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Information card for entry 4519409
Preview
| Coordinates | 4519409.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C24 H48 N6 Si2 |
|---|---|
| Calculated formula | C24 H48 N6 Si2 |
| Title of publication | Disilanes with Pentacoordinate Si Atoms by Carbon Dioxide Insertion into Aminodisilanes: Syntheses, Molecular Structures, and Dynamic Behavior. |
| Authors of publication | Ryll, Christopher; Kraushaar, Konstantin; Wagler, Jörg; Brendler, Erica; Kroke, Edwin |
| Journal of publication | ACS omega |
| Year of publication | 2022 |
| Journal volume | 7 |
| Journal issue | 11 |
| Pages of publication | 9527 - 9536 |
| a | 10.0211 ± 0.0005 Å |
| b | 17.9266 ± 0.0008 Å |
| c | 15.5703 ± 0.0008 Å |
| α | 90° |
| β | 103.901 ± 0.004° |
| γ | 90° |
| Cell volume | 2715.2 ± 0.2 Å3 |
| Cell temperature | 180 ± 2 K |
| Ambient diffraction temperature | 180 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0672 |
| Residual factor for significantly intense reflections | 0.0453 |
| Weighted residual factors for significantly intense reflections | 0.1176 |
| Weighted residual factors for all reflections included in the refinement | 0.1313 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.086 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
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structural data.