#------------------------------------------------------------------------------ #$Date: 2023-01-04 13:33:26 +0000 (Wed, 04 Jan 2023) $ #$Revision: 280096 $ #$URL: svn://www.crystallography.net/cod/hkl/4/51/94/4519440.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519440 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.7875 _cell_length_b 18.9102 _cell_length_c 5.8053 _exptl_crystal_F_000 366.56 _reflns_d_resolution_high 0.8199 _cod_data_source_file 04-46DBT_54DBF.fcf _cod_data_source_block jw2252 _shelx_title ' jw2252_a.res in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 95.00 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 47.08 51.77 1.74 o 6 0 0 498.35 497.81 15.84 o 8 0 0 0.18 0.28 0.19 o 2 1 0 8311.71 7849.99 396.84 o 4 1 0 159.80 159.29 3.15 o 6 1 0 88.88 73.55 2.08 o 8 1 0 0.90 0.84 0.16 o 0 2 0 5497.59 4290.03 176.61 o 2 2 0 1291.37 1280.39 21.68 o 4 2 0 210.01 215.24 4.16 o 6 2 0 70.72 69.66 1.57 o 8 2 0 17.79 17.29 0.55 o 2 3 0 2265.24 2080.22 33.28 o 4 3 0 127.77 122.41 2.50 o 6 3 0 395.65 337.37 7.13 o 8 3 0 257.53 245.34 5.22 o 0 4 0 874.39 723.12 29.68 o 2 4 0 422.91 397.84 6.49 o 4 4 0 0.62 0.78 0.20 o 6 4 0 348.47 307.04 6.50 o 8 4 0 1.16 1.29 0.23 o 2 5 0 0.21 0.77 0.15 o 4 5 0 24.68 26.04 0.86 o 6 5 0 507.85 450.21 8.80 o 8 5 0 356.34 348.93 7.35 o 0 6 0 2608.19 2781.32 70.31 o 2 6 0 1609.51 1611.59 28.96 o 4 6 0 0.88 0.89 0.23 o 6 6 0 19.20 18.96 0.64 o 8 6 0 6.16 5.36 0.38 o 2 7 0 609.29 641.30 11.67 o 4 7 0 410.75 429.15 8.61 o 6 7 0 468.08 426.50 9.02 o 8 7 0 69.31 73.65 2.20 o 0 8 0 388.17 387.52 9.04 o 2 8 0 388.03 404.89 7.53 o 4 8 0 611.81 632.45 13.57 o 6 8 0 172.09 163.14 3.93 o 8 8 0 37.51 39.14 1.87 o 2 9 0 2124.29 2250.56 40.52 o 4 9 0 669.14 707.22 16.54 o 6 9 0 159.07 151.12 4.13 o 8 9 0 166.75 174.63 4.33 o 0 10 0 77.15 99.70 2.90 o 2 10 0 3.41 6.74 0.43 o 4 10 0 106.07 117.46 3.29 o 6 10 0 2.32 2.81 0.27 o 8 10 0 103.01 112.33 2.70 o 2 11 0 4.12 6.52 0.46 o 4 11 0 430.09 430.21 9.21 o 6 11 0 33.02 31.78 0.99 o 8 11 0 57.01 60.52 1.71 o 0 12 0 759.66 809.46 20.94 o 2 12 0 2.85 2.53 0.39 o 4 12 0 7.28 7.51 0.51 o 6 12 0 100.16 107.40 2.69 o 8 12 0 169.99 173.79 5.24 o 2 13 0 52.23 43.43 1.66 o 4 13 0 624.58 625.27 16.09 o 6 13 0 1.23 1.20 0.27 o 0 14 0 176.12 165.90 5.48 o 2 14 0 285.72 260.25 6.78 o 4 14 0 704.85 650.89 14.92 o 6 14 0 283.09 288.90 6.75 o 2 15 0 404.30 400.36 10.34 o 4 15 0 0.27 0.99 0.27 o 6 15 0 21.65 26.71 0.92 o 0 16 0 172.92 168.74 5.17 o 2 16 0 1040.90 931.36 23.76 o 4 16 0 628.84 602.24 13.84 o 6 16 0 9.68 13.12 0.53 o 2 17 0 84.10 69.45 1.81 o 4 17 0 48.98 46.23 1.26 o 6 17 0 0.72 0.93 0.19 o 0 18 0 45.91 49.00 1.73 o 2 18 0 126.78 115.46 2.84 o 4 18 0 42.29 37.20 1.22 o 2 19 0 40.86 39.54 1.23 o 4 19 0 147.89 134.96 5.04 o 0 20 0 47.86 47.67 1.65 o 2 20 0 7.84 10.03 0.58 o 4 20 0 3.13 3.77 0.26 o 2 21 0 0.06 0.08 0.16 o 0 22 0 232.70 284.55 8.48 o 2 22 0 102.34 106.59 2.82 o 1 0 1 3966.26 3569.75 57.06 o 2 0 1 4880.01 4765.32 76.23 o 3 0 1 4694.76 4906.67 87.81 o 4 0 1 768.97 858.55 15.66 o 5 0 1 198.77 198.21 3.98 o 6 0 1 11.75 12.07 0.55 o 7 0 1 24.89 23.11 0.74 o 8 0 1 57.44 55.54 2.33 o 9 0 1 25.88 24.02 0.79 o 0 1 1 339.80 336.41 5.45 o 1 1 1 4699.05 4261.38 50.77 o 2 1 1 9024.34 8714.59 139.28 o 3 1 1 9.09 9.32 0.38 o 4 1 1 2672.69 2810.18 35.71 o 5 1 1 92.47 92.04 1.46 o 6 1 1 1.32 1.92 0.15 o 7 1 1 7.31 7.69 0.30 o 8 1 1 9.61 11.32 0.47 o 9 1 1 15.78 15.06 0.40 o 1 2 1 38.97 39.24 0.54 o 2 2 1 417.20 424.96 5.66 o 3 2 1 82.08 90.40 1.31 o 4 2 1 136.13 125.49 1.88 o 5 2 1 0.33 0.77 0.22 o 6 2 1 60.16 54.15 0.96 o 7 2 1 0.94 0.86 0.13 o 8 2 1 8.54 7.55 0.38 o 9 2 1 37.48 40.97 0.83 o 0 3 1 1495.33 1422.04 25.51 o 1 3 1 1076.10 1001.17 11.37 o 2 3 1 37.08 29.89 0.47 o 3 3 1 120.65 123.17 1.62 o 4 3 1 1.30 2.15 0.18 o 5 3 1 30.50 33.10 0.78 o 6 3 1 112.68 108.85 1.79 o 7 3 1 6.01 6.20 0.31 o 8 3 1 33.69 34.67 0.70 o 9 3 1 40.82 39.57 0.85 o 1 4 1 5.85 5.42 0.17 o 2 4 1 64.10 56.15 0.79 o 3 4 1 74.39 83.08 1.23 o 4 4 1 1209.49 1180.23 15.65 o 5 4 1 9.49 8.40 0.38 o 6 4 1 180.60 167.61 2.98 o 7 4 1 19.64 19.43 0.48 o 8 4 1 9.47 8.88 0.29 o 9 4 1 0.16 0.56 0.11 o 0 5 1 806.79 762.63 12.99 o 1 5 1 91.46 84.47 1.12 o 2 5 1 0.56 0.93 0.13 o 3 5 1 205.82 218.61 3.06 o 4 5 1 19.82 15.18 0.47 o 5 5 1 336.26 353.23 5.34 o 6 5 1 31.48 29.81 0.61 o 7 5 1 42.73 42.00 0.88 o 8 5 1 91.79 87.18 1.52 o 9 5 1 0.95 0.83 0.10 o 1 6 1 344.17 336.80 4.03 o 2 6 1 231.91 247.66 3.30 o 3 6 1 281.03 295.28 3.95 o 4 6 1 490.94 484.46 6.61 o 5 6 1 10.83 9.31 0.47 o 6 6 1 61.05 60.43 1.09 o 7 6 1 1.37 1.53 0.16 o 8 6 1 97.62 99.47 1.81 o 9 6 1 0.87 0.87 0.12 o 0 7 1 1715.17 1718.84 29.11 o 1 7 1 316.74 334.87 4.26 o 2 7 1 445.85 462.54 5.68 o 3 7 1 140.06 148.82 2.04 o 4 7 1 384.26 377.04 5.63 o 5 7 1 0.20 0.32 0.16 o 6 7 1 65.53 61.79 1.12 o 7 7 1 10.70 11.36 0.40 o 8 7 1 0.18 0.46 0.13 o 1 8 1 174.92 173.17 2.39 o 2 8 1 9.08 12.25 0.36 o 3 8 1 444.08 471.56 6.40 o 4 8 1 560.39 538.66 8.62 o 5 8 1 19.54 18.80 0.56 o 6 8 1 270.98 268.42 4.47 o 7 8 1 5.76 5.52 0.27 o 8 8 1 82.45 83.63 1.62 o 0 9 1 930.12 984.72 17.87 o 1 9 1 1374.21 1507.03 19.82 o 2 9 1 76.14 93.26 1.41 o 3 9 1 17.69 17.66 0.52 o 4 9 1 1.01 1.18 0.27 o 5 9 1 19.09 19.24 0.53 o 6 9 1 38.45 38.60 0.86 o 7 9 1 0.02 0.35 0.16 o 8 9 1 17.18 16.72 0.47 o 1 10 1 75.84 95.24 1.43 o 2 10 1 27.85 30.49 0.70 o 3 10 1 43.73 54.85 1.16 o 4 10 1 171.49 156.24 3.15 o 5 10 1 19.39 19.73 0.59 o 6 10 1 466.07 476.22 8.23 o 7 10 1 2.91 3.12 0.22 o 8 10 1 124.87 130.97 2.32 o 0 11 1 31.34 33.44 0.95 o 1 11 1 138.52 159.89 2.26 o 2 11 1 127.68 137.80 2.34 o 3 11 1 42.33 42.93 1.15 o 4 11 1 2.48 2.69 0.22 o 5 11 1 22.54 22.48 0.58 o 6 11 1 132.90 137.81 2.52 o 7 11 1 68.54 71.62 1.38 o 8 11 1 0.20 0.36 0.11 o 1 12 1 0.19 0.21 0.18 o 2 12 1 338.48 338.41 5.54 o 3 12 1 0.06 -0.02 0.20 o 4 12 1 15.99 15.49 0.58 o 5 12 1 19.31 15.94 0.54 o 6 12 1 135.41 139.87 2.70 o 7 12 1 80.93 85.11 1.58 o 8 12 1 198.65 201.53 10.46 o 0 13 1 68.23 66.56 1.71 o 1 13 1 186.50 171.71 3.04 o 2 13 1 573.09 558.08 9.35 o 3 13 1 1.45 1.49 0.17 o 4 13 1 122.55 120.81 2.74 o 5 13 1 95.11 95.21 1.80 o 6 13 1 57.44 63.41 1.32 o 7 13 1 9.77 11.48 0.37 o 1 14 1 75.47 72.24 1.14 o 2 14 1 2.13 3.22 0.21 o 3 14 1 86.08 85.05 1.46 o 4 14 1 1.80 1.09 0.21 o 5 14 1 19.22 21.45 0.65 o 6 14 1 41.28 43.57 0.95 o 7 14 1 131.84 142.59 2.66 o 0 15 1 1560.99 1473.62 33.49 o 1 15 1 29.12 37.51 0.71 o 2 15 1 434.31 415.44 7.15 o 3 15 1 95.15 87.37 1.57 o 4 15 1 58.57 50.33 1.19 o 5 15 1 60.60 61.24 1.49 o 6 15 1 124.02 125.59 2.58 o 7 15 1 0.11 -0.10 0.13 o 1 16 1 4.60 3.50 0.18 o 2 16 1 142.34 114.10 2.08 o 3 16 1 36.28 37.27 0.73 o 4 16 1 110.63 108.92 2.13 o 5 16 1 163.85 172.80 3.78 o 6 16 1 24.06 25.97 0.78 o 0 17 1 785.21 735.83 15.38 o 1 17 1 9.38 9.50 0.29 o 2 17 1 94.58 82.67 1.48 o 3 17 1 19.36 15.40 0.44 o 4 17 1 16.42 13.82 0.44 o 5 17 1 0.37 0.52 0.17 o 6 17 1 56.67 54.90 1.38 o 1 18 1 0.35 0.78 0.13 o 2 18 1 2.27 2.71 0.18 o 3 18 1 0.80 0.73 0.16 o 4 18 1 56.15 56.62 1.25 o 5 18 1 7.05 5.18 0.26 o 0 19 1 16.18 15.96 0.55 o 1 19 1 68.96 65.04 1.07 o 2 19 1 30.44 26.47 0.65 o 3 19 1 27.66 26.81 0.58 o 4 19 1 23.22 22.84 0.60 o 5 19 1 4.23 5.22 0.30 o 1 20 1 0.04 0.11 0.11 o 2 20 1 41.60 36.39 0.78 o 3 20 1 1.88 1.61 0.15 o 4 20 1 15.33 15.60 0.56 o 0 21 1 42.57 51.50 1.21 o 1 21 1 0.08 -0.01 0.10 o 2 21 1 52.69 57.63 1.14 o 3 21 1 4.81 3.71 0.18 o 1 22 1 10.01 10.60 0.26 o 2 22 1 10.40 11.54 0.33 o 0 0 2 2607.09 2599.18 53.75 o 1 0 2 46.46 47.78 0.84 o 2 0 2 1.28 1.25 0.18 o 3 0 2 1983.57 2120.60 38.06 o 4 0 2 486.65 512.87 11.04 o 5 0 2 290.93 305.73 7.53 o 6 0 2 1118.39 1127.17 28.72 o 7 0 2 12.02 10.05 0.46 o 8 0 2 7.45 8.14 0.43 o 9 0 2 0.29 0.27 0.16 o 1 1 2 135.92 142.17 1.66 o 2 1 2 29.23 28.15 0.43 o 3 1 2 31.36 28.53 0.52 o 4 1 2 1220.45 1264.10 18.78 o 5 1 2 992.94 1013.82 15.88 o 6 1 2 9.37 9.21 0.34 o 7 1 2 382.92 376.55 6.15 o 8 1 2 16.82 14.73 0.39 o 9 1 2 80.97 85.33 2.15 o 0 2 2 1005.46 1006.44 16.25 o 1 2 2 244.66 249.17 3.19 o 2 2 2 591.17 580.52 6.72 o 3 2 2 0.70 1.61 0.15 o 4 2 2 204.27 215.87 3.49 o 5 2 2 51.75 55.99 1.25 o 6 2 2 2.81 2.83 0.21 o 7 2 2 2.95 2.80 0.25 o 8 2 2 71.35 74.13 1.38 o 9 2 2 12.53 12.57 0.34 o 1 3 2 32.75 32.79 0.57 o 2 3 2 314.21 342.66 4.13 o 3 3 2 10.12 13.63 0.35 o 4 3 2 38.87 37.54 0.86 o 5 3 2 1.09 1.05 0.26 o 6 3 2 10.36 9.28 0.37 o 7 3 2 137.10 148.14 2.66 o 8 3 2 130.78 141.80 2.52 o 9 3 2 35.98 36.23 0.79 o 0 4 2 662.78 685.00 11.73 o 1 4 2 903.61 969.97 12.40 o 2 4 2 208.00 202.81 2.46 o 3 4 2 729.11 757.73 8.99 o 4 4 2 154.08 169.04 2.82 o 5 4 2 24.72 23.66 0.97 o 6 4 2 95.77 94.30 1.88 o 7 4 2 4.67 5.89 0.27 o 8 4 2 10.38 11.36 0.37 o 1 5 2 3.86 3.18 0.17 o 2 5 2 1291.79 1393.86 16.77 o 3 5 2 0.17 0.90 0.14 o 4 5 2 173.59 182.41 3.02 o 5 5 2 37.82 33.31 0.94 o 6 5 2 136.53 129.63 2.15 o 7 5 2 42.80 40.86 0.86 o 8 5 2 31.53 33.87 0.74 o 0 6 2 7.08 5.22 0.42 o 1 6 2 776.30 858.23 11.03 o 2 6 2 306.23 291.88 3.67 o 3 6 2 30.77 37.75 0.74 o 4 6 2 185.35 185.38 2.97 o 5 6 2 16.77 16.53 0.47 o 6 6 2 33.89 30.93 0.63 o 7 6 2 26.44 28.90 0.62 o 8 6 2 35.17 34.76 0.71 o 1 7 2 43.26 45.51 0.79 o 2 7 2 35.88 31.70 0.61 o 3 7 2 5.05 4.60 0.31 o 4 7 2 7.66 8.15 0.46 o 5 7 2 22.30 21.06 0.55 o 6 7 2 117.96 116.78 2.07 o 7 7 2 0.68 0.73 0.13 o 8 7 2 27.36 31.78 0.66 o 0 8 2 1455.27 1687.04 30.47 o 1 8 2 242.84 258.82 3.52 o 2 8 2 1187.72 1191.03 15.29 o 3 8 2 255.49 246.78 3.78 o 4 8 2 87.50 84.21 2.68 o 5 8 2 40.33 36.23 0.80 o 6 8 2 9.56 10.57 0.46 o 7 8 2 22.68 23.33 0.69 o 8 8 2 0.56 0.55 0.11 o 1 9 2 87.40 92.76 1.44 o 2 9 2 0.12 2.48 0.32 o 3 9 2 25.93 29.59 0.92 o 4 9 2 0.44 0.67 0.16 o 5 9 2 99.53 98.65 1.86 o 6 9 2 52.84 50.61 0.99 o 7 9 2 17.15 15.81 0.49 o 8 9 2 87.31 93.13 2.05 o 0 10 2 233.43 287.41 5.96 o 1 10 2 210.68 204.76 3.12 o 2 10 2 24.81 27.29 0.87 o 3 10 2 674.62 640.84 10.75 o 4 10 2 11.47 12.49 0.45 o 5 10 2 234.17 214.00 3.80 o 6 10 2 7.08 8.21 0.34 o 7 10 2 0.02 0.01 0.12 o 8 10 2 0.92 0.73 0.12 o 1 11 2 20.03 20.89 0.69 o 2 11 2 0.17 0.63 0.29 o 3 11 2 72.35 59.83 1.17 o 4 11 2 480.92 471.81 8.61 o 5 11 2 4.25 3.49 0.25 o 6 11 2 127.68 130.31 2.38 o 7 11 2 21.96 23.17 0.58 o 0 12 2 641.07 646.33 12.91 o 1 12 2 137.47 138.82 2.64 o 2 12 2 6.67 6.13 0.33 o 3 12 2 53.13 53.55 0.99 o 4 12 2 52.94 51.08 1.07 o 5 12 2 199.86 194.69 3.49 o 6 12 2 47.76 47.03 0.92 o 7 12 2 37.61 41.61 0.82 o 1 13 2 6.55 6.52 0.25 o 2 13 2 235.02 234.46 3.72 o 3 13 2 137.11 130.69 2.28 o 4 13 2 68.34 66.34 1.32 o 5 13 2 112.92 116.62 3.14 o 6 13 2 76.88 79.93 1.60 o 7 13 2 0.12 0.30 0.11 o 0 14 2 1003.29 1021.46 21.20 o 1 14 2 43.18 37.71 0.66 o 2 14 2 278.64 267.05 4.41 o 3 14 2 2.59 2.70 0.22 o 4 14 2 0.28 0.35 0.20 o 5 14 2 7.10 7.77 0.40 o 6 14 2 2.75 3.44 0.30 o 7 14 2 10.35 8.54 0.44 o 1 15 2 160.47 157.35 2.33 o 2 15 2 10.06 7.49 0.27 o 3 15 2 183.15 191.54 3.23 o 4 15 2 2.72 2.20 0.24 o 5 15 2 21.72 24.01 0.79 o 6 15 2 30.33 31.32 0.82 o 0 16 2 0.21 0.23 0.16 o 1 16 2 138.89 114.78 1.74 o 2 16 2 170.54 156.11 2.41 o 3 16 2 18.62 21.97 0.53 o 4 16 2 107.91 108.88 2.47 o 5 16 2 0.08 0.46 0.21 o 6 16 2 0.37 0.75 0.16 o 1 17 2 47.90 43.19 0.81 o 2 17 2 147.28 145.60 2.26 o 3 17 2 85.75 81.26 1.76 o 4 17 2 9.29 9.57 0.41 o 5 17 2 33.86 38.22 1.04 o 0 18 2 21.84 17.18 0.53 o 1 18 2 23.17 26.28 0.51 o 2 18 2 50.99 48.52 1.02 o 3 18 2 6.53 5.65 0.28 o 4 18 2 0.28 0.05 0.12 o 5 18 2 11.30 11.88 0.42 o 1 19 2 3.81 4.62 0.19 o 2 19 2 7.97 8.18 0.30 o 3 19 2 4.13 3.72 0.23 o 4 19 2 0.59 0.27 0.16 o 0 20 2 103.80 95.87 2.51 o 1 20 2 66.80 62.47 1.01 o 2 20 2 24.95 26.48 0.59 o 3 20 2 10.45 9.94 0.32 o 1 21 2 0.73 1.17 0.12 o 2 21 2 15.16 19.51 0.52 o 0 22 2 1.76 2.12 0.22 o 1 0 3 185.76 209.27 3.46 o 2 0 3 210.63 202.60 3.24 o 3 0 3 66.34 69.66 1.78 o 4 0 3 0.10 -0.02 0.41 o 5 0 3 13.52 11.72 0.46 o 6 0 3 534.43 519.77 11.92 o 7 0 3 490.87 496.25 11.37 o 8 0 3 265.19 280.75 8.36 o 0 1 3 12.89 13.31 0.50 o 1 1 3 25.32 38.05 0.59 o 2 1 3 163.04 156.37 1.86 o 3 1 3 17.84 16.42 0.58 o 4 1 3 19.56 19.84 0.88 o 5 1 3 94.70 97.34 1.83 o 6 1 3 109.06 107.94 1.88 o 7 1 3 65.07 61.76 1.12 o 8 1 3 84.88 82.12 1.71 o 1 2 3 24.74 23.84 0.50 o 2 2 3 28.34 29.46 0.59 o 3 2 3 245.51 240.20 3.56 o 4 2 3 1.15 1.28 0.33 o 5 2 3 324.55 322.28 5.30 o 6 2 3 198.27 209.28 3.49 o 7 2 3 103.27 104.34 1.90 o 8 2 3 103.82 104.29 2.27 o 0 3 3 973.72 1074.82 18.43 o 1 3 3 383.47 423.49 5.44 o 2 3 3 38.05 43.67 0.71 o 3 3 3 11.53 9.48 0.41 o 4 3 3 50.80 48.68 1.93 o 5 3 3 200.78 212.21 3.41 o 6 3 3 7.17 6.22 0.28 o 7 3 3 175.18 181.44 3.20 o 8 3 3 2.23 2.20 0.17 o 1 4 3 87.85 112.75 1.73 o 2 4 3 160.45 172.60 2.31 o 3 4 3 5.74 3.38 0.31 o 4 4 3 119.23 111.03 2.84 o 5 4 3 149.09 148.69 2.73 o 6 4 3 59.23 69.53 1.29 o 7 4 3 2.22 2.22 0.18 o 8 4 3 5.07 5.26 0.21 o 0 5 3 630.14 717.78 14.15 o 1 5 3 1303.29 1431.36 18.93 o 2 5 3 10.20 13.43 0.45 o 3 5 3 293.25 281.84 4.30 o 4 5 3 7.14 9.72 0.45 o 5 5 3 43.90 48.96 0.99 o 6 5 3 39.68 40.05 1.05 o 7 5 3 2.29 2.50 0.18 o 8 5 3 3.41 3.65 0.18 o 1 6 3 15.22 11.76 0.45 o 2 6 3 19.09 21.24 0.63 o 3 6 3 0.31 0.16 0.23 o 4 6 3 114.57 105.49 2.12 o 5 6 3 3.48 4.12 0.25 o 6 6 3 10.37 12.97 0.44 o 7 6 3 30.01 30.84 0.71 o 8 6 3 0.21 0.23 0.09 o 0 7 3 698.31 703.32 13.93 o 1 7 3 43.91 47.21 0.97 o 2 7 3 224.38 233.08 3.64 o 3 7 3 146.87 144.62 3.49 o 4 7 3 98.56 92.51 1.68 o 5 7 3 7.79 10.00 0.38 o 6 7 3 47.31 49.14 1.12 o 7 7 3 22.88 23.26 0.72 o 8 7 3 9.76 8.01 0.28 o 1 8 3 33.84 39.87 1.04 o 2 8 3 1.11 1.37 0.28 o 3 8 3 113.42 123.71 2.24 o 4 8 3 3.64 2.09 0.19 o 5 8 3 89.65 99.48 1.87 o 6 8 3 20.38 18.69 0.49 o 7 8 3 2.49 2.35 0.17 o 0 9 3 173.02 154.58 4.56 o 1 9 3 245.92 230.97 3.38 o 2 9 3 280.30 290.85 6.13 o 3 9 3 30.55 24.39 0.65 o 4 9 3 205.33 198.20 3.37 o 5 9 3 62.39 63.79 1.38 o 6 9 3 19.08 20.19 0.53 o 7 9 3 30.61 29.85 0.67 o 1 10 3 21.04 21.64 0.81 o 2 10 3 154.04 151.12 2.41 o 3 10 3 7.33 5.85 0.29 o 4 10 3 1.18 0.50 0.15 o 5 10 3 10.50 11.54 0.39 o 6 10 3 2.32 1.84 0.18 o 7 10 3 0.42 0.31 0.11 o 0 11 3 104.70 92.01 2.11 o 1 11 3 655.15 616.70 8.80 o 2 11 3 70.16 72.90 1.26 o 3 11 3 427.80 422.12 6.97 o 4 11 3 137.84 135.62 2.26 o 5 11 3 31.44 36.65 0.82 o 6 11 3 0.02 0.08 0.12 o 7 11 3 0.01 0.12 0.11 o 1 12 3 86.77 73.33 1.34 o 2 12 3 375.65 342.21 4.79 o 3 12 3 22.49 27.55 0.66 o 4 12 3 3.09 2.69 0.21 o 5 12 3 6.32 5.73 0.27 o 6 12 3 0.98 1.81 0.17 o 7 12 3 36.86 35.93 1.06 o 0 13 3 120.82 119.76 2.68 o 1 13 3 2.70 4.84 0.66 o 2 13 3 25.80 24.79 0.53 o 3 13 3 167.24 167.44 2.88 o 4 13 3 103.25 97.26 2.07 o 5 13 3 25.77 33.28 0.99 o 6 13 3 6.28 7.46 0.26 o 1 14 3 53.74 54.99 1.05 o 2 14 3 132.78 139.80 2.11 o 3 14 3 225.93 248.87 4.15 o 4 14 3 19.40 22.46 0.62 o 5 14 3 143.36 146.06 4.81 o 6 14 3 0.18 0.03 0.11 o 0 15 3 0.36 0.14 0.20 o 1 15 3 0.55 0.35 0.15 o 2 15 3 0.17 0.15 0.13 o 3 15 3 60.28 55.85 1.18 o 4 15 3 30.00 31.15 0.89 o 5 15 3 0.60 0.53 0.15 o 1 16 3 28.90 28.46 0.61 o 2 16 3 16.07 16.93 0.44 o 3 16 3 6.78 7.53 0.30 o 4 16 3 167.49 178.86 3.85 o 5 16 3 107.16 105.49 2.30 o 0 17 3 10.18 10.63 0.47 o 1 17 3 77.00 83.49 1.56 o 2 17 3 14.84 17.54 0.49 o 3 17 3 1.13 2.57 0.19 o 4 17 3 1.20 1.47 0.16 o 1 18 3 15.46 18.94 0.47 o 2 18 3 3.09 2.66 0.16 o 3 18 3 34.94 39.14 0.94 o 4 18 3 68.61 74.26 2.29 o 0 19 3 9.47 10.96 0.60 o 1 19 3 4.83 4.77 0.21 o 2 19 3 2.30 1.44 0.13 o 3 19 3 92.22 99.90 2.15 o 1 20 3 16.57 15.16 0.36 o 2 20 3 1.94 1.85 0.16 o 0 0 4 7.58 5.92 0.61 o 1 0 4 43.14 42.41 1.14 o 2 0 4 114.66 111.49 5.18 o 3 0 4 16.14 19.11 0.64 o 4 0 4 61.71 59.11 2.60 o 5 0 4 53.44 52.92 3.24 o 6 0 4 0.49 0.07 0.17 o 7 0 4 8.12 10.85 0.61 o 1 1 4 4.91 4.69 0.30 o 2 1 4 1.33 1.71 0.30 o 3 1 4 221.87 198.41 3.44 o 4 1 4 195.50 180.64 3.63 o 5 1 4 126.20 120.88 2.72 o 6 1 4 23.45 23.69 0.54 o 7 1 4 1.94 2.00 0.14 o 0 2 4 58.80 63.93 1.54 o 1 2 4 2.15 2.16 0.27 o 2 2 4 60.93 58.16 1.14 o 3 2 4 167.37 154.38 2.80 o 4 2 4 0.94 0.23 0.15 o 5 2 4 140.69 125.92 3.46 o 6 2 4 23.68 23.18 0.71 o 7 2 4 0.13 0.43 0.10 o 1 3 4 254.36 278.45 3.76 o 2 3 4 101.69 104.20 1.72 o 3 3 4 254.88 230.78 3.85 o 4 3 4 65.90 61.89 1.34 o 5 3 4 1.05 0.95 0.19 o 6 3 4 13.44 11.98 0.43 o 7 3 4 14.40 17.63 0.42 o 0 4 4 0.95 0.52 0.37 o 1 4 4 136.77 135.16 2.09 o 2 4 4 55.79 56.97 0.90 o 3 4 4 685.16 679.07 11.02 o 4 4 4 26.12 28.21 0.87 o 5 4 4 124.56 115.99 2.48 o 6 4 4 2.70 3.50 0.22 o 7 4 4 1.47 1.83 0.14 o 1 5 4 40.89 45.62 1.00 o 2 5 4 9.34 9.73 0.26 o 3 5 4 22.51 22.11 0.51 o 4 5 4 103.02 93.56 2.70 o 5 5 4 6.99 6.66 0.38 o 6 5 4 1.91 1.91 0.20 o 7 5 4 15.69 16.40 0.48 o 0 6 4 28.81 29.67 0.87 o 1 6 4 203.13 210.89 2.62 o 2 6 4 190.11 190.14 2.61 o 3 6 4 39.49 47.62 0.92 o 4 6 4 39.97 41.67 1.07 o 5 6 4 2.24 3.33 0.29 o 6 6 4 57.04 48.92 1.14 o 7 6 4 0.29 0.34 0.12 o 1 7 4 0.07 0.05 0.10 o 2 7 4 21.03 22.60 0.46 o 3 7 4 34.39 37.72 0.77 o 4 7 4 29.53 22.86 0.67 o 5 7 4 135.68 127.81 2.71 o 6 7 4 3.54 4.26 0.24 o 7 7 4 57.85 52.13 2.04 o 0 8 4 32.75 29.49 0.87 o 1 8 4 15.06 11.99 0.31 o 2 8 4 56.86 48.11 0.85 o 3 8 4 0.48 0.88 0.17 o 4 8 4 42.91 41.38 1.00 o 5 8 4 7.50 6.53 0.36 o 6 8 4 11.11 12.40 0.44 o 7 8 4 2.26 3.03 0.18 o 1 9 4 12.39 13.90 0.36 o 2 9 4 11.13 12.24 0.36 o 3 9 4 21.09 24.55 0.55 o 4 9 4 0.35 0.80 0.19 o 5 9 4 29.46 28.69 0.78 o 6 9 4 1.69 2.41 0.18 o 0 10 4 438.56 452.96 9.56 o 1 10 4 257.36 261.70 3.57 o 2 10 4 69.13 66.26 1.07 o 3 10 4 98.80 101.51 1.84 o 4 10 4 1.85 1.60 0.19 o 5 10 4 2.73 2.24 0.22 o 6 10 4 7.45 6.99 0.26 o 1 11 4 35.81 30.58 0.59 o 2 11 4 108.29 108.67 1.71 o 3 11 4 8.46 8.43 0.30 o 4 11 4 1.28 0.56 0.15 o 5 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o 6 0 5 4.00 2.23 0.28 o 0 1 5 316.94 311.51 5.76 o 1 1 5 101.22 95.73 1.31 o 2 1 5 41.28 37.18 0.64 o 3 1 5 101.65 92.20 1.46 o 4 1 5 1.31 0.84 0.14 o 5 1 5 9.36 10.10 0.55 o 6 1 5 21.83 27.15 0.76 o 1 2 5 6.72 8.81 0.24 o 2 2 5 122.32 115.20 1.55 o 3 2 5 15.14 13.05 0.35 o 4 2 5 6.03 4.59 0.28 o 5 2 5 15.39 17.40 0.69 o 6 2 5 0.30 0.25 0.13 o 0 3 5 78.06 76.53 1.47 o 1 3 5 549.01 566.72 6.86 o 2 3 5 3.70 3.67 0.17 o 3 3 5 23.25 17.89 0.45 o 4 3 5 31.35 26.00 0.62 o 5 3 5 2.98 3.57 0.27 o 6 3 5 4.31 2.69 0.51 o 1 4 5 31.87 35.90 0.58 o 2 4 5 0.98 0.72 0.11 o 3 4 5 2.61 2.76 0.18 o 4 4 5 1.85 1.61 0.17 o 5 4 5 77.31 71.57 2.09 o 6 4 5 26.85 21.12 0.96 o 0 5 5 92.50 91.57 1.74 o 1 5 5 90.35 99.79 1.36 o 2 5 5 0.81 1.59 0.14 o 3 5 5 12.50 13.64 0.41 o 4 5 5 0.39 0.61 0.16 o 5 5 5 42.99 37.55 1.12 o 6 5 5 17.03 12.74 0.60 o 1 6 5 12.74 12.29 0.30 o 2 6 5 80.61 82.72 1.22 o 3 6 5 109.29 102.15 1.66 o 4 6 5 1.87 1.15 0.19 o 5 6 5 66.44 58.48 2.28 o 6 6 5 11.42 13.94 0.56 o 0 7 5 37.01 38.52 1.01 o 1 7 5 0.26 0.40 0.11 o 2 7 5 7.38 6.01 0.22 o 3 7 5 0.38 0.34 0.15 o 4 7 5 16.22 12.27 0.45 o 5 7 5 1.28 2.93 0.22 o 6 7 5 3.88 2.84 0.19 o 1 8 5 2.81 2.31 0.17 o 2 8 5 5.34 4.39 0.22 o 3 8 5 32.04 27.81 0.60 o 4 8 5 0.18 0.42 0.17 o 5 8 5 48.25 44.40 1.02 o 0 9 5 0.84 0.22 0.19 o 1 9 5 6.34 7.98 0.30 o 2 9 5 12.94 11.64 0.34 o 3 9 5 0.11 0.41 0.18 o 4 9 5 2.58 2.04 0.20 o 5 9 5 0.03 0.05 0.11 o 1 10 5 17.31 18.92 0.46 o 2 10 5 1.47 1.27 0.15 o 3 10 5 70.76 69.99 1.29 o 4 10 5 60.61 61.10 1.25 o 5 10 5 43.17 40.22 1.10 o 0 11 5 38.08 38.56 1.47 o 1 11 5 3.97 5.15 0.21 o 2 11 5 57.26 60.30 1.03 o 3 11 5 104.13 108.43 1.88 o 4 11 5 0.46 0.47 0.14 o 1 12 5 77.81 77.44 1.33 o 2 12 5 15.56 13.45 0.35 o 3 12 5 52.38 50.34 0.93 o 4 12 5 24.66 21.56 0.66 o 0 13 5 1.80 1.96 0.21 o 1 13 5 24.01 33.69 0.64 o 2 13 5 4.95 4.42 0.17 o 3 13 5 136.82 141.13 2.53 o 4 13 5 32.76 31.07 1.21 o 1 14 5 8.30 7.12 0.22 o 2 14 5 0.04 -0.08 0.08 o 3 14 5 9.69 11.34 0.31 o 0 15 5 23.94 20.57 0.54 o 1 15 5 21.60 22.42 0.43 o 2 15 5 34.63 37.92 0.76 o 1 16 5 0.82 0.63 0.10 o 0 0 6 14.09 12.67 0.59 o 1 0 6 122.66 123.85 2.39 o 2 0 6 73.54 73.23 1.60 o 3 0 6 0.33 0.94 0.17 o 4 0 6 57.46 64.52 4.58 o 5 0 6 14.12 15.77 1.08 o 1 1 6 19.77 18.98 0.38 o 2 1 6 34.91 38.86 0.67 o 3 1 6 0.12 0.45 0.12 o 4 1 6 0.10 -0.07 0.19 o 5 1 6 12.20 16.63 0.79 o 0 2 6 40.11 42.30 0.94 o 1 2 6 142.34 143.93 1.89 o 2 2 6 6.11 7.06 0.23 o 3 2 6 27.27 28.82 0.77 o 4 2 6 55.26 60.74 3.06 o 1 3 6 1.00 2.01 0.13 o 2 3 6 88.71 91.57 1.28 o 3 3 6 0.39 0.21 0.11 o 4 3 6 16.75 15.98 0.82 o 0 4 6 13.80 13.81 0.41 o 1 4 6 35.79 39.52 0.59 o 2 4 6 5.56 4.51 0.17 o 3 4 6 60.08 64.30 1.24 o 4 4 6 2.96 3.32 0.21 o 1 5 6 22.08 21.66 0.38 o 2 5 6 4.12 3.54 0.15 o 3 5 6 18.03 19.78 0.48 o 4 5 6 22.36 21.99 0.83 o 0 6 6 130.50 125.11 2.48 o 1 6 6 0.31 0.34 0.10 o 2 6 6 2.54 1.82 0.13 o 3 6 6 1.77 0.48 0.12 o 4 6 6 0.73 0.21 0.12 o 1 7 6 7.83 6.61 0.21 o 2 7 6 11.45 8.13 0.23 o 3 7 6 22.37 23.00 0.52 o 4 7 6 17.12 18.71 0.53 o 0 8 6 30.95 30.49 0.71 o 1 8 6 1.25 1.37 0.12 o 2 8 6 14.66 12.93 0.31 o 3 8 6 1.12 1.59 0.13 o 1 9 6 5.30 5.19 0.20 o 2 9 6 5.37 5.47 0.21 o 3 9 6 20.68 20.66 0.49 o 0 10 6 0.33 0.64 0.15 o 1 10 6 0.12 -0.02 0.11 o 2 10 6 7.02 7.43 0.21 o 1 11 6 0.71 0.52 0.10 o 2 11 6 2.46 2.29 0.15 o 0 12 6 18.40 15.10 0.57 o 1 0 7 19.74 22.13 0.67 o 0 1 7 24.44 27.30 0.60 o 1 1 7 1.75 1.24 0.15 o 1 2 7 14.81 14.16 0.29 o 0 3 7 1.00 1.39 0.15 o