#------------------------------------------------------------------------------ #$Date: 2022-04-03 21:10:54 +0100 (Sun, 03 Apr 2022) $ #$Revision: 274257 $ #$URL: svn://www.crystallography.net/cod/cif/4/51/94/4519400.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519400 loop_ _publ_author_name 'Zhang, Tingting' 'Yang, Shiying' 'Zhang, Baoxi' 'Yang, Dezhi' 'Lu, Yang' 'Du, Guanhua' _publ_section_title ; Insights Into the Properties of Amygdalin Solvatomorphs: X-ray Structures, Intermolecular Interactions, and Transformations. ; _journal_issue 10 _journal_name_full 'ACS omega' _journal_page_first 8906 _journal_page_last 8918 _journal_paper_doi 10.1021/acsomega.1c07314 _journal_volume 7 _journal_year 2022 _chemical_absolute_configuration ad _chemical_formula_sum 'C23 H39 N O14' _chemical_formula_weight 553.55 _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 91.4070(10) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 9.50870(10) _cell_length_b 7.87930(10) _cell_length_c 18.5965(2) _cell_measurement_reflns_used 11062 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 72.1620 _cell_measurement_theta_min 4.6430 _cell_volume 1392.87(3) _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 0.985 _diffrn_measured_fraction_theta_max 0.972 _diffrn_measurement_device_type 'Cu K\a' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0478 _diffrn_reflns_av_unetI/netI 0.0331 _diffrn_reflns_Laue_measured_fraction_full 0.985 _diffrn_reflns_Laue_measured_fraction_max 0.972 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 13386 _diffrn_reflns_point_group_measured_fraction_full 0.857 _diffrn_reflns_point_group_measured_fraction_max 0.837 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 72.098 _diffrn_reflns_theta_min 4.652 _exptl_absorpt_coefficient_mu 0.937 _exptl_absorpt_correction_type multi-scan _exptl_crystal_density_diffrn 1.320 _exptl_crystal_description prism _exptl_crystal_F_000 592 _exptl_crystal_size_max 0.350 _exptl_crystal_size_mid 0.250 _exptl_crystal_size_min 0.100 _exptl_transmission_factor_max 1.00000 _exptl_transmission_factor_min 0.44611 _refine_diff_density_max 0.259 _refine_diff_density_min -0.218 _refine_diff_density_rms 0.050 _refine_ls_abs_structure_details ; Flack x determined using 1473 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.00(13) _refine_ls_extinction_coef 0.0037(11) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.064 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 388 _refine_ls_number_reflns 4598 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.064 _refine_ls_R_factor_all 0.0476 _refine_ls_R_factor_gt 0.0452 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0837P)^2^+0.1978P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1239 _refine_ls_wR_factor_ref 0.1282 _reflns_Friedel_coverage 0.599 _reflns_Friedel_fraction_full 0.708 _reflns_Friedel_fraction_max 0.680 _reflns_number_gt 4357 _reflns_number_total 4598 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ao1c07314_si_002.cif _cod_data_source_block 6245 _cod_original_sg_symbol_H-M 'P 21' _cod_database_code 4519400 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.735 _shelx_estimated_absorpt_t_max 0.912 _shelx_res_file ; TITL 6245_a.res in P2(1) 6245.res created by SHELXL-2018/3 at 10:09:58 on 11-Oct-2021 REM Old TITL 6245 in P2(1)/m ***Colorless ***Prism REM SHELXT solution in P2(1): R1 0.132, Rweak 0.030, Alpha 0.008 REM 0.319 for 5 systematic absences, Orientation as input REM Flack x = 0.137 ( 0.125 ) from 1521 Parsons' quotients REM Formula found by SHELXT: C23 N3 O12 CELL 1.54184 9.5087 7.8793 18.5965 90 91.407 90 ZERR 2 0.0001 0.0001 0.0002 0 0.001 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H N O UNIT 46 78 2 28 L.S. 20 PLAN 4 SIZE 0.1 0.25 0.35 CONF htab BOND list 4 MORE -1 BOND $H fmap 2 53 acta OMIT 0 0 1 OMIT -1 -2 7 OMIT -1 -2 6 OMIT 4 9 4 OMIT 4 8 10 OMIT 6 7 6 OMIT -7 2 18 OMIT 4 9 3 OMIT 7 7 5 OMIT 5 8 8 REM REM REM WGHT 0.083700 0.197800 EXTI 0.003718 FVAR 0.92165 0.75365 O1 4 0.296812 0.700678 0.276443 11.00000 0.04276 0.04584 = 0.03170 0.00038 -0.01398 -0.00762 O2 4 0.175587 0.850171 0.398268 11.00000 0.02347 0.04605 = 0.05221 0.00627 -0.00974 0.00355 H2 2 0.122855 0.795311 0.421174 11.00000 0.06763 O3 4 0.364563 0.796642 0.521648 11.00000 0.04052 0.04598 = 0.03170 -0.00323 -0.00549 -0.00621 H3 2 0.403274 0.838539 0.561049 11.00000 0.08320 O4 4 0.646200 0.939844 0.492224 11.00000 0.03515 0.03793 = 0.04292 -0.00640 -0.01824 -0.00164 H4 2 0.628284 1.055625 0.478171 11.00000 0.06922 O5 4 0.515117 0.763619 0.320673 11.00000 0.02933 0.03760 = 0.03488 -0.00272 -0.00962 0.00172 O6 4 0.787226 0.673409 0.386374 11.00000 0.03404 0.03455 = 0.04179 0.00575 -0.00132 0.01013 O7 4 1.039423 0.597478 0.465948 11.00000 0.03090 0.03920 = 0.04157 -0.00935 -0.00953 -0.00170 H7 2 0.975662 0.643015 0.497330 11.00000 0.05969 O8 4 1.135849 0.257906 0.445071 11.00000 0.03168 0.03708 = 0.03787 0.00313 -0.01421 0.00249 PART 1 H8A 2 1.180225 0.324982 0.469259 21.00000 0.02340 PART 2 H8B 2 1.231412 0.277014 0.446612 -21.00000 0.01581 PART 0 O9 4 1.086650 0.119296 0.306608 11.00000 0.04519 0.03871 = 0.04150 -0.00439 -0.00841 0.01014 H9 2 1.125099 0.055121 0.335085 11.00000 0.06799 O10 4 0.832917 0.466026 0.306848 11.00000 0.02942 0.03903 = 0.04084 -0.00365 -0.01423 0.00506 O11 4 0.729882 0.160966 0.256878 11.00000 0.05968 0.06416 = 0.04639 0.00447 -0.02060 -0.02493 AFIX 147 H11 2 0.670568 0.131278 0.226691 11.00000 -1.50000 AFIX 0 N1 3 0.534005 0.574119 0.152391 11.00000 0.06759 0.13319 = 0.07961 -0.02855 0.00955 -0.00147 C1 1 0.313981 0.733003 0.201682 11.00000 0.05089 0.05553 = 0.03270 0.00264 -0.01205 -0.00659 AFIX 13 H1 2 0.328564 0.855094 0.195117 11.00000 -1.20000 AFIX 0 C2 1 0.438084 0.642132 0.174705 11.00000 0.05449 0.08475 = 0.04591 -0.00931 -0.00331 -0.01050 C3 1 0.178619 0.682808 0.162282 11.00000 0.05275 0.06600 = 0.03358 0.00362 -0.01685 -0.00725 C4 1 0.168981 0.544671 0.117749 11.00000 0.07253 0.08848 = 0.05372 -0.01397 -0.01226 -0.01796 AFIX 43 H4A 2 0.247471 0.477192 0.110143 11.00000 -1.20000 AFIX 0 C5 1 0.040207 0.505988 0.083840 11.00000 0.10262 0.13094 = 0.06547 -0.01747 -0.02932 -0.04429 AFIX 43 H5 2 0.034126 0.414921 0.052102 11.00000 -1.20000 AFIX 0 C6 1 -0.076246 0.600074 0.096761 11.00000 0.07566 0.15082 = 0.07668 0.01959 -0.04484 -0.03531 AFIX 43 H6 2 -0.161353 0.573166 0.073820 11.00000 -1.20000 AFIX 0 C7 1 -0.068680 0.735348 0.143781 11.00000 0.06348 0.13842 = 0.10287 0.01549 -0.04060 0.00594 AFIX 43 H7A 2 -0.148814 0.798252 0.153392 11.00000 -1.20000 AFIX 0 C8 1 0.059069 0.776851 0.176581 11.00000 0.06709 0.09097 = 0.07643 -0.00027 -0.02977 0.01183 AFIX 43 H8 2 0.064773 0.868011 0.208285 11.00000 -1.20000 AFIX 0 C9 1 0.371108 0.810552 0.322418 11.00000 0.03082 0.03274 = 0.03670 0.00339 -0.01354 0.00093 AFIX 13 H9A 2 0.358383 0.928634 0.307037 11.00000 -1.20000 AFIX 0 C10 1 0.314742 0.784395 0.396831 11.00000 0.02661 0.03361 = 0.03631 -0.00082 -0.01181 0.00116 AFIX 13 H10 2 0.311347 0.662300 0.406685 11.00000 -1.20000 AFIX 0 C11 1 0.406757 0.869380 0.454838 11.00000 0.03096 0.02693 = 0.03446 -0.00350 -0.00904 0.00091 AFIX 13 H11A 2 0.387670 0.991600 0.455135 11.00000 -1.20000 AFIX 0 C12 1 0.562535 0.839989 0.443520 11.00000 0.02849 0.02788 = 0.03481 -0.00212 -0.01276 0.00065 AFIX 13 H12 2 0.582224 0.720415 0.454208 11.00000 -1.20000 AFIX 0 C13 1 0.601978 0.871875 0.365540 11.00000 0.03075 0.02619 = 0.03858 0.00154 -0.01027 0.00042 AFIX 13 H13 2 0.583795 0.990875 0.353125 11.00000 -1.20000 AFIX 0 C14 1 0.753209 0.828985 0.350824 11.00000 0.03102 0.03150 = 0.04940 0.00703 -0.00625 0.00193 AFIX 23 H14A 2 0.765948 0.817302 0.299469 11.00000 -1.20000 H14B 2 0.814531 0.918875 0.368553 11.00000 -1.20000 AFIX 0 C15 1 0.895756 0.579029 0.357110 11.00000 0.02691 0.03000 = 0.03657 0.00156 -0.00556 0.00130 AFIX 13 H15 2 0.963289 0.653481 0.333661 11.00000 -1.20000 AFIX 0 C16 1 0.966520 0.482314 0.419167 11.00000 0.02397 0.03293 = 0.03132 -0.00098 -0.00744 -0.00138 AFIX 13 H16 2 0.895390 0.420544 0.446026 11.00000 -1.20000 AFIX 0 C17 1 1.071976 0.358233 0.389499 11.00000 0.02676 0.02857 = 0.03171 0.00272 -0.00758 0.00007 AFIX 13 H17 2 1.144804 0.420577 0.364079 11.00000 -1.20000 AFIX 0 C18 1 0.994865 0.239339 0.337153 11.00000 0.02532 0.03260 = 0.03343 -0.00166 -0.00659 0.00153 AFIX 13 H18 2 0.920655 0.179353 0.362530 11.00000 -1.20000 AFIX 0 C19 1 0.928034 0.346601 0.276544 11.00000 0.03254 0.03705 = 0.03204 -0.00035 -0.00743 0.00255 AFIX 13 H19 2 1.002073 0.408018 0.251635 11.00000 -1.20000 AFIX 0 C20 1 0.841559 0.245613 0.222316 11.00000 0.04483 0.04886 = 0.03512 -0.00052 -0.01360 -0.00204 AFIX 23 H20A 2 0.803373 0.321081 0.185542 11.00000 -1.20000 H20B 2 0.901033 0.162950 0.199192 11.00000 -1.20000 AFIX 0 O1I 4 0.505893 1.081991 0.163536 11.00000 0.07070 0.08176 = 0.04714 -0.00842 -0.01511 -0.00519 AFIX 147 H1I 2 0.449374 1.142610 0.184040 11.00000 -1.50000 AFIX 0 C1I 1 0.632411 1.062363 0.057672 11.00000 0.11800 0.26088 = 0.06968 -0.02383 0.01030 0.01849 AFIX 137 H1IA 2 0.631339 0.940554 0.058638 11.00000 -1.50000 H1IB 2 0.713425 1.103092 0.084227 11.00000 -1.50000 H1IC 2 0.636252 1.100743 0.008765 11.00000 -1.50000 AFIX 0 C2I 1 0.507824 1.125859 0.089472 11.00000 0.08588 0.09926 = 0.05744 0.00459 -0.01461 -0.01175 AFIX 13 H2I 2 0.512918 1.249950 0.087087 11.00000 -1.20000 AFIX 0 C3I 1 0.373073 1.075823 0.053849 11.00000 0.11120 0.16861 = 0.06840 0.00565 -0.04412 -0.01534 AFIX 137 H3IA 2 0.370029 0.954650 0.048650 11.00000 -1.50000 H3IB 2 0.365657 1.127960 0.007253 11.00000 -1.50000 H3IC 2 0.296205 1.112430 0.082556 11.00000 -1.50000 AFIX 6 O1W 4 0.538519 0.389181 0.341668 11.00000 0.05079 0.04900 = 0.04842 0.00407 -0.00467 -0.00133 H1WA 2 0.610764 0.362230 0.318182 11.00000 -1.50000 H1WB 2 0.534700 0.496771 0.338818 11.00000 -1.50000 AFIX 0 O2W 4 0.328594 0.264388 0.247208 11.00000 0.06469 0.09521 = 0.08254 -0.00845 0.00254 -0.02081 H2WA 2 0.368966 0.269263 0.279076 11.00000 0.17205 H2WB 2 0.251262 0.233208 0.267005 11.00000 0.08498 HKLF 4 REM 6245_a.res in P2(1) REM wR2 = 0.1282, GooF = S = 1.064, Restrained GooF = 1.064 for all data REM R1 = 0.0452 for 4357 Fo > 4sig(Fo) and 0.0476 for all 4598 data REM 388 parameters refined using 1 restraints END WGHT 0.0837 0.1978 REM Instructions for potential hydrogen bonds EQIV $1 x-1, y, z HTAB O2 O7_$1 EQIV $2 -x+1, y+1/2, -z+1 HTAB O3 O1W_$2 HTAB O4 O3_$2 EQIV $3 -x+2, y+1/2, -z+1 HTAB O7 O8_$3 EQIV $4 -x+2, y-1/2, -z+1 HTAB O8 O4_$4 EQIV $5 x+1, y-1, z HTAB O9 O2_$5 EQIV $6 x, y-1, z HTAB O11 O1I_$6 HTAB C1 O1I EQIV $7 -x+1, y-1/2, -z+1 HTAB C10 O4_$7 EQIV $8 x, y+1, z HTAB C13 O11_$8 HTAB O1I O2W_$8 HTAB O2W O1W HTAB O2W O9_$1 REM Highest difference peak 0.259, deepest hole -0.218, 1-sigma level 0.050 Q1 1 0.3405 0.8088 0.3619 11.00000 0.05 0.26 Q2 1 0.5858 0.8592 0.4042 11.00000 0.05 0.26 Q3 1 0.4841 0.8574 0.4434 11.00000 0.05 0.26 Q4 1 0.3674 0.8229 0.4201 11.00000 0.05 0.25 ; _shelx_res_checksum 37855 _shelx_hkl_file ; 0 0 1 0.00 0.03 0 0 2 1109.79 6.69 0 0 2 1222.38 6.55 0 0 3 8.48 0.68 0 0 3 8.43 0.71 0 0 4 1913.20 11.87 0 0 4 1900.37 11.30 0 0 5 1325.57 10.39 0 0 5 1411.47 11.82 0 0 6 527.90 8.28 0 0 6 526.69 6.94 0 0 7 56.03 3.03 0 0 7 58.52 2.40 0 0 8 432.36 9.34 0 0 8 451.23 6.75 0 0 9 317.72 5.80 0 0 10 123.54 6.22 0 0 11 109.37 6.44 0 0 11 142.13 4.38 0 0 12 145.51 8.23 0 0 -12 149.41 5.30 0 0 -12 169.08 6.14 0 0 12 160.36 4.89 0 0 -13 236.53 7.15 0 0 13 235.58 11.58 0 0 -13 233.18 6.55 0 0 13 233.82 5.52 0 0 13 242.37 6.39 0 0 -14 212.66 7.27 0 0 14 228.60 12.47 0 0 -14 214.04 6.40 0 0 14 205.82 6.24 0 0 -15 13.81 2.04 0 0 -15 17.82 2.53 0 0 15 10.87 3.43 0 0 -15 13.70 1.80 0 0 -15 16.14 2.74 0 0 15 12.90 1.74 0 0 16 16.14 4.35 0 0 -16 21.43 2.60 0 0 -16 25.43 3.19 0 0 -16 25.75 3.49 0 0 16 17.20 2.04 0 0 -17 25.05 2.86 0 0 -17 31.49 3.78 0 0 -17 30.85 3.55 0 0 17 19.09 2.30 0 0 -18 96.28 6.13 0 0 -18 79.62 4.97 0 0 -19 2.27 1.13 0 0 -19 2.25 1.32 0 0 19 1.47 0.87 0 0 -20 12.87 1.99 0 0 -20 10.50 2.01 0 0 -21 33.58 3.07 0 0 -21 43.23 3.28 0 0 -22 1.07 0.76 0 0 -22 1.73 0.90 0 -1 0 -0.02 0.21 0 -1 1 1226.39 11.48 0 -1 2 164.35 4.21 0 -1 2 193.58 3.39 0 -1 3 2484.92 16.16 0 1 3 2566.81 19.14 0 -1 4 1302.86 11.31 0 1 4 1293.00 14.41 0 1 5 4432.45 29.46 0 -1 5 4996.81 23.13 0 -1 6 629.35 10.50 0 1 6 634.95 12.06 0 -1 7 264.06 6.96 0 -1 7 286.48 6.49 0 1 8 494.18 12.69 0 -1 8 544.18 10.17 0 -1 9 173.30 5.44 0 1 9 168.12 8.05 0 1 10 106.58 7.08 0 -1 10 117.87 5.43 0 1 11 298.29 12.54 0 -1 11 323.04 10.09 0 -1 11 312.09 5.51 0 -1 -11 333.48 8.36 0 -1 -11 302.76 7.53 0 1 11 303.64 6.74 0 -1 -12 46.86 3.43 0 -1 -12 36.79 2.81 0 1 -12 51.50 3.49 0 -1 12 40.11 3.89 0 1 12 39.47 4.97 0 -1 12 40.08 2.17 0 -1 -12 30.95 2.62 0 1 12 44.54 2.54 0 1 12 43.58 2.72 0 -1 -13 7.89 1.64 0 1 -13 8.63 1.62 0 1 13 7.70 2.60 0 -1 13 7.14 1.08 0 -1 13 6.05 1.84 0 -1 -13 5.77 1.30 0 -1 -13 2.51 1.24 0 1 13 6.98 1.17 0 1 13 7.31 1.25 0 -1 13 8.65 1.26 0 -1 -14 10.57 1.98 0 1 -14 11.06 1.92 0 -1 14 6.48 2.20 0 -1 -14 8.13 1.56 0 1 14 5.99 2.94 0 -1 -14 7.50 1.45 0 -1 14 9.30 1.37 0 1 14 13.12 1.64 0 1 14 8.67 1.41 0 -1 15 74.89 7.25 0 1 -15 83.82 4.68 0 1 -15 99.22 5.75 0 -1 -15 73.98 4.66 0 -1 -15 94.73 5.79 0 1 15 75.92 4.33 0 -1 15 80.56 4.11 0 1 15 82.99 4.13 0 -1 16 59.39 7.11 0 1 -16 59.48 4.08 0 -1 -16 73.92 5.35 0 1 -16 73.57 5.15 0 -1 -16 52.46 4.08 0 1 16 64.92 3.81 0 1 16 58.37 4.06 0 -1 16 62.50 3.81 0 -1 -17 27.85 3.11 0 -1 -17 31.43 3.51 0 1 -17 29.60 3.04 0 1 -17 38.20 3.84 0 1 17 35.52 3.28 0 -1 17 30.16 2.73 0 1 17 30.33 2.66 0 1 -17 37.56 4.22 0 -1 -18 7.10 1.64 0 1 -18 6.68 1.57 0 1 -18 9.03 2.03 0 -1 -18 9.14 2.08 0 1 18 7.95 1.69 0 -1 18 5.85 1.32 0 1 -19 2.21 1.07 0 -1 -19 2.73 1.17 0 1 -19 1.37 1.13 0 1 -19 1.93 1.42 0 -1 -19 1.48 1.21 0 1 19 0.90 0.80 0 -1 19 1.83 0.99 0 1 -20 24.00 2.91 0 -1 -20 23.94 2.74 0 -1 -20 24.42 2.94 0 1 -20 20.50 2.34 0 1 -20 24.72 2.91 0 -1 20 22.15 2.40 0 1 20 22.59 2.55 0 1 -21 25.24 2.39 0 -1 -21 24.79 2.53 0 1 -21 29.01 2.82 0 -1 -21 25.79 2.70 0 1 21 29.19 2.69 0 -1 21 27.83 2.58 0 1 -22 9.07 1.50 0 -1 -22 9.86 1.52 0 1 -22 9.41 1.37 0 -1 -22 10.37 1.50 0 -1 22 12.00 1.63 0 1 22 9.95 1.48 0 -2 0 5337.68 27.03 0 -2 -1 9999.00 40.12 0 -2 1 9737.58 48.76 0 -2 -2 3959.39 27.46 0 -2 2 3584.17 28.25 0 -2 3 1260.74 12.30 0 -2 3 1039.98 15.05 0 -2 4 316.52 5.68 0 -2 4 262.09 7.27 0 -2 5 1187.06 11.20 0 -2 5 943.46 13.59 0 -2 6 40.96 2.71 0 -2 7 234.79 6.60 0 -2 8 17.23 2.37 0 -2 8 17.67 1.94 0 -2 9 337.16 8.80 0 -2 9 308.13 9.85 0 -2 10 133.23 3.19 0 -2 10 126.06 5.70 0 -2 11 170.39 7.03 0 -2 11 167.12 3.84 0 -2 -11 137.63 5.70 0 2 -11 186.33 5.93 0 -2 -11 164.75 6.57 0 2 11 155.28 5.66 0 2 11 149.99 5.16 0 -2 12 12.35 2.13 0 -2 12 12.90 1.21 0 2 -12 14.67 1.91 0 -2 -12 13.86 2.11 0 -2 -12 9.35 1.69 0 2 12 10.42 1.52 0 2 12 12.59 1.73 0 -2 13 86.34 3.31 0 -2 13 92.04 6.15 0 -2 -13 97.01 5.55 0 -2 -13 82.77 4.82 0 2 13 87.08 4.27 0 2 13 85.55 4.57 0 -2 14 152.30 8.65 0 -2 14 146.02 4.59 0 -2 -14 141.28 6.52 0 -2 -14 177.11 7.84 0 2 -14 177.98 7.08 0 2 14 151.28 6.26 0 2 14 155.24 5.84 0 -2 15 211.36 10.96 0 -2 15 196.54 5.66 0 -2 -15 226.72 9.30 0 -2 -15 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1.62 2 3 21 12.62 1.59 2 4 -20 21.42 2.40 2 -4 -20 17.28 1.79 2 -4 -20 16.79 1.67 -2 -4 20 22.45 1.69 2 4 -19 37.79 2.36 2 -4 -19 43.58 3.27 2 -4 -19 41.22 3.04 2 4 -19 43.27 3.80 -2 -4 19 49.97 2.74 2 4 -18 10.80 1.46 2 -4 -18 11.68 2.00 2 -4 -18 10.67 1.83 2 4 -18 10.24 2.16 -2 -4 18 13.21 1.56 2 4 -17 29.91 2.45 2 -4 -17 29.98 3.21 2 -4 -17 32.05 3.46 2 -4 -16 13.23 2.31 2 -4 -16 11.04 2.33 2 -4 -15 18.41 2.80 2 -4 -15 17.70 2.90 2 -4 -14 7.63 2.11 2 -4 -14 7.11 1.32 -2 -4 14 7.25 1.03 2 -4 -14 8.15 2.10 2 -4 -13 52.40 4.64 2 -4 -13 50.02 4.68 2 -4 -13 55.05 3.31 -2 -4 13 51.19 4.63 -2 -4 13 57.41 2.55 2 -4 -13 42.08 8.22 2 -4 -12 433.31 12.71 2 -4 -12 398.76 12.80 2 4 -12 298.46 18.77 2 -4 -12 503.24 10.13 -2 -4 12 522.23 13.38 -2 -4 12 535.09 7.35 2 -4 -12 326.73 20.11 2 -4 -11 436.47 12.18 2 -4 -11 387.71 11.98 2 -4 -11 469.67 9.97 2 4 -11 328.17 19.99 -2 -4 11 435.18 11.90 -2 -4 11 459.30 6.45 2 -4 -11 327.14 19.23 2 -4 -10 37.38 3.46 2 -4 -10 37.74 3.64 2 -4 -10 39.95 2.99 -2 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2 -4 3 323.41 13.69 2 -4 4 417.56 15.03 2 -4 4 396.25 14.37 2 4 4 405.30 7.28 2 -4 5 163.31 4.15 2 -4 5 161.90 9.19 2 -4 5 158.98 4.72 2 -4 5 153.17 8.80 2 -4 5 164.20 5.12 2 4 5 160.28 4.78 2 4 5 144.69 5.61 -2 -4 -6 237.55 7.25 2 -4 6 250.05 11.07 2 -4 6 253.13 10.84 2 -4 6 271.22 6.05 2 -4 6 265.37 6.39 2 4 6 264.43 6.38 2 4 6 252.29 7.61 -2 -4 -7 206.19 7.09 2 -4 7 226.32 5.29 2 -4 7 209.88 9.55 2 -4 7 203.79 9.45 2 4 7 205.63 5.82 2 -4 7 217.36 5.67 2 4 7 215.60 7.38 -2 -4 -8 85.26 4.83 2 -4 8 88.84 3.25 2 -4 8 82.78 6.03 2 4 8 91.83 4.01 2 4 8 91.25 5.18 2 -4 8 89.68 3.60 -2 -4 -9 131.88 6.34 2 -4 9 144.13 4.12 2 -4 9 128.49 10.19 2 -4 9 135.22 7.58 2 4 9 152.18 5.24 2 -4 9 144.54 4.53 2 4 9 153.62 7.22 -2 -4 -10 55.71 4.40 2 -4 10 60.77 5.27 2 -4 10 55.28 7.16 2 -4 10 66.25 2.82 2 -4 10 67.77 3.11 2 4 10 66.64 3.51 2 -4 10 65.90 2.98 2 4 10 78.82 5.54 -2 -4 -11 16.71 2.66 -2 4 -11 18.76 2.28 2 -4 11 19.07 1.62 2 -4 11 19.22 3.28 2 -4 11 18.44 4.70 2 -4 11 20.14 1.78 2 4 11 20.83 1.96 2 4 11 20.64 3.07 2 -4 11 20.48 1.65 -2 4 -12 4.30 1.33 2 -4 12 4.64 2.07 -2 -4 -12 3.13 1.50 2 -4 12 3.96 0.82 2 4 12 4.75 1.02 2 -4 12 3.83 0.77 2 4 12 2.94 1.59 2 -4 13 125.06 4.28 2 -4 13 116.14 7.90 -2 -4 -13 91.12 5.56 -2 -4 -13 109.33 6.71 -2 4 -13 101.38 4.94 2 4 13 108.38 6.86 2 -4 13 110.59 3.46 2 -4 14 15.44 1.62 -2 -4 -14 17.92 2.84 -2 -4 -14 13.38 2.31 -2 4 -14 13.75 2.03 2 4 14 16.57 2.71 2 -4 15 10.71 1.42 -2 -4 -15 7.43 1.81 -2 4 -15 10.07 1.81 2 4 15 11.60 2.23 2 -4 16 5.93 1.16 -2 -4 -16 4.23 1.52 -2 4 -16 5.02 1.33 -2 -4 -16 4.05 1.42 2 4 16 5.09 1.51 2 -4 17 38.37 2.66 -2 -4 -17 45.16 3.85 -2 -4 -17 36.86 3.31 2 4 17 42.15 3.70 -2 4 -18 14.86 2.00 -2 -4 -18 11.14 1.91 -2 -4 -18 10.26 1.80 2 4 18 14.68 2.09 -2 4 -19 9.66 1.57 -2 -4 -19 8.88 1.60 2 4 19 10.29 1.61 -2 4 -20 1.36 0.72 -2 -4 -20 1.46 0.83 2 4 20 1.00 0.64 2 5 -19 19.46 2.24 2 -5 -18 2.43 0.92 2 5 -18 2.36 1.28 2 -5 -18 1.91 0.84 -2 -5 18 2.01 0.61 2 5 -17 4.39 1.00 2 -5 -17 8.06 1.56 2 5 -17 6.71 1.81 2 -5 -17 6.36 1.38 -2 -5 17 8.06 1.16 2 -5 -16 18.96 2.48 2 -5 -16 21.22 2.62 2 5 -16 17.41 2.75 2 -5 -15 35.93 3.58 2 -5 -15 34.56 3.56 -2 -5 15 37.19 2.14 2 -5 -14 97.67 6.11 2 -5 -14 116.09 6.56 -2 -5 14 109.41 3.59 2 -5 -13 11.33 2.31 2 -5 -13 7.64 2.00 -2 -5 13 10.88 1.17 2 -5 -12 99.20 6.26 2 -5 -12 114.40 6.66 2 -5 -11 204.04 8.61 2 -5 -11 230.03 9.21 2 5 -11 158.27 14.15 -2 -5 11 231.76 9.23 2 -5 -11 169.99 14.17 -2 -5 11 259.66 5.07 2 -5 -10 81.48 5.37 2 -5 -10 73.38 5.03 2 5 -10 61.55 7.31 -2 -5 10 82.83 5.46 -2 -5 10 85.74 2.88 2 -5 -10 62.64 8.51 2 -5 -9 46.32 3.94 2 -5 -9 39.01 3.53 2 5 -9 40.67 4.81 -2 -5 9 49.87 2.18 2 -5 -9 44.38 7.10 -2 -5 9 49.43 4.17 2 -5 -8 9.07 1.85 2 -5 -8 8.77 1.82 2 5 -8 7.67 1.95 -2 -5 8 11.86 1.18 -2 -5 8 13.18 2.49 2 -5 -8 9.00 3.77 2 -5 -7 1.84 1.26 2 5 -7 0.83 1.02 2 -5 -7 2.48 1.41 -2 -5 7 4.20 0.73 2 -5 -7 1.69 2.89 2 -5 -6 55.32 4.11 2 -5 -6 44.46 3.54 2 5 -6 51.02 4.13 -2 -5 6 60.20 2.65 -2 -5 6 67.74 5.44 2 -5 -6 50.48 6.93 2 -5 -5 47.44 3.85 2 5 -5 29.35 3.11 2 -5 -5 42.16 6.69 -2 -5 5 37.31 2.29 -2 -5 5 52.32 4.90 2 -5 -5 32.74 5.76 2 -5 -4 17.99 2.65 2 5 -4 9.29 1.83 2 -5 -4 20.23 5.63 -2 -5 4 25.96 2.11 -2 -5 4 20.38 5.18 2 -5 -4 15.49 5.07 -2 -5 3 22.81 1.91 -2 -5 3 27.04 3.86 2 -5 -3 20.38 4.32 2 -5 -3 22.23 4.45 2 -5 -3 21.95 1.90 2 -5 -3 24.22 2.60 2 -5 -2 34.36 5.47 -2 -5 2 12.35 2.85 2 -5 -2 31.53 6.57 2 -5 -2 6.24 1.08 2 -5 -2 15.24 2.11 -2 -5 2 10.15 2.20 2 -5 -1 133.32 5.71 -2 -5 1 125.61 4.96 2 -5 -1 125.56 9.84 -2 -5 1 123.20 8.86 2 -5 -1 141.65 9.90 2 5 -1 144.04 5.09 2 5 -1 142.20 5.65 2 -5 0 94.28 4.75 -2 -5 0 89.39 4.27 2 -5 0 82.56 3.25 -2 -5 0 83.93 7.15 2 -5 0 94.42 8.65 2 5 0 104.70 4.44 2 5 0 103.90 4.96 2 -5 1 267.93 5.70 -2 -5 -1 270.41 7.60 2 -5 1 315.95 8.34 -2 -5 -1 272.16 13.10 2 -5 1 312.90 15.04 2 5 1 343.28 7.62 2 5 1 350.34 9.15 2 -5 2 360.37 6.51 2 -5 2 394.27 9.15 -2 -5 -2 356.44 8.77 -2 -5 -2 346.56 15.09 2 -5 2 409.17 17.21 2 5 2 403.68 8.14 2 5 2 427.98 10.25 2 -5 3 5.21 0.84 2 -5 3 5.05 2.55 -2 -5 -3 4.90 2.25 2 -5 3 6.06 1.22 -2 -5 -3 4.56 1.15 2 -5 3 7.28 2.75 2 5 3 5.14 0.97 2 5 3 5.06 1.29 -2 -5 -4 386.65 9.62 2 -5 4 407.12 6.93 2 -5 4 436.56 17.25 2 -5 4 415.91 8.80 2 -5 4 411.44 15.96 2 5 4 416.70 8.37 2 5 4 410.95 10.20 2 -5 5 482.82 9.14 2 -5 5 502.21 18.20 2 -5 5 487.98 9.61 2 5 5 512.56 9.58 2 5 5 486.91 11.17 -2 -5 -6 243.23 7.99 2 -5 6 285.89 13.28 2 -5 6 268.57 6.66 2 5 6 273.26 7.26 2 -5 6 267.69 7.01 2 5 6 246.63 8.11 -2 -5 -7 221.23 7.90 2 -5 7 240.29 6.04 2 -5 7 237.32 11.80 2 5 7 228.18 6.80 2 5 7 226.00 8.07 2 -5 7 248.04 6.73 -2 -5 -8 59.11 4.32 2 -5 8 60.58 5.83 2 -5 8 70.08 3.25 2 5 8 67.68 3.78 2 5 8 64.39 4.57 2 -5 8 67.98 3.43 -2 -5 -9 38.72 3.78 2 -5 9 33.20 6.16 2 -5 9 46.00 2.56 2 -5 9 43.68 4.94 2 5 9 47.99 3.20 2 -5 9 47.41 2.80 2 5 9 45.18 4.03 -2 -5 -10 104.40 6.32 2 -5 10 99.92 10.25 2 -5 10 108.99 7.76 2 -5 10 112.80 4.01 2 -5 10 113.91 4.35 2 5 10 112.87 4.92 2 -5 10 112.98 4.12 2 5 10 110.31 6.59 -2 -5 -11 77.19 5.66 2 -5 11 77.69 6.68 2 -5 11 89.84 3.57 2 5 11 86.94 4.25 2 -5 11 87.71 3.78 2 5 11 86.91 6.13 2 -5 11 84.92 3.42 -2 -5 -12 31.43 3.75 2 -5 12 40.76 2.46 2 5 12 40.22 2.85 2 5 12 32.59 3.85 2 -5 13 32.05 2.24 -2 -5 -13 24.65 3.26 2 5 13 29.04 3.56 -2 -5 -14 11.07 2.25 2 -5 14 13.52 1.52 2 5 14 11.94 2.31 2 -5 15 11.69 1.43 -2 -5 -15 10.48 2.08 2 5 15 10.53 2.01 2 -5 16 28.16 2.11 -2 -5 -16 25.25 2.80 2 5 16 28.36 2.91 -2 -5 -17 11.67 1.80 2 5 17 12.14 1.82 -2 -5 -18 6.05 1.26 -2 5 -18 7.63 1.36 2 5 18 6.49 1.22 -2 5 -19 1.30 0.64 2 -6 -17 1.33 0.71 2 6 -17 0.91 0.96 2 -6 -16 1.11 0.77 2 6 -16 0.69 0.64 2 6 -16 0.40 1.02 2 -6 -15 7.95 1.57 -2 -6 15 8.23 0.95 2 6 -15 8.12 1.88 -2 -6 15 12.09 1.29 2 -6 -14 42.35 3.56 -2 -6 14 43.51 2.12 2 -6 -13 17.58 2.50 -2 -6 13 21.89 1.51 2 -6 -12 15.86 2.43 -2 -6 12 20.42 1.47 2 -6 -11 13.96 2.29 -2 -6 11 19.93 1.45 2 -6 -10 27.40 3.18 -2 -6 10 32.06 1.84 2 -6 -9 16.00 2.38 2 6 -9 13.05 3.38 -2 -6 9 22.95 1.56 2 -6 -8 79.61 5.07 2 6 -8 94.38 6.88 2 -6 -8 66.28 8.46 -2 -6 8 89.45 3.13 -2 -6 8 75.38 5.61 2 -6 -7 181.82 7.56 2 6 -7 238.51 9.54 2 -6 -7 148.94 12.67 -2 -6 7 205.50 4.93 -2 -6 7 206.73 9.58 2 -6 -6 145.91 6.73 2 6 -6 181.15 7.76 2 -6 -6 132.97 11.89 -2 -6 6 164.09 4.57 -2 -6 6 207.66 10.12 2 -6 -5 103.65 5.64 2 6 -5 125.91 6.09 2 -6 -5 96.65 10.07 -2 -6 5 124.01 8.39 -2 -6 5 105.52 3.87 2 -6 -4 47.38 3.78 2 6 -4 53.60 3.90 2 -6 -4 49.99 7.37 -2 -6 4 55.73 5.98 -2 -6 4 46.29 2.70 2 -6 -3 154.06 6.72 2 6 -3 165.59 7.03 -2 -6 3 145.02 9.60 -2 -6 3 143.31 5.00 2 -6 -3 144.49 11.75 2 -6 -2 114.68 10.58 -2 -6 2 106.53 8.72 -2 -6 2 105.75 4.46 2 -6 -2 112.37 5.70 2 -6 -1 33.20 5.82 -2 -6 1 35.42 5.41 2 -6 -1 34.81 2.22 2 -6 -1 34.16 3.20 -2 -6 1 32.69 2.65 2 -6 0 237.96 15.17 -2 -6 0 205.42 12.29 -2 -6 0 220.62 6.99 2 -6 0 226.77 5.36 2 -6 0 215.39 7.55 -2 -6 -1 76.95 7.62 2 -6 1 87.09 9.04 -2 -6 -1 82.73 4.33 2 -6 1 87.76 4.64 2 -6 1 87.29 3.33 2 6 1 103.19 5.16 2 -6 2 38.93 3.05 -2 -6 -2 38.11 5.77 2 -6 2 44.03 6.64 -2 -6 -2 34.75 2.90 2 -6 2 39.92 2.27 2 6 2 42.17 3.42 -2 -6 -3 54.27 3.72 2 -6 3 66.06 7.45 2 -6 3 61.08 3.61 2 6 3 68.28 3.85 2 6 3 62.91 4.06 -2 -6 -4 116.59 5.39 2 -6 4 127.71 5.05 -2 -6 -4 107.98 9.70 2 -6 4 123.14 9.75 2 -6 4 119.06 5.01 2 6 4 138.54 6.06 -2 -6 -5 172.40 6.80 2 -6 5 196.34 6.07 -2 -6 -5 151.02 11.54 2 -6 5 193.93 11.97 2 6 5 233.39 7.49 2 -6 5 191.47 6.26 2 6 5 191.70 7.19 2 -6 6 612.48 10.44 2 -6 6 614.90 20.21 2 -6 6 608.32 10.80 2 6 6 602.77 12.93 -2 -6 -7 124.84 6.18 2 -6 7 139.37 4.75 2 -6 7 135.05 9.22 2 6 7 154.95 6.33 2 6 7 137.54 6.35 2 -6 7 140.73 5.01 2 -6 8 5.03 1.00 2 -6 8 2.96 2.09 -2 -6 -8 5.53 1.55 -2 -6 -8 7.65 4.55 2 6 8 8.26 1.57 2 -6 8 4.80 1.04 2 6 8 4.98 1.45 -2 -6 -9 37.18 3.70 2 -6 9 36.59 2.35 2 6 9 48.00 3.44 2 -6 9 38.51 2.48 2 6 9 35.85 3.48 -2 -6 -10 139.19 7.22 2 -6 10 157.89 4.70 2 -6 10 155.51 5.06 2 6 10 144.64 6.97 2 -6 10 149.19 4.58 2 -6 11 9.00 1.15 -2 -6 -11 7.58 1.95 2 -6 11 7.77 1.20 2 6 11 7.16 1.78 2 -6 12 10.70 1.24 -2 -6 -12 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820.03 8.75 4 -3 8 851.99 23.95 4 -3 8 840.53 10.06 4 3 8 783.97 11.36 4 -3 8 842.00 10.97 4 -3 8 860.67 11.68 4 -3 8 856.07 11.26 4 3 8 813.42 10.18 4 3 8 711.82 11.83 4 3 8 856.29 16.95 4 -3 9 80.66 8.65 4 -3 9 79.81 5.42 4 -3 9 85.29 2.92 4 -3 9 94.53 8.27 4 -3 9 96.22 3.29 4 3 9 82.85 3.79 4 -3 9 82.81 3.52 4 -3 9 89.69 3.69 4 3 9 82.40 3.40 4 -3 9 91.26 3.70 4 3 9 77.39 4.04 4 3 9 92.56 5.93 -4 -3 -10 258.96 9.97 4 -3 10 219.51 13.94 4 -3 10 214.83 9.30 4 -3 10 228.58 5.02 4 3 10 207.79 6.08 4 -3 10 215.54 5.71 4 3 10 199.40 6.74 4 -3 10 231.50 5.99 4 -3 10 224.18 5.49 4 3 10 208.95 5.67 4 3 10 240.13 10.15 -4 -3 -11 24.37 3.38 4 -3 11 21.51 4.74 4 -3 11 28.62 3.66 4 -3 11 28.00 1.90 4 -3 11 26.95 2.04 4 3 11 27.44 2.25 4 -3 11 28.29 1.89 4 3 11 27.55 2.66 4 -3 11 27.52 2.09 4 3 11 26.53 2.17 4 3 11 29.82 3.79 -4 -3 -12 112.96 5.67 -4 -3 -12 127.72 7.24 4 -3 12 117.27 9.78 4 -3 12 114.75 4.05 4 -3 12 121.07 7.71 4 -3 12 124.64 4.41 4 3 12 121.36 4.73 4 3 12 124.57 4.87 4 -3 12 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31.25 3.12 4 -4 -9 29.26 2.80 4 -4 -9 27.45 5.76 4 -4 -9 28.70 2.57 4 4 -9 21.19 3.79 4 4 -9 33.67 4.19 4 -4 -8 18.31 2.28 4 -4 -8 15.82 2.26 4 -4 -8 19.96 2.28 4 -4 -8 18.09 1.96 4 4 -8 16.76 2.82 4 -4 -8 16.44 4.69 4 -4 -7 81.38 4.51 4 -4 -7 72.02 4.47 4 -4 -7 88.78 4.62 4 -4 -7 82.96 4.03 4 4 -7 83.53 5.51 4 -4 -7 79.22 7.46 4 -4 -7 72.05 8.61 4 -4 -6 170.98 6.28 4 -4 -6 147.36 6.26 4 -4 -6 147.13 5.97 4 -4 -6 155.92 5.36 4 4 -6 166.55 6.92 4 -4 -6 133.02 9.62 4 -4 -6 136.24 11.62 4 -4 -5 17.95 2.13 4 -4 -5 16.48 2.13 4 -4 -5 16.94 2.06 4 -4 -5 15.51 1.65 4 4 -5 21.56 2.35 4 -4 -5 14.91 3.72 4 -4 -5 17.60 4.62 4 -4 -4 300.36 8.33 4 -4 -4 253.87 7.64 4 -4 -4 249.02 7.98 4 -4 -4 246.84 6.22 4 4 -4 317.57 8.67 4 -4 -4 298.38 14.31 4 -4 -4 269.54 15.90 4 -4 -3 56.76 3.78 4 -4 -3 66.22 3.96 4 -4 -3 59.66 3.69 4 -4 -3 60.67 6.49 4 -4 -3 64.09 7.74 4 4 -3 78.12 3.60 4 -4 -3 54.81 2.88 4 4 -3 69.19 4.09 4 -4 -2 105.21 4.83 4 -4 -2 92.86 4.49 4 -4 -2 83.47 4.47 4 -4 -2 104.33 8.39 4 -4 -2 84.39 8.82 4 4 -2 122.59 4.48 4 -4 -2 81.58 3.45 4 4 -2 108.12 5.02 4 4 -2 115.37 5.26 4 -4 -1 79.41 4.09 4 -4 -1 82.09 4.39 4 -4 -1 91.02 4.38 4 -4 -1 98.10 7.87 4 -4 -1 86.29 8.68 4 4 -1 103.93 4.14 4 -4 -1 73.15 3.27 4 4 -1 94.84 4.76 4 -4 0 57.08 3.40 4 -4 0 64.87 3.51 4 -4 0 58.44 3.71 4 -4 0 68.47 6.60 4 -4 0 57.87 6.99 4 -4 0 65.28 7.46 4 4 0 72.14 3.41 4 4 0 71.35 4.17 4 -4 0 58.56 3.63 4 -4 1 152.32 5.42 4 -4 1 156.29 5.14 4 -4 1 171.63 9.96 4 -4 1 149.90 11.06 4 4 1 172.18 5.18 4 4 1 169.25 6.49 4 -4 1 155.35 5.79 4 -4 2 263.19 6.84 4 -4 2 264.60 6.37 4 -4 2 274.62 12.11 4 -4 2 263.76 14.32 4 -4 2 247.74 6.88 4 4 2 266.91 6.45 4 4 2 291.32 8.63 4 -4 2 261.61 7.42 4 -4 3 1188.23 14.14 4 -4 3 1199.22 24.38 4 -4 3 1193.75 30.21 4 -4 3 1190.54 14.80 4 4 3 1170.88 17.51 4 -4 3 1151.77 15.03 4 -4 4 371.50 7.67 4 -4 4 371.16 6.89 4 -4 4 372.67 13.12 4 -4 4 384.45 17.23 4 4 4 374.04 7.87 4 -4 4 386.28 8.43 4 4 4 357.28 6.88 4 -4 4 380.41 8.62 4 4 4 382.81 10.14 4 -4 5 63.81 3.15 4 -4 5 54.20 6.84 4 -4 5 60.36 2.66 4 -4 5 61.60 5.17 4 -4 5 69.46 7.47 4 -4 5 64.21 3.14 4 4 5 62.28 3.29 4 4 5 58.29 2.85 4 -4 5 63.85 3.41 4 -4 5 60.77 3.40 4 4 5 61.54 4.20 4 -4 6 136.33 4.49 4 -4 6 127.97 10.74 4 -4 6 135.87 3.92 4 -4 6 127.82 7.16 4 -4 6 140.66 10.58 4 4 6 129.56 4.87 4 -4 6 143.47 4.55 4 4 6 133.03 5.36 4 -4 6 136.84 4.94 4 4 6 114.76 4.17 4 4 6 139.67 6.67 4 -4 6 137.82 5.17 4 -4 7 103.62 3.91 4 -4 7 85.24 9.09 4 -4 7 102.52 3.31 4 -4 7 105.01 9.40 4 -4 7 100.39 6.37 4 4 7 86.79 4.07 4 -4 7 104.16 3.71 4 -4 7 112.33 4.21 4 4 7 92.84 3.90 4 4 7 93.20 4.71 4 4 7 111.45 6.29 4 -4 7 102.65 4.45 4 -4 7 100.42 4.19 4 -4 8 62.90 5.14 4 -4 8 60.16 8.02 4 -4 8 69.48 2.76 4 -4 8 69.79 7.83 4 -4 8 68.63 3.37 4 4 8 60.87 3.50 4 -4 8 69.71 2.91 4 -4 8 75.45 3.72 4 -4 8 69.68 3.53 4 4 8 62.11 3.30 4 4 8 70.93 4.28 4 4 8 81.79 5.87 -4 -4 -9 89.33 5.84 4 -4 9 64.05 8.38 4 -4 9 65.85 5.46 4 -4 9 72.35 2.87 4 -4 9 70.79 3.46 4 4 9 72.93 3.83 4 -4 9 75.97 3.55 4 4 9 67.84 3.55 4 -4 9 79.44 3.82 4 4 9 62.81 4.21 4 4 9 95.45 6.72 -4 -4 -10 144.15 7.89 4 -4 10 110.21 10.95 4 -4 10 114.27 7.33 4 -4 10 126.21 3.90 4 4 10 126.52 5.09 4 -4 10 126.68 4.60 4 -4 10 143.29 5.06 4 4 10 109.30 5.71 4 4 10 165.34 9.28 -4 -4 -11 136.97 7.91 4 -4 11 117.57 11.14 4 -4 11 110.53 7.36 4 -4 11 129.46 4.10 4 4 11 106.80 4.64 4 -4 11 122.75 4.52 4 4 11 133.51 8.58 4 4 11 107.34 5.70 4 -4 11 140.75 4.97 -4 -4 -12 40.70 4.39 4 -4 12 41.54 2.43 4 4 12 41.28 2.87 4 -4 12 38.61 2.55 4 4 12 41.94 3.66 4 -4 12 45.99 2.76 4 4 12 41.37 4.79 -4 4 -13 63.76 4.11 4 -4 13 65.10 3.12 4 -4 13 72.83 3.38 4 4 13 68.32 3.58 4 -4 13 80.59 3.49 4 4 13 65.93 5.74 -4 4 -14 1.05 0.85 -4 -4 -14 1.81 1.35 4 -4 14 0.88 0.59 4 4 14 1.50 0.71 4 -4 14 0.72 0.58 4 4 14 1.47 1.10 4 -4 14 0.88 0.52 -4 -4 -15 21.25 2.74 -4 4 -15 18.54 2.30 4 -4 15 17.86 1.73 4 4 15 21.88 1.85 4 4 15 20.57 2.95 4 -4 15 21.19 1.72 -4 4 -16 1.69 0.84 -4 -4 -16 0.99 1.04 -4 4 -16 2.81 1.12 4 4 16 1.89 1.05 4 -4 16 2.36 0.64 -4 4 -17 12.80 1.83 -4 4 -17 15.22 1.91 -4 -4 -17 12.34 1.77 4 -4 17 14.70 1.33 4 4 17 15.65 2.17 -4 4 -18 3.30 0.96 -4 4 -18 2.73 1.08 4 4 18 3.35 1.08 4 4 19 5.15 1.09 -4 -5 18 4.40 0.69 4 -5 -17 0.85 0.74 4 5 -17 1.19 0.95 -4 -5 17 1.28 0.52 4 5 -16 35.96 3.25 4 -5 -16 37.56 2.92 4 -5 -15 90.07 4.14 4 5 -15 94.00 5.45 4 -5 -15 87.24 4.84 4 -5 -14 82.64 4.34 4 -5 -14 85.26 5.06 4 -5 -13 4.95 1.44 4 5 -13 0.52 1.91 4 -5 -13 4.63 1.27 4 -5 -12 38.17 3.27 4 5 -12 45.61 4.56 4 -5 -12 33.83 3.38 4 -5 -12 49.88 3.30 4 -5 -11 21.34 2.50 4 5 -11 24.33 3.58 4 -5 -11 21.17 2.29 4 -5 -11 19.89 2.58 4 -5 -11 26.64 2.47 4 -5 -10 10.76 1.84 4 -5 -10 9.07 1.63 4 -5 -10 12.20 2.07 4 -5 -10 13.07 1.81 4 5 -10 16.02 3.10 4 -5 -9 7.90 1.65 4 -5 -9 9.15 1.68 4 5 -9 8.84 2.44 4 -5 -9 7.68 1.58 4 -5 -9 11.08 1.65 4 5 -9 6.41 2.47 4 -5 -9 5.13 4.34 4 -5 -8 41.46 3.26 4 -5 -8 41.10 3.25 4 -5 -8 35.35 3.13 4 -5 -8 41.04 3.09 4 5 -8 33.23 4.76 4 -5 -8 27.06 5.70 4 -5 -8 38.17 7.00 4 -5 -7 61.56 3.95 4 -5 -7 56.03 3.89 4 -5 -7 62.78 3.84 4 -5 -7 68.21 3.84 4 5 -7 65.33 5.31 4 -5 -7 53.11 6.91 4 -5 -7 66.09 8.74 4 -5 -6 156.51 5.99 4 -5 -6 167.73 6.34 4 -5 -6 145.66 6.23 4 -5 -6 168.56 5.89 4 -5 -6 152.03 11.10 4 -5 -6 162.61 13.17 4 -5 -5 1.01 0.88 4 -5 -5 1.72 0.82 4 5 -5 1.08 0.92 4 -5 -5 1.48 0.71 4 -5 -5 0.67 2.42 4 -5 -5 1.82 1.15 4 -5 -5 0.86 2.58 4 -5 -4 61.80 3.66 4 -5 -4 59.31 4.01 4 -5 -4 75.77 4.28 4 -5 -4 66.77 7.46 4 -5 -4 72.89 8.99 4 -5 -3 102.70 4.99 4 -5 -3 88.44 4.85 4 -5 -3 86.79 4.29 4 5 -3 102.82 5.36 4 -5 -3 96.17 8.81 4 -5 -3 100.79 10.39 4 -5 -2 322.60 8.16 4 -5 -2 339.34 9.49 4 -5 -2 374.17 9.50 4 -5 -2 382.84 17.28 4 -5 -2 374.99 19.40 4 5 -2 392.38 10.40 4 -5 -1 147.10 5.88 4 -5 -1 121.86 4.87 4 -5 -1 148.04 10.97 4 -5 -1 141.50 11.99 4 5 -1 151.93 6.43 4 -5 0 2.16 0.81 4 -5 0 1.13 0.78 4 -5 0 3.31 2.53 4 -5 0 2.62 2.70 4 5 0 3.96 1.06 4 -5 0 2.24 1.01 4 5 0 2.52 0.99 4 -5 1 35.15 2.54 4 -5 1 38.31 2.78 4 -5 1 37.63 5.54 4 -5 1 34.91 6.06 4 5 1 35.33 2.62 4 5 1 37.06 3.19 4 -5 1 34.46 2.98 4 -5 2 84.95 3.88 4 -5 2 84.69 3.97 4 -5 2 87.27 7.97 4 -5 2 81.35 8.92 4 -5 2 91.48 4.64 4 5 2 89.39 4.11 4 5 2 85.00 4.86 4 -5 2 83.87 4.48 4 -5 3 150.24 4.99 4 -5 3 157.23 5.23 4 -5 3 162.80 10.17 4 -5 3 160.03 12.01 4 5 3 149.60 5.36 4 -5 3 163.42 6.06 4 5 3 153.41 6.56 4 -5 3 153.59 5.82 4 -5 4 119.85 4.40 4 -5 4 120.73 4.40 4 -5 4 126.24 8.79 4 -5 4 109.66 9.76 4 -5 4 122.36 5.20 4 5 4 117.65 4.88 4 -5 4 117.38 4.29 4 5 4 123.29 6.09 4 -5 4 119.84 5.00 4 -5 5 568.26 9.49 4 -5 5 537.93 8.78 4 -5 5 571.44 17.70 4 -5 5 537.05 21.23 4 -5 5 536.74 23.60 4 -5 5 570.29 9.11 4 5 5 520.76 12.82 4 -5 5 557.27 10.88 4 -5 5 546.55 10.51 4 -5 6 8.73 1.24 4 -5 6 6.60 1.00 4 -5 6 7.16 3.58 4 -5 6 3.75 1.88 4 -5 6 7.53 3.71 4 5 6 7.83 1.35 4 -5 6 8.29 1.11 4 -5 6 7.83 1.39 4 5 6 6.52 1.70 4 -5 6 7.01 1.34 4 -5 7 150.24 13.14 4 -5 7 176.11 4.80 4 -5 7 165.94 8.95 4 -5 7 179.90 4.66 4 5 7 143.92 5.72 4 5 7 182.31 8.55 4 -5 7 173.93 5.92 4 -5 7 164.82 5.59 4 -5 8 225.51 16.26 4 -5 8 236.56 5.48 4 -5 8 222.92 10.40 4 -5 8 241.58 6.77 4 -5 8 257.23 5.41 4 5 8 204.94 6.80 4 -5 8 237.06 6.84 4 5 8 262.77 10.78 -4 -5 -9 159.56 7.88 4 -5 9 107.81 11.73 4 -5 9 126.49 8.08 4 -5 9 138.70 4.20 4 -5 9 142.84 5.14 4 5 9 131.69 5.42 4 5 9 161.68 9.06 4 -5 9 146.68 5.29 -4 -5 -10 130.17 7.42 4 -5 10 119.16 3.94 4 5 10 107.35 4.81 4 -5 10 117.76 4.62 4 -5 10 130.29 4.98 4 5 10 143.83 8.74 4 -5 11 27.43 1.90 4 -5 11 27.04 2.18 4 5 11 25.17 2.28 4 -5 11 27.70 2.24 4 5 11 25.57 3.80 -4 5 -12 2.96 1.05 -4 -5 -12 4.06 1.73 4 -5 12 3.11 0.74 4 -5 12 2.90 0.79 4 5 12 4.32 1.02 4 5 12 2.02 1.40 4 -5 12 4.47 0.94 -4 5 -13 3.68 1.23 4 -5 13 5.58 0.96 -4 -5 -13 5.97 1.78 4 5 13 7.06 1.23 4 -5 13 6.02 1.01 4 -5 13 6.43 0.97 4 5 13 5.08 1.75 -4 -5 -14 33.78 3.18 -4 5 -14 23.78 2.34 4 -5 14 29.21 2.07 4 5 14 34.14 2.39 4 -5 14 29.04 1.94 4 5 14 30.78 3.43 4 -5 14 32.77 1.91 4 -5 15 6.97 1.05 -4 -5 -15 6.21 1.41 4 5 15 5.97 1.53 4 -5 15 7.17 0.91 -4 5 -16 23.28 2.13 4 5 16 24.74 2.56 -4 5 -17 17.06 1.72 4 5 17 19.99 2.02 4 -6 -15 42.12 2.56 4 -6 -14 75.87 3.81 4 -6 -14 71.00 3.35 4 6 -13 54.46 4.18 4 -6 -13 45.53 3.18 4 -6 -13 50.50 3.08 4 -6 -12 36.27 3.00 4 -6 -12 42.52 3.10 4 -6 -11 35.92 3.06 4 -6 -11 33.02 2.84 4 -6 -10 3.78 1.20 4 6 -10 0.37 2.42 4 -6 -10 3.96 1.21 4 -6 -9 2.17 1.09 4 6 -9 0.59 1.87 4 -6 -9 2.43 0.99 4 -6 -8 30.40 2.87 4 -6 -8 28.11 2.65 4 6 -8 23.45 4.57 4 -6 -7 25.02 2.28 4 -6 -7 23.16 2.50 4 -6 -7 26.27 2.52 4 6 -7 23.79 3.80 4 -6 -6 171.50 6.25 4 -6 -6 167.12 6.59 4 -6 -5 73.10 3.76 4 -6 -5 70.06 4.07 4 -6 -5 69.28 4.28 4 -6 -4 28.11 2.32 4 -6 -4 26.93 2.76 4 -6 -4 30.52 2.76 4 6 -4 33.27 3.30 4 -6 -4 24.76 5.10 4 -6 -3 17.92 1.82 4 -6 -3 21.51 2.37 4 6 -3 24.25 2.82 4 -6 -2 2.03 0.76 4 -6 -2 1.78 0.98 4 -6 -2 1.10 2.63 4 -6 -2 2.12 2.91 4 6 -2 0.65 0.80 4 -6 -2 1.29 0.82 4 -6 -1 118.54 4.48 4 -6 -1 126.00 5.28 4 -6 -1 130.15 10.65 4 -6 -1 117.85 11.16 4 6 -1 133.54 6.27 4 -6 -1 121.74 5.64 4 -6 0 14.64 1.59 4 -6 0 17.46 4.53 4 -6 0 15.42 1.87 4 -6 0 16.46 5.00 4 6 0 19.50 2.22 4 -6 0 16.62 2.12 4 -6 1 13.14 1.49 4 -6 1 15.06 4.01 4 -6 1 16.03 1.85 4 -6 1 14.74 4.68 4 -6 1 15.33 2.05 4 6 1 19.84 2.25 4 6 1 16.68 2.23 4 -6 1 14.58 1.99 4 -6 2 47.79 2.75 4 -6 2 47.49 3.07 4 -6 2 42.17 5.92 4 -6 2 47.86 7.33 4 -6 2 49.91 3.53 4 6 2 65.01 4.05 4 6 2 50.49 3.77 4 -6 2 47.02 3.36 4 -6 3 79.61 3.51 4 -6 3 83.04 3.90 4 -6 3 71.49 7.38 4 -6 3 65.54 8.22 4 -6 3 80.99 4.45 4 6 3 95.00 4.77 4 6 3 73.30 4.49 4 -6 3 73.30 4.07 4 -6 4 81.46 3.62 4 -6 4 82.39 3.77 4 -6 4 79.03 7.40 4 -6 4 81.10 4.31 4 6 4 93.27 4.68 4 6 4 77.24 4.76 4 -6 4 71.74 3.90 4 -6 5 110.12 4.11 4 6 5 120.13 5.29 4 -6 5 109.57 4.90 4 6 5 102.45 5.67 4 -6 5 108.42 4.55 4 -6 6 115.76 4.07 4 6 6 116.64 5.36 4 -6 6 109.39 4.75 4 6 6 113.19 6.15 4 -6 7 5.64 0.95 4 -6 7 4.65 1.10 4 6 7 4.36 1.17 4 -6 7 4.63 1.06 4 6 7 5.18 1.55 4 -6 8 75.17 3.10 4 6 8 70.27 4.08 4 -6 8 78.50 3.89 4 -6 8 74.21 3.62 4 6 8 82.98 5.63 4 -6 9 26.81 1.83 4 -6 9 24.36 2.14 4 6 9 25.51 2.43 4 6 9 27.67 3.48 4 -6 9 26.23 2.16 4 -6 10 63.35 2.77 4 -6 10 62.30 3.25 4 6 10 66.24 3.78 4 -6 10 62.61 3.08 4 6 10 64.08 5.21 4 -6 11 24.28 1.72 4 -6 11 20.72 1.82 4 6 11 24.08 2.27 4 6 11 21.90 3.04 4 -6 11 22.27 1.77 4 -6 12 47.12 2.38 4 -6 12 46.95 2.50 4 6 12 48.93 2.98 4 6 12 45.33 4.03 4 -6 12 49.24 2.30 4 -6 13 4.44 0.78 4 -6 13 4.37 0.77 4 -6 13 4.53 0.68 4 6 13 5.73 1.50 4 -6 14 15.38 1.35 4 6 14 16.66 2.02 4 6 15 23.33 2.07 4 -7 -13 21.63 1.69 4 -7 -12 2.25 0.73 4 -7 -12 2.73 0.80 4 7 -11 0.48 1.70 4 -7 -11 5.25 1.05 4 -7 -10 9.93 1.41 4 7 -10 1.67 2.64 4 -7 -9 16.06 1.81 4 7 -9 13.58 4.17 4 -7 -8 27.57 2.35 4 7 -8 19.22 4.43 4 -7 -7 37.45 2.68 4 7 -7 45.09 5.16 4 -7 -6 87.45 4.08 4 7 -6 123.40 7.59 4 -7 -5 110.96 4.58 4 -7 -5 109.84 4.86 4 -7 -4 40.42 2.33 4 -7 -4 31.31 2.46 4 7 -4 43.34 3.85 4 -7 -4 27.65 2.47 4 -7 -3 7.07 1.06 4 -7 -3 8.62 1.45 4 7 -3 8.35 1.78 4 -7 -3 5.43 1.25 4 -7 -2 70.04 3.08 4 -7 -2 59.09 3.28 4 -7 -1 34.48 2.16 4 -7 -1 27.09 2.25 4 -7 0 18.07 1.57 4 -7 0 15.32 1.68 4 7 0 18.62 2.39 4 -7 1 7.73 1.17 4 -7 1 8.69 1.14 4 -7 1 7.21 1.29 4 -7 2 21.05 1.84 4 -7 2 21.79 2.11 4 -7 3 102.21 3.86 4 -7 3 100.65 4.60 4 -7 3 97.03 4.17 4 -7 4 148.92 4.51 4 7 4 160.13 6.32 4 -7 4 157.83 5.55 4 -7 5 39.22 2.24 4 -7 5 38.61 2.68 4 7 5 38.50 3.12 4 -7 6 2.71 0.64 4 -7 6 3.48 0.87 4 7 6 2.74 1.08 4 -7 6 2.64 0.79 4 -7 7 4.77 0.80 4 -7 7 4.58 0.98 4 -7 7 5.19 0.96 4 7 7 5.85 1.38 4 -7 8 0.46 0.39 4 -7 8 0.06 0.47 4 -7 8 0.74 0.54 4 7 8 0.75 0.81 4 -7 9 14.52 1.22 4 -7 9 14.53 1.44 4 7 9 14.70 2.05 4 -7 9 13.70 1.32 4 -7 10 61.90 2.39 4 -7 10 58.63 2.66 4 -7 10 58.61 2.43 4 7 10 54.48 3.60 4 -7 11 11.44 1.08 4 -7 11 10.09 1.06 4 -7 11 11.19 0.96 4 7 11 10.93 1.60 4 -7 12 19.28 1.27 4 -7 12 16.44 1.15 4 7 12 16.63 1.71 4 -7 13 31.17 1.53 4 -8 -10 5.14 0.76 4 -8 -10 5.98 0.93 4 -8 -9 6.05 0.90 4 -8 -9 6.61 1.02 4 -8 -8 21.33 1.51 4 -8 -8 24.22 1.92 4 -8 -7 26.73 1.73 4 8 -7 27.08 3.83 4 -8 -7 29.33 2.13 4 -8 -6 52.48 2.45 4 -8 -6 47.63 2.64 4 -8 -6 49.42 2.75 4 -8 -5 53.82 2.52 4 -8 -5 46.68 2.63 4 -8 -5 52.84 2.82 4 -8 -4 7.15 1.00 4 8 -4 4.75 1.33 4 -8 -4 7.39 1.08 4 -8 -4 7.68 1.13 4 -8 -3 26.94 1.80 4 -8 -3 27.55 2.05 4 8 -3 33.12 3.10 4 -8 -3 26.45 1.98 4 -8 -2 29.22 1.85 4 8 -2 33.11 3.06 4 -8 -2 31.74 2.17 4 -8 -2 28.80 2.02 4 -8 -1 3.65 0.70 4 8 -1 3.48 1.12 4 -8 -1 4.18 0.87 4 -8 -1 2.99 0.82 4 -8 0 2.84 0.64 4 8 0 1.85 0.98 4 -8 0 1.54 0.69 4 -8 0 2.59 0.72 4 -8 1 7.24 0.91 4 8 1 4.86 1.32 4 -8 1 8.17 1.14 4 -8 2 1.34 0.53 4 8 2 1.33 0.89 4 -8 2 1.94 0.66 4 -8 3 15.51 1.21 4 -8 3 15.89 1.50 4 -8 4 9.93 0.94 4 -8 4 8.69 1.05 4 -8 4 9.87 1.16 4 -8 5 16.14 1.14 4 -8 5 15.58 1.36 4 -8 5 17.27 1.45 4 -8 6 50.99 1.92 4 -8 6 55.80 2.44 4 -8 7 38.53 1.61 4 -8 7 35.86 1.88 4 -8 7 42.08 1.95 4 -8 8 17.94 1.07 4 -8 8 18.09 1.28 4 -8 8 16.67 1.12 4 -8 9 0.83 0.32 4 -8 9 0.49 0.32 4 8 9 0.22 0.63 4 8 10 -0.14 0.57 4 -9 -4 7.27 0.78 4 -9 -3 6.91 0.78 4 -9 -2 0.49 0.33 4 9 -1 0.05 0.66 4 -9 -1 0.37 0.29 4 -9 -1 0.39 0.35 4 -9 0 12.59 0.96 4 -9 0 13.45 1.00 4 -9 1 23.20 1.26 4 -9 1 24.30 1.28 4 9 2 0.84 0.80 4 -9 2 0.18 0.25 4 9 3 4.35 1.09 4 -9 3 16.63 1.04 4 9 4 0.15 0.68 5 0 -20 1.35 0.75 -5 0 20 0.82 0.49 5 0 -19 0.49 0.87 5 0 -19 0.51 0.75 5 0 -19 0.52 0.56 5 0 -19 0.39 0.58 -5 0 19 0.63 0.54 5 0 -18 5.78 1.66 5 0 -18 3.97 1.23 5 0 -18 5.41 1.12 5 0 -18 4.94 1.02 -5 0 18 6.10 1.03 5 0 -17 94.99 5.26 5 0 -17 92.38 5.94 5 0 -17 103.85 4.80 5 0 -17 89.62 4.37 -5 0 17 106.80 4.11 5 0 -16 38.26 4.00 5 0 -16 46.01 4.09 5 0 -16 46.36 3.55 5 0 -16 48.04 3.52 -5 0 16 50.15 2.88 5 0 -15 2.80 1.47 5 0 -15 3.23 1.58 5 0 -15 3.42 1.06 5 0 -15 3.51 1.29 -5 0 15 5.70 1.08 5 0 -14 2.85 1.41 5 0 -14 3.88 1.76 5 0 -14 3.58 1.29 5 0 -14 1.70 1.04 5 0 -14 1.24 4.99 5 0 -13 32.21 3.90 5 0 -13 39.75 4.28 5 0 -13 33.57 3.33 5 0 -13 32.63 3.38 5 0 -13 24.17 7.24 5 0 -12 302.20 11.16 5 0 -12 341.91 12.25 5 0 -12 265.71 9.14 5 0 -12 327.82 10.56 5 0 -12 281.74 19.81 5 0 -11 225.78 9.38 5 0 -11 328.19 11.49 5 0 -11 277.73 9.71 5 0 -11 205.60 8.15 5 0 -11 273.80 18.56 5 0 -10 239.00 9.28 5 0 -10 374.95 11.51 5 0 -10 301.55 10.14 5 0 -10 196.14 8.21 5 0 -10 309.18 18.51 5 0 -9 1.06 0.93 5 0 -9 1.75 1.35 5 0 -9 0.48 1.00 5 0 -9 0.28 1.00 5 0 -9 1.89 2.22 5 0 -8 59.92 4.34 5 0 -8 75.62 4.58 5 0 -8 56.05 4.36 5 0 -8 65.01 7.38 5 0 -7 32.59 3.17 5 0 -7 34.23 5.29 5 0 -6 5.28 2.52 5 0 -6 8.01 2.25 5 0 -6 6.87 1.55 5 0 -5 385.10 16.48 5 0 -5 474.58 13.96 5 0 -4 71.08 3.33 5 0 -4 68.37 6.90 5 0 -4 79.23 5.72 5 0 -3 218.66 6.38 5 0 -3 203.84 11.37 5 0 -3 219.37 9.38 5 0 -2 3003.09 26.03 5 0 -2 2836.33 32.93 5 0 -1 2392.76 25.83 5 0 -1 2303.40 36.18 5 0 0 106.89 6.14 5 0 0 84.19 6.03 5 0 0 94.74 7.31 5 0 1 179.04 8.59 5 0 1 143.63 8.03 5 0 2 327.26 12.10 5 0 2 308.21 12.01 5 0 3 92.11 6.61 5 0 3 91.16 6.77 5 0 4 10.67 2.47 5 0 4 9.66 2.42 5 0 5 1.21 1.32 5 0 5 1.47 1.63 5 0 5 1.05 0.54 5 0 5 0.95 0.52 5 0 6 25.94 3.74 5 0 6 27.92 1.67 5 0 6 33.25 2.01 5 0 6 30.92 1.92 5 0 6 30.74 1.71 5 0 7 902.60 9.02 5 0 7 929.95 10.68 5 0 7 937.38 9.60 5 0 8 103.48 7.25 5 0 8 119.25 3.97 5 0 8 115.61 3.72 5 0 8 119.78 3.52 5 0 8 96.39 4.69 5 0 9 43.02 4.83 5 0 9 41.36 2.41 5 0 9 43.69 2.30 5 0 9 43.67 2.26 5 0 9 42.99 3.44 5 0 10 238.20 11.42 5 0 10 246.80 5.89 5 0 10 253.31 5.50 5 0 10 231.73 8.33 5 0 10 257.13 5.72 5 0 11 1039.03 23.91 5 0 11 1047.88 12.52 5 0 11 1070.08 11.39 5 0 11 1071.83 12.49 -5 0 -12 103.38 5.13 5 0 12 100.55 7.55 5 0 12 108.79 4.09 5 0 12 104.39 4.11 5 0 12 106.96 3.63 -5 0 -13 1.30 0.97 5 0 13 2.60 2.24 5 0 13 2.29 0.75 5 0 13 1.47 0.70 5 0 13 0.80 1.01 5 0 13 1.72 0.60 -5 0 -14 48.66 3.68 -5 0 -14 51.09 3.93 5 0 14 54.92 2.97 5 0 14 54.77 2.77 5 0 14 53.82 4.20 5 0 14 57.00 3.31 -5 0 -15 21.09 2.62 5 0 15 17.30 2.36 5 0 15 21.58 1.78 5 0 15 22.65 2.16 -5 0 -16 190.11 7.11 -5 0 -16 190.74 7.75 5 0 16 198.46 5.30 5 0 16 208.96 5.56 5 0 16 205.18 6.48 -5 0 -17 0.77 1.02 -5 0 -17 0.34 0.81 5 0 17 0.12 0.48 5 0 17 0.41 0.59 5 0 17 0.76 0.94 -5 0 -18 0.21 0.85 -5 0 -18 0.64 0.97 5 0 18 0.73 0.93 5 0 18 0.84 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-14 252.00 8.34 5 1 -14 197.30 8.33 5 -1 -14 276.49 8.53 -5 1 14 282.86 6.59 5 1 -13 63.46 5.25 5 -1 -13 65.98 5.42 5 -1 -13 74.18 5.68 5 1 -13 64.29 5.16 5 -1 -13 79.23 4.55 5 1 -13 51.93 4.44 5 -1 -13 71.82 4.50 5 -1 -13 49.57 8.76 5 1 -12 20.01 3.01 5 -1 -12 23.77 3.31 5 -1 -12 21.02 3.15 5 1 -12 17.59 2.83 5 1 -12 19.11 2.89 5 -1 -12 25.16 2.85 5 -1 -12 27.70 2.87 5 -1 -12 14.60 5.33 5 1 -11 206.70 8.99 5 -1 -11 182.91 8.63 5 -1 -11 254.74 10.08 5 -1 -11 256.15 8.43 5 -1 -11 285.98 8.54 5 1 -11 122.17 7.53 5 -1 -11 211.29 16.22 5 1 -11 210.65 15.70 5 1 -10 20.85 2.90 5 -1 -10 27.13 3.25 5 -1 -10 29.59 3.41 5 1 -10 16.45 3.36 5 -1 -10 32.03 2.86 5 -1 -10 29.16 2.91 5 -1 -10 24.92 5.83 5 1 -10 25.43 5.59 5 1 -9 117.01 6.39 5 -1 -9 135.54 6.81 5 -1 -9 154.26 7.26 5 -1 -9 98.62 4.93 5 1 -9 95.00 8.73 5 -1 -9 140.04 6.21 5 -1 -9 126.50 11.66 5 1 -9 123.52 10.31 5 1 -8 141.78 6.87 5 -1 -8 138.60 6.50 5 -1 -8 161.98 7.15 5 1 -8 132.48 11.17 5 -1 -8 158.22 6.55 5 -1 -8 142.79 11.95 5 1 -8 135.31 10.04 5 -1 -8 127.25 8.92 5 1 -7 144.45 6.73 5 -1 -7 138.78 6.19 5 -1 -7 149.19 6.68 5 1 -7 146.83 11.25 5 -1 -7 128.18 5.78 5 -1 -7 122.14 10.70 5 1 -7 136.69 9.60 5 -1 -7 142.09 9.11 5 1 -6 59.67 4.31 5 -1 -6 52.53 3.71 5 -1 -6 61.14 4.09 5 1 -6 45.99 5.97 5 -1 -6 46.26 3.37 5 -1 -6 55.31 7.20 5 1 -6 53.92 5.88 5 -1 -6 58.83 5.81 5 -1 -5 89.36 8.85 5 1 -5 86.22 7.28 5 -1 -5 81.77 6.63 5 -1 -5 82.30 4.54 5 -1 -4 911.01 14.50 5 -1 -4 937.30 27.97 5 1 -4 905.31 22.02 5 1 -4 923.33 16.35 5 -1 -3 599.50 21.76 5 -1 -3 557.48 16.83 5 1 -3 605.09 17.53 5 1 -3 624.41 14.02 5 1 -2 241.74 7.10 5 -1 -2 245.28 13.60 5 -1 -2 213.08 10.36 5 1 -2 247.29 10.70 5 1 -2 231.13 8.84 5 -1 -1 50.08 5.14 5 1 -1 43.43 3.16 5 -1 -1 39.38 4.61 5 -1 -1 49.03 6.02 5 1 -1 45.65 4.14 5 1 0 163.40 6.56 5 -1 0 164.27 9.08 5 -1 0 179.15 11.27 5 1 0 172.52 8.18 5 -1 1 143.93 9.34 5 1 1 150.67 6.68 5 -1 1 133.68 8.24 5 -1 2 217.74 11.54 5 1 2 213.42 8.54 5 -1 2 190.27 9.95 5 -1 3 19.19 3.53 5 1 3 18.42 2.74 5 -1 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-4 -3 8.55 3.87 5 -4 -3 10.06 3.65 5 -4 -3 8.43 1.27 5 4 -3 10.54 1.87 5 -4 -2 30.92 2.84 5 -4 -2 29.23 2.90 5 -4 -2 30.28 5.68 5 -4 -2 33.35 6.08 5 -4 -2 28.08 5.45 5 4 -2 36.44 2.55 5 -4 -2 29.75 2.26 5 4 -2 35.20 3.08 5 -4 -2 32.93 2.84 5 -4 -1 149.42 6.13 5 -4 -1 148.32 6.39 5 -4 -1 147.55 9.05 5 -4 -1 152.36 11.98 5 -4 -1 164.80 13.17 5 -4 -1 131.63 10.89 5 -4 -1 142.64 4.91 5 4 -1 168.60 5.38 5 4 -1 155.81 6.41 5 -4 -1 152.75 6.05 5 4 -1 166.05 6.52 5 -4 0 40.95 3.19 5 -4 0 38.33 4.56 5 -4 0 42.93 6.54 5 -4 0 47.28 6.74 5 -4 0 37.21 2.72 5 4 0 44.91 3.35 5 4 0 45.12 2.78 5 4 0 43.42 3.45 5 -4 0 44.10 3.30 5 -4 1 82.69 4.38 5 -4 1 65.98 7.74 5 -4 1 81.24 6.07 5 -4 1 73.86 8.34 5 4 1 85.89 3.78 5 -4 1 73.50 3.80 5 4 1 83.16 4.75 5 -4 1 82.52 4.41 5 -4 2 48.81 3.24 5 -4 2 39.22 5.98 5 -4 2 38.03 4.23 5 -4 2 43.38 6.54 5 -4 2 46.14 3.02 5 4 2 50.72 2.95 5 4 2 49.27 3.69 5 -4 2 46.11 3.27 5 -4 3 126.65 5.00 5 -4 3 111.69 9.97 5 -4 3 114.95 6.69 5 -4 3 134.74 11.02 5 4 3 135.24 4.88 5 -4 3 122.46 4.85 5 4 3 124.18 5.93 5 -4 3 125.88 5.25 5 -4 4 554.90 10.19 5 -4 4 532.49 13.87 5 -4 4 568.01 22.26 5 -4 4 519.91 9.88 5 4 4 559.73 10.09 5 -4 4 556.21 9.07 5 4 4 524.83 12.47 5 -4 4 536.78 10.07 5 4 4 536.98 8.53 5 -4 4 550.84 10.75 5 -4 5 217.18 6.14 5 -4 5 206.28 4.55 5 -4 5 211.29 13.74 5 -4 5 214.83 8.84 5 -4 5 209.08 6.14 5 4 5 198.62 6.20 5 -4 5 217.37 5.83 5 4 5 212.45 8.20 5 -4 5 202.18 6.17 5 4 5 200.64 5.47 5 -4 5 209.61 6.66 5 -4 6 127.89 4.60 5 -4 6 122.33 11.14 5 -4 6 120.99 3.46 5 -4 6 114.92 10.37 5 -4 6 111.38 6.35 5 4 6 108.26 4.76 5 -4 6 126.67 4.62 5 -4 6 126.14 4.53 5 4 6 120.98 6.49 5 -4 6 126.56 4.85 5 4 6 111.65 4.23 5 4 6 125.38 5.49 5 -4 6 129.91 5.28 5 -4 7 22.81 1.96 5 -4 7 19.10 2.95 5 -4 7 18.25 5.04 5 -4 7 22.64 1.55 5 -4 7 22.78 5.20 5 4 7 21.22 2.12 5 -4 7 23.02 1.92 5 -4 7 20.75 1.90 5 -4 7 23.16 2.11 5 4 7 22.81 2.00 5 4 7 22.05 2.44 5 4 7 19.78 2.87 5 -4 7 21.23 2.21 5 -4 8 4.15 3.23 5 -4 8 4.30 0.74 5 -4 8 4.68 1.87 5 -4 8 3.39 3.06 5 -4 8 3.49 0.81 5 -4 8 3.83 0.94 5 4 8 3.30 0.97 5 4 8 4.80 1.72 5 -4 8 3.73 1.03 5 -4 8 4.00 0.96 5 4 8 3.52 0.90 5 4 8 3.21 1.22 5 -4 9 2.09 3.62 5 -4 9 1.07 1.59 5 -4 9 1.20 0.52 5 -4 9 1.54 3.68 5 -4 9 1.20 0.62 5 4 9 1.41 0.76 5 -4 9 1.16 0.59 5 4 9 1.11 1.11 5 -4 9 0.45 0.59 5 -4 9 1.70 0.77 5 4 9 1.06 0.69 5 4 9 0.84 0.96 5 -4 10 88.27 3.27 5 -4 10 84.89 3.87 5 4 10 81.01 4.20 5 -4 10 91.93 3.93 5 -4 10 93.18 4.17 5 4 10 76.52 3.87 5 4 10 77.10 4.94 5 4 10 106.17 7.48 5 -4 11 11.53 1.26 5 4 11 12.97 1.70 5 -4 11 11.74 1.48 5 -4 11 11.55 1.34 5 4 11 12.15 2.87 5 -4 11 12.18 1.54 5 4 11 11.71 2.03 5 -4 12 26.52 1.96 5 4 12 23.44 3.59 -5 4 -13 82.13 4.64 5 4 13 85.94 4.02 5 -4 13 84.04 3.62 5 -4 13 95.77 3.71 5 4 13 86.61 6.31 -5 4 -14 40.22 3.27 5 -4 14 36.93 2.32 5 -4 14 47.29 2.55 5 4 14 45.70 2.78 5 -4 14 48.88 2.59 5 4 14 46.18 4.31 -5 4 -15 102.08 4.49 -5 4 -15 103.07 4.93 5 4 15 111.39 4.00 5 -4 15 113.14 3.58 5 4 15 107.54 6.02 -5 4 -16 1.71 0.83 -5 4 -16 1.97 0.95 5 4 16 3.85 1.26 5 -4 16 2.58 0.67 -5 4 -17 21.89 2.10 -5 4 -17 21.22 1.85 5 4 17 24.67 2.48 5 -4 17 24.71 1.57 5 4 18 3.76 0.99 5 -5 -17 12.83 1.33 -5 -5 17 20.15 1.36 5 5 -16 25.37 2.28 5 -5 -16 27.31 2.18 5 5 -16 19.47 2.14 5 -5 -15 7.07 1.36 5 5 -15 6.64 1.53 5 5 -15 5.68 1.31 5 -5 -15 6.32 1.05 5 -5 -14 0.08 0.67 5 5 -14 0.52 1.14 5 5 -14 0.34 0.97 5 -5 -14 0.95 0.66 5 -5 -13 1.44 0.94 5 5 -13 2.26 1.50 5 -5 -13 1.77 0.84 5 5 -13 0.30 1.25 5 -5 -12 8.82 1.70 5 5 -12 17.23 2.93 5 -5 -12 11.97 1.66 5 5 -12 19.55 4.81 5 -5 -12 13.87 1.69 5 5 -11 35.69 4.11 5 -5 -11 26.59 2.56 5 -5 -11 22.70 2.66 5 -5 -11 32.53 2.65 5 5 -11 15.71 5.02 5 -5 -10 9.96 1.84 5 5 -10 7.97 3.78 5 -5 -10 13.62 1.79 5 -5 -9 10.44 1.74 5 -5 -9 9.74 1.80 5 -5 -9 11.86 1.67 5 5 -9 5.61 2.94 5 -5 -8 7.66 1.56 5 -5 -8 7.39 1.49 5 5 -8 5.00 2.29 5 -5 -8 8.12 1.40 5 -5 -7 0.08 0.76 5 -5 -7 0.28 0.65 5 5 -7 -0.02 0.98 5 -5 -7 0.05 0.63 5 -5 -7 -0.63 3.35 5 -5 -6 3.58 1.19 5 -5 -6 2.95 1.06 5 5 -6 1.22 1.10 5 -5 -6 2.45 0.85 5 -5 -6 1.27 3.69 5 -5 -5 28.99 2.69 5 -5 -5 25.06 2.70 5 5 -5 31.81 3.80 5 -5 -5 30.47 2.49 5 -5 -5 26.73 6.29 5 -5 -4 8.97 1.56 5 -5 -4 10.00 1.83 5 -5 -4 6.42 3.97 5 5 -4 7.82 2.00 5 -5 -3 8.46 1.66 5 -5 -3 8.54 1.54 5 -5 -3 6.70 3.85 5 -5 -3 6.96 3.80 5 5 -3 7.99 1.72 5 5 -3 13.47 1.82 5 -5 -3 9.24 1.63 5 -5 -2 27.75 2.68 5 -5 -2 30.62 3.04 5 -5 -2 33.93 6.79 5 -5 -2 27.63 2.41 5 -5 -2 22.98 5.67 5 5 -2 36.35 2.82 5 5 -2 27.74 2.92 5 -5 -2 27.85 2.87 5 -5 -1 66.96 4.02 5 -5 -1 69.18 3.64 5 -5 -1 69.51 8.95 5 5 -1 82.52 4.07 5 5 -1 60.46 4.37 5 -5 -1 71.39 4.45 5 -5 0 83.19 4.44 5 -5 0 78.80 3.70 5 -5 0 76.65 9.39 5 -5 0 73.04 8.81 5 -5 0 81.87 4.39 5 5 0 91.34 4.30 5 5 0 78.88 4.86 5 -5 0 91.57 5.07 5 5 0 89.00 5.05 5 -5 1 1201.55 16.18 5 -5 1 1202.23 13.82 5 -5 1 1175.58 27.00 5 -5 1 1243.95 36.63 5 -5 1 1075.00 32.46 5 5 1 1308.26 15.87 5 -5 1 1188.24 16.75 5 -5 1 1204.81 17.88 5 5 1 1189.23 18.45 5 -5 2 1152.91 15.36 5 -5 2 1122.11 12.86 5 -5 2 1126.91 25.75 5 -5 2 1153.14 34.68 5 5 2 1152.89 15.17 5 -5 2 1149.73 16.58 5 5 2 1106.30 18.02 5 -5 2 1120.97 16.80 5 -5 3 547.19 10.30 5 -5 3 517.10 8.50 5 -5 3 505.40 15.90 5 -5 3 517.46 22.94 5 -5 3 500.04 9.76 5 5 3 537.49 10.52 5 -5 3 528.75 11.15 5 5 3 531.64 12.60 5 -5 3 524.49 11.16 5 -5 4 108.06 4.46 5 -5 4 90.78 10.00 5 -5 4 102.91 3.67 5 -5 4 85.79 6.55 5 -5 4 103.90 10.29 5 -5 4 104.34 4.37 5 5 4 106.37 4.83 5 -5 4 101.51 4.81 5 5 4 95.32 5.59 5 -5 4 100.93 4.82 5 -5 5 409.86 8.57 5 -5 5 421.64 7.27 5 -5 5 394.03 19.41 5 -5 5 372.54 13.00 5 5 5 417.40 9.66 5 -5 5 436.23 8.51 5 -5 5 424.79 8.68 5 5 5 412.88 12.03 5 -5 5 436.26 9.63 5 -5 5 414.39 9.57 5 -5 6 254.36 6.63 5 -5 6 224.21 15.96 5 -5 6 256.12 5.49 5 -5 6 229.11 14.96 5 5 6 223.69 7.25 5 -5 6 254.37 6.09 5 -5 6 254.69 6.81 5 5 6 244.78 9.62 5 -5 6 248.76 7.15 5 -5 6 235.36 7.09 5 -5 7 127.41 3.83 5 -5 7 130.12 4.18 5 5 7 113.30 5.20 5 -5 7 124.92 4.81 5 5 7 133.42 7.56 5 -5 7 125.96 5.01 5 -5 7 125.92 5.05 5 -5 8 1.62 0.59 5 -5 8 0.34 0.58 5 -5 8 1.64 0.57 5 5 8 0.53 0.76 5 -5 8 0.10 0.57 5 -5 8 0.42 0.58 5 5 8 0.84 1.17 5 -5 9 51.23 2.47 5 5 9 45.15 3.23 5 -5 9 49.15 3.01 5 -5 9 48.23 2.75 5 -5 9 50.50 3.12 5 -5 10 0.29 0.41 5 -5 10 0.13 0.52 5 -5 11 8.73 1.08 5 5 11 9.92 1.48 5 -5 11 9.39 1.36 5 -5 11 9.78 1.33 5 5 11 7.27 2.12 -5 5 -12 40.46 3.03 5 -5 12 43.91 2.41 5 -5 12 49.41 2.73 5 5 12 47.00 2.93 5 5 12 40.68 4.34 5 -5 12 52.03 2.72 -5 5 -13 7.80 1.41 5 -5 13 8.33 1.10 5 -5 13 9.71 1.20 5 5 13 9.89 1.32 5 -5 13 11.14 1.20 5 5 13 10.17 2.14 -5 5 -14 2.97 1.06 5 -5 14 2.29 0.68 5 -5 14 2.79 0.69 5 5 14 2.77 0.79 5 5 14 1.87 1.05 5 -5 14 3.43 0.69 -5 5 -15 0.97 0.73 5 5 15 2.17 0.68 5 5 15 2.48 1.02 5 -5 15 2.02 0.56 5 5 16 4.17 1.04 5 -6 -14 2.29 0.82 5 6 -14 1.56 0.81 5 -6 -14 2.07 0.67 5 -6 -13 17.36 1.90 5 -6 -13 15.54 1.56 5 -6 -12 0.21 0.69 5 6 -12 -0.01 1.30 5 -6 -12 0.18 0.53 5 -6 -11 10.64 1.72 5 -6 -11 12.03 1.54 5 -6 -10 11.31 1.71 5 6 -10 7.50 3.61 5 -6 -9 2.13 1.00 5 -6 -9 1.88 0.83 5 6 -9 0.45 1.97 5 -6 -8 11.07 1.51 5 -6 -8 12.10 1.58 5 -6 -8 10.78 1.75 5 6 -8 9.93 3.28 5 -6 -7 45.34 2.89 5 -6 -7 52.77 3.23 5 -6 -7 45.94 3.39 5 6 -7 47.03 6.17 5 -6 -6 12.22 1.59 5 6 -6 12.28 2.67 5 -6 -6 11.88 1.77 5 -6 -5 15.71 1.77 5 -6 -5 19.09 1.97 5 -6 -5 17.04 2.21 5 6 -5 16.83 2.81 5 -6 -5 16.23 2.09 5 -6 -4 58.68 3.40 5 -6 -4 54.27 3.13 5 6 -4 61.49 4.88 5 -6 -4 51.10 3.63 5 -6 -3 7.23 1.23 5 -6 -3 7.37 1.24 5 6 -3 8.03 1.76 5 -6 -3 6.06 1.36 5 -6 -2 42.84 2.85 5 -6 -2 41.99 2.78 5 6 -2 47.35 3.83 5 -6 -2 40.50 3.35 5 -6 -1 112.24 4.60 5 -6 -1 117.74 4.56 5 -6 -1 111.66 5.19 5 6 -1 121.39 6.00 5 -6 -1 109.40 5.39 5 -6 0 168.10 5.55 5 -6 0 158.94 5.19 5 6 0 151.18 6.63 5 -6 0 152.63 6.13 5 -6 0 154.64 6.29 5 -6 1 2.44 0.85 5 -6 1 3.13 0.86 5 -6 1 2.33 0.85 5 6 1 3.83 1.17 5 6 1 3.15 1.23 5 -6 1 3.08 1.07 5 -6 1 2.30 0.96 5 -6 2 64.95 3.40 5 -6 2 65.20 3.16 5 6 2 72.82 4.11 5 -6 2 65.42 4.05 5 -6 2 66.41 3.37 5 -6 2 57.58 3.69 5 6 2 62.72 4.23 5 -6 3 0.92 0.61 5 -6 3 0.63 0.56 5 -6 3 0.24 0.53 5 6 3 1.08 0.76 5 -6 3 0.72 0.67 5 6 3 1.33 0.90 5 -6 3 0.70 0.74 5 -6 4 244.92 6.46 5 -6 4 238.90 5.61 5 6 4 245.26 7.61 5 -6 4 236.21 5.72 5 -6 4 231.99 7.18 5 6 4 222.57 8.22 5 -6 5 84.15 3.24 5 6 5 81.76 4.43 5 -6 5 80.37 4.08 5 6 5 74.63 4.94 5 -6 5 76.99 3.89 5 -6 6 78.40 3.03 5 -6 6 72.10 3.57 5 -6 7 42.78 2.24 5 6 7 37.86 3.00 5 -6 7 43.55 2.88 5 -6 7 37.14 2.45 5 -6 7 43.17 2.85 5 6 7 47.24 4.30 5 -6 8 17.11 1.40 5 -6 8 18.56 1.87 5 6 8 18.95 2.12 5 -6 8 16.81 1.72 5 6 8 19.03 2.91 5 -6 9 33.31 1.91 5 6 9 35.03 2.76 5 -6 9 33.99 2.43 5 -6 9 35.64 2.38 5 6 9 37.52 4.02 5 -6 10 25.79 1.70 5 -6 10 26.52 2.05 5 6 10 27.39 2.43 5 -6 10 26.98 1.97 5 6 10 27.42 3.41 5 -6 11 14.09 1.25 5 6 11 18.01 1.94 5 -6 11 15.26 1.52 5 6 11 15.49 2.42 5 -6 11 14.93 1.35 5 -6 12 2.41 0.63 5 -6 12 1.73 0.59 5 6 12 1.87 0.69 5 6 12 1.69 1.11 5 -6 12 1.79 0.52 5 -6 13 54.50 2.21 5 6 13 62.30 3.85 5 -6 13 58.57 2.11 5 6 14 40.22 2.69 5 -7 -12 11.71 1.19 5 -7 -11 12.59 1.08 5 -7 -11 16.50 1.50 5 -7 -10 9.74 1.08 5 -7 -10 12.28 1.41 5 7 -9 3.36 3.28 5 7 -8 13.58 3.60 5 -7 -8 13.71 1.62 5 -7 -7 5.46 0.90 5 7 -7 4.05 2.10 5 -7 -7 5.77 1.12 5 -7 -6 57.63 2.57 5 -7 -6 51.97 3.18 5 -7 -5 41.82 2.27 5 -7 -5 33.16 2.04 5 7 -5 44.18 4.48 5 -7 -5 33.61 2.42 5 -7 -5 35.53 2.66 5 -7 -4 38.26 2.23 5 -7 -4 29.95 1.96 5 -7 -4 30.50 2.36 5 7 -4 37.46 3.77 5 -7 -4 30.57 2.46 5 -7 -3 6.13 1.00 5 -7 -3 3.96 0.88 5 7 -3 5.37 1.50 5 -7 -3 5.13 1.07 5 -7 -3 4.52 1.02 5 -7 -2 17.30 1.53 5 -7 -2 12.87 1.36 5 -7 -2 12.05 1.56 5 7 -2 17.96 2.48 5 -7 -2 13.09 1.65 5 -7 -1 12.08 1.31 5 -7 -1 9.74 1.21 5 -7 -1 8.46 1.38 5 7 -1 11.29 1.94 5 -7 -1 9.38 1.42 5 -7 0 78.80 3.06 5 7 0 68.67 4.38 5 -7 0 78.59 3.87 5 -7 0 69.27 3.63 5 -7 1 82.98 3.11 5 -7 1 83.31 3.99 5 7 1 76.32 4.75 5 -7 1 74.53 3.71 5 -7 2 28.19 1.79 5 7 2 24.76 2.79 5 -7 2 29.44 2.36 5 -7 2 25.92 2.18 5 -7 3 100.81 3.23 5 -7 3 105.61 3.94 5 -7 3 106.23 4.38 5 -7 3 101.85 4.10 5 -7 4 43.05 2.11 5 -7 4 42.18 2.54 5 -7 4 40.44 2.63 5 -7 4 41.84 2.56 5 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1.29 5 -8 1 29.48 1.70 5 -8 1 31.47 1.90 5 -8 1 30.31 1.76 5 -8 2 11.33 0.82 5 -8 2 14.60 1.22 5 8 2 9.69 1.70 5 -8 2 15.31 1.31 5 -8 3 5.41 0.56 5 -8 3 6.53 0.84 5 -8 3 6.73 0.87 5 -8 4 7.27 0.63 5 -8 4 9.90 0.99 5 8 4 4.03 1.32 5 -8 4 12.85 1.15 5 -8 5 25.52 1.52 5 -8 5 30.38 1.69 5 -8 6 14.60 1.12 5 -8 6 17.36 1.21 5 -8 7 0.52 0.32 5 8 7 -0.41 0.73 5 -8 7 0.66 0.33 5 -8 8 8.80 0.79 5 8 8 0.58 0.76 6 0 -19 5.58 1.20 6 0 -19 4.64 0.74 6 0 -18 12.15 1.93 6 0 -18 7.62 1.19 6 0 -18 11.91 1.35 6 0 -17 16.08 2.35 6 0 -17 14.01 1.74 6 0 -17 19.33 1.92 6 0 -17 15.26 1.70 6 0 -16 1.52 1.06 6 0 -16 1.73 1.03 6 0 -16 1.04 0.72 6 0 -16 1.87 0.94 -6 0 16 1.99 0.67 6 0 -15 -0.25 0.99 6 0 -15 0.39 1.02 6 0 -15 0.73 0.80 6 0 -15 0.33 0.66 -6 0 15 0.01 0.45 6 0 -14 0.36 0.99 6 0 -14 0.08 1.15 6 0 -14 0.24 0.69 6 0 -14 0.46 0.89 6 0 -13 32.43 3.72 6 0 -13 38.50 3.90 6 0 -13 43.88 3.59 6 0 -13 38.20 3.56 6 0 -12 62.33 4.95 6 0 -12 74.49 5.48 6 0 -12 77.58 5.14 6 0 -12 69.42 4.57 6 0 -12 64.68 10.81 6 0 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1.90 6 3 -15 15.28 2.47 6 -3 -15 17.16 2.20 6 -3 -15 11.58 1.79 6 3 -15 14.28 2.28 6 -3 -15 17.15 1.77 6 3 -14 23.12 3.19 6 -3 -14 21.20 2.70 6 -3 -14 16.63 2.21 6 3 -14 15.25 2.67 6 -3 -14 22.72 2.15 6 -3 -13 4.98 1.38 6 3 -13 8.38 2.21 6 -3 -13 6.26 1.59 6 -3 -13 6.04 1.22 6 3 -13 1.96 1.53 6 3 -12 42.09 4.66 6 -3 -12 33.20 3.55 6 -3 -12 21.81 2.69 6 3 -12 11.60 3.71 6 -3 -12 36.31 2.89 6 -3 -11 10.78 1.97 6 3 -11 14.05 2.94 6 -3 -11 8.70 1.99 6 -3 -11 13.34 1.87 6 3 -11 6.14 3.36 6 -3 -11 14.17 1.93 6 -3 -10 7.16 1.70 6 3 -10 5.23 2.06 6 -3 -10 4.56 1.55 6 -3 -10 5.26 4.16 6 3 -10 1.72 2.79 6 -3 -10 5.82 1.32 6 -3 -10 7.49 1.40 6 -3 -10 6.47 1.48 6 3 -9 94.09 6.75 6 -3 -9 77.06 5.17 6 -3 -9 78.07 5.06 6 -3 -9 78.02 10.55 6 -3 -9 73.87 9.51 6 3 -9 69.44 9.20 6 -3 -9 77.10 4.32 6 -3 -9 97.08 4.53 6 -3 -9 88.28 4.87 6 3 -8 91.06 6.23 6 -3 -8 65.37 4.63 6 -3 -8 70.99 4.82 6 -3 -8 78.88 10.78 6 -3 -8 65.52 8.96 6 3 -8 77.66 8.45 6 -3 -8 65.77 3.91 6 -3 -8 79.17 3.97 6 -3 -8 81.63 4.68 6 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6 -3 -1 43.32 2.64 6 -3 -1 51.62 2.73 6 3 -1 49.53 3.63 6 -3 -1 40.79 2.57 6 -3 -1 46.36 3.13 6 3 -1 52.16 3.57 6 -3 0 308.40 8.74 6 -3 0 260.25 15.28 6 -3 0 285.15 15.77 6 3 0 315.93 6.78 6 -3 0 289.98 6.74 6 -3 0 297.08 6.64 6 3 0 298.82 8.58 6 3 0 320.00 8.78 6 -3 0 296.41 7.77 6 -3 1 17.94 2.13 6 -3 1 18.38 4.56 6 3 1 19.35 1.73 6 -3 1 21.01 1.80 6 3 1 15.94 2.08 6 -3 1 17.33 1.69 6 3 1 16.65 2.10 6 -3 1 17.10 1.97 6 -3 2 39.42 2.98 6 -3 2 32.54 5.90 6 -3 2 37.31 5.96 6 3 2 40.82 2.58 6 -3 2 41.40 2.51 6 3 2 37.96 2.92 6 -3 2 37.28 2.48 6 3 2 38.04 3.16 6 -3 2 34.56 2.73 6 -3 3 47.05 3.17 6 -3 3 39.55 6.29 6 -3 3 54.33 6.96 6 3 3 46.99 2.91 6 3 3 41.85 3.03 6 -3 3 46.71 2.66 6 -3 3 46.61 2.75 6 3 3 44.49 2.22 6 3 3 43.19 3.35 6 -3 3 48.62 3.17 6 -3 4 171.74 5.73 6 -3 4 166.21 12.50 6 -3 4 168.60 12.34 6 3 4 179.51 5.87 6 3 4 149.14 5.74 6 -3 4 167.01 5.02 6 3 4 150.17 6.38 6 -3 4 162.97 5.15 6 3 4 158.23 4.31 6 -3 4 162.52 5.84 6 -3 5 347.59 7.95 6 -3 5 322.26 17.44 6 -3 5 362.79 18.24 6 3 5 352.13 8.51 6 -3 5 359.26 8.41 6 -3 5 334.26 7.25 6 3 5 303.94 9.27 6 -3 5 353.86 7.67 6 3 5 345.04 6.59 6 -3 5 351.80 8.55 6 -3 6 186.59 5.63 6 -3 6 162.51 12.80 6 -3 6 191.07 13.49 6 3 6 182.31 6.28 6 -3 6 192.72 6.07 6 -3 6 184.34 5.42 6 3 6 157.06 6.91 6 -3 6 193.29 5.75 6 3 6 189.91 5.05 6 3 6 206.99 6.89 6 -3 6 188.88 6.28 6 -3 7 118.74 4.39 6 -3 7 101.56 9.84 6 -3 7 115.25 10.63 6 3 7 100.91 4.79 6 -3 7 123.18 4.65 6 -3 7 108.86 4.30 6 -3 7 111.55 4.79 6 -3 7 113.17 4.42 6 3 7 110.08 3.97 6 3 7 117.65 5.50 6 3 7 103.79 5.91 6 -3 8 139.60 11.66 6 -3 8 133.50 11.67 6 3 8 146.13 5.75 6 -3 8 156.15 4.99 6 -3 8 152.31 5.13 6 -3 8 150.65 5.45 6 -3 8 145.80 5.00 6 3 8 141.71 4.64 6 3 8 139.67 6.19 6 3 8 139.75 7.23 6 -3 9 237.12 15.22 6 3 9 261.10 7.66 6 -3 9 266.88 6.91 6 -3 9 284.11 7.26 6 -3 9 273.20 6.82 6 3 9 257.43 6.49 6 3 9 254.00 8.38 6 3 9 267.48 10.51 6 3 10 58.29 3.61 6 -3 10 57.09 3.22 6 -3 10 62.12 3.30 6 -3 10 62.01 3.22 6 3 10 54.87 3.09 6 3 10 62.15 4.22 6 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2.78 1.28 6 4 -14 13.49 2.32 6 -4 -14 12.87 1.74 6 -4 -14 11.86 1.71 6 4 -14 6.57 1.65 6 -4 -14 14.20 1.58 6 -4 -13 7.79 1.54 6 4 -13 8.36 2.13 6 -4 -13 7.37 1.55 6 -4 -13 11.08 1.51 6 -4 -13 7.82 1.27 6 4 -12 16.14 2.92 6 -4 -12 14.51 2.14 6 -4 -12 10.73 1.80 6 -4 -12 18.56 1.99 6 -4 -12 16.53 1.92 6 4 -11 6.15 2.17 6 -4 -11 3.12 1.23 6 4 -11 1.00 2.65 6 -4 -11 5.50 1.31 6 -4 -10 5.19 1.41 6 4 -10 5.99 2.32 6 -4 -10 3.01 1.24 6 4 -10 0.65 2.63 6 -4 -10 4.37 1.10 6 -4 -10 4.53 1.28 6 -4 -9 20.67 2.56 6 -4 -9 19.41 2.47 6 -4 -9 21.52 2.25 6 -4 -9 19.72 2.40 6 -4 -8 18.11 2.41 6 -4 -8 16.59 2.30 6 -4 -8 14.59 5.28 6 4 -8 8.30 3.74 6 -4 -8 20.48 2.15 6 -4 -8 19.96 2.44 6 -4 -7 25.31 2.73 6 -4 -7 25.63 2.82 6 -4 -7 27.41 6.27 6 -4 -7 27.46 6.53 6 4 -7 21.40 4.17 6 -4 -7 27.52 2.42 6 -4 -7 35.70 3.16 6 -4 -6 64.95 4.34 6 -4 -6 67.73 4.57 6 -4 -6 75.98 9.40 6 -4 -6 65.58 9.35 6 -4 -6 64.94 3.66 6 4 -6 78.57 6.46 6 -4 -6 73.17 4.44 6 -4 -5 137.81 6.24 6 -4 -5 146.11 6.71 6 -4 -5 145.93 12.45 6 -4 -5 151.82 13.99 6 -4 -5 141.54 5.21 6 4 -5 172.36 9.20 6 -4 -5 151.16 6.28 6 -4 -4 143.90 6.31 6 -4 -4 143.69 6.74 6 -4 -4 139.49 11.83 6 -4 -4 150.47 13.65 6 -4 -4 144.49 5.27 6 -4 -4 144.26 5.17 6 4 -4 170.84 8.24 6 -4 -4 149.31 6.20 6 -4 -3 1.26 1.00 6 -4 -3 0.68 0.78 6 -4 -3 1.89 3.85 6 -4 -3 0.99 2.69 6 4 -3 1.62 1.16 6 -4 -3 1.97 0.79 6 -4 -3 0.96 0.86 6 -4 -3 0.42 0.64 6 -4 -2 20.88 2.47 6 -4 -2 22.33 2.71 6 -4 -2 19.88 5.44 6 -4 -2 14.89 4.78 6 -4 -2 18.38 4.92 6 4 -2 24.13 2.06 6 -4 -2 22.81 2.08 6 -4 -2 20.57 2.00 6 4 -2 23.34 2.82 6 -4 -2 20.40 2.25 6 -4 -1 482.33 11.36 6 -4 -1 381.29 19.84 6 -4 -1 424.36 8.92 6 4 -1 514.49 9.27 6 -4 -1 456.11 8.68 6 4 -1 500.48 12.04 6 -4 -1 441.77 10.42 6 -4 0 729.39 13.97 6 -4 0 726.45 26.96 6 -4 0 719.37 10.94 6 4 0 775.51 14.48 6 4 0 730.02 11.12 6 -4 0 687.59 11.33 6 -4 0 710.45 13.16 6 4 0 743.43 14.28 6 -4 1 78.25 4.40 6 -4 1 69.23 8.77 6 -4 1 61.85 8.22 6 4 1 76.22 3.69 6 -4 1 73.12 3.76 6 -4 1 83.41 3.72 6 4 1 78.06 4.55 6 4 1 72.67 4.53 6 -4 1 72.93 4.19 6 -4 2 499.51 10.73 6 -4 2 447.15 21.50 6 -4 2 498.96 22.44 6 4 2 493.67 9.54 6 -4 2 499.43 9.00 6 4 2 504.62 11.56 6 -4 2 454.40 9.22 6 4 2 448.47 11.26 6 -4 2 460.73 10.50 6 -4 3 544.03 10.76 6 -4 3 466.72 21.76 6 -4 3 525.53 23.03 6 4 3 540.03 12.14 6 -4 3 523.98 9.29 6 4 3 549.78 10.38 6 4 3 474.91 11.73 6 -4 3 502.04 9.67 6 -4 3 534.62 11.26 6 -4 4 82.36 4.05 6 -4 4 65.43 8.41 6 -4 4 81.15 9.26 6 -4 4 80.82 4.08 6 -4 4 79.69 3.65 6 4 4 82.24 4.22 6 -4 4 77.94 3.85 6 4 4 70.55 4.62 6 -4 4 81.07 4.37 6 -4 5 116.49 4.66 6 -4 5 94.85 10.10 6 -4 5 105.94 10.67 6 -4 5 111.89 4.62 6 4 5 118.91 5.20 6 -4 5 108.81 4.27 6 -4 5 113.15 4.64 6 4 5 112.17 4.31 6 4 5 102.98 5.73 6 -4 5 116.01 5.19 6 -4 6 81.65 3.78 6 -4 6 59.62 8.27 6 -4 6 63.80 8.42 6 -4 6 77.66 3.75 6 4 6 69.32 4.05 6 -4 6 71.38 3.49 6 4 6 74.08 5.10 6 -4 6 80.50 3.89 6 4 6 74.01 3.62 6 -4 6 79.98 4.22 6 -4 7 6.25 1.14 6 -4 7 2.25 3.63 6 -4 7 5.90 4.05 6 -4 7 7.46 1.18 6 4 7 5.09 1.19 6 -4 7 7.35 1.21 6 -4 7 6.11 1.34 6 -4 7 5.93 1.17 6 4 7 5.49 1.08 6 4 7 6.23 1.76 6 4 8 43.67 3.26 6 -4 8 50.03 2.75 6 -4 8 44.85 2.80 6 -4 8 45.94 3.11 6 4 8 44.89 4.38 6 -4 8 51.44 3.11 6 4 8 41.89 2.83 6 4 9 155.59 6.01 6 -4 9 151.01 5.23 6 -4 9 162.02 5.43 6 4 9 172.61 8.97 6 -4 9 177.88 5.65 6 4 9 145.21 5.30 6 4 10 5.39 1.22 6 -4 10 7.03 1.19 6 4 10 6.22 2.00 6 4 10 5.23 1.11 6 4 11 25.93 2.39 6 -4 11 24.25 2.04 6 4 11 24.59 3.42 6 -4 11 24.85 1.88 6 -4 11 28.09 2.12 6 4 12 20.32 2.03 6 -4 12 18.91 1.78 6 4 12 17.97 2.96 6 -4 12 19.71 1.52 6 -4 12 19.35 1.68 -6 4 -13 28.71 2.72 6 4 13 32.71 2.44 6 -4 13 29.75 2.06 6 4 13 28.67 3.36 6 -4 13 31.83 2.03 -6 4 -14 95.93 4.69 6 4 14 106.46 4.06 6 -4 14 104.16 3.52 6 4 14 100.68 5.63 6 -4 14 113.07 3.71 -6 4 -15 36.26 2.82 6 4 15 41.86 2.29 6 -4 15 41.31 2.00 6 4 15 40.21 3.28 6 -4 15 44.37 2.23 -6 4 -16 45.40 2.85 6 4 16 50.48 3.24 6 -5 -16 12.31 1.29 6 -5 -15 21.84 1.88 6 5 -15 15.76 1.96 6 5 -15 18.77 1.86 6 -5 -14 4.79 1.05 6 5 -14 2.56 1.23 6 5 -14 1.21 0.85 6 -5 -14 2.75 0.74 6 -5 -13 4.99 1.14 6 -5 -13 5.60 1.06 6 -5 -13 4.31 0.92 6 -5 -12 6.26 1.35 6 -5 -12 11.83 1.59 6 5 -12 3.96 1.93 6 -5 -12 11.41 1.48 6 -5 -11 2.42 0.94 6 -5 -11 5.08 1.26 6 5 -11 0.74 2.33 6 -5 -11 3.92 1.01 6 -5 -10 28.33 2.65 6 -5 -10 30.81 2.90 6 -5 -10 37.95 2.79 6 -5 -10 31.79 2.65 6 -5 -9 5.44 1.35 6 -5 -9 7.57 1.54 6 -5 -9 5.80 1.23 6 -5 -9 6.42 1.38 6 -5 -8 54.83 3.42 6 -5 -8 51.39 3.60 6 -5 -7 30.92 2.84 6 -5 -7 23.56 2.63 6 5 -7 22.34 4.52 6 -5 -7 25.75 2.38 6 -5 -7 25.42 2.64 6 -5 -6 19.35 2.32 6 -5 -6 15.26 2.13 6 5 -6 18.34 3.65 6 -5 -6 20.41 2.38 6 -5 -5 27.05 2.71 6 -5 -5 24.44 2.67 6 5 -5 27.17 3.92 6 -5 -5 27.27 2.42 6 -5 -5 29.92 2.91 6 -5 -4 12.78 1.90 6 -5 -4 11.88 1.97 6 -5 -4 13.53 1.76 6 5 -4 9.61 2.28 6 -5 -4 12.80 1.93 6 -5 -3 6.29 1.37 6 5 -3 8.16 1.84 6 -5 -3 8.47 1.21 6 -5 -3 6.19 1.45 6 -5 -3 6.21 1.27 6 -5 -2 45.19 3.42 6 -5 -2 38.20 6.98 6 -5 -2 50.13 2.89 6 -5 -2 43.20 3.03 6 5 -2 48.03 4.02 6 -5 -2 42.06 3.44 6 -5 -1 138.49 5.88 6 -5 -1 104.63 11.48 6 -5 -1 119.64 12.03 6 -5 -1 123.64 5.19 6 5 -1 152.18 5.38 6 -5 -1 130.34 4.76 6 5 -1 134.05 6.38 6 -5 -1 129.73 5.98 6 -5 0 411.57 9.96 6 -5 0 391.87 21.36 6 -5 0 367.61 8.99 6 5 0 411.34 8.72 6 -5 0 405.62 8.42 6 5 0 387.95 10.58 6 -5 0 388.39 10.24 6 -5 1 432.33 9.97 6 -5 1 431.81 22.25 6 -5 1 413.08 9.54 6 5 1 428.95 9.02 6 -5 1 435.33 8.70 6 5 1 411.57 10.85 6 -5 1 431.23 10.70 6 5 1 413.31 11.06 6 -5 2 43.23 3.12 6 -5 2 36.25 7.31 6 -5 2 39.71 7.32 6 5 2 42.06 2.92 6 -5 2 45.62 2.84 6 5 2 39.75 3.42 6 -5 2 39.99 2.96 6 5 2 38.43 3.40 6 -5 2 41.57 3.36 6 -5 3 179.70 6.08 6 5 3 176.13 6.18 6 -5 3 170.71 5.42 6 5 3 162.76 7.00 6 -5 3 163.69 5.76 6 -5 3 178.03 6.21 6 5 3 176.95 7.27 6 -5 3 170.65 6.54 6 -5 4 120.05 4.80 6 -5 4 109.07 4.55 6 5 4 114.42 5.13 6 5 4 96.99 5.58 6 -5 4 107.10 4.29 6 -5 4 113.95 4.92 6 5 4 111.27 5.93 6 -5 4 108.46 5.12 6 -5 5 7.02 1.22 6 5 5 9.51 1.61 6 -5 5 9.93 1.37 6 -5 5 7.76 1.20 6 -5 5 10.23 1.54 6 5 5 11.22 2.04 6 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4.93 1.33 7 0 -11 141.03 6.59 7 0 -11 155.51 6.83 7 0 -10 613.66 15.05 7 0 -10 659.00 13.98 7 0 -9 585.38 14.63 7 0 -9 610.28 13.01 7 0 -9 623.00 14.12 7 0 -8 43.51 4.00 7 0 -8 43.76 3.46 7 0 -8 44.65 3.86 7 0 -8 26.74 3.11 7 0 -8 37.94 7.29 7 0 -7 48.73 4.20 7 0 -7 45.35 3.48 7 0 -7 41.67 3.68 7 0 -7 46.18 7.43 7 0 -6 3.32 1.13 7 0 -6 3.83 1.43 7 0 -6 3.67 1.35 7 0 -6 2.82 1.40 7 0 -6 2.67 3.35 7 0 -5 132.70 6.71 7 0 -5 123.83 5.46 7 0 -5 107.64 5.37 7 0 -5 124.86 11.11 7 0 -4 30.07 3.21 7 0 -4 28.35 2.71 7 0 -4 24.71 2.55 7 0 -4 28.48 5.64 7 0 -3 14.40 2.26 7 0 -3 13.72 4.12 7 0 -3 12.76 3.63 7 0 -3 9.79 1.57 7 0 -2 7.52 3.02 7 0 -2 6.19 1.58 7 0 -2 7.85 1.23 7 0 -1 23.31 3.18 7 0 -1 22.75 4.25 7 0 -1 20.17 2.40 7 0 -1 22.27 1.91 7 0 0 225.04 10.50 7 0 0 194.90 11.69 7 0 0 226.74 5.49 7 0 0 202.57 5.56 7 0 1 48.90 5.47 7 0 1 34.51 5.25 7 0 1 45.83 2.67 7 0 1 37.21 2.41 7 0 2 56.92 6.24 7 0 2 41.34 5.75 7 0 2 40.07 2.54 7 0 2 58.61 3.16 7 0 2 48.82 2.73 7 0 3 19.98 4.00 7 0 3 21.19 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2.82 7 5 -2 48.33 4.44 7 -5 -2 44.92 2.86 7 -5 -2 49.46 3.49 7 -5 -1 92.17 4.58 7 5 -1 97.22 4.21 7 -5 -1 93.39 3.81 7 5 -1 85.16 5.66 7 -5 -1 80.74 3.78 7 -5 -1 86.89 4.60 7 -5 0 8.19 1.43 7 5 0 7.77 1.86 7 5 0 6.53 1.20 7 -5 0 8.64 1.30 7 -5 0 8.51 1.29 7 -5 0 8.55 1.51 7 -5 1 91.75 4.40 7 5 1 87.92 4.08 7 -5 1 88.18 3.85 7 5 1 91.47 5.54 7 -5 1 80.37 3.82 7 -5 1 92.55 4.77 7 -5 2 110.46 4.67 7 5 2 105.72 4.60 7 -5 2 108.27 4.25 7 5 2 98.40 5.79 7 -5 2 104.75 4.38 7 -5 3 52.77 3.15 7 5 3 58.38 3.58 7 -5 3 59.06 3.13 7 5 3 50.73 4.24 7 -5 3 56.40 3.22 7 5 3 47.96 3.67 7 -5 4 53.14 3.03 7 -5 4 55.01 3.04 7 5 4 57.70 3.72 7 -5 4 52.00 2.92 7 -5 4 56.41 3.20 7 5 4 51.61 3.88 7 -5 4 53.63 3.56 7 -5 5 11.24 1.42 7 -5 5 13.05 1.60 7 5 5 12.25 1.82 7 -5 5 10.68 1.36 7 -5 5 11.39 1.51 7 5 5 7.33 1.61 7 -5 5 10.35 1.59 7 -5 6 19.24 1.64 7 5 6 16.22 2.11 7 -5 6 12.11 1.47 7 -5 6 17.46 1.93 7 -5 6 17.46 1.80 7 5 6 14.94 2.24 7 -5 7 33.81 2.03 7 5 7 31.61 2.85 7 -5 7 30.03 2.16 7 -5 7 33.43 2.44 7 -5 7 37.07 2.51 7 5 7 31.93 3.33 7 5 8 4.67 1.24 7 -5 8 4.72 0.94 7 5 8 4.92 1.57 7 -5 8 4.93 0.98 7 -5 8 4.19 0.89 7 5 9 58.71 3.49 7 -5 9 54.55 2.84 7 -5 9 55.94 2.58 7 -5 9 60.96 2.96 7 5 9 55.31 4.33 7 5 10 5.78 1.09 7 -5 10 6.46 1.03 7 5 10 4.03 1.32 7 -5 10 6.09 0.83 7 -5 10 7.82 1.03 7 -5 11 1.31 0.54 7 5 11 1.13 0.59 7 5 11 0.87 0.87 7 -5 11 1.99 0.58 -7 5 -12 47.57 2.77 7 5 12 55.91 2.76 7 -5 12 58.96 2.49 7 -5 12 61.42 2.36 7 5 12 48.95 3.28 7 5 13 14.69 1.34 7 -5 13 12.87 1.05 7 -5 13 14.84 1.12 7 5 13 11.74 1.49 7 6 -12 1.10 0.69 7 6 -11 3.39 1.15 7 -6 -11 5.75 0.79 7 -6 -10 3.38 0.69 7 -6 -10 3.02 0.66 7 -6 -9 3.24 0.74 7 6 -9 0.97 1.73 7 -6 -9 2.50 0.69 7 -6 -8 2.39 0.70 7 6 -8 1.33 2.08 7 -6 -8 2.91 0.76 7 -6 -7 2.42 0.72 7 6 -7 2.18 2.01 7 -6 -7 2.31 0.74 7 -6 -7 2.37 0.61 7 -6 -6 26.31 2.03 7 6 -6 18.42 3.86 7 -6 -6 21.06 1.59 7 -6 -6 24.54 2.04 7 -6 -5 121.40 3.90 7 -6 -5 134.38 4.84 7 -6 -4 116.85 4.33 7 6 -4 128.25 7.69 7 -6 -3 26.59 2.08 7 6 -3 23.24 3.17 7 -6 -3 23.95 1.91 7 -6 -3 27.99 2.31 7 -6 -2 1.58 0.65 7 6 -2 0.39 0.85 7 -6 -2 1.09 0.54 7 -6 -2 1.08 0.67 7 -6 -2 1.19 0.58 7 -6 -1 17.19 1.68 7 -6 -1 16.23 1.61 7 -6 -1 18.32 1.48 7 6 -1 15.59 2.32 7 -6 -1 17.95 1.74 7 -6 -1 16.84 1.90 7 -6 0 44.05 2.63 7 -6 0 40.07 2.48 7 -6 0 35.46 2.11 7 6 0 40.66 3.61 7 -6 0 39.29 2.49 7 -6 0 40.01 2.85 7 -6 1 40.38 2.49 7 -6 1 35.94 2.27 7 6 1 45.41 2.92 7 -6 1 34.47 2.16 7 6 1 33.53 3.35 7 -6 1 37.99 2.47 7 -6 1 36.66 2.75 7 -6 2 6.44 1.04 7 6 2 4.28 1.46 7 -6 2 6.51 1.05 7 6 2 6.83 1.29 7 -6 2 5.34 0.91 7 -6 2 5.89 1.07 7 -6 2 4.82 1.11 7 -6 3 5.46 0.97 7 6 3 3.19 1.35 7 -6 3 6.34 0.96 7 6 3 5.05 1.27 7 -6 3 5.53 0.92 7 -6 3 4.59 0.94 7 -6 3 6.01 1.16 7 6 4 0.64 1.05 7 -6 4 2.00 0.63 7 -6 4 0.60 0.47 7 6 4 1.22 0.73 7 -6 4 1.53 0.74 7 -6 4 0.84 0.58 7 -6 5 19.57 1.44 7 6 5 21.91 2.32 7 -6 5 16.64 1.51 7 -6 5 15.36 1.59 7 -6 5 17.48 1.67 7 6 6 36.99 2.96 7 -6 6 28.57 1.96 7 6 6 36.58 3.39 7 -6 6 29.76 2.01 7 -6 6 32.77 2.19 7 6 7 27.58 2.45 7 -6 7 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7.72 1.29 8 -2 15 8.18 0.90 8 2 15 7.64 0.96 8 -2 15 7.97 0.84 8 -2 15 7.76 0.97 8 -3 -15 7.56 1.04 8 -3 -15 8.71 1.12 8 3 -15 7.17 1.12 8 -3 -14 1.47 0.74 8 -3 -14 1.62 0.73 8 3 -14 0.54 0.58 8 3 -14 0.97 0.73 8 -3 -14 1.67 0.62 8 -3 -13 19.93 2.02 8 -3 -13 20.68 2.04 8 3 -13 18.82 2.18 8 -3 -13 23.11 1.87 8 -3 -12 28.61 2.56 8 -3 -12 33.36 2.77 8 3 -12 31.93 3.09 8 -3 -12 38.92 2.57 8 -3 -11 10.78 1.72 8 -3 -11 11.68 1.81 8 3 -11 13.83 2.19 8 -3 -11 15.38 1.73 8 -3 -10 10.08 1.70 8 -3 -10 11.98 1.88 8 3 -10 11.66 2.21 8 -3 -10 14.75 1.75 8 -3 -9 2.40 1.08 8 3 -9 1.39 1.09 8 -3 -9 2.18 0.85 8 3 -9 0.33 1.43 8 -3 -8 1.97 1.12 8 -3 -8 0.87 0.78 8 3 -8 1.32 1.16 8 3 -8 0.31 1.86 8 -3 -8 1.49 0.70 8 -3 -8 2.21 0.94 8 -3 -7 7.65 1.69 8 -3 -7 6.15 1.42 8 -3 -7 4.03 1.00 8 -3 -7 6.74 1.33 8 -3 -6 8.42 1.79 8 -3 -6 6.54 1.49 8 -3 -6 4.96 1.04 8 -3 -6 6.70 1.31 8 -3 -5 71.35 4.40 8 -3 -5 68.38 3.39 8 -3 -4 70.49 4.39 8 -3 -4 65.51 3.17 8 -3 -4 74.76 4.03 8 -3 -3 79.62 4.63 8 -3 -3 84.46 4.28 8 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7 31.28 2.07 8 3 7 33.34 2.37 8 3 7 25.94 2.83 8 -3 8 2.60 0.72 8 -3 8 2.47 0.74 8 3 8 2.45 0.96 8 3 8 2.28 1.14 8 -3 8 2.75 0.82 8 -3 8 1.53 0.53 8 3 8 2.61 0.79 8 3 9 70.61 3.94 8 -3 9 61.26 3.08 8 -3 9 70.93 3.27 8 -3 9 67.25 2.91 8 3 9 65.87 4.56 8 3 9 64.74 3.22 8 3 10 21.71 2.11 8 -3 10 18.68 1.67 8 -3 10 20.02 1.64 8 -3 10 18.44 1.52 8 3 10 16.39 2.34 8 3 10 18.34 1.72 8 3 11 36.60 2.59 8 -3 11 32.52 2.10 8 -3 11 36.52 2.02 8 -3 11 33.60 2.00 8 3 11 28.52 2.78 8 3 11 30.41 2.19 -8 3 -12 13.72 1.80 8 3 12 14.19 1.56 8 -3 12 13.81 1.34 8 -3 12 15.17 1.24 8 -3 12 12.93 1.25 8 3 12 12.07 1.74 -8 3 -13 8.93 1.39 8 -3 13 10.05 1.06 8 3 13 8.77 1.16 8 -3 13 9.60 0.93 8 -3 13 7.86 0.99 8 3 13 7.24 1.24 8 -3 14 20.64 1.40 8 3 14 22.92 1.64 8 -3 14 20.87 1.47 8 4 -14 0.17 0.42 8 4 -14 0.55 0.51 8 -4 -13 0.40 0.51 8 4 -13 -0.11 0.57 8 4 -13 0.19 0.57 8 -4 -12 2.08 0.73 8 -4 -12 2.32 0.78 8 4 -12 1.22 0.84 8 -4 -12 2.57 0.75 8 4 -12 0.79 0.77 8 -4 -11 0.47 0.67 8 -4 -11 0.86 0.68 8 4 -11 0.07 0.81 8 -4 -11 0.99 0.56 8 4 -11 0.05 0.74 8 -4 -10 6.79 1.33 8 -4 -10 7.43 1.36 8 -4 -10 9.10 1.30 8 4 -10 4.90 1.62 8 4 -10 2.81 1.54 8 -4 -10 8.13 1.12 8 -4 -9 4.74 1.17 8 -4 -9 4.33 1.12 8 -4 -9 4.60 0.97 8 -4 -9 5.47 1.07 8 -4 -8 23.35 2.36 8 -4 -8 25.44 2.11 8 -4 -8 30.89 2.44 8 -4 -7 12.12 1.75 8 -4 -7 12.01 1.48 8 -4 -7 11.29 1.59 8 -4 -6 11.95 1.77 8 -4 -6 14.16 1.56 8 -4 -6 15.14 1.88 8 -4 -5 24.38 2.43 8 4 -5 18.86 5.08 8 -4 -5 24.62 1.96 8 -4 -5 27.58 2.49 8 -4 -4 16.53 2.02 8 -4 -4 18.51 2.07 8 -4 -3 9.16 1.55 8 -4 -3 12.30 1.68 8 -4 -2 49.74 3.39 8 4 -2 47.28 5.87 8 -4 -2 59.42 2.98 8 -4 -2 52.30 3.38 8 -4 -1 131.00 5.43 8 4 -1 139.65 8.75 8 -4 -1 148.51 4.72 8 -4 -1 138.56 5.48 8 -4 0 40.08 2.99 8 4 0 45.71 2.80 8 -4 0 50.67 2.78 8 -4 0 46.93 2.63 8 -4 0 44.09 3.12 8 -4 1 38.88 2.84 8 4 1 44.79 2.94 8 -4 1 46.37 2.74 8 4 1 33.94 4.34 8 -4 1 41.33 2.47 8 -4 1 38.27 2.90 8 -4 2 17.88 1.89 8 4 2 19.86 2.11 8 -4 2 20.38 1.89 8 -4 2 16.92 1.59 8 -4 3 38.41 2.63 8 -4 3 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4.74 0.83 8 -6 -4 3.27 0.69 8 6 -4 1.57 1.89 8 -6 -4 2.51 0.69 8 -6 -3 5.34 0.84 8 6 -3 1.80 1.70 8 -6 -3 3.89 0.72 8 -6 -3 3.43 0.82 8 -6 -3 2.81 0.57 8 -6 -2 5.84 0.85 8 -6 -2 6.66 1.01 8 -6 -2 5.21 0.76 8 -6 -2 6.54 1.01 8 -6 -1 48.42 2.31 8 6 -1 46.99 4.91 8 -6 -1 43.34 2.16 8 -6 -1 47.66 2.19 8 -6 -1 49.59 2.69 8 -6 0 56.37 2.48 8 -6 0 54.27 2.37 8 -6 0 49.34 1.99 8 6 0 58.53 5.21 8 -6 0 59.13 2.47 8 -6 0 59.42 2.97 8 -6 1 33.32 1.77 8 -6 1 29.53 1.62 8 -6 1 35.98 1.95 8 -6 1 34.55 2.27 8 -6 2 17.01 1.38 8 -6 2 17.57 1.27 8 -6 2 15.15 1.22 8 -6 2 17.71 1.61 8 -6 2 17.63 1.41 8 -6 3 6.40 0.76 8 -6 3 6.47 0.83 8 -6 3 6.90 1.00 8 -6 3 7.22 0.92 8 -6 4 19.74 1.21 8 -6 4 19.07 1.39 8 -6 4 19.55 1.53 8 -6 4 19.89 1.44 8 6 5 7.54 1.35 8 -6 5 5.89 0.79 8 -6 5 5.37 0.79 8 -6 5 6.13 0.81 8 -6 6 23.19 1.47 8 -6 6 24.57 1.43 8 -6 6 26.80 1.54 8 -6 7 2.73 0.53 8 6 7 3.41 0.93 8 -6 7 2.99 0.55 8 -6 7 2.60 0.47 8 -6 8 36.05 1.66 8 -6 8 42.72 1.67 8 -7 -3 9.58 0.86 8 7 -2 1.33 2.20 8 -7 -2 10.84 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40.52 2.69 9 0 12 38.88 2.32 9 0 13 1.36 0.55 9 0 13 0.92 0.44 9 0 13 1.11 0.64 9 0 14 4.23 0.71 9 0 14 4.00 0.69 9 1 -14 13.59 1.49 9 -1 -14 13.30 1.40 9 1 -14 14.70 1.36 9 -1 -14 15.44 1.30 9 1 -13 37.34 2.67 9 -1 -13 29.84 2.28 9 1 -13 31.69 2.13 9 -1 -13 32.40 1.99 9 1 -12 18.29 2.14 9 -1 -12 15.23 1.79 9 1 -12 19.60 1.85 9 -1 -12 17.00 1.55 9 1 -11 49.97 3.59 9 -1 -11 42.10 3.06 9 1 -11 52.36 3.11 9 -1 -11 49.10 2.74 9 1 -10 22.70 2.53 9 -1 -10 20.76 2.28 9 1 -10 21.43 2.11 9 -1 -10 21.76 1.93 9 1 -9 20.54 2.38 9 -1 -9 13.61 1.94 9 1 -9 15.88 1.87 9 -1 -9 16.22 1.71 9 1 -8 0.72 0.91 9 -1 -8 1.38 1.01 9 1 -8 1.04 0.79 9 -1 -8 0.48 0.55 9 -1 -7 0.80 0.94 9 1 -7 0.05 0.69 9 -1 -7 0.16 0.57 9 1 -6 37.39 2.85 9 -1 -6 37.14 2.48 9 -1 -5 27.25 2.81 9 -1 -4 36.48 3.13 9 -1 -3 10.61 1.80 9 -1 -3 9.84 1.35 9 -1 -2 13.28 1.91 9 -1 -2 15.02 1.66 9 -1 -1 18.49 2.16 9 -1 -1 20.08 1.87 9 -1 0 18.87 1.90 9 -1 0 20.69 1.87 9 -1 1 4.56 1.05 9 -1 1 4.37 0.91 9 1 1 3.41 0.90 9 -1 1 5.50 1.01 9 -1 2 28.15 2.16 9 1 2 28.18 2.40 9 -1 2 25.73 2.07 9 -1 2 27.76 2.15 9 1 2 28.80 1.91 9 -1 3 2.94 0.83 9 1 3 3.57 1.09 9 -1 3 3.37 0.84 9 1 3 3.75 0.80 9 1 4 44.60 3.20 9 -1 4 45.85 2.50 9 -1 4 42.04 2.75 9 -1 4 44.55 2.61 9 1 4 44.49 2.34 9 1 5 148.77 5.78 9 -1 5 156.85 4.39 9 -1 5 143.06 5.05 9 -1 5 153.87 4.79 9 1 5 152.90 4.26 9 -1 6 152.95 5.16 9 1 6 149.41 5.72 9 -1 6 159.33 4.80 9 1 6 159.75 4.40 9 -1 6 148.21 4.30 9 -1 7 169.11 5.33 9 1 7 173.96 6.02 9 -1 7 172.26 4.85 9 1 7 169.48 4.54 9 -1 7 158.92 4.46 9 -1 8 35.92 2.42 9 1 8 38.98 2.78 9 -1 8 40.90 2.30 9 1 8 39.03 2.22 9 -1 8 37.56 2.19 9 -1 9 17.84 1.67 9 1 9 19.09 1.92 9 -1 9 18.90 1.54 9 1 9 17.12 1.50 9 -1 9 15.35 1.45 9 -1 10 8.59 1.18 9 1 10 7.30 1.17 9 1 10 8.84 1.10 9 -1 10 9.22 1.12 -9 1 -11 3.64 1.22 9 -1 11 3.96 0.77 9 1 11 4.09 0.89 9 -1 11 3.90 0.71 9 1 11 4.18 0.77 9 -1 11 3.41 0.75 9 1 11 2.19 0.89 -9 1 -12 6.86 1.48 9 -1 12 4.47 0.83 9 1 12 4.63 0.90 9 -1 12 5.53 0.77 9 -1 12 4.60 0.87 9 1 12 4.22 0.77 9 1 12 3.21 0.90 -9 1 -13 6.85 1.19 9 -1 13 8.35 1.00 9 1 13 8.31 1.04 9 -1 13 9.86 0.97 9 1 13 8.57 1.02 9 -1 13 7.98 1.00 9 -1 14 4.83 0.68 9 1 14 3.61 0.69 9 -2 -14 9.65 1.11 9 2 -14 12.55 1.21 9 -2 -14 11.80 1.03 9 -2 -13 26.35 1.96 9 2 -13 30.21 2.08 9 -2 -13 32.04 1.83 9 -2 -12 20.99 1.91 9 2 -12 24.60 2.06 9 -2 -12 26.51 1.82 9 -2 -11 16.25 1.81 9 2 -11 20.00 2.01 9 -2 -11 20.27 1.69 9 -2 -10 8.94 1.51 9 2 -10 8.28 1.56 9 2 -10 12.24 1.64 9 -2 -10 14.00 1.50 9 -2 -9 -0.49 0.70 9 2 -9 0.32 0.74 9 -2 -9 -0.18 0.55 9 -2 -8 17.23 2.07 9 2 -8 17.46 2.11 9 -2 -8 16.38 1.64 9 -2 -7 7.56 1.43 9 -2 -7 7.39 1.13 9 2 -7 6.68 1.40 9 -2 -6 44.33 3.41 9 2 -6 34.78 2.94 9 -2 -6 40.64 2.45 9 -2 -5 35.96 3.11 9 -2 -5 43.58 2.74 9 -2 -4 162.64 6.50 9 -2 -4 166.14 5.51 9 -2 -3 310.67 8.95 9 -2 -3 335.52 7.90 9 -2 -2 88.61 4.73 9 -2 -2 90.70 4.12 9 -2 -1 64.13 3.98 9 -2 -1 63.62 3.45 9 -2 0 25.54 2.48 9 -2 0 29.74 2.47 9 -2 0 24.86 2.15 9 -2 1 20.72 2.12 9 2 1 23.49 2.10 9 -2 1 25.90 2.38 9 -2 1 25.16 1.88 9 -2 1 22.71 2.06 9 -2 2 13.44 1.70 9 2 2 15.53 1.85 9 -2 2 15.93 1.64 9 -2 2 17.52 1.83 9 2 3 14.71 1.95 9 -2 3 13.93 1.53 9 -2 3 13.82 1.58 9 2 4 8.50 1.60 9 -2 4 9.61 1.33 9 -2 4 6.02 1.07 9 2 4 5.96 1.00 9 -2 4 5.98 0.89 9 -2 4 5.44 1.05 9 2 5 43.29 3.37 9 -2 5 43.00 2.43 9 -2 5 33.95 2.38 9 -2 5 35.56 2.39 9 2 5 35.66 2.20 9 -2 5 33.96 1.91 9 2 6 10.37 1.70 9 -2 6 12.40 1.29 9 -2 6 11.04 1.37 9 -2 6 10.48 1.30 9 2 6 10.73 1.25 9 -2 6 10.02 1.07 9 -2 7 0.99 0.61 9 2 7 1.45 0.81 9 2 7 0.96 0.51 9 -2 7 0.83 0.43 9 2 8 119.26 4.97 9 -2 8 110.25 4.00 9 -2 8 119.42 3.89 9 2 8 123.13 3.99 9 -2 8 116.58 3.59 9 -2 9 90.06 3.50 9 2 9 99.53 4.29 9 2 9 95.07 3.52 9 -2 9 88.13 3.15 9 -2 10 59.97 2.80 9 2 10 63.87 3.29 9 2 10 64.83 2.85 9 -2 10 62.47 2.62 -9 2 -11 53.39 3.21 9 -2 11 45.43 2.33 9 2 11 49.79 2.73 9 -2 11 50.21 2.19 9 -2 11 44.12 2.15 9 2 11 47.76 2.43 -9 2 -12 19.86 1.93 9 -2 12 15.50 1.30 9 2 12 18.43 1.59 9 -2 12 16.84 1.22 9 -2 12 15.20 1.26 9 2 12 17.31 1.45 -9 2 -13 17.82 1.69 9 -2 13 16.90 1.27 9 2 13 17.61 1.43 9 -2 13 18.99 1.21 9 -2 13 14.94 1.20 9 -3 -13 8.81 1.01 9 3 -13 8.32 1.03 9 -3 -13 9.77 0.92 9 -3 -12 8.79 1.13 9 3 -12 7.28 1.13 9 -3 -12 8.98 0.99 9 -3 -11 36.12 2.38 9 3 -11 42.81 2.76 9 -3 -11 40.61 2.15 9 -3 -10 0.32 0.55 9 3 -10 0.61 0.72 9 3 -10 0.31 0.66 9 -3 -10 -0.18 0.43 9 -3 -9 15.16 1.74 9 3 -9 17.17 2.09 9 -3 -9 16.62 1.51 9 -3 -8 29.29 2.44 9 3 -8 30.50 2.88 9 -3 -8 31.97 2.07 9 -3 -7 31.59 2.63 9 3 -7 25.44 2.67 9 -3 -7 28.51 1.95 9 -3 -6 37.18 2.87 9 3 -6 32.29 3.06 9 -3 -6 35.36 2.12 9 -3 -5 48.13 3.28 9 -3 -5 51.63 3.08 9 -3 -4 79.29 4.24 9 -3 -4 91.54 4.18 9 -3 -3 65.65 3.91 9 -3 -3 80.10 3.98 9 -3 -2 10.32 1.60 9 -3 -2 12.63 1.62 9 -3 -1 137.68 5.47 9 -3 -1 133.33 5.04 9 -3 0 64.90 3.62 9 -3 0 75.61 4.09 9 -3 0 67.98 3.56 9 -3 1 20.91 2.02 9 -3 1 22.17 2.17 9 3 1 20.96 1.95 9 -3 1 19.64 1.67 9 -3 1 19.37 1.92 9 -3 2 20.76 1.94 9 3 2 20.18 2.04 9 -3 2 18.79 1.73 9 -3 2 18.49 1.88 9 -3 3 29.50 2.16 9 3 3 35.32 2.86 9 -3 3 31.73 2.23 9 -3 3 32.43 2.41 9 -3 3 32.86 1.90 9 -3 4 3.35 0.78 9 -3 4 3.96 0.89 9 3 4 5.25 1.30 9 -3 4 4.16 0.96 9 -3 4 4.27 0.74 9 3 5 22.72 2.47 9 -3 5 25.20 1.90 9 -3 5 19.87 1.75 9 -3 5 20.38 1.84 9 -3 5 18.53 1.40 9 3 6 36.62 3.06 9 -3 6 39.98 2.28 9 -3 6 32.99 2.20 9 -3 6 39.22 2.40 9 -3 6 33.18 1.81 9 3 7 63.41 3.79 9 -3 7 58.79 2.79 9 -3 7 57.65 2.34 9 3 7 56.12 2.88 9 3 8 8.44 1.38 9 -3 8 5.48 0.88 9 -3 8 7.47 1.02 9 -3 8 5.31 0.79 9 3 8 6.16 1.07 9 3 9 4.61 1.00 9 -3 9 4.68 0.79 9 -3 9 5.74 0.82 9 -3 9 4.85 0.73 9 3 9 4.18 0.87 9 3 10 0.35 0.49 9 -3 10 0.50 0.40 9 -3 10 -0.04 0.33 -9 3 -11 5.93 1.15 9 -3 11 5.33 0.77 9 3 11 5.09 0.88 9 -3 11 4.90 0.65 9 -3 11 4.90 0.72 -9 3 -12 23.94 1.91 9 -3 12 18.49 1.29 9 3 12 21.90 1.55 9 -3 12 20.40 1.18 9 -3 12 17.08 1.19 9 -4 -11 0.79 0.44 9 4 -11 0.11 0.50 9 4 -11 0.40 0.60 9 -4 -10 9.27 1.14 9 4 -10 5.85 1.12 9 -4 -9 1.64 0.64 9 4 -9 -0.10 0.75 9 4 -9 0.62 0.72 9 4 -8 21.72 2.35 9 -4 -8 22.85 1.57 9 -4 -7 15.24 1.65 9 4 -7 13.03 2.01 9 -4 -6 41.24 2.67 9 4 -6 16.52 3.86 9 4 -6 29.46 2.89 9 -4 -6 52.95 2.87 9 -4 -5 7.10 1.21 9 -4 -5 7.79 1.22 9 -4 -4 5.20 1.02 9 4 -4 2.42 2.75 9 -4 -4 6.17 1.15 9 -4 -3 4.02 0.98 9 4 -3 1.56 2.89 9 -4 -3 3.89 0.94 9 -4 -2 5.95 1.08 9 -4 -2 7.06 1.18 9 -4 -1 14.76 1.61 9 -4 -1 14.47 1.71 9 -4 -1 14.43 1.66 9 -4 0 4.14 0.95 9 -4 0 2.91 0.85 9 -4 1 3.46 0.86 9 -4 1 4.05 0.99 9 -4 1 3.16 0.78 9 -4 1 2.73 0.81 9 -4 1 3.07 0.70 9 -4 2 28.49 2.03 9 4 2 31.93 2.36 9 -4 2 30.11 2.02 9 -4 2 27.51 2.18 9 -4 2 30.19 1.80 9 -4 3 28.11 1.96 9 4 3 29.65 2.45 9 -4 3 26.02 1.90 9 -4 3 28.15 2.18 9 -4 3 26.86 1.67 9 -4 4 0.32 0.43 9 -4 4 1.60 0.61 9 -4 4 0.37 0.46 9 4 4 1.69 0.88 9 -4 4 0.14 0.44 9 -4 4 0.36 0.38 9 -4 5 49.45 2.40 9 4 5 45.40 3.22 9 -4 5 36.28 2.17 9 -4 5 37.89 2.36 9 -4 5 37.09 1.87 9 -4 6 14.88 1.29 9 4 6 11.42 1.67 9 -4 6 10.31 1.16 9 -4 6 13.26 1.36 9 -4 6 10.95 1.03 9 -4 7 3.98 0.69 9 4 7 5.01 1.12 9 -4 7 5.94 0.92 9 -4 7 5.41 0.73 9 4 8 15.24 1.66 9 -4 8 12.47 1.18 9 -4 8 15.15 1.35 9 -4 8 13.36 1.06 9 4 9 25.36 1.93 9 -4 9 20.63 1.42 9 -4 9 26.77 1.48 9 -4 9 24.27 1.39 9 4 10 21.40 1.61 9 -4 10 20.00 1.14 9 -4 10 18.82 1.21 9 -5 -9 0.18 0.33 9 -5 -8 7.05 0.88 9 5 -8 1.63 0.84 9 -5 -7 3.35 0.66 9 -5 -7 2.40 0.60 9 -5 -6 6.33 0.91 9 -5 -6 7.05 0.94 9 -5 -5 5.63 0.85 9 -5 -5 5.45 0.89 9 -5 -4 25.74 1.74 9 -5 -4 28.29 1.94 9 -5 -3 30.24 1.90 9 -5 -3 32.01 2.01 9 -5 -3 35.63 2.23 9 -5 -2 8.36 1.02 9 -5 -2 8.60 1.10 9 -5 -2 9.87 1.23 9 -5 -1 50.18 2.50 9 -5 -1 51.97 2.73 9 -5 0 32.69 1.90 9 -5 0 37.51 2.11 9 -5 0 31.80 2.18 9 -5 1 3.36 0.69 9 -5 1 2.72 0.57 9 -5 2 6.30 0.88 9 -5 2 4.44 0.74 9 -5 2 6.32 1.02 9 -5 2 5.08 0.70 9 -5 3 3.22 0.65 9 5 3 3.61 1.04 9 -5 3 3.99 0.65 9 -5 3 3.20 0.75 9 -5 4 63.49 2.30 9 -5 4 65.54 2.79 9 -5 4 60.05 2.14 9 5 5 94.66 4.09 9 -5 5 67.20 2.45 9 -5 5 84.53 2.99 9 -5 5 73.08 2.29 9 -5 6 2.10 0.52 9 5 6 2.86 0.87 9 -5 6 2.35 0.55 9 -5 6 2.32 0.46 9 5 7 21.12 1.81 9 -5 7 19.56 1.26 9 -5 7 21.89 1.28 9 -5 7 19.74 1.12 9 -5 8 1.89 0.44 9 5 8 2.30 0.71 9 -6 -4 22.98 1.22 9 -6 -4 17.48 1.14 9 -6 -3 58.55 1.95 9 -6 -3 52.10 1.77 9 -6 -3 53.15 2.05 9 -6 -2 14.55 0.99 9 -6 -2 13.67 0.91 9 -6 -2 11.54 1.00 9 -6 -1 4.01 0.57 9 -6 -1 3.94 0.52 9 -6 0 7.32 0.65 9 -6 0 7.12 0.79 9 -6 1 1.42 0.33 9 -6 1 0.81 0.34 9 -6 2 5.47 0.60 9 -6 2 0.29 0.29 9 -6 3 2.26 0.46 10 0 -11 1.21 0.52 10 0 -10 1.13 0.81 10 0 -10 0.80 0.51 10 0 -9 3.93 1.17 10 0 -9 1.63 0.63 10 0 -8 8.60 1.41 10 0 1 3.35 0.71 10 0 2 148.86 3.89 10 0 3 303.76 6.77 10 0 3 296.36 5.51 10 0 4 66.73 3.32 10 0 4 71.44 2.68 10 0 5 9.56 1.35 10 0 5 11.99 1.15 10 0 6 45.43 2.74 10 0 6 48.99 2.20 10 0 7 25.87 2.03 10 0 7 26.93 1.63 10 0 8 74.03 3.25 10 0 8 76.74 2.68 10 0 9 39.42 2.28 10 0 9 38.90 1.88 10 0 10 10.72 1.16 10 0 10 12.45 1.06 10 0 11 8.23 0.94 10 0 11 6.41 0.80 10 -1 -11 29.19 1.93 10 -1 -10 19.46 1.73 10 1 -10 19.18 1.46 10 -1 -10 17.85 1.28 10 -1 -9 1.02 0.73 10 1 -9 0.38 0.60 10 -1 -9 0.17 0.48 10 -1 -8 20.15 1.96 10 -1 -7 28.71 2.35 10 -1 -6 2.91 1.03 10 -1 -5 31.66 2.38 10 -1 -5 30.26 2.03 10 -1 -4 3.47 0.98 10 -1 -4 2.91 0.80 10 -1 -3 15.36 1.48 10 -1 -2 47.60 2.42 10 -1 -1 12.39 1.30 10 -1 -1 7.62 1.07 10 -1 0 48.92 2.33 10 -1 0 58.00 2.62 10 -1 1 76.16 2.80 10 -1 1 82.96 3.12 10 -1 2 23.23 1.51 10 -1 2 24.49 1.73 10 -1 3 0.84 0.46 10 -1 3 0.49 0.52 10 1 3 1.16 0.78 10 -1 3 0.53 0.44 10 -1 4 39.23 2.43 10 1 4 45.20 2.86 10 -1 4 42.58 2.15 10 1 4 40.21 2.08 10 -1 5 51.77 2.80 10 1 5 59.20 3.31 10 -1 5 63.16 2.54 10 1 5 58.26 2.46 10 -1 6 67.59 3.15 10 1 6 70.37 3.56 10 -1 6 77.15 2.73 10 1 6 74.32 2.75 10 -1 7 61.01 2.91 10 1 7 61.59 3.23 10 -1 7 61.20 2.37 10 1 7 58.73 2.42 10 -1 8 27.12 1.88 10 1 8 28.11 2.09 10 -1 8 28.59 1.59 10 1 8 27.54 1.65 10 -1 9 21.99 1.62 10 1 9 20.41 1.70 10 -1 9 21.13 1.33 10 1 9 20.83 1.43 10 -1 10 4.78 0.74 10 1 10 6.54 0.93 10 -1 10 5.94 0.72 10 1 10 5.65 0.78 10 -1 11 0.78 0.37 10 1 11 1.07 0.47 10 -1 11 1.11 0.41 10 -2 -11 12.09 1.16 10 -2 -10 29.66 1.93 10 -2 -9 3.80 0.83 10 -2 -8 2.07 0.74 10 -2 -7 10.10 1.34 10 -2 -6 22.89 2.06 10 -2 -5 6.14 1.18 10 -2 -4 63.87 3.32 10 -2 -3 81.16 3.62 10 -2 -3 86.40 3.50 10 -2 -2 4.60 1.03 10 -2 -2 5.42 0.96 10 -2 -1 5.92 1.10 10 -2 -1 8.24 1.15 10 -2 -1 8.74 1.16 10 -2 0 50.41 2.57 10 -2 0 58.11 2.74 10 -2 1 24.31 1.73 10 -2 1 27.01 1.86 10 -2 2 18.53 1.53 10 -2 2 14.55 1.40 10 -2 3 11.09 1.28 10 2 3 13.29 1.54 10 -2 3 17.31 1.42 10 -2 3 16.78 1.46 10 -2 4 29.92 2.02 10 2 4 40.70 2.71 10 -2 4 36.21 1.86 10 -2 4 34.50 1.95 10 -2 5 100.22 3.62 10 2 5 109.41 4.43 10 -2 5 105.02 3.29 10 -2 6 2.94 0.71 10 2 6 2.32 0.80 10 -2 6 3.27 0.66 10 -2 7 8.13 1.02 10 2 7 9.07 1.31 10 -2 7 9.09 0.94 10 2 7 5.20 0.86 10 -2 8 0.42 0.40 10 2 8 0.14 0.46 10 -2 8 0.44 0.33 10 2 8 0.12 0.47 10 -2 9 20.78 1.43 10 2 9 21.85 1.68 10 -2 9 22.03 1.29 10 -2 10 11.33 1.01 10 2 10 13.01 1.21 10 -2 10 15.17 1.04 10 -3 -10 9.42 0.94 10 -3 -9 17.46 1.36 10 -3 -8 25.07 1.73 10 -3 -7 15.88 1.46 10 -3 -6 31.14 2.08 10 -3 -5 27.91 2.01 10 -3 -4 1.03 0.63 10 -3 -4 3.08 0.76 10 -3 -4 1.59 0.75 10 -3 -3 43.00 2.45 10 -3 -3 43.57 2.50 10 -3 -3 45.09 2.42 10 -3 -2 52.75 2.71 10 -3 -2 47.83 2.58 10 -3 -2 56.19 2.74 10 -3 -1 21.15 1.68 10 -3 -1 20.64 1.69 10 -3 -1 24.32 1.83 10 -3 0 18.68 1.53 10 -3 0 21.34 1.70 10 -3 0 23.78 1.79 10 -3 1 6.55 0.94 10 -3 1 9.96 1.23 10 -3 2 7.06 0.98 10 -3 2 4.36 0.89 10 -3 3 32.50 1.88 10 -3 3 34.90 1.90 10 -3 3 35.13 1.95 10 -3 4 120.11 3.38 10 3 4 113.90 4.12 10 -3 4 109.15 3.33 10 -3 5 49.96 2.34 10 3 5 54.73 2.93 10 -3 5 50.21 2.21 10 -3 6 4.23 0.73 10 3 6 4.54 0.97 10 -3 6 5.19 0.76 10 -3 7 0.93 0.43 10 3 7 0.72 0.57 10 -3 8 2.72 0.55 10 3 8 3.02 0.74 10 -3 8 3.49 0.56 10 -3 9 5.71 0.70 10 -3 9 6.81 0.70 10 -4 -7 6.13 0.76 10 -4 -7 5.26 0.76 10 -4 -6 15.31 1.18 10 -4 -6 15.96 1.25 10 -4 -5 5.94 0.81 10 -4 -5 7.04 0.92 10 -4 -4 9.19 0.99 10 -4 -4 9.67 1.04 10 -4 -4 8.39 0.97 10 -4 -3 13.87 1.20 10 -4 -3 16.10 1.36 10 -4 -3 15.60 1.32 10 -4 -2 38.72 1.96 10 -4 -2 39.88 2.11 10 -4 -2 44.94 2.24 10 -4 -1 20.41 1.43 10 -4 -1 20.39 1.51 10 -4 -1 22.79 1.62 10 -4 0 8.39 0.93 10 -4 0 11.42 1.12 10 -4 0 10.45 1.12 10 -4 1 26.93 1.62 10 -4 1 23.70 1.61 10 -4 2 14.50 1.15 10 -4 2 14.10 1.21 10 -4 3 4.84 0.70 10 -4 3 3.42 0.64 10 -4 4 12.57 1.04 10 -4 4 11.52 1.02 10 -4 5 4.88 0.71 10 -4 6 6.23 0.70 10 -5 -2 1.94 0.42 10 -5 -1 18.33 1.03 10 -5 0 16.36 0.96 10 -5 0 14.74 1.03 10 -5 1 12.55 0.83 10 -5 1 13.57 0.96 11 -1 3 0.76 0.39 11 -1 4 19.51 1.12 11 -1 5 83.32 2.22 11 -2 0 4.70 0.57 11 -2 1 27.87 1.33 11 -2 2 10.68 0.85 11 -2 3 0.33 0.29 11 -2 4 7.96 0.71 0 0 0 0.00 0.00 TITL 6245 in P2(1)/m REM P2(1)/m (#11 in standard setting) CELL 1.54184 9.508747 7.879312 18.596498 90.0000 91.4065 90.0000 ZERR 6.00 0.000134 0.000117 0.000222 0.0000 0.0011 0.0000 LATT 1 SYMM -x, y+1/2,-z SFAC C H N O UNIT 66.00 60.00 6.00 6.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 9544 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.2968(2) 0.7007(3) 0.27644(10) 0.0403(5) Uani 1 1 d . . . . . O2 O 0.1756(2) 0.8502(3) 0.39827(12) 0.0408(5) Uani 1 1 d . . . . . H2 H 0.123(5) 0.795(8) 0.421(3) 0.068(15) Uiso 1 1 d . . . . . O3 O 0.3646(2) 0.7966(3) 0.52165(11) 0.0395(5) Uani 1 1 d . . . . . H3 H 0.403(6) 0.839(9) 0.561(3) 0.083(16) Uiso 1 1 d . . . . . O4 O 0.6462(2) 0.9398(3) 0.49222(11) 0.0390(5) Uani 1 1 d . . . . . H4 H 0.628(5) 1.056(8) 0.478(3) 0.069(14) Uiso 1 1 d . . . . . O5 O 0.51512(19) 0.7636(3) 0.32067(10) 0.0341(4) Uani 1 1 d . . . . . O6 O 0.7872(2) 0.6734(3) 0.38637(11) 0.0368(5) Uani 1 1 d . . . . . O7 O 1.0394(2) 0.5975(3) 0.46595(11) 0.0374(5) Uani 1 1 d . . . . . H7 H 0.976(5) 0.643(7) 0.497(3) 0.060(12) Uiso 1 1 d . . . . . O8 O 1.1358(2) 0.2579(3) 0.44507(11) 0.0358(5) Uani 1 1 d . . . . . H8A H 1.180(5) 0.325(7) 0.469(3) 0.023(17) Uiso 0.75(18) 1 d . . P A 1 H8B H 1.231(18) 0.277(18) 0.447(7) 0.02(5) Uiso 0.25(18) 1 d . . P A 2 O9 O 1.0867(2) 0.1193(3) 0.30661(12) 0.0420(5) Uani 1 1 d . . . . . H9 H 1.125(5) 0.055(8) 0.335(3) 0.068(14) Uiso 1 1 d . . . . . O10 O 0.8329(2) 0.4660(3) 0.30685(10) 0.0367(5) Uani 1 1 d . . . . . O11 O 0.7299(3) 0.1610(4) 0.25688(13) 0.0571(7) Uani 1 1 d . . . . . H11 H 0.670568 0.131278 0.226691 0.086 Uiso 1 1 calc R U . . . N1 N 0.5340(5) 0.5741(9) 0.1524(3) 0.0933(17) Uani 1 1 d . . . . . C1 C 0.3140(3) 0.7330(5) 0.20168(16) 0.0466(8) Uani 1 1 d . . . . . H1 H 0.328564 0.855094 0.195117 0.056 Uiso 1 1 calc R U . . . C2 C 0.4381(4) 0.6421(7) 0.17470(19) 0.0618(11) Uani 1 1 d . . . . . C3 C 0.1786(4) 0.6828(5) 0.16228(16) 0.0511(8) Uani 1 1 d . . . . . C4 C 0.1690(5) 0.5447(8) 0.1177(2) 0.0718(12) Uani 1 1 d . . . . . H4A H 0.247471 0.477192 0.110143 0.086 Uiso 1 1 calc R U . . . C5 C 0.0402(7) 0.5060(11) 0.0838(3) 0.100(2) Uani 1 1 d . . . . . H5 H 0.034126 0.414921 0.052102 0.120 Uiso 1 1 calc R U . . . C6 C -0.0762(6) 0.6001(12) 0.0968(3) 0.102(2) Uani 1 1 d . . . . . H6 H -0.161353 0.573166 0.073820 0.122 Uiso 1 1 calc R U . . . C7 C -0.0687(6) 0.7353(12) 0.1438(3) 0.102(2) Uani 1 1 d . . . . . H7A H -0.148814 0.798252 0.153392 0.123 Uiso 1 1 calc R U . . . C8 C 0.0591(5) 0.7769(8) 0.1766(3) 0.0787(14) Uani 1 1 d . . . . . H8 H 0.064773 0.868011 0.208285 0.094 Uiso 1 1 calc R U . . . C9 C 0.3711(3) 0.8106(4) 0.32242(14) 0.0337(6) Uani 1 1 d . . . . . H9A H 0.358383 0.928634 0.307037 0.040 Uiso 1 1 calc R U . . . C10 C 0.3147(3) 0.7844(4) 0.39683(14) 0.0324(6) Uani 1 1 d . . . . . H10 H 0.311347 0.662300 0.406685 0.039 Uiso 1 1 calc R U . . . C11 C 0.4068(3) 0.8694(4) 0.45484(13) 0.0309(5) Uani 1 1 d . . . . . H11A H 0.387670 0.991600 0.455135 0.037 Uiso 1 1 calc R U . . . C12 C 0.5625(3) 0.8400(4) 0.44352(13) 0.0306(6) Uani 1 1 d . . . . . H12 H 0.582224 0.720415 0.454208 0.037 Uiso 1 1 calc R U . . . C13 C 0.6020(3) 0.8719(4) 0.36554(14) 0.0320(6) Uani 1 1 d . . . . . H13 H 0.583795 0.990875 0.353125 0.038 Uiso 1 1 calc R U . . . C14 C 0.7532(3) 0.8290(4) 0.35082(16) 0.0374(6) Uani 1 1 d . . . . . H14A H 0.765948 0.817302 0.299469 0.045 Uiso 1 1 calc R U . . . H14B H 0.814531 0.918875 0.368553 0.045 Uiso 1 1 calc R U . . . C15 C 0.8958(3) 0.5790(4) 0.35711(14) 0.0313(6) Uani 1 1 d . . . . . H15 H 0.963289 0.653481 0.333661 0.038 Uiso 1 1 calc R U . . . C16 C 0.9665(3) 0.4823(4) 0.41917(13) 0.0295(5) Uani 1 1 d . . . . . H16 H 0.895390 0.420544 0.446026 0.035 Uiso 1 1 calc R U . . . C17 C 1.0720(3) 0.3582(4) 0.38950(13) 0.0291(5) Uani 1 1 d . . . . . H17 H 1.144804 0.420577 0.364079 0.035 Uiso 1 1 calc R U . . . C18 C 0.9949(3) 0.2393(4) 0.33715(14) 0.0306(5) Uani 1 1 d . . . . . H18 H 0.920655 0.179353 0.362530 0.037 Uiso 1 1 calc R U . . . C19 C 0.9280(3) 0.3466(4) 0.27654(14) 0.0340(6) Uani 1 1 d . . . . . H19 H 1.002073 0.408018 0.251635 0.041 Uiso 1 1 calc R U . . . C20 C 0.8416(3) 0.2456(5) 0.22232(15) 0.0432(7) Uani 1 1 d . . . . . H20A H 0.803373 0.321081 0.185542 0.052 Uiso 1 1 calc R U . . . H20B H 0.901033 0.162950 0.199192 0.052 Uiso 1 1 calc R U . . . O1I O 0.5059(3) 1.0820(5) 0.16354(14) 0.0668(8) Uani 1 1 d . . . . . H1I H 0.449374 1.142610 0.184040 0.100 Uiso 1 1 calc R U . . . C1I C 0.6324(8) 1.062(2) 0.0577(4) 0.149(5) Uani 1 1 d . . . . . H1IA H 0.631339 0.940554 0.058638 0.224 Uiso 1 1 calc R U . . . H1IB H 0.713425 1.103092 0.084227 0.224 Uiso 1 1 calc R U . . . H1IC H 0.636252 1.100743 0.008765 0.224 Uiso 1 1 calc R U . . . C2I C 0.5078(5) 1.1259(10) 0.0895(2) 0.0811(14) Uani 1 1 d . . . . . H2I H 0.512918 1.249950 0.087087 0.097 Uiso 1 1 calc R U . . . C3I C 0.3731(7) 1.0758(14) 0.0538(3) 0.117(3) Uani 1 1 d . . . . . H3IA H 0.370029 0.954650 0.048650 0.175 Uiso 1 1 calc R U . . . H3IB H 0.365657 1.127960 0.007253 0.175 Uiso 1 1 calc R U . . . H3IC H 0.296205 1.112430 0.082556 0.175 Uiso 1 1 calc R U . . . O1W O 0.5385(3) 0.3892(3) 0.34167(13) 0.0495(6) Uani 1 1 d G . . . . H1WA H 0.610764 0.362230 0.318182 0.074 Uiso 1 1 d G U . . . H1WB H 0.534700 0.496771 0.338818 0.074 Uiso 1 1 d G U . . . O2W O 0.3286(4) 0.2644(6) 0.2472(2) 0.0808(10) Uani 1 1 d . . . . . H2WA H 0.369(12) 0.27(2) 0.279(6) 0.17(5) Uiso 1 1 d . . . . . H2WB H 0.251(7) 0.233(10) 0.267(3) 0.085(18) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0428(11) 0.0458(13) 0.0317(9) 0.0004(9) -0.0140(8) -0.0076(9) O2 0.0235(10) 0.0461(13) 0.0522(11) 0.0063(10) -0.0097(8) 0.0035(8) O3 0.0405(10) 0.0460(13) 0.0317(9) -0.0032(9) -0.0055(7) -0.0062(9) O4 0.0352(10) 0.0379(12) 0.0429(10) -0.0064(10) -0.0182(8) -0.0016(8) O5 0.0293(9) 0.0376(11) 0.0349(9) -0.0027(8) -0.0096(7) 0.0017(8) O6 0.0340(10) 0.0345(11) 0.0418(10) 0.0058(9) -0.0013(7) 0.0101(8) O7 0.0309(10) 0.0392(11) 0.0416(10) -0.0093(9) -0.0095(8) -0.0017(8) O8 0.0317(12) 0.0371(12) 0.0379(9) 0.0031(9) -0.0142(8) 0.0025(8) O9 0.0452(11) 0.0387(12) 0.0415(10) -0.0044(10) -0.0084(8) 0.0101(9) O10 0.0294(9) 0.0390(11) 0.0408(9) -0.0036(9) -0.0142(7) 0.0051(8) O11 0.0597(14) 0.0642(17) 0.0464(12) 0.0045(12) -0.0206(10) -0.0249(13) N1 0.068(3) 0.133(5) 0.080(3) -0.029(3) 0.0096(19) -0.001(3) C1 0.0509(18) 0.056(2) 0.0327(13) 0.0026(13) -0.0121(12) -0.0066(15) C2 0.054(2) 0.085(3) 0.0459(17) -0.0093(19) -0.0033(14) -0.010(2) C3 0.0528(19) 0.066(2) 0.0336(13) 0.0036(15) -0.0169(12) -0.0073(16) C4 0.073(3) 0.088(3) 0.054(2) -0.014(2) -0.0123(17) -0.018(2) C5 0.103(4) 0.131(6) 0.065(3) -0.017(3) -0.029(3) -0.044(4) C6 0.076(4) 0.151(6) 0.077(3) 0.020(4) -0.045(3) -0.035(4) C7 0.063(3) 0.138(6) 0.103(4) 0.015(4) -0.041(3) 0.006(3) C8 0.067(3) 0.091(4) 0.076(3) 0.000(3) -0.030(2) 0.012(3) C9 0.0308(13) 0.0327(15) 0.0367(12) 0.0034(11) -0.0135(10) 0.0009(10) C10 0.0266(12) 0.0336(14) 0.0363(12) -0.0008(11) -0.0118(9) 0.0012(10) C11 0.0310(13) 0.0269(13) 0.0345(12) -0.0035(10) -0.0090(9) 0.0009(10) C12 0.0285(13) 0.0279(13) 0.0348(12) -0.0021(11) -0.0128(9) 0.0006(10) C13 0.0308(14) 0.0262(14) 0.0386(13) 0.0015(11) -0.0103(10) 0.0004(10) C14 0.0310(14) 0.0315(15) 0.0494(15) 0.0070(12) -0.0063(11) 0.0019(10) C15 0.0269(12) 0.0300(14) 0.0366(12) 0.0016(11) -0.0056(9) 0.0013(10) C16 0.0240(11) 0.0329(14) 0.0313(11) -0.0010(10) -0.0074(8) -0.0014(10) C17 0.0268(12) 0.0286(13) 0.0317(11) 0.0027(11) -0.0076(9) 0.0001(9) C18 0.0253(12) 0.0326(14) 0.0334(12) -0.0017(11) -0.0066(9) 0.0015(10) C19 0.0325(13) 0.0370(15) 0.0320(12) -0.0004(11) -0.0074(9) 0.0025(11) C20 0.0448(16) 0.0489(18) 0.0351(13) -0.0005(13) -0.0136(11) -0.0020(13) O1I 0.0707(19) 0.082(2) 0.0471(13) -0.0084(14) -0.0151(12) -0.0052(15) C1I 0.118(5) 0.261(15) 0.070(3) -0.024(6) 0.010(3) 0.018(7) C2I 0.086(3) 0.099(4) 0.057(2) 0.005(3) -0.015(2) -0.012(3) C3I 0.111(4) 0.169(8) 0.068(3) 0.006(4) -0.044(3) -0.015(5) O1W 0.0508(13) 0.0490(14) 0.0484(12) 0.0041(11) -0.0047(9) -0.0013(10) O2W 0.065(2) 0.095(3) 0.083(2) -0.008(2) 0.0025(17) -0.0208(19) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C9 O1 C1 114.7(2) . . ? C10 O2 H2 114(4) . . ? C11 O3 H3 117(4) . . ? C12 O4 H4 105(3) . . ? C9 O5 C13 111.9(2) . . ? C15 O6 C14 116.1(2) . . ? C16 O7 H7 108(3) . . ? C17 O8 H8A 104(3) . . ? C17 O8 H8B 110(7) . . ? C18 O9 H9 115(4) . . ? C15 O10 C19 114.46(18) . . ? C20 O11 H11 109.5 . . ? O1 C1 C2 110.8(3) . . ? O1 C1 C3 107.9(3) . . ? C2 C1 C3 112.6(3) . . ? O1 C1 H1 108.5 . . ? C2 C1 H1 108.5 . . ? C3 C1 H1 108.5 . . ? N1 C2 C1 178.4(6) . . ? C4 C3 C8 119.8(4) . . ? C4 C3 C1 122.8(4) . . ? C8 C3 C1 117.2(4) . . ? C3 C4 C5 119.4(6) . . ? C3 C4 H4A 120.3 . . ? C5 C4 H4A 120.3 . . ? C6 C5 C4 120.7(6) . . ? C6 C5 H5 119.7 . . ? C4 C5 H5 119.7 . . ? C5 C6 C7 120.2(4) . . ? C5 C6 H6 119.9 . . ? C7 C6 H6 119.9 . . ? C6 C7 C8 119.5(7) . . ? C6 C7 H7A 120.2 . . ? C8 C7 H7A 120.2 . . ? C7 C8 C3 120.2(6) . . ? C7 C8 H8 119.9 . . ? C3 C8 H8 119.9 . . ? O1 C9 O5 107.4(2) . . ? O1 C9 C10 106.9(2) . . ? O5 C9 C10 110.46(19) . . ? O1 C9 H9A 110.7 . . ? O5 C9 H9A 110.7 . . ? C10 C9 H9A 110.7 . . ? O2 C10 C9 108.6(2) . . ? O2 C10 C11 110.1(2) . . ? C9 C10 C11 112.2(2) . . ? O2 C10 H10 108.6 . . ? C9 C10 H10 108.6 . . ? C11 C10 H10 108.6 . . ? O3 C11 C12 110.7(2) . . ? O3 C11 C10 105.6(2) . . ? C12 C11 C10 112.3(2) . . ? O3 C11 H11A 109.4 . . ? C12 C11 H11A 109.4 . . ? C10 C11 H11A 109.4 . . ? O4 C12 C11 111.0(2) . . ? O4 C12 C13 111.5(2) . . ? C11 C12 C13 111.68(19) . . ? O4 C12 H12 107.5 . . ? C11 C12 H12 107.5 . . ? C13 C12 H12 107.5 . . ? O5 C13 C14 107.3(2) . . ? O5 C13 C12 107.6(2) . . ? C14 C13 C12 113.1(2) . . ? O5 C13 H13 109.6 . . ? C14 C13 H13 109.6 . . ? C12 C13 H13 109.6 . . ? O6 C14 C13 108.3(2) . . ? O6 C14 H14A 110.0 . . ? C13 C14 H14A 110.0 . . ? O6 C14 H14B 110.0 . . ? C13 C14 H14B 110.0 . . ? H14A C14 H14B 108.4 . . ? O6 C15 O10 106.8(2) . . ? O6 C15 C16 106.8(2) . . ? O10 C15 C16 110.9(2) . . ? O6 C15 H15 110.7 . . ? O10 C15 H15 110.7 . . ? C16 C15 H15 110.7 . . ? O7 C16 C17 108.5(2) . . ? O7 C16 C15 110.0(2) . . ? C17 C16 C15 109.3(2) . . ? O7 C16 H16 109.7 . . ? C17 C16 H16 109.7 . . ? C15 C16 H16 109.7 . . ? O8 C17 C16 111.6(2) . . ? O8 C17 C18 108.2(2) . . ? C16 C17 C18 108.5(2) . . ? O8 C17 H17 109.5 . . ? C16 C17 H17 109.5 . . ? C18 C17 H17 109.5 . . ? O9 C18 C17 112.0(2) . . ? O9 C18 C19 108.8(2) . . ? C17 C18 C19 108.3(2) . . ? O9 C18 H18 109.2 . . ? C17 C18 H18 109.2 . . ? C19 C18 H18 109.2 . . ? O10 C19 C20 105.7(2) . . ? O10 C19 C18 109.1(2) . . ? C20 C19 C18 114.1(3) . . ? O10 C19 H19 109.3 . . ? C20 C19 H19 109.3 . . ? C18 C19 H19 109.3 . . ? O11 C20 C19 110.2(2) . . ? O11 C20 H20A 109.6 . . ? C19 C20 H20A 109.6 . . ? O11 C20 H20B 109.6 . . ? C19 C20 H20B 109.6 . . ? H20A C20 H20B 108.1 . . ? C2I O1I H1I 109.5 . . ? C2I C1I H1IA 109.5 . . ? C2I C1I H1IB 109.5 . . ? H1IA C1I H1IB 109.5 . . ? C2I C1I H1IC 109.5 . . ? H1IA C1I H1IC 109.5 . . ? H1IB C1I H1IC 109.5 . . ? O1I C2I C1I 110.3(6) . . ? O1I C2I C3I 109.7(5) . . ? C1I C2I C3I 116.0(7) . . ? O1I C2I H2I 106.8 . . ? C1I C2I H2I 106.8 . . ? C3I C2I H2I 106.8 . . ? C2I C3I H3IA 109.5 . . ? C2I C3I H3IB 109.5 . . ? H3IA C3I H3IB 109.5 . . ? C2I C3I H3IC 109.5 . . ? H3IA C3I H3IC 109.5 . . ? H3IB C3I H3IC 109.5 . . ? H1WA O1W H1WB 104.5 . . ? H2WA O2W H2WB 96(10) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C9 1.396(3) . ? O1 C1 1.427(4) . ? O2 C10 1.422(3) . ? O2 H2 0.79(6) . ? O3 C11 1.434(3) . ? O3 H3 0.88(6) . ? O4 C12 1.427(3) . ? O4 H4 0.96(7) . ? O5 C9 1.420(3) . ? O5 C13 1.439(3) . ? O6 C15 1.393(3) . ? O6 C14 1.426(4) . ? O7 C16 1.425(3) . ? O7 H7 0.92(5) . ? O8 C17 1.425(3) . ? O8 H8A 0.81(6) . ? O8 H8B 0.92(17) . ? O9 C18 1.415(3) . ? O9 H9 0.81(6) . ? O10 C15 1.413(3) . ? O10 C19 1.430(4) . ? O11 C20 1.421(4) . ? O11 H11 0.8200 . ? N1 C2 1.144(7) . ? C1 C2 1.478(6) . ? C1 C3 1.518(4) . ? C1 H1 0.9800 . ? C3 C4 1.369(7) . ? C3 C8 1.388(7) . ? C4 C5 1.397(7) . ? C4 H4A 0.9300 . ? C5 C6 1.359(11) . ? C5 H5 0.9300 . ? C6 C7 1.379(12) . ? C6 H6 0.9300 . ? C7 C8 1.385(7) . ? C7 H7A 0.9300 . ? C8 H8 0.9300 . ? C9 C10 1.510(4) . ? C9 H9A 0.9800 . ? C10 C11 1.527(3) . ? C10 H10 0.9800 . ? C11 C12 1.519(4) . ? C11 H11A 0.9800 . ? C12 C13 1.528(4) . ? C12 H12 0.9800 . ? C13 C14 1.509(4) . ? C13 H13 0.9800 . ? C14 H14A 0.9700 . ? C14 H14B 0.9700 . ? C15 C16 1.526(3) . ? C15 H15 0.9800 . ? C16 C17 1.514(4) . ? C16 H16 0.9800 . ? C17 C18 1.526(3) . ? C17 H17 0.9800 . ? C18 C19 1.534(3) . ? C18 H18 0.9800 . ? C19 C20 1.512(4) . ? C19 H19 0.9800 . ? C20 H20A 0.9700 . ? C20 H20B 0.9700 . ? O1I C2I 1.421(6) . ? O1I H1I 0.8200 . ? C1I C2I 1.428(10) . ? C1I H1IA 0.9600 . ? C1I H1IB 0.9600 . ? C1I H1IC 0.9600 . ? C2I C3I 1.481(7) . ? C2I H2I 0.9800 . ? C3I H3IA 0.9600 . ? C3I H3IB 0.9600 . ? C3I H3IC 0.9600 . ? O1W H1WA 0.8500 . ? O1W H1WB 0.8501 . ? O2W H2WA 0.70(11) . ? O2W H2WB 0.87(7) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C9 O1 C1 C2 87.5(4) . . . . ? C9 O1 C1 C3 -148.7(3) . . . . ? O1 C1 C3 C4 -110.0(4) . . . . ? C2 C1 C3 C4 12.7(5) . . . . ? O1 C1 C3 C8 65.9(5) . . . . ? C2 C1 C3 C8 -171.5(4) . . . . ? C8 C3 C4 C5 3.8(7) . . . . ? C1 C3 C4 C5 179.5(4) . . . . ? C3 C4 C5 C6 -2.5(9) . . . . ? C4 C5 C6 C7 -0.1(10) . . . . ? C5 C6 C7 C8 1.4(11) . . . . ? C6 C7 C8 C3 -0.1(10) . . . . ? C4 C3 C8 C7 -2.5(8) . . . . ? C1 C3 C8 C7 -178.5(5) . . . . ? C1 O1 C9 O5 -74.4(3) . . . . ? C1 O1 C9 C10 167.1(2) . . . . ? C13 O5 C9 O1 178.9(2) . . . . ? C13 O5 C9 C10 -64.9(3) . . . . ? O1 C9 C10 O2 -69.9(3) . . . . ? O5 C9 C10 O2 173.6(2) . . . . ? O1 C9 C10 C11 168.2(2) . . . . ? O5 C9 C10 C11 51.7(3) . . . . ? O2 C10 C11 O3 74.4(3) . . . . ? C9 C10 C11 O3 -164.6(2) . . . . ? O2 C10 C11 C12 -164.9(2) . . . . ? C9 C10 C11 C12 -43.8(3) . . . . ? O3 C11 C12 O4 -70.4(3) . . . . ? C10 C11 C12 O4 171.8(2) . . . . ? O3 C11 C12 C13 164.5(2) . . . . ? C10 C11 C12 C13 46.8(3) . . . . ? C9 O5 C13 C14 -171.3(2) . . . . ? C9 O5 C13 C12 66.6(3) . . . . ? O4 C12 C13 O5 178.7(2) . . . . ? C11 C12 C13 O5 -56.5(3) . . . . ? O4 C12 C13 C14 60.3(3) . . . . ? C11 C12 C13 C14 -174.9(2) . . . . ? C15 O6 C14 C13 154.6(2) . . . . ? O5 C13 C14 O6 -76.3(3) . . . . ? C12 C13 C14 O6 42.2(3) . . . . ? C14 O6 C15 O10 -91.4(3) . . . . ? C14 O6 C15 C16 149.9(2) . . . . ? C19 O10 C15 O6 -174.0(2) . . . . ? C19 O10 C15 C16 -58.1(3) . . . . ? O6 C15 C16 O7 -68.9(3) . . . . ? O10 C15 C16 O7 175.0(2) . . . . ? O6 C15 C16 C17 172.0(2) . . . . ? O10 C15 C16 C17 56.0(3) . . . . ? O7 C16 C17 O8 63.1(3) . . . . ? C15 C16 C17 O8 -176.9(2) . . . . ? O7 C16 C17 C18 -177.8(2) . . . . ? C15 C16 C17 C18 -57.8(3) . . . . ? O8 C17 C18 O9 -59.1(3) . . . . ? C16 C17 C18 O9 179.7(2) . . . . ? O8 C17 C18 C19 -179.1(2) . . . . ? C16 C17 C18 C19 59.7(3) . . . . ? C15 O10 C19 C20 -177.3(2) . . . . ? C15 O10 C19 C18 59.6(3) . . . . ? O9 C18 C19 O10 178.8(2) . . . . ? C17 C18 C19 O10 -59.2(3) . . . . ? O9 C18 C19 C20 60.9(3) . . . . ? C17 C18 C19 C20 -177.1(2) . . . . ? O10 C19 C20 O11 -60.2(3) . . . . ? C18 C19 C20 O11 59.7(3) . . . . ?