9 69.19 3.30 -3 5 -9 69.49 6.50 -3 5 -9 63.29 3.60 3 -5 9 68.19 3.50 3 -5 9 67.59 3.80 3 -5 9 72.09 4.10 3 -5 9 69.69 4.00 3 -5 9 64.79 4.10 -4 5 -9 25.90 1.70 -4 5 -9 26.80 1.90 -4 5 -9 22.20 4.30 -4 5 -9 25.50 1.80 4 -5 9 26.40 1.90 4 -5 9 25.90 2.70 4 -5 9 25.70 2.60 4 -5 9 34.40 4.00 4 -5 9 27.50 2.20 -5 5 -9 18.00 1.40 -5 5 -9 22.10 1.60 -5 5 -9 18.30 1.20 5 -5 9 17.40 1.50 5 -5 9 17.50 1.90 5 -5 9 15.20 2.10 5 -5 9 12.50 2.10 -6 5 -9 19.00 1.30 -6 5 -9 22.70 1.10 -6 5 -9 22.90 1.90 6 -5 9 19.80 3.00 6 -5 9 15.20 2.10 6 -5 9 20.20 1.50 6 -5 9 17.30 2.40 -7 5 -9 0.80 0.50 7 -5 9 -0.20 0.60 7 4 -9 15.10 2.70 -7 -4 9 17.80 1.30 -7 -4 9 14.60 1.30 -7 -4 9 15.00 1.30 -7 -4 9 14.70 1.20 6 4 -9 32.70 2.80 -6 -4 9 31.50 2.30 -6 -4 9 31.80 2.00 -6 -4 9 30.50 2.20 -6 -4 9 31.30 2.00 -6 -4 9 29.90 2.30 -6 -4 9 30.30 2.10 5 4 -9 10.30 1.60 5 4 -9 10.60 1.90 5 4 -9 11.20 1.40 -5 -4 9 9.80 1.50 -5 -4 9 11.60 1.40 -5 -4 9 10.30 1.30 -5 -4 9 6.90 1.30 -5 -4 9 10.70 1.70 -5 -4 9 10.20 1.50 4 4 -9 6.90 1.50 4 4 -9 7.20 1.10 -4 -4 9 6.00 1.30 -4 -4 9 5.70 1.00 -4 -4 9 6.40 1.60 -4 -4 9 6.30 1.20 3 4 -9 63.59 3.20 3 4 -9 58.29 3.90 3 4 -9 61.29 3.30 -3 -4 9 62.49 3.40 -3 -4 9 61.89 3.70 -3 -4 9 60.79 3.20 -3 -4 9 62.79 3.60 -3 -4 9 62.79 4.00 -3 -4 9 62.49 3.30 -3 -4 9 59.19 4.40 2 4 -9 234.98 9.30 2 4 -9 242.28 10.30 2 4 -9 247.58 9.50 -2 -4 9 233.68 9.30 -2 -4 9 244.58 9.60 -2 -4 9 241.58 9.90 -2 -4 9 229.78 9.50 -2 -4 9 239.68 10.10 -2 -4 9 239.68 9.50 -2 -4 9 229.58 10.00 1 4 -9 25.30 2.30 1 4 -9 31.10 2.10 1 4 -9 28.50 2.60 1 4 -9 34.80 2.10 -1 -4 9 33.10 2.70 -1 -4 9 26.20 2.90 -1 -4 9 32.10 2.40 -1 -4 9 31.20 2.20 -1 -4 9 28.80 2.50 -1 -4 9 31.80 3.00 0 4 -9 1.50 0.90 0 4 -9 0.90 0.70 0 4 -9 1.90 0.70 0 4 -9 2.40 1.80 0 4 -9 3.90 7.50 0 4 -9 1.10 0.60 0 -4 9 0.40 0.80 0 -4 9 2.20 0.90 0 -4 9 1.00 0.70 0 -4 9 -1.00 1.20 0 -4 9 1.80 1.00 -1 4 -9 28.70 2.00 -1 4 -9 32.50 3.50 -1 4 -9 29.60 2.00 -1 4 -9 25.60 1.90 -1 4 -9 27.30 2.60 1 -4 9 27.60 2.20 1 -4 9 29.00 2.20 1 -4 9 26.40 2.00 1 -4 9 28.50 2.50 -2 4 -9 267.17 10.80 -2 4 -9 250.87 11.00 -2 4 -9 257.77 9.80 -2 4 -9 253.07 9.80 2 -4 9 254.57 10.20 2 -4 9 242.68 9.80 2 -4 9 253.57 10.20 -3 4 -9 47.90 2.50 -3 4 -9 41.80 4.80 -3 4 -9 42.10 2.60 -3 4 -9 43.30 2.50 -3 4 -9 43.50 2.50 3 -4 9 45.20 3.00 3 -4 9 47.40 2.80 3 -4 9 44.90 2.70 3 -4 9 49.50 3.10 3 -4 9 42.10 3.00 -4 4 -9 -0.40 3.10 -4 4 -9 -1.10 0.70 -4 4 -9 0.10 0.40 -4 4 -9 1.50 0.70 4 -4 9 0.90 0.90 4 -4 9 -0.30 0.60 4 -4 9 0.30 0.70 4 -4 9 0.90 1.60 -5 4 -9 40.80 2.50 -5 4 -9 39.60 5.40 -5 4 -9 41.60 2.20 -5 4 -9 40.50 2.30 5 -4 9 44.20 2.90 5 -4 9 38.80 2.90 5 -4 9 43.20 2.70 5 -4 9 40.90 2.50 -6 4 -9 1.90 0.60 -6 4 -9 2.40 0.40 6 -4 9 2.10 0.90 6 -4 9 2.90 1.70 6 -4 9 3.00 0.80 6 -4 9 2.50 1.10 -7 4 -9 27.00 1.60 -7 4 -9 32.60 2.20 7 -4 9 26.90 1.70 7 -4 9 26.20 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10 0.90 0.80 -1 4 -10 9.30 1.20 -1 4 -10 12.90 3.50 -1 4 -10 8.20 1.70 -1 4 -10 8.00 1.20 -1 4 -10 9.70 1.20 1 -4 10 10.40 1.30 1 -4 10 10.00 1.40 1 -4 10 9.40 1.60 1 -4 10 8.90 1.80 -2 4 -10 238.78 9.20 -2 4 -10 238.98 9.30 -2 4 -10 225.98 11.00 -2 4 -10 237.68 9.20 2 -4 10 249.58 9.70 2 -4 10 242.68 9.20 2 -4 10 222.48 9.50 2 -4 10 219.78 9.70 2 -4 10 234.08 9.50 -3 4 -10 66.89 3.40 -3 4 -10 67.39 3.20 -3 4 -10 64.79 3.20 -3 4 -10 56.69 6.90 3 -4 10 66.49 3.40 3 -4 10 61.39 3.90 3 -4 10 65.79 3.80 3 -4 10 64.59 3.50 3 -4 10 61.09 4.80 -4 4 -10 1.80 5.20 -4 4 -10 -0.30 0.70 -4 4 -10 1.00 1.00 -4 4 -10 0.50 0.40 4 -4 10 0.70 0.70 4 -4 10 -0.50 0.60 4 -4 10 -1.20 1.50 4 -4 10 1.40 1.10 4 -4 10 -1.20 1.00 -5 4 -10 71.79 3.30 -5 4 -10 75.99 3.40 -5 4 -10 68.49 3.20 5 -4 10 64.29 3.90 5 -4 10 73.59 4.00 5 -4 10 69.39 3.50 -6 4 -10 50.29 2.40 -6 4 -10 52.99 2.30 6 -4 10 48.10 3.10 6 -4 10 49.10 3.30 6 -4 10 50.69 2.80 6 -4 10 49.50 2.60 -7 4 -10 1.60 0.60 7 -4 10 1.70 0.60 7 -4 10 -1.20 1.20 7 -4 10 1.60 1.20 -7 -3 10 18.50 1.20 -7 -3 10 15.80 1.10 -7 -3 10 17.60 1.10 -7 -3 10 18.80 1.20 6 3 -10 136.89 6.00 -6 -3 10 125.09 5.40 -6 -3 10 125.89 5.30 -6 -3 10 127.29 5.50 -6 -3 10 131.99 5.40 -6 -3 10 135.49 5.60 5 3 -10 30.60 2.00 5 3 -10 29.00 2.50 -5 -3 10 29.70 2.00 -5 -3 10 28.30 2.20 -5 -3 10 28.70 2.30 -5 -3 10 32.50 2.30 -5 -3 10 30.00 2.00 4 3 -10 71.79 4.20 4 3 -10 68.49 3.60 4 3 -10 72.09 3.40 -4 -3 10 69.59 3.50 -4 -3 10 69.89 3.60 -4 -3 10 72.09 3.60 -4 -3 10 62.49 3.90 -4 -3 10 71.89 3.90 -4 -3 10 68.59 3.90 3 3 -10 118.29 5.00 3 3 -10 112.49 5.80 -3 -3 10 115.19 5.10 -3 -3 10 107.79 4.90 -3 -3 10 115.49 5.40 -3 -3 10 113.99 5.10 -3 -3 10 111.59 5.60 2 3 -10 10.80 1.70 2 3 -10 11.00 1.30 2 3 -10 11.60 1.50 -2 -3 10 11.70 1.50 -2 -3 10 8.60 1.40 -2 -3 10 9.80 2.40 -2 -3 10 12.40 2.00 -2 -3 10 10.90 1.60 -2 -3 10 9.70 1.30 -2 -3 10 9.10 1.30 1 3 -10 6.00 1.00 1 3 -10 8.60 1.30 1 3 -10 7.30 1.60 -1 -3 10 8.00 1.50 -1 -3 10 9.10 1.60 -1 -3 10 6.80 1.90 -1 -3 10 5.70 1.20 -1 -3 10 7.30 1.20 -1 -3 10 7.40 1.20 0 3 -10 166.18 6.80 0 3 -10 162.68 6.60 0 3 -10 160.38 7.50 0 -3 10 173.98 7.30 0 -3 10 157.68 6.80 0 -3 10 158.98 6.50 0 -3 10 171.48 7.10 0 -3 10 167.68 6.90 0 -3 10 140.99 7.20 -1 3 -10 153.08 8.30 -1 3 -10 153.58 7.30 -1 3 -10 158.68 6.50 -1 3 -10 155.18 16.40 -1 3 -10 161.78 6.70 -1 3 -10 164.68 6.60 1 -3 10 158.38 6.80 1 -3 10 157.68 6.80 1 -3 10 161.38 6.50 1 -3 10 165.38 7.00 -2 3 -10 86.39 3.90 -2 3 -10 83.49 4.20 -2 3 -10 73.39 6.00 -2 3 -10 73.79 4.60 -2 3 -10 87.09 4.00 2 -3 10 86.69 4.70 2 -3 10 85.89 4.20 2 -3 10 81.29 4.20 2 -3 10 76.49 4.30 2 -3 10 81.49 3.80 -3 3 -10 291.27 11.00 -3 3 -10 293.37 11.10 -3 3 -10 277.87 12.70 -3 3 -10 298.37 11.20 3 -3 10 293.67 11.10 3 -3 10 288.87 11.50 3 -3 10 289.97 11.40 3 -3 10 295.27 11.20 3 -3 10 290.17 11.40 -4 3 -10 13.80 1.50 -4 3 -10 11.70 1.50 -4 3 -10 12.10 3.80 -4 3 -10 11.70 1.10 4 -3 10 10.80 1.60 4 -3 10 11.50 1.40 4 -3 10 10.90 1.30 4 -3 10 10.80 1.70 4 -3 10 7.60 1.80 -5 3 -10 41.90 2.40 -5 3 -10 55.59 7.80 -5 3 -10 43.40 2.50 -5 3 -10 44.00 2.30 5 -3 10 40.20 2.50 5 -3 10 42.70 2.90 5 -3 10 44.00 2.90 5 -3 10 42.00 2.60 -6 3 -10 59.09 2.80 -6 3 -10 56.59 2.70 6 -3 10 58.09 3.50 6 -3 10 59.89 3.10 6 -3 10 61.19 3.40 6 -3 10 58.39 3.00 -7 3 -10 24.70 2.00 -7 3 -10 23.50 1.10 -7 3 -10 21.60 1.40 7 -3 10 23.70 2.00 7 -3 10 22.70 1.90 7 -3 10 21.40 2.70 7 -3 10 22.20 1.60 -8 3 -10 14.40 1.20 8 -3 10 10.60 1.90 -7 -2 10 35.30 1.70 -7 -2 10 35.20 1.80 -7 -2 10 34.00 1.70 6 2 -10 135.79 6.10 -6 -2 10 143.69 5.70 -6 -2 10 142.19 5.80 -6 -2 10 136.49 5.60 -6 -2 10 136.19 5.90 -6 -2 10 137.49 5.60 5 2 -10 97.19 4.90 5 2 -10 95.39 4.20 -5 -2 10 97.09 4.30 -5 -2 10 96.39 4.70 -5 -2 10 98.19 4.80 -5 -2 10 95.69 4.40 -5 -2 10 93.29 4.50 -4 -2 10 133.99 5.60 -4 -2 10 131.39 6.30 -4 -2 10 137.19 5.80 -4 -2 10 128.19 6.00 -4 -2 10 134.99 6.20 3 2 -10 32.00 2.50 3 2 -10 30.70 2.20 -3 -2 10 34.10 2.50 -3 -2 10 34.50 2.60 -3 -2 10 36.90 2.20 -3 -2 10 32.70 2.60 -3 -2 10 34.10 2.30 -3 -2 10 30.30 2.10 2 2 -10 5.80 1.00 2 2 -10 3.90 1.10 -2 -2 10 4.70 0.90 -2 -2 10 4.80 2.70 -2 -2 10 6.30 1.30 -2 -2 10 6.60 1.00 -2 -2 10 5.50 1.20 -2 -2 10 2.20 1.00 1 2 -10 491.15 17.90 -1 -2 10 477.05 17.90 -1 -2 10 507.95 18.70 -1 -2 10 498.55 18.10 -1 -2 10 508.95 18.30 -1 -2 10 500.55 18.40 -1 -2 10 481.85 17.90 -1 -2 10 464.95 17.70 0 2 -10 1.30 0.60 0 2 -10 1.30 0.80 0 2 -10 1.40 0.80 0 2 -10 0.00 5.80 0 2 -10 1.40 0.60 0 -2 10 3.50 1.10 0 -2 10 3.20 0.90 0 -2 10 1.70 1.00 0 -2 10 0.30 1.00 0 -2 10 1.80 1.00 0 -2 10 1.20 0.70 0 -2 10 0.20 1.30 -1 2 -10 47.50 3.20 -1 2 -10 51.89 7.90 -1 2 -10 49.10 2.70 -1 2 -10 53.29 2.70 -1 2 -10 53.09 3.30 1 -2 10 51.99 2.80 1 -2 10 49.30 2.90 1 -2 10 52.49 3.10 1 -2 10 49.00 3.50 -2 2 -10 10.20 9.30 -2 2 -10 8.80 2.80 -2 2 -10 7.80 1.10 -2 2 -10 10.20 1.50 -2 2 -10 7.50 1.50 -2 2 -10 6.10 0.90 2 -2 10 6.70 1.20 2 -2 10 7.00 1.40 2 -2 10 7.20 1.20 2 -2 10 6.80 1.50 2 -2 10 7.00 1.00 -3 2 -10 279.07 12.10 -3 2 -10 289.77 10.90 -3 2 -10 290.27 10.90 3 -2 10 281.17 11.20 3 -2 10 285.47 11.10 3 -2 10 294.67 10.80 3 -2 10 283.67 10.80 3 -2 10 280.47 10.90 -4 2 -10 156.58 8.50 -4 2 -10 156.18 6.50 -4 2 -10 159.18 6.20 -4 2 -10 152.98 6.30 -4 2 -10 155.58 6.30 4 -2 10 143.49 6.80 4 -2 10 154.48 6.30 4 -2 10 155.18 6.50 4 -2 10 153.68 6.40 4 -2 10 153.78 6.60 -5 2 -10 173.78 7.50 -5 2 -10 201.08 7.70 -5 2 -10 188.18 7.70 -5 2 -10 192.38 10.30 -5 2 -10 204.18 7.70 5 -2 10 203.18 7.80 5 -2 10 199.88 8.40 5 -2 10 201.28 8.20 5 -2 10 197.58 7.80 -6 2 -10 28.90 2.10 -6 2 -10 34.60 2.10 -6 2 -10 33.00 1.90 -6 2 -10 31.60 6.00 6 -2 10 32.60 2.10 6 -2 10 31.30 2.30 6 -2 10 31.70 2.40 6 -2 10 35.20 2.20 -7 2 -10 110.09 5.00 -7 2 -10 116.79 4.50 -7 2 -10 100.39 4.40 -7 2 -10 119.59 4.80 7 -2 10 115.29 4.90 7 -2 10 120.29 5.30 7 -2 10 119.79 5.00 -8 2 -10 21.30 1.70 -8 2 -10 23.70 1.80 8 -2 10 21.50 2.10 8 -2 10 15.80 1.50 8 -2 10 19.90 2.90 8 -2 10 23.30 1.80 6 1 -10 187.18 8.30 6 1 -10 208.48 8.30 -6 -1 10 204.58 8.00 -6 -1 10 204.08 7.60 -6 -1 10 201.68 7.80 -6 -1 10 200.08 7.90 -6 -1 10 200.68 7.70 5 1 -10 5.30 1.20 -5 -1 10 4.60 1.10 -5 -1 10 5.30 1.20 -5 -1 10 3.90 1.00 -5 -1 10 4.90 0.80 -5 -1 10 5.70 1.00 4 1 -10 0.10 1.10 4 1 -10 1.30 0.90 -4 -1 10 0.00 0.50 -4 -1 10 0.80 0.80 -4 -1 10 0.20 0.60 -4 -1 10 1.30 1.00 -4 -1 10 -0.20 0.70 3 1 -10 1.20 0.80 3 1 -10 0.30 0.80 -3 -1 10 1.40 0.60 -3 -1 10 1.40 0.90 -3 -1 10 1.70 0.90 -3 -1 10 1.40 0.70 -3 -1 10 2.00 0.90 2 1 -10 237.48 9.20 -2 -1 10 247.38 9.80 -2 -1 10 234.78 9.70 -2 -1 10 240.08 9.20 -2 -1 10 239.68 9.30 -2 -1 10 233.18 9.10 1 1 -10 262.17 10.80 -1 -1 10 258.57 10.20 -1 -1 10 274.47 10.90 -1 -1 10 273.77 10.70 -1 -1 10 267.37 10.20 -1 -1 10 275.27 10.70 -1 -1 10 276.77 10.90 0 1 -10 19.70 1.50 0 1 -10 17.30 1.70 0 1 -10 15.30 1.80 0 -1 10 18.60 1.80 0 -1 10 18.90 2.20 0 -1 10 18.00 1.50 0 -1 10 20.50 2.20 0 -1 10 18.00 1.90 0 -1 10 18.70 1.80 -1 1 -10 27.30 1.80 -1 1 -10 26.50 1.80 -1 1 -10 29.60 2.40 -1 1 -10 40.40 6.10 1 -1 10 26.90 1.80 1 -1 10 27.00 2.00 1 -1 10 21.80 2.30 1 -1 10 28.80 1.80 -2 1 -10 207.08 8.10 -2 1 -10 209.58 8.20 -2 1 -10 211.08 8.10 -2 1 -10 210.48 13.70 -2 1 -10 203.98 8.80 2 -1 10 217.98 8.00 2 -1 10 212.68 8.20 2 -1 10 208.68 8.30 2 -1 10 214.58 8.10 2 -1 10 201.38 8.20 -3 1 -10 438.56 14.90 -3 1 -10 377.66 15.40 -3 1 -10 397.46 14.70 -3 1 -10 386.76 23.90 3 -1 10 390.36 14.60 3 -1 10 374.76 14.70 3 -1 10 431.96 15.20 3 -1 10 393.96 14.70 3 -1 10 396.96 14.90 -4 1 -10 125.89 7.10 -4 1 -10 124.49 5.30 -4 1 -10 126.29 5.20 -4 1 -10 119.59 5.40 -4 1 -10 121.59 5.20 4 -1 10 127.79 5.90 4 -1 10 123.89 5.40 4 -1 10 129.09 5.60 4 -1 10 131.19 5.30 4 -1 10 126.39 5.20 -5 1 -10 98.09 7.00 -5 1 -10 97.09 4.30 -5 1 -10 96.69 4.60 -5 1 -10 96.99 4.30 5 -1 10 99.09 4.50 5 -1 10 100.69 4.70 5 -1 10 104.19 4.40 5 -1 10 99.39 4.40 -6 1 -10 114.39 4.80 -6 1 -10 117.09 8.50 -6 1 -10 113.29 4.90 6 -1 10 114.79 5.00 6 -1 10 113.99 5.10 6 -1 10 111.69 5.20 6 -1 10 104.59 5.00 -7 1 -10 23.10 1.40 -7 1 -10 20.10 1.80 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16 47.30 2.40 -6 0 -16 1.30 0.30 6 0 16 0.10 0.40 1 -1 -16 72.29 4.00 1 -1 -16 74.69 3.10 -1 1 16 71.29 3.20 -1 1 16 72.09 3.00 0 -1 -16 64.49 2.90 0 -1 -16 66.69 2.90 0 -1 -16 63.99 3.50 0 1 16 62.89 2.70 0 1 16 66.09 2.90 -1 -1 -16 109.39 4.40 -1 -1 -16 110.19 4.40 -1 -1 -16 96.39 6.40 1 1 16 108.09 4.40 1 1 16 110.79 4.40 -2 -1 -16 0.30 0.70 -2 -1 -16 0.50 0.40 -2 -1 -16 -0.50 1.00 2 1 16 1.90 0.90 2 1 16 0.60 0.40 -3 -1 -16 69.59 3.30 -3 -1 -16 74.29 3.20 -3 -1 -16 71.09 3.10 3 1 16 71.39 3.30 -4 -1 -16 107.29 4.30 -4 -1 -16 109.49 4.30 4 1 16 105.39 4.10 4 1 16 105.19 4.50 -5 -1 -16 59.59 2.60 5 1 16 58.89 2.80 5 1 16 58.29 2.50 -6 -1 -16 3.30 0.50 6 1 16 3.80 0.50 6 1 16 2.30 1.50 1 -2 -16 0.60 0.60 1 -2 -16 0.60 0.30 -1 2 16 0.70 0.40 0 -2 -16 126.89 5.70 0 -2 -16 131.49 5.10 0 -2 -16 135.69 5.10 0 2 16 130.59 4.90 0 2 16 132.69 5.20 0 2 16 131.99 5.00 -1 -2 -16 169.28 6.30 -1 -2 -16 159.78 6.20 1 2 16 160.48 6.20 1 2 16 162.18 6.30 -2 -2 -16 15.10 1.40 -2 -2 -16 14.70 1.50 -2 -2 -16 18.50 1.30 2 2 16 16.20 1.20 2 2 16 14.80 1.20 -3 -2 -16 1.50 0.50 -3 -2 -16 2.70 1.20 -3 -2 -16 1.90 0.50 3 2 16 1.80 0.70 3 2 16 1.40 0.60 -4 -2 -16 156.68 6.00 4 2 16 154.68 5.80 4 2 16 157.48 6.20 -5 -2 -16 116.79 4.70 -5 -2 -16 129.99 5.00 5 2 16 134.09 4.90 5 2 16 132.49 5.20 -6 -2 -16 0.30 0.30 6 2 16 0.40 0.40 6 2 16 -0.20 0.90 -7 -2 -16 0.30 0.30 7 2 16 -0.10 0.40 0 -3 -16 31.50 1.70 0 -3 -16 32.20 1.60 0 -3 -16 29.80 2.40 0 3 16 31.20 1.70 -1 -3 -16 100.39 5.70 -1 -3 -16 115.09 4.40 -1 -3 -16 108.59 4.40 1 3 16 114.39 4.30 1 3 16 109.19 4.50 -2 -3 -16 44.20 2.10 -2 -3 -16 40.10 2.20 2 3 16 41.00 2.10 -3 -3 -16 0.10 0.30 -3 -3 -16 -0.30 0.50 3 3 16 0.10 0.40 -4 -3 -16 103.29 4.20 -4 -3 -16 102.89 4.20 4 3 16 101.39 3.90 4 3 16 104.79 4.30 -5 -3 -16 161.88 6.10 5 3 16 159.08 5.90 5 3 16 158.78 6.20 -6 -3 -16 21.90 1.20 6 3 16 20.60 1.20 6 3 16 20.80 1.60 -7 -3 -16 22.70 1.20 7 3 16 23.70 1.20 0 -4 -16 8.30 0.70 0 4 16 9.00 0.90 -1 -4 -16 134.09 6.10 -1 -4 -16 156.78 5.70 1 4 16 150.98 5.50 1 4 16 151.38 5.80 -2 -4 -16 124.49 4.80 -2 -4 -16 112.39 5.30 2 4 16 122.79 4.70 -3 -4 -16 4.10 0.60 -3 -4 -16 5.20 0.80 3 4 16 4.30 0.70 -4 -4 -16 63.99 2.80 -4 -4 -16 62.19 2.70 4 4 16 64.49 2.80 4 4 16 59.29 2.80 -5 -4 -16 4.70 0.60 5 4 16 6.10 0.90 5 4 16 4.10 0.60 -6 -4 -16 80.49 3.30 6 4 16 81.69 3.50 6 4 16 80.79 3.20 -7 -4 -16 25.30 1.20 7 4 16 25.20 1.30 -1 -5 -16 40.80 1.90 1 5 16 40.30 1.70 1 5 16 39.90 2.00 -2 -5 -16 134.49 5.10 2 5 16 131.79 5.00 -3 -5 -16 0.60 0.30 -3 -5 -16 2.30 0.60 3 5 16 1.10 0.40 -4 -5 -16 25.80 1.40 -4 -5 -16 26.50 1.40 4 5 16 26.50 1.50 -5 -5 -16 64.89 2.70 5 5 16 61.99 2.60 5 5 16 63.89 2.80 -6 -5 -16 92.99 3.70 6 5 16 93.89 3.60 6 5 16 94.89 3.90 -7 -5 -16 8.50 0.60 7 5 16 6.40 0.90 -2 -6 -16 29.00 1.40 2 6 16 29.80 1.40 -3 -6 -16 63.19 2.60 3 6 16 62.79 2.60 -4 -6 -16 3.10 0.50 -4 -6 -16 2.70 0.40 4 6 16 3.40 0.50 -5 -6 -16 92.89 3.50 -5 -6 -16 94.39 3.70 5 6 16 94.79 3.80 -6 -6 -16 89.89 3.50 6 6 16 91.29 3.40 6 6 16 90.69 3.70 -7 -6 -16 25.60 1.20 7 6 16 23.70 1.10 -3 -7 -16 15.90 0.90 3 7 16 14.50 0.90 -4 -7 -16 4.00 0.50 -4 -7 -16 4.50 0.60 4 7 16 4.60 0.50 -5 -7 -16 18.80 1.00 5 7 16 18.70 1.10 -6 -7 -16 50.59 2.30 6 7 16 66.99 2.90 -2 1 -17 5.00 0.60 2 -1 17 5.80 0.70 -3 1 -17 19.50 1.20 3 -1 17 22.30 1.30 -1 0 -17 -0.20 0.40 1 0 17 0.60 0.40 -2 0 -17 14.10 0.90 2 0 17 13.70 1.00 -3 0 -17 76.19 3.00 -3 0 -17 73.39 3.10 3 0 17 75.69 3.10 -4 0 -17 34.90 1.60 4 0 17 33.20 1.70 -1 -1 -17 9.10 0.80 1 1 17 8.20 0.90 -2 -1 -17 1.20 0.40 2 1 17 0.50 0.40 -3 -1 -17 161.08 6.00 -3 -1 -17 165.08 6.00 3 1 17 154.68 6.10 -4 -1 -17 26.60 1.40 4 1 17 25.60 1.60 -5 -1 -17 5.30 0.60 5 1 17 5.50 0.80 -1 -2 -17 151.68 5.50 1 2 17 123.59 5.30 1 2 17 139.59 5.10 -2 -2 -17 40.20 1.90 2 2 17 38.10 1.80 -3 -2 -17 47.30 2.20 3 2 17 47.50 2.20 -4 -2 -17 5.00 0.60 -4 -2 -17 3.80 0.50 4 2 17 3.30 0.50 -5 -2 -17 48.30 2.10 5 2 17 47.20 2.20 -1 -3 -17 119.19 4.40 1 3 17 113.09 4.10 1 3 17 110.49 4.30 -2 -3 -17 0.60 0.30 2 3 17 1.40 0.40 2 3 17 1.40 0.50 -3 -3 -17 28.20 1.40 -3 -3 -17 26.10 1.60 3 3 17 27.30 1.50 3 3 17 28.60 1.50 -4 -3 -17 45.80 2.10 -4 -3 -17 47.60 2.00 4 3 17 47.60 2.20 -5 -3 -17 91.09 3.60 5 3 17 92.29 3.70 2 4 17 8.10 0.80 2 4 17 10.10 0.80 -3 -4 -17 0.10 0.30 3 4 17 0.70 0.40 3 4 17 0.30 0.30 -4 -4 -17 21.50 1.20 -4 -4 -17 22.10 1.10 4 4 17 21.70 1.30 4 4 17 21.50 1.80 -5 -4 -17 114.19 4.30 5 4 17 113.79 4.40 -3 -5 -17 36.00 1.60 3 5 17 36.20 1.70 3 5 17 37.60 1.70 -4 -5 -17 24.20 1.30 -4 -5 -17 25.60 1.20 4 5 17 25.30 1.40 -5 -5 -17 15.50 1.00 5 5 17 17.50 1.10 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 40892 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn1 Zn 0.88415(2) 0.53405(2) 0.43513(2) 0.02758(7) Uani 1 1 d . . . . . O1 O 0.88881(12) 0.58413(11) 0.55838(7) 0.0314(2) Uani 1 1 d . . . . . N1 N 0.75856(14) 0.43038(13) 0.41907(9) 0.0255(3) Uani 1 1 d . . . . . C1 C 0.77733(17) 0.49487(15) 0.25402(10) 0.0244(3) Uani 1 1 d . . . . . N2 N 0.74139(14) 0.41612(13) 0.33405(8) 0.0247(3) Uani 1 1 d . . . . . C2 C 0.75602(17) 0.46073(14) 0.16233(10) 0.0232(3) Uani 1 1 d . . . . . C3 C 0.68559(19) 0.36689(15) 0.16361(10) 0.0274(3) Uani 1 1 d . . . . . H3 H 0.649991 0.322796 0.224059 0.033 Uiso 1 1 calc R U . . . N3 N 0.81548(14) 0.60508(13) 0.24350(9) 0.0256(3) Uani 1 1 d . . . . . C4 C 0.66716(19) 0.33748(15) 0.07716(11) 0.0277(3) Uani 1 1 d . . . . . H4 H 0.619114 0.273249 0.079625 0.033 Uiso 1 1 calc R U . . . N4 N 0.85259(15) 0.64335(13) 0.31364(9) 0.0277(3) Uani 1 1 d . . . . . C5 C 0.71750(17) 0.40001(14) -0.01305(10) 0.0238(3) Uani 1 1 d . . . . . C6 C 0.78759(19) 0.49250(15) -0.01373(10) 0.0275(3) Uani 1 1 d . . . . . H6 H 0.822887 0.536692 -0.074200 0.033 Uiso 1 1 calc R U . . . C8 C 0.69639(19) 0.36831(16) -0.10673(10) 0.0287(3) Uani 1 1 d . . . . . H8A H 0.704314 0.439880 -0.157219 0.043 Uiso 1 1 calc R U . . . H8B H 0.588944 0.360940 -0.094282 0.043 Uiso 1 1 calc R U . . . H8C H 0.782219 0.283541 -0.129468 0.043 Uiso 1 1 calc R U . . . C7 C 0.80751(18) 0.52220(16) 0.07223(11) 0.0277(3) Uani 1 1 d . . . . . H7 H 0.857091 0.585515 0.069302 0.033 Uiso 1 1 calc R U . . . C9 C 0.70617(17) 0.34430(15) 0.49593(10) 0.0255(3) Uani 1 1 d . . . . . C10 C 0.65651(18) 0.38507(16) 0.59195(11) 0.0281(3) Uani 1 1 d . . . . . H10 H 0.657629 0.468094 0.604076 0.034 Uiso 1 1 calc R U . . . C11 C 0.60570(19) 0.30397(17) 0.66931(11) 0.0310(3) Uani 1 1 d . . . . . H11 H 0.570282 0.332264 0.734507 0.037 Uiso 1 1 calc R U . . . C12 C 0.6061(2) 0.18179(18) 0.65238(12) 0.0344(3) Uani 1 1 d . . . . . H12 H 0.570641 0.126588 0.705667 0.041 Uiso 1 1 calc R U . . . C13 C 0.6589(2) 0.14045(17) 0.55660(12) 0.0358(4) Uani 1 1 d . . . . . H13 H 0.661001 0.056079 0.544892 0.043 Uiso 1 1 calc R U . . . C14 C 0.70805(19) 0.22117(16) 0.47856(11) 0.0312(3) Uani 1 1 d . . . . . H14 H 0.742970 0.192801 0.413406 0.037 Uiso 1 1 calc R U . . . C15 C 0.88003(18) 0.76597(15) 0.29031(12) 0.0312(3) Uani 1 1 d . . . . . C16 C 0.93917(19) 0.80572(18) 0.35627(13) 0.0369(4) Uani 1 1 d . . . . . H16 H 0.956470 0.752334 0.414685 0.044 Uiso 1 1 calc R U . . . C17 C 0.9724(2) 0.92215(19) 0.33668(16) 0.0451(5) Uani 1 1 d . . . . . H17 H 1.013662 0.947856 0.381339 0.054 Uiso 1 1 calc R U . . . C18 C 0.9461(2) 1.00119(18) 0.25294(18) 0.0506(5) Uani 1 1 d . . . . . H18 H 0.968983 1.081267 0.239612 0.061 Uiso 1 1 calc R U . . . C19 C 0.8856(3) 0.96269(18) 0.18800(18) 0.0533(5) Uani 1 1 d . . . . . H19 H 0.866846 1.017213 0.130245 0.064 Uiso 1 1 calc R U . . . C20 C 0.8525(2) 0.84584(16) 0.20648(15) 0.0431(4) Uani 1 1 d . . . . . H20 H 0.810913 0.820659 0.161694 0.052 Uiso 1 1 calc R U . . . C21 C 0.77585(17) 0.67826(15) 0.62097(10) 0.0246(3) Uani 1 1 d . . . . . C22 C 0.80182(19) 0.68386(16) 0.71141(11) 0.0297(3) Uani 1 1 d . . . . . H22 H 0.897907 0.622615 0.729265 0.036 Uiso 1 1 calc R U . . . C23 C 0.6868(2) 0.77931(17) 0.77549(11) 0.0353(4) Uani 1 1 d . . . . . H23 H 0.705045 0.783323 0.837142 0.042 Uiso 1 1 calc R U . . . C24 C 0.5464(2) 0.86840(16) 0.75093(12) 0.0326(3) Uani 1 1 d . . . . . H24 H 0.468098 0.933225 0.795421 0.039 Uiso 1 1 calc R U . . . C25 C 0.52021(19) 0.86270(16) 0.66084(12) 0.0315(3) Uani 1 1 d . . . . . H25 H 0.423745 0.923845 0.643353 0.038 Uiso 1 1 calc R U . . . C26 C 0.63527(19) 0.76736(16) 0.59588(11) 0.0301(3) Uani 1 1 d . . . . . H26 H 0.617051 0.763583 0.534169 0.036 Uiso 1 1 calc R U . . . C27 C 0.8669(4) 0.8465(3) -0.0397(2) 0.0355(7) Uani 0.5 1 d . . P A -1 H27A H 0.904735 0.808507 -0.104107 0.053 Uiso 0.5 1 calc R U P A -1 H27B H 0.885782 0.774062 0.011393 0.053 Uiso 0.5 1 calc R U P A -1 H27C H 0.927345 0.903354 -0.038599 0.053 Uiso 0.5 1 calc R U P A -1 C28 C 0.6766(15) 0.9334(13) -0.0196(11) 0.0332(19) Uani 0.5 1 d G . P A -1 C29 C 0.5646(14) 0.8840(12) 0.0466(10) 0.0268(13) Uani 0.5 1 d G . P A -1 H29 H 0.602070 0.801231 0.082483 0.032 Uiso 0.5 1 calc R U P A -1 C30 C 0.3979(14) 0.9558(12) 0.0604(10) 0.0307(15) Uani 0.5 1 d G . P A -1 H30 H 0.321328 0.922075 0.105627 0.037 Uiso 0.5 1 calc R U P A -1 C31 C 0.3431(15) 1.0770(12) 0.0079(10) 0.036(2) Uani 0.5 1 d G . P A -1 H31 H 0.229081 1.126059 0.017299 0.043 Uiso 0.5 1 calc R U P A -1 C32 C 0.4550(16) 1.1264(13) -0.0583(11) 0.045(3) Uani 0.5 1 d G . P A -1 H32 H 0.417577 1.209201 -0.094173 0.054 Uiso 0.5 1 calc R U P A -1 C33 C 0.6218(16) 1.0546(14) -0.0721(11) 0.039(2) Uani 0.5 1 d G . P A -1 H33 H 0.698321 1.088359 -0.117319 0.047 Uiso 0.5 1 calc R U P A -1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zn1 0.02090(11) 0.04291(13) 0.02229(11) -0.01638(8) -0.00777(8) -0.00767(9) O1 0.0210(5) 0.0480(6) 0.0251(5) -0.0218(5) -0.0072(4) -0.0038(5) N1 0.0203(6) 0.0373(7) 0.0202(6) -0.0113(5) -0.0074(5) -0.0061(5) C1 0.0192(7) 0.0340(7) 0.0219(7) -0.0107(6) -0.0076(5) -0.0062(6) N2 0.0199(6) 0.0363(7) 0.0190(6) -0.0107(5) -0.0075(4) -0.0057(5) C2 0.0197(6) 0.0309(7) 0.0204(7) -0.0095(5) -0.0082(5) -0.0051(6) C3 0.0325(8) 0.0342(8) 0.0199(7) -0.0027(6) -0.0094(6) -0.0142(6) N3 0.0201(6) 0.0338(6) 0.0252(6) -0.0138(5) -0.0089(5) -0.0048(5) C4 0.0341(8) 0.0319(7) 0.0240(7) -0.0048(6) -0.0109(6) -0.0153(6) N4 0.0204(6) 0.0351(7) 0.0300(6) -0.0158(5) -0.0100(5) -0.0044(5) C5 0.0226(7) 0.0292(7) 0.0200(7) -0.0076(5) -0.0078(5) -0.0055(6) C6 0.0305(8) 0.0357(8) 0.0190(7) -0.0043(6) -0.0060(6) -0.0137(6) C8 0.0335(8) 0.0362(8) 0.0202(7) -0.0081(6) -0.0096(6) -0.0120(6) C7 0.0279(7) 0.0355(8) 0.0251(7) -0.0083(6) -0.0064(6) -0.0147(6) C9 0.0189(7) 0.0367(8) 0.0209(7) -0.0079(6) -0.0088(5) -0.0048(6) C10 0.0235(7) 0.0372(8) 0.0239(7) -0.0110(6) -0.0092(6) -0.0054(6) C11 0.0260(7) 0.0453(9) 0.0205(7) -0.0090(6) -0.0084(6) -0.0068(7) C12 0.0332(8) 0.0439(9) 0.0276(8) -0.0010(7) -0.0125(6) -0.0123(7) C13 0.0408(9) 0.0385(9) 0.0321(8) -0.0064(7) -0.0151(7) -0.0125(7) C14 0.0319(8) 0.0387(8) 0.0248(7) -0.0110(6) -0.0114(6) -0.0079(7) C15 0.0207(7) 0.0304(8) 0.0430(9) -0.0192(7) -0.0126(6) 0.0004(6) C16 0.0262(8) 0.0428(9) 0.0452(10) -0.0224(7) -0.0132(7) -0.0054(7) C17 0.0297(9) 0.0435(10) 0.0685(13) -0.0307(9) -0.0200(8) -0.0036(7) C18 0.0417(10) 0.0289(9) 0.0874(16) -0.0204(9) -0.0306(10) -0.0023(8) C19 0.0572(12) 0.0282(9) 0.0837(15) -0.0062(9) -0.0452(12) -0.0042(8) C20 0.0457(10) 0.0273(8) 0.0650(12) -0.0108(8) -0.0373(9) -0.0022(7) C21 0.0232(7) 0.0330(7) 0.0205(7) -0.0118(5) -0.0012(5) -0.0121(6) C22 0.0322(8) 0.0346(8) 0.0221(7) -0.0090(6) -0.0085(6) -0.0078(6) C23 0.0443(9) 0.0376(8) 0.0227(7) -0.0127(6) -0.0068(7) -0.0100(7) C24 0.0373(9) 0.0291(8) 0.0280(8) -0.0127(6) 0.0011(6) -0.0104(7) C25 0.0271(8) 0.0325(8) 0.0331(8) -0.0076(6) -0.0051(6) -0.0081(6) C26 0.0262(7) 0.0416(9) 0.0251(7) -0.0110(6) -0.0070(6) -0.0111(7) C27 0.0344(17) 0.0392(17) 0.0302(16) 0.0014(13) -0.0055(13) -0.0135(14) C28 0.049(3) 0.040(4) 0.022(3) -0.002(3) -0.009(2) -0.028(3) C29 0.038(3) 0.021(2) 0.027(3) 0.007(2) -0.016(2) -0.014(3) C30 0.044(3) 0.030(3) 0.027(3) 0.003(3) -0.011(3) -0.023(3) C31 0.057(5) 0.021(3) 0.034(5) 0.000(3) -0.029(5) -0.006(4) C32 0.074(7) 0.032(4) 0.034(4) 0.005(3) -0.018(4) -0.024(4) C33 0.055(4) 0.031(3) 0.032(4) 0.004(2) -0.012(3) -0.019(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn -1.5491 0.6778 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Zn1 N4 129.69(5) . . ? O1 Zn1 N1 126.12(5) . . ? N4 Zn1 N1 92.25(5) . . ? O1 Zn1 O1 80.09(4) . 2_766 ? N4 Zn1 O1 118.30(5) . 2_766 ? N1 Zn1 O1 111.38(5) . 2_766 ? O1 Zn1 Zn1 40.79(3) . 2_766 ? N4 Zn1 Zn1 136.48(4) . 2_766 ? N1 Zn1 Zn1 128.37(4) . 2_766 ? O1 Zn1 Zn1 39.30(3) 2_766 2_766 ? C21 O1 Zn1 131.06(9) . . ? C21 O1 Zn1 128.92(9) . 2_766 ? Zn1 O1 Zn1 99.90(4) . 2_766 ? N2 N1 C9 113.73(12) . . ? N2 N1 Zn1 123.17(10) . . ? C9 N1 Zn1 122.06(9) . . ? N3 C1 N2 131.63(12) . . ? N3 C1 C2 114.12(13) . . ? N2 C1 C2 113.98(12) . . ? N1 N2 C1 121.49(12) . . ? C7 C2 C3 117.86(12) . . ? C7 C2 C1 120.23(13) . . ? C3 C2 C1 121.91(13) . . ? C4 C3 C2 120.55(14) . . ? C4 C3 H3 119.7 . . ? C2 C3 H3 119.7 . . ? N4 N3 C1 122.46(13) . . ? C3 C4 C5 121.57(14) . . ? C3 C4 H4 119.2 . . ? C5 C4 H4 119.2 . . ? N3 N4 C15 113.89(13) . . ? N3 N4 Zn1 122.89(10) . . ? C15 N4 Zn1 123.06(9) . . ? C6 C5 C4 117.52(13) . . ? C6 C5 C8 121.09(13) . . ? C4 C5 C8 121.39(13) . . ? C5 C6 C7 121.43(14) . . ? C5 C6 H6 119.3 . . ? C7 C6 H6 119.3 . . ? C5 C8 H8A 109.5 . . ? C5 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C5 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C2 C7 C6 121.07(13) . . ? C2 C7 H7 119.5 . . ? C6 C7 H7 119.5 . . ? C14 C9 C10 120.04(14) . . ? C14 C9 N1 122.28(13) . . ? C10 C9 N1 117.65(13) . . ? C11 C10 C9 119.70(14) . . ? C11 C10 H10 120.1 . . ? C9 C10 H10 120.1 . . ? C10 C11 C12 120.50(14) . . ? C10 C11 H11 119.7 . . ? C12 C11 H11 119.7 . . ? C11 C12 C13 119.53(16) . . ? C11 C12 H12 120.2 . . ? C13 C12 H12 120.2 . . ? C14 C13 C12 120.56(16) . . ? C14 C13 H13 119.7 . . ? C12 C13 H13 119.7 . . ? C13 C14 C9 119.65(14) . . ? C13 C14 H14 120.2 . . ? C9 C14 H14 120.2 . . ? C20 C15 C16 119.29(16) . . ? C20 C15 N4 123.34(13) . . ? C16 C15 N4 117.36(15) . . ? C17 C16 C15 120.26(18) . . ? C17 C16 H16 119.9 . . ? C15 C16 H16 119.9 . . ? C18 C17 C16 120.48(16) . . ? C18 C17 H17 119.8 . . ? C16 C17 H17 119.8 . . ? C17 C18 C19 119.33(18) . . ? C17 C18 H18 120.3 . . ? C19 C18 H18 120.3 . . ? C20 C19 C18 120.8(2) . . ? C20 C19 H19 119.6 . . ? C18 C19 H19 119.6 . . ? C15 C20 C19 119.80(16) . . ? C15 C20 H20 120.1 . . ? C19 C20 H20 120.1 . . ? O1 C21 C26 120.76(12) . . ? O1 C21 C22 119.50(13) . . ? C26 C21 C22 119.73(13) . . ? C23 C22 C21 119.67(15) . . ? C23 C22 H22 120.2 . . ? C21 C22 H22 120.2 . . ? C24 C23 C22 120.88(14) . . ? C24 C23 H23 119.6 . . ? C22 C23 H23 119.6 . . ? C23 C24 C25 119.48(14) . . ? C23 C24 H24 120.3 . . ? C25 C24 H24 120.3 . . ? C24 C25 C26 120.05(15) . . ? C24 C25 H25 120.0 . . ? C26 C25 H25 120.0 . . ? C21 C26 C25 120.18(14) . . ? C21 C26 H26 119.9 . . ? C25 C26 H26 119.9 . . ? C28 C27 H27A 109.5 . . ? C28 C27 H27B 109.5 . . ? H27A C27 H27B 109.5 . . ? C28 C27 H27C 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? C29 C28 C33 120.0 . . ? C29 C28 C27 119.6(6) . . ? C33 C28 C27 120.3(6) . . ? C30 C29 C28 120.0 . . ? C30 C29 H29 120.0 . . ? C28 C29 H29 120.0 . . ? C31 C30 C29 120.0 . . ? C31 C30 H30 120.0 . . ? C29 C30 H30 120.0 . . ? C32 C31 C30 120.0 . . ? C32 C31 H31 120.0 . . ? C30 C31 H31 120.0 . . ? C31 C32 C33 120.0 . . ? C31 C32 H32 120.0 . . ? C33 C32 H32 120.0 . . ? C32 C33 C28 120.0 . . ? C32 C33 H33 120.0 . . ? C28 C33 H33 120.0 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zn1 O1 1.9352(10) . ? Zn1 N4 1.9612(13) . ? Zn1 N1 1.9694(12) . ? Zn1 O1 1.9959(10) 2_766 ? Zn1 Zn1 3.0095(4) 2_766 ? O1 C21 1.3617(17) . ? N1 N2 1.3048(16) . ? N1 C9 1.420(2) . ? C1 N3 1.347(2) . ? C1 N2 1.351(2) . ? C1 C2 1.4961(18) . ? C2 C7 1.390(2) . ? C2 C3 1.397(2) . ? C3 C4 1.390(2) . ? C3 H3 0.9500 . ? N3 N4 1.3129(16) . ? C4 C5 1.394(2) . ? C4 H4 0.9500 . ? N4 C15 1.420(2) . ? C5 C6 1.384(2) . ? C5 C8 1.5107(18) . ? C6 C7 1.392(2) . ? C6 H6 0.9500 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C7 H7 0.9500 . ? C9 C14 1.393(2) . ? C9 C10 1.3973(19) . ? C10 C11 1.384(2) . ? C10 H10 0.9500 . ? C11 C12 1.386(2) . ? C11 H11 0.9500 . ? C12 C13 1.394(2) . ? C12 H12 0.9500 . ? C13 C14 1.382(2) . ? C13 H13 0.9500 . ? C14 H14 0.9500 . ? C15 C20 1.383(3) . ? C15 C16 1.402(2) . ? C16 C17 1.381(3) . ? C16 H16 0.9500 . ? C17 C18 1.376(3) . ? C17 H17 0.9500 . ? C18 C19 1.391(3) . ? C18 H18 0.9500 . ? C19 C20 1.385(3) . ? C19 H19 0.9500 . ? C20 H20 0.9500 . ? C21 C26 1.382(2) . ? C21 C22 1.389(2) . ? C22 C23 1.387(2) . ? C22 H22 0.9500 . ? C23 C24 1.378(2) . ? C23 H23 0.9500 . ? C24 C25 1.386(2) . ? C24 H24 0.9500 . ? C25 C26 1.393(2) . ? C25 H25 0.9500 . ? C26 H26 0.9500 . ? C27 C28 1.592(13) . ? C27 H27A 0.9800 . ? C27 H27B 0.9800 . ? C27 H27C 0.9800 . ? C28 C29 1.3900 . ? C28 C33 1.3900 . ? C29 C30 1.3900 . ? C29 H29 0.9500 . ? C30 C31 1.3900 . ? C30 H30 0.9500 . ? C31 C32 1.3900 . ? C31 H31 0.9500 . ? C32 C33 1.3900 . ? C32 H32 0.9500 . ? C33 H33 0.9500 . ?