#------------------------------------------------------------------------------ #$Date: 2023-11-01 18:46:33 +0000 (Wed, 01 Nov 2023) $ #$Revision: 287202 $ #$URL: svn://www.crystallography.net/cod/hkl/4/51/94/4519453.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519453 _cell_angle_alpha 107.877 _cell_angle_beta 101.122 _cell_angle_gamma 93.657 _cell_length_a 7.1490 _cell_length_b 10.0023 _cell_length_c 11.5460 _exptl_crystal_F_000 380.00 _reflns_d_resolution_high 0.8152 _cod_data_source_file S07_Pq-Br2_2H2O_P-1.fcf _cod_data_source_block jw23092 _shelx_title ' jw23092_a.res in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 99.76 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 550.93 579.42 17.04 o 5 0 0 0.15 2.25 0.53 o 6 0 0 2069.67 2149.51 31.10 o 7 0 0 30.16 29.85 0.78 o 8 0 0 727.65 724.57 12.27 o -8 1 0 39.27 38.40 0.96 o -7 1 0 830.06 830.51 14.06 o -6 1 0 465.62 488.99 7.93 o -5 1 0 2649.71 2493.72 39.42 o -4 1 0 81.18 89.47 2.29 o -3 1 0 3248.40 3085.22 108.75 o -1 1 0 598.24 646.07 22.82 o 0 1 0 121.43 131.66 3.82 o 2 1 0 1891.83 1529.17 81.55 o 4 1 0 1047.77 1075.65 17.19 o 5 1 0 2390.46 2334.56 36.97 o 6 1 0 343.62 345.68 5.03 o 7 1 0 848.73 900.16 14.15 o 8 1 0 133.61 130.95 2.62 o -8 2 0 426.39 421.67 7.71 o -7 2 0 508.60 529.33 9.63 o -6 2 0 2085.73 2108.54 35.20 o -5 2 0 1501.34 1448.51 22.98 o -4 2 0 3117.55 2929.41 65.43 o -3 2 0 3504.65 3319.61 116.99 o 4 2 0 3449.00 3458.20 57.46 o 5 2 0 2764.62 2760.63 39.86 o 6 2 0 343.45 344.96 5.03 o 7 2 0 856.48 861.37 12.16 o 8 2 0 307.34 308.97 6.53 o -8 3 0 662.56 643.43 11.57 o -7 3 0 143.68 145.65 2.70 o -6 3 0 2269.23 2214.87 39.18 o -5 3 0 453.43 435.32 9.15 o -4 3 0 3170.12 2949.35 85.05 o -3 3 0 960.11 884.26 22.25 o 1 3 0 134.87 159.85 6.83 o 3 3 0 14.70 8.90 0.44 o 4 3 0 874.94 818.87 9.86 o 5 3 0 58.38 72.37 1.13 o 6 3 0 1030.54 989.24 13.93 o 7 3 0 10.50 13.58 0.63 o -8 4 0 6.71 6.75 0.53 o -7 4 0 895.34 884.92 14.95 o -6 4 0 8.88 9.43 0.50 o -5 4 0 2009.77 1862.64 41.71 o -4 4 0 379.37 373.68 9.71 o -3 4 0 7948.56 7076.99 302.03 o -2 4 0 436.29 488.95 12.40 o -1 4 0 3186.42 3093.49 142.56 o 0 4 0 435.52 433.84 10.05 o 2 4 0 166.91 207.14 3.42 o 3 4 0 5923.71 5981.72 280.90 o 4 4 0 16.14 16.50 0.43 o 5 4 0 2730.84 2790.94 40.32 o 6 4 0 59.18 61.35 1.14 o 7 4 0 555.28 570.24 11.10 o -8 5 0 622.13 624.43 14.19 o -7 5 0 91.29 88.21 1.88 o -6 5 0 1086.24 1053.88 21.75 o -5 5 0 467.63 452.44 11.78 o -4 5 0 2436.20 2283.02 57.12 o -3 5 0 130.86 95.16 3.28 o -1 5 0 1686.88 1646.24 47.53 o 0 5 0 3766.71 3715.39 131.07 o 1 5 0 2030.48 2069.29 29.97 o 2 5 0 2897.55 2941.88 39.57 o 3 5 0 1282.70 1285.40 16.42 o 4 5 0 1124.44 1105.90 14.46 o 5 5 0 563.50 568.75 8.86 o 6 5 0 639.86 633.68 10.30 o 7 5 0 125.10 122.27 2.60 o -7 6 0 404.77 393.23 8.31 o -6 6 0 693.50 665.66 12.88 o -5 6 0 739.50 712.58 18.31 o -4 6 0 1825.50 1777.69 37.42 o -3 6 0 1211.20 1147.97 23.64 o -2 6 0 1881.44 1895.20 42.45 o -1 6 0 731.49 685.34 12.54 o 0 6 0 3151.96 3047.43 57.93 o 1 6 0 883.06 900.45 12.39 o 2 6 0 2074.24 2106.97 26.63 o 3 6 0 3.86 4.16 0.24 o 4 6 0 611.99 590.09 7.97 o 5 6 0 184.79 193.23 3.04 o 6 6 0 576.07 564.87 10.96 o -7 7 0 354.44 341.75 8.00 o -6 7 0 35.61 37.40 1.29 o -5 7 0 1315.05 1289.20 29.19 o -4 7 0 198.83 193.69 4.37 o -3 7 0 1518.45 1460.35 30.03 o -2 7 0 117.42 112.05 2.78 o -1 7 0 2713.17 2688.64 43.02 o 0 7 0 340.22 362.03 6.71 o 1 7 0 616.61 621.07 8.74 o 2 7 0 1472.82 1543.52 21.11 o 3 7 0 2354.51 2416.65 33.81 o 4 7 0 84.56 87.76 1.60 o 5 7 0 482.11 495.70 8.33 o 6 7 0 57.33 52.09 1.20 o -6 8 0 613.64 592.66 13.62 o -5 8 0 16.71 16.57 0.90 o -4 8 0 920.13 915.42 19.04 o -3 8 0 153.10 153.57 4.10 o -2 8 0 1613.45 1593.03 28.73 o -1 8 0 99.54 105.86 2.50 o 0 8 0 2950.17 3012.99 50.90 o 1 8 0 1318.28 1402.43 22.92 o 2 8 0 703.64 704.48 10.86 o 3 8 0 319.96 336.03 5.16 o 4 8 0 372.91 362.77 5.93 o 5 8 0 44.52 42.96 1.15 o -6 9 0 59.03 55.41 1.72 o -5 9 0 393.99 366.80 8.64 o -4 9 0 144.53 139.67 3.59 o -3 9 0 514.82 518.35 11.54 o -2 9 0 276.41 291.31 8.69 o -1 9 0 349.74 365.26 7.06 o 0 9 0 71.89 77.39 1.91 o 1 9 0 371.91 395.55 7.91 o 2 9 0 69.46 72.51 1.67 o 3 9 0 432.27 427.02 8.26 o 4 9 0 176.48 154.02 5.05 o -5 10 0 159.19 154.38 5.79 o -4 10 0 129.88 126.11 3.91 o -3 10 0 400.90 409.87 9.30 o -2 10 0 161.17 163.16 4.12 o -1 10 0 326.61 322.55 11.40 o 0 10 0 139.31 140.37 3.13 o 1 10 0 341.99 350.31 7.05 o 2 10 0 62.94 61.59 2.05 o 3 10 0 188.14 182.51 4.15 o -3 11 0 6.46 6.14 0.60 o -2 11 0 302.98 308.84 7.51 o -1 11 0 6.06 6.61 0.81 o 0 11 0 426.88 421.96 9.91 o 1 11 0 3.49 3.55 0.40 o -2 -11 1 47.86 42.14 1.20 o -1 -11 1 1019.88 1013.11 20.99 o 0 -11 1 113.93 116.27 2.89 o 1 -11 1 819.47 854.93 19.64 o 2 -11 1 315.76 310.08 7.54 o 3 -11 1 401.16 448.48 10.64 o 4 -11 1 60.50 63.69 2.38 o -3 -10 1 439.97 415.83 9.86 o -2 -10 1 536.65 540.16 10.61 o -1 -10 1 576.60 573.68 11.23 o 0 -10 1 357.04 365.76 7.96 o 1 -10 1 722.12 747.42 17.29 o 2 -10 1 824.48 810.54 17.38 o 3 -10 1 427.52 444.89 9.92 o 4 -10 1 663.11 637.17 14.82 o 5 -10 1 674.37 621.58 14.36 o -4 -9 1 625.79 592.61 10.77 o -3 -9 1 35.65 34.13 0.91 o -2 -9 1 713.57 723.04 13.09 o -1 -9 1 17.69 19.58 0.84 o 0 -9 1 867.68 885.79 17.09 o 1 -9 1 39.99 39.11 1.26 o 2 -9 1 1338.07 1323.71 30.10 o 3 -9 1 39.76 33.10 1.54 o 4 -9 1 464.73 485.72 10.30 o 5 -9 1 10.85 11.06 0.78 o 6 -9 1 375.49 365.96 8.66 o -5 -8 1 491.81 493.36 9.00 o -4 -8 1 1.59 1.97 0.28 o -3 -8 1 835.71 835.23 12.89 o -2 -8 1 184.07 194.31 3.24 o -1 -8 1 2174.64 2187.14 35.14 o 0 -8 1 15.76 15.63 0.63 o 1 -8 1 1585.01 1580.69 28.42 o 2 -8 1 29.44 23.22 1.02 o 3 -8 1 1231.43 1144.28 23.62 o 4 -8 1 57.32 61.38 1.70 o 5 -8 1 579.12 576.82 13.34 o 6 -8 1 0.19 1.52 0.43 o -6 -7 1 228.33 207.54 6.49 o -5 -7 1 203.40 196.58 3.21 o -4 -7 1 933.03 917.26 12.95 o -3 -7 1 434.79 445.24 6.06 o -2 -7 1 585.56 590.64 8.02 o -1 -7 1 1048.39 1038.17 14.26 o 0 -7 1 1868.71 1868.82 31.73 o 1 -7 1 473.13 478.71 8.37 o 2 -7 1 677.90 668.74 15.25 o 3 -7 1 676.40 675.56 15.41 o 4 -7 1 773.69 737.20 15.39 o 5 -7 1 294.20 282.54 6.17 o 6 -7 1 218.35 212.62 5.17 o 7 -7 1 370.86 356.26 8.85 o -6 -6 1 291.61 288.36 4.73 o -5 -6 1 311.33 307.52 4.67 o -4 -6 1 331.99 338.02 4.76 o -3 -6 1 102.84 105.21 1.70 o -2 -6 1 1275.08 1292.84 16.49 o -1 -6 1 903.90 899.69 12.20 o 0 -6 1 819.72 773.69 13.19 o 1 -6 1 344.58 340.74 6.59 o 2 -6 1 878.38 771.87 22.51 o 3 -6 1 924.73 961.18 24.31 o 4 -6 1 784.35 775.17 19.77 o 5 -6 1 161.84 159.82 4.52 o 6 -6 1 10.68 10.28 0.67 o 7 -6 1 664.75 636.21 14.45 o -7 -5 1 251.23 240.08 6.32 o -6 -5 1 81.45 85.39 1.61 o -5 -5 1 460.10 461.93 7.08 o -4 -5 1 77.55 79.22 1.40 o -3 -5 1 1291.67 1288.21 17.46 o -2 -5 1 111.55 112.88 1.72 o -1 -5 1 1666.67 1715.09 28.70 o 0 -5 1 84.36 80.70 2.51 o 1 -5 1 2847.89 2992.27 85.94 o 2 -5 1 399.81 471.58 13.85 o 3 -5 1 1113.28 1010.70 28.98 o 4 -5 1 0.79 0.86 0.32 o 5 -5 1 1079.98 1078.82 27.37 o 6 -5 1 152.11 153.24 3.84 o 7 -5 1 227.52 228.79 4.60 o 8 -5 1 27.89 25.89 0.88 o -7 -4 1 26.03 27.75 0.81 o -6 -4 1 275.99 273.38 4.64 o -5 -4 1 8.89 10.07 0.43 o -4 -4 1 446.43 444.98 6.36 o -3 -4 1 157.78 155.93 2.35 o -2 -4 1 2148.28 2222.70 80.20 o -1 -4 1 3.31 2.51 0.29 o 0 -4 1 279.82 267.64 7.06 o 1 -4 1 1.83 2.19 0.29 o 2 -4 1 1760.73 1679.24 53.71 o 3 -4 1 37.26 35.12 1.91 o 4 -4 1 479.33 479.64 12.33 o 5 -4 1 24.45 26.63 0.86 o 6 -4 1 156.12 158.09 3.56 o 7 -4 1 16.68 18.23 0.62 o 8 -4 1 50.76 52.74 1.47 o -8 -3 1 67.99 69.31 1.68 o -7 -3 1 255.74 259.55 4.64 o -6 -3 1 12.44 13.97 0.47 o -5 -3 1 334.44 340.36 4.54 o -4 -3 1 829.31 846.71 11.04 o -3 -3 1 1071.05 1029.44 16.36 o -2 -3 1 66.54 75.54 2.02 o -1 -3 1 384.86 419.77 10.82 o 0 -3 1 1823.78 1881.50 66.30 o 1 -3 1 1952.22 1984.43 69.99 o 2 -3 1 703.88 713.84 23.98 o 3 -3 1 161.93 151.73 4.66 o 4 -3 1 77.58 74.87 2.00 o 5 -3 1 96.60 91.95 1.90 o 6 -3 1 2.07 2.61 0.27 o 7 -3 1 169.23 168.36 3.50 o 8 -3 1 14.06 12.87 0.58 o -8 -2 1 50.68 49.50 1.18 o -7 -2 1 72.04 73.87 1.34 o -6 -2 1 5.19 6.38 0.32 o -5 -2 1 151.54 154.04 2.17 o -4 -2 1 331.03 334.65 4.40 o -3 -2 1 275.36 284.41 8.50 o -2 -2 1 14.39 14.18 0.70 o -1 -2 1 1410.49 1422.44 70.93 o 0 -2 1 145.32 149.93 4.41 o 1 -2 1 1440.10 1429.56 40.30 o 2 -2 1 105.17 102.70 3.81 o 3 -2 1 681.17 671.20 25.27 o 4 -2 1 252.42 261.92 4.81 o 5 -2 1 876.73 902.71 15.20 o 6 -2 1 21.32 23.44 0.65 o 7 -2 1 67.63 71.27 1.39 o 8 -2 1 0.02 0.53 0.22 o -8 -1 1 31.74 30.32 0.78 o -7 -1 1 22.94 23.56 0.60 o -6 -1 1 162.66 167.96 2.68 o -5 -1 1 3.06 3.81 0.23 o -4 -1 1 290.96 292.30 5.28 o -3 -1 1 128.94 130.54 4.03 o -2 -1 1 198.05 213.38 8.58 o -1 -1 1 0.32 0.98 0.15 o 0 -1 1 76.41 89.26 3.19 o 1 -1 1 230.25 244.19 8.74 o 2 -1 1 69.67 79.79 6.58 o 3 -1 1 46.65 53.91 2.22 o 4 -1 1 96.16 112.44 2.18 o 5 -1 1 7.70 9.90 0.38 o 6 -1 1 33.78 33.95 0.80 o 7 -1 1 8.23 6.79 0.33 o 8 -1 1 0.93 1.18 0.23 o -8 0 1 0.27 0.11 0.21 o -7 0 1 6.17 5.68 0.30 o -6 0 1 77.54 81.09 1.41 o -5 0 1 32.73 30.49 0.62 o -4 0 1 1.39 2.68 0.31 o -3 0 1 3.62 2.96 0.47 o -2 0 1 1060.22 1069.49 37.80 o -1 0 1 0.70 1.31 0.23 o 0 0 1 3.31 4.79 0.85 o 1 0 1 206.62 215.03 8.64 o 2 0 1 2.65 2.54 0.33 o 3 0 1 20.33 26.10 1.03 o 4 0 1 53.26 55.75 1.06 o 5 0 1 22.78 25.26 0.69 o 6 0 1 1.83 2.70 0.24 o 7 0 1 0.04 0.48 0.18 o 8 0 1 0.13 0.10 0.20 o -8 1 1 0.66 0.76 0.24 o -7 1 1 18.97 19.77 0.57 o -6 1 1 295.94 310.43 4.68 o -5 1 1 0.01 0.59 0.19 o -4 1 1 1.14 2.07 0.37 o -3 1 1 131.59 146.97 4.10 o -2 1 1 976.81 960.49 34.76 o -1 1 1 24.42 28.09 1.60 o 0 1 1 3.03 3.09 0.33 o 1 1 1 51.97 57.58 3.01 o 2 1 1 14.73 17.04 0.84 o 3 1 1 1.74 1.32 0.46 o 4 1 1 38.81 41.90 0.86 o 5 1 1 48.43 48.27 0.92 o 6 1 1 3.37 3.34 0.25 o 7 1 1 0.02 0.57 0.19 o 8 1 1 192.16 180.63 3.94 o -8 2 1 52.13 46.42 1.18 o -7 2 1 114.25 116.22 2.36 o -6 2 1 26.03 27.90 0.85 o -5 2 1 33.62 31.83 0.86 o -4 2 1 10.14 9.28 0.96 o -3 2 1 33.30 39.04 1.44 o -2 2 1 56.84 59.09 1.95 o -1 2 1 22.69 26.06 1.12 o 0 2 1 104.41 111.66 3.65 o 1 2 1 0.74 1.14 0.22 o 2 2 1 394.98 445.93 13.94 o 3 2 1 0.10 0.16 0.15 o 4 2 1 8.99 11.62 0.37 o 5 2 1 4.39 4.41 0.26 o 6 2 1 107.70 109.62 1.70 o 7 2 1 43.91 42.76 0.92 o 8 2 1 55.56 54.74 1.70 o -8 3 1 14.21 13.03 0.63 o -7 3 1 19.98 21.87 0.60 o -6 3 1 13.99 14.09 0.55 o -5 3 1 20.29 18.32 0.71 o -4 3 1 93.98 90.18 4.15 o -3 3 1 173.77 157.38 4.23 o -2 3 1 175.88 184.23 4.80 o -1 3 1 298.44 321.00 11.56 o 0 3 1 111.21 106.71 3.00 o 1 3 1 837.35 883.88 23.04 o 2 3 1 86.51 95.51 2.55 o 3 3 1 163.10 173.63 2.36 o 4 3 1 55.82 55.73 0.92 o 5 3 1 379.76 391.18 5.28 o 6 3 1 12.34 12.97 0.45 o 7 3 1 94.74 94.24 1.72 o -8 4 1 12.55 12.72 0.62 o -7 4 1 66.61 68.58 1.63 o -6 4 1 116.99 123.20 2.68 o -5 4 1 165.35 167.16 4.67 o -4 4 1 490.16 494.28 14.72 o -3 4 1 702.23 703.65 80.90 o -2 4 1 38.41 33.45 1.22 o -1 4 1 245.43 231.19 6.22 o 0 4 1 911.48 970.07 28.88 o 1 4 1 0.99 1.24 0.29 o 2 4 1 227.65 237.59 3.34 o 3 4 1 163.77 159.77 2.21 o 4 4 1 207.30 204.11 2.67 o 5 4 1 20.21 19.91 0.52 o 6 4 1 57.55 57.08 1.08 o 7 4 1 12.54 11.53 0.65 o -8 5 1 25.74 24.45 0.87 o -7 5 1 119.65 119.15 2.42 o -6 5 1 66.56 64.27 1.59 o -5 5 1 10.31 9.09 0.74 o -4 5 1 1.76 4.61 0.47 o -3 5 1 483.96 543.40 13.93 o -2 5 1 603.30 570.95 14.50 o -1 5 1 352.53 367.18 7.97 o 0 5 1 691.08 701.71 11.38 o 1 5 1 407.81 420.23 6.20 o 2 5 1 542.67 558.37 7.10 o 3 5 1 131.94 140.33 2.15 o 4 5 1 429.02 430.55 5.53 o 5 5 1 134.91 135.55 2.25 o 6 5 1 165.05 159.38 3.04 o -7 6 1 133.43 138.10 3.51 o -6 6 1 45.83 49.29 1.57 o -5 6 1 561.16 546.99 17.21 o -4 6 1 4.71 5.09 0.51 o -3 6 1 617.52 613.96 12.82 o -2 6 1 1.21 0.63 0.22 o -1 6 1 1331.91 1278.34 18.86 o 0 6 1 52.12 53.44 0.96 o 1 6 1 734.09 745.69 9.67 o 2 6 1 55.30 55.13 0.97 o 3 6 1 773.25 764.29 10.00 o 4 6 1 36.89 38.26 0.81 o 5 6 1 141.20 143.94 2.39 o 6 6 1 5.50 4.52 0.40 o -7 7 1 0.06 0.21 0.37 o -6 7 1 271.11 261.10 6.28 o -5 7 1 0.81 1.71 0.42 o -4 7 1 338.77 361.76 8.57 o -3 7 1 3.19 4.44 0.59 o -2 7 1 862.58 863.91 15.15 o -1 7 1 0.35 1.03 0.24 o 0 7 1 98.52 104.53 1.99 o 1 7 1 41.45 46.68 0.93 o 2 7 1 1040.40 1052.26 14.05 o 3 7 1 1.63 1.70 0.24 o 4 7 1 277.97 271.87 4.01 o 5 7 1 59.48 59.16 1.24 o -6 8 1 82.99 78.90 2.53 o -5 8 1 480.51 483.86 11.90 o -4 8 1 525.29 525.33 11.53 o -3 8 1 638.06 638.24 11.49 o -2 8 1 233.51 242.13 4.72 o -1 8 1 1797.09 1834.54 31.42 o 0 8 1 1410.01 1489.53 25.69 o 1 8 1 568.73 595.31 10.76 o 2 8 1 428.76 442.48 6.78 o 3 8 1 327.88 323.89 4.90 o 4 8 1 133.00 129.25 2.20 o 5 8 1 132.81 124.22 2.67 o -6 9 1 1.09 2.79 0.47 o -5 9 1 44.38 44.59 2.44 o -4 9 1 118.85 117.31 2.85 o -3 9 1 394.64 392.85 8.95 o -2 9 1 35.72 36.78 1.56 o -1 9 1 222.58 235.03 5.04 o 0 9 1 65.60 68.88 1.63 o 1 9 1 417.82 423.74 7.89 o 2 9 1 231.63 227.22 4.32 o 3 9 1 306.47 297.04 5.98 o 4 9 1 46.18 41.74 1.66 o -5 10 1 22.78 21.10 1.40 o -4 10 1 671.53 663.06 17.24 o -3 10 1 8.08 6.74 0.65 o -2 10 1 422.49 421.52 9.44 o -1 10 1 4.50 4.63 0.56 o 0 10 1 675.72 695.49 13.59 o 1 10 1 17.17 17.32 0.70 o 2 10 1 385.27 380.08 11.91 o -3 11 1 517.01 503.96 13.78 o -2 11 1 9.83 8.61 0.70 o -1 11 1 945.45 955.29 21.80 o 0 11 1 87.98 88.64 2.51 o 0 -12 2 4.55 3.97 0.60 o 1 -12 2 51.60 53.42 1.75 o -2 -11 2 129.79 129.15 3.35 o -1 -11 2 84.73 87.41 2.05 o 0 -11 2 116.31 124.17 3.02 o 1 -11 2 137.40 140.61 3.77 o 2 -11 2 63.01 65.94 2.10 o 3 -11 2 74.09 74.00 2.25 o 4 -11 2 59.13 54.76 1.77 o -4 -10 2 74.46 71.60 1.77 o -3 -10 2 49.51 50.33 1.36 o -2 -10 2 264.34 270.79 5.78 o -1 -10 2 64.73 63.00 1.61 o 0 -10 2 319.04 330.10 6.65 o 1 -10 2 81.61 81.76 2.53 o 2 -10 2 330.00 340.41 8.27 o 3 -10 2 30.74 31.17 1.29 o 4 -10 2 280.66 285.77 6.97 o 5 -10 2 17.43 14.29 0.95 o -5 -9 2 337.30 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o -3 -3 13 169.46 161.47 4.38 o -2 -3 13 792.36 771.80 14.82 o -1 -3 13 262.32 260.85 5.96 o 0 -3 13 470.87 476.51 12.27 o 1 -3 13 120.95 122.29 3.06 o -4 -2 13 452.12 426.80 27.15 o -3 -2 13 102.20 98.02 2.86 o -2 -2 13 804.83 802.54 20.31 o -1 -2 13 205.58 200.66 7.10 o 0 -2 13 439.45 427.17 8.96 o 1 -2 13 191.78 190.88 4.38 o -4 -1 13 10.15 9.37 0.71 o -3 -1 13 492.67 481.16 12.33 o -2 -1 13 66.86 67.39 2.06 o -1 -1 13 397.53 407.26 12.22 o 0 -1 13 3.27 3.11 0.36 o 1 -1 13 386.03 371.77 9.12 o -4 0 13 345.25 345.36 9.43 o -3 0 13 3.04 3.64 0.46 o -2 0 13 458.91 460.30 10.94 o -1 0 13 55.78 53.60 1.75 o 0 0 13 402.12 395.68 10.24 o -2 1 13 108.70 111.02 3.13 o -2 -5 14 26.27 23.44 0.86 o -1 -5 14 0.02 0.54 0.32 o -2 -4 14 1.93 1.34 0.35 o -1 -4 14 0.52 0.10 0.25 o -2 -3 14 11.13 11.19 1.03 o -1 -3 14 0.13 0.31 0.33 o