Crystallography Open Database

Information card for entry 4519414

4519413 << 4519414 >> 4519415

Preview

Coordinates	4519414.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H48 Cl6 N4 O8 Si2
Calculated formula	C28 H48 Cl6 N4 O8 Si2
Title of publication	Disilanes with Pentacoordinate Si Atoms by Carbon Dioxide Insertion into Aminodisilanes: Syntheses, Molecular Structures, and Dynamic Behavior.
Authors of publication	Ryll, Christopher; Kraushaar, Konstantin; Wagler, Jörg; Brendler, Erica; Kroke, Edwin
Journal of publication	ACS omega
Year of publication	2022
Journal volume	7
Journal issue	11
Pages of publication	9527 - 9536
a	9.3555 ± 0.0006 Å
b	19.1906 ± 0.0008 Å
c	10.8119 ± 0.0006 Å
α	90°
β	91.602 ± 0.005°
γ	90°
Cell volume	1940.38 ± 0.18 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0455
Residual factor for significantly intense reflections	0.0336
Weighted residual factors for significantly intense reflections	0.0826
Weighted residual factors for all reflections included in the refinement	0.0893
Goodness-of-fit parameter for all reflections included in the refinement	1.072
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
274265 (current)	2022-04-03	cif/ Adding structures of 4519408, 4519409, 4519410, 4519411, 4519412, 4519413, 4519414 via cif-deposit CGI script.	4519414.cif