#------------------------------------------------------------------------------ #$Date: 2023-11-01 19:06:43 +0000 (Wed, 01 Nov 2023) $ #$Revision: 287214 $ #$URL: svn://www.crystallography.net/cod/hkl/4/51/94/4519465.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519465 _cell_angle_alpha 90.000 _cell_angle_beta 109.414 _cell_angle_gamma 90.000 _cell_length_a 9.1539 _cell_length_b 16.0477 _cell_length_c 11.3448 _exptl_crystal_F_000 691.28 _reflns_d_resolution_high 0.7698 _cod_data_source_file S20_Pq-Br_0_49_Cl_1_51_3H2O.fcf _cod_data_source_block jw2299 _shelx_title ' jw2299_a.res in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 139.67 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 345.43 382.64 14.91 o 3 0 0 9.17 9.63 1.53 o 4 0 0 7660.19 7613.37 234.72 o 5 0 0 298.73 330.03 11.78 o 6 0 0 1730.07 1754.65 55.96 o 7 0 0 1009.28 1075.43 30.38 o 8 0 0 16.39 18.05 1.52 o 9 0 0 672.02 692.85 22.56 o 10 0 0 416.62 460.70 15.59 o 11 0 0 246.34 270.44 11.00 o 1 1 0 88.83 88.80 2.95 o 2 1 0 477.71 393.64 9.66 o 3 1 0 1200.56 1226.97 22.14 o 4 1 0 1582.46 1550.61 31.70 o 5 1 0 1550.85 1514.25 34.05 o 6 1 0 2313.74 2329.61 52.03 o 7 1 0 18.59 14.10 1.05 o 8 1 0 1690.68 1754.35 31.99 o 9 1 0 63.62 66.86 1.87 o 10 1 0 111.16 120.10 3.40 o 11 1 0 70.61 75.18 2.67 o 1 2 0 842.21 916.14 21.96 o 2 2 0 1454.19 1401.46 33.62 o 3 2 0 177.08 172.09 4.65 o 4 2 0 647.45 614.87 13.45 o 5 2 0 472.88 481.73 12.92 o 6 2 0 1910.81 1943.90 40.19 o 7 2 0 529.15 502.75 10.30 o 8 2 0 588.32 607.54 11.02 o 9 2 0 4.88 4.70 0.64 o 10 2 0 1035.63 1119.63 27.12 o 11 2 0 16.26 10.99 1.27 o 1 3 0 68.38 70.41 1.83 o 2 3 0 893.77 777.17 21.13 o 3 3 0 649.74 649.09 17.96 o 4 3 0 4785.40 5162.31 112.57 o 5 3 0 316.15 319.64 7.24 o 6 3 0 39.03 44.90 1.74 o 7 3 0 505.19 505.97 9.76 o 8 3 0 15.07 17.76 1.15 o 9 3 0 74.58 79.32 2.36 o 10 3 0 109.39 119.78 3.88 o 11 3 0 37.33 45.29 2.37 o 0 4 0 604.21 834.47 20.16 o 1 4 0 9.96 8.71 0.58 o 2 4 0 12473.93 11604.26 443.51 o 3 4 0 8.50 6.70 0.84 o 4 4 0 5424.13 5487.61 119.40 o 5 4 0 157.53 146.17 2.91 o 6 4 0 4129.07 3979.96 80.75 o 7 4 0 95.78 96.95 2.63 o 8 4 0 1466.29 1431.05 47.46 o 9 4 0 31.28 32.82 1.40 o 10 4 0 360.25 381.77 9.61 o 11 4 0 11.24 12.84 1.59 o 1 5 0 103.50 115.80 3.19 o 2 5 0 132.84 141.31 3.25 o 3 5 0 444.80 467.21 13.89 o 4 5 0 2627.12 2700.75 64.78 o 5 5 0 227.17 204.25 4.08 o 6 5 0 19.93 22.92 1.04 o 7 5 0 184.71 173.65 4.25 o 8 5 0 52.84 54.14 1.93 o 9 5 0 11.46 13.01 0.92 o 10 5 0 4.05 4.64 0.75 o 1 6 0 62.75 61.89 1.59 o 2 6 0 7990.66 7801.07 213.35 o 3 6 0 760.10 782.90 21.63 o 4 6 0 5466.42 5297.49 202.79 o 5 6 0 2.85 4.53 0.43 o 6 6 0 1716.72 1625.90 29.62 o 7 6 0 40.92 38.67 1.31 o 8 6 0 551.91 562.68 11.61 o 9 6 0 226.39 234.95 6.16 o 10 6 0 85.60 81.07 2.56 o 1 7 0 7.11 6.37 0.55 o 2 7 0 75.66 85.27 2.26 o 3 7 0 257.61 251.02 9.73 o 4 7 0 1486.32 1475.33 37.52 o 5 7 0 442.39 417.38 7.85 o 6 7 0 420.13 383.73 7.60 o 7 7 0 8.89 9.39 0.72 o 8 7 0 558.59 547.93 11.30 o 9 7 0 44.36 42.72 2.59 o 10 7 0 7.62 3.88 0.72 o 0 8 0 1075.24 1204.37 32.78 o 1 8 0 391.09 393.08 8.37 o 2 8 0 371.42 402.56 9.19 o 3 8 0 450.09 428.08 13.57 o 4 8 0 750.33 706.99 15.84 o 5 8 0 424.39 418.73 7.91 o 6 8 0 797.87 776.84 14.57 o 7 8 0 125.83 108.78 2.68 o 8 8 0 223.30 243.59 6.00 o 9 8 0 11.85 10.52 0.91 o 10 8 0 450.54 459.90 12.67 o 1 9 0 364.58 368.05 9.72 o 2 9 0 343.77 336.60 8.60 o 3 9 0 456.36 433.57 11.73 o 4 9 0 921.80 881.38 18.17 o 5 9 0 445.75 438.73 8.27 o 6 9 0 747.25 722.65 12.88 o 7 9 0 572.33 506.49 9.31 o 8 9 0 191.92 214.51 5.95 o 9 9 0 129.00 130.55 5.39 o 10 9 0 289.25 329.98 11.51 o 0 10 0 8060.01 8372.49 316.30 o 1 10 0 314.22 326.13 7.21 o 2 10 0 8543.60 8065.10 181.34 o 3 10 0 390.41 366.24 8.54 o 4 10 0 4177.43 4021.14 81.24 o 5 10 0 3.37 3.47 0.44 o 6 10 0 2176.48 1952.44 35.35 o 7 10 0 105.66 94.42 2.31 o 8 10 0 198.15 202.98 7.35 o 9 10 0 123.39 119.19 5.63 o 1 11 0 112.89 114.57 2.47 o 2 11 0 252.06 257.10 4.60 o 3 11 0 125.75 113.11 2.61 o 4 11 0 683.51 641.10 14.61 o 5 11 0 152.06 145.64 3.56 o 6 11 0 559.39 511.88 10.66 o 7 11 0 262.81 268.96 5.91 o 8 11 0 315.39 296.08 10.29 o 9 11 0 52.67 61.40 3.93 o 0 12 0 298.75 240.75 6.86 o 1 12 0 536.94 535.46 9.11 o 2 12 0 18.40 20.27 0.81 o 3 12 0 1599.00 1525.94 26.36 o 4 12 0 1498.94 1445.99 26.42 o 5 12 0 23.45 23.88 1.02 o 6 12 0 889.00 816.91 16.30 o 7 12 0 0.03 0.76 0.63 o 8 12 0 448.09 429.99 15.63 o 9 12 0 0.73 0.94 1.41 o 1 13 0 4.80 5.17 0.43 o 2 13 0 39.35 35.33 1.14 o 3 13 0 305.82 299.06 5.72 o 4 13 0 637.60 631.26 12.05 o 5 13 0 31.06 32.29 1.38 o 6 13 0 75.06 74.53 3.00 o 7 13 0 113.69 121.24 3.98 o 8 13 0 41.63 47.32 2.37 o 0 14 0 144.99 140.25 4.39 o 1 14 0 17.61 17.57 1.39 o 2 14 0 1671.37 1639.38 31.66 o 3 14 0 152.42 145.85 3.07 o 4 14 0 2059.50 2028.58 34.90 o 5 14 0 16.79 17.36 1.21 o 6 14 0 628.19 600.35 12.57 o 7 14 0 1.84 2.51 0.61 o 8 14 0 448.04 447.63 15.14 o 1 15 0 4.75 4.74 0.56 o 2 15 0 184.17 182.93 4.14 o 3 15 0 153.50 150.49 3.72 o 4 15 0 35.85 36.88 1.54 o 5 15 0 6.33 5.05 0.72 o 6 15 0 57.78 61.42 3.86 o 7 15 0 3.86 6.04 0.85 o 0 16 0 800.89 812.96 30.94 o 1 16 0 0.36 0.65 0.44 o 2 16 0 3137.97 3046.48 66.62 o 3 16 0 67.84 67.71 2.63 o 4 16 0 746.15 706.07 15.24 o 5 16 0 15.64 14.91 1.84 o 6 16 0 212.14 201.31 8.80 o 7 16 0 1.90 1.52 0.65 o 1 17 0 133.04 126.36 3.33 o 2 17 0 257.73 257.59 7.00 o 3 17 0 211.62 210.90 7.15 o 4 17 0 140.44 134.63 5.16 o 5 17 0 91.01 87.69 4.18 o 6 17 0 104.23 101.78 3.69 o 0 18 0 71.47 75.74 5.68 o 1 18 0 350.95 346.41 8.37 o 2 18 0 3.98 2.97 1.49 o 3 18 0 162.44 161.52 10.70 o 4 18 0 58.65 68.00 3.44 o 5 18 0 34.55 39.03 2.29 o 1 19 0 16.58 16.54 1.63 o 2 19 0 238.64 234.04 9.86 o 3 19 0 87.24 90.91 6.96 o 4 19 0 341.47 390.03 15.36 o 0 20 0 1384.62 1373.73 52.26 o 1 20 0 134.44 144.89 5.40 o 2 20 0 1091.56 1169.82 44.55 o 3 20 0 16.68 11.59 1.68 o -11 1 1 411.95 427.32 10.59 o -10 1 1 17.25 20.31 1.40 o -9 1 1 457.33 468.97 9.81 o -8 1 1 196.19 203.14 6.38 o -7 1 1 19.98 23.77 1.80 o -6 1 1 67.97 64.93 2.12 o -5 1 1 2919.14 2984.63 57.03 o -4 1 1 68.25 68.71 1.96 o -3 1 1 1386.12 1315.26 26.86 o -2 1 1 1228.94 1170.82 23.82 o -1 1 1 128.39 165.68 5.28 o 0 1 1 220.59 239.95 7.57 o 1 1 1 3736.70 3928.14 104.35 o 2 1 1 853.39 842.91 23.61 o 3 1 1 142.87 128.12 3.77 o 4 1 1 309.03 293.51 7.16 o 5 1 1 1035.18 944.90 15.71 o 6 1 1 1.59 1.57 0.36 o 7 1 1 5179.61 5142.45 91.85 o 8 1 1 46.85 44.95 1.46 o 9 1 1 745.65 765.91 16.13 o 10 1 1 61.08 77.49 2.39 o -11 2 1 1.64 0.84 0.67 o -10 2 1 1.51 0.89 0.59 o -9 2 1 325.43 320.64 6.56 o -8 2 1 1117.23 1194.76 27.36 o -7 2 1 2486.95 2601.35 53.72 o -6 2 1 593.90 606.65 12.45 o -5 2 1 115.59 128.49 3.63 o -4 2 1 137.97 148.70 3.44 o -3 2 1 3987.29 3834.97 91.42 o -2 2 1 1.68 1.03 0.42 o -1 2 1 6173.21 5094.30 270.99 o 0 2 1 10.82 10.24 0.47 o 2 2 1 513.23 495.75 16.19 o 3 2 1 116.49 87.65 3.28 o 4 2 1 30.43 34.13 1.32 o 5 2 1 125.90 107.78 2.44 o 6 2 1 0.96 1.34 0.34 o 7 2 1 104.18 101.87 2.38 o 8 2 1 59.86 61.00 2.17 o 9 2 1 174.27 179.54 4.78 o 10 2 1 132.36 154.58 4.21 o -11 3 1 10.75 7.55 0.80 o -10 3 1 62.79 68.70 2.96 o -9 3 1 337.77 351.66 7.64 o -8 3 1 20.51 23.68 1.05 o -7 3 1 918.07 972.08 22.51 o -6 3 1 855.46 832.14 22.29 o -5 3 1 4243.56 4063.26 107.71 o -4 3 1 24.18 20.19 1.04 o -2 3 1 325.70 345.03 9.61 o -1 3 1 2437.00 2841.54 107.04 o 0 3 1 334.10 370.16 8.65 o 2 3 1 1125.81 1181.12 28.40 o 3 3 1 7115.36 6983.89 217.34 o 4 3 1 73.31 68.38 4.06 o 5 3 1 7169.31 6669.02 118.61 o 6 3 1 3.84 6.17 0.63 o 7 3 1 2077.89 2061.85 37.38 o 8 3 1 59.11 61.54 2.00 o 9 3 1 625.67 663.52 14.34 o 10 3 1 11.61 9.88 0.84 o -11 4 1 419.64 493.51 12.16 o -10 4 1 4.79 5.52 0.99 o -9 4 1 164.35 163.02 5.21 o -8 4 1 445.34 474.72 9.94 o -7 4 1 792.96 801.47 18.71 o -6 4 1 755.11 727.40 12.89 o -5 4 1 301.74 261.95 7.50 o -4 4 1 1090.47 1063.73 30.83 o -3 4 1 689.90 693.84 15.55 o -2 4 1 68.18 70.12 2.19 o -1 4 1 8920.19 8584.72 281.47 o 0 4 1 0.66 1.58 0.33 o 1 4 1 509.44 485.82 11.91 o 2 4 1 358.92 374.36 9.34 o 3 4 1 8662.57 8828.94 234.93 o 4 4 1 21.63 30.72 0.88 o 5 4 1 1637.56 1600.65 27.44 o 6 4 1 929.76 911.56 16.92 o 7 4 1 463.39 476.49 9.92 o 8 4 1 652.84 668.82 13.63 o 9 4 1 192.06 192.71 4.64 o 10 4 1 85.67 92.36 3.88 o -11 5 1 792.93 833.66 20.18 o -10 5 1 78.09 87.16 2.74 o -9 5 1 967.68 977.34 25.35 o -8 5 1 0.07 0.39 0.62 o -7 5 1 876.10 894.47 19.06 o -6 5 1 8.30 7.91 0.54 o -5 5 1 16.11 19.56 0.84 o -4 5 1 159.17 149.57 3.99 o -3 5 1 2662.63 2799.24 69.55 o -2 5 1 1207.69 1287.71 30.96 o -1 5 1 138.63 129.40 3.36 o 0 5 1 3160.51 3252.73 54.87 o 1 5 1 69.00 70.84 1.91 o 2 5 1 1948.83 1985.08 47.65 o 3 5 1 2005.72 2014.66 48.32 o 4 5 1 347.78 318.70 6.74 o 5 5 1 256.41 264.40 4.80 o 6 5 1 105.03 92.60 2.33 o 7 5 1 843.61 805.82 16.17 o 8 5 1 130.04 129.09 3.15 o 9 5 1 959.57 964.27 20.31 o 10 5 1 1.47 1.44 0.62 o -10 6 1 31.14 26.34 1.38 o -9 6 1 152.40 157.11 4.27 o -8 6 1 201.49 214.64 5.37 o -7 6 1 269.46 294.96 6.46 o -6 6 1 463.59 418.83 7.78 o -5 6 1 818.64 652.20 15.13 o -4 6 1 603.37 591.67 14.78 o -3 6 1 2892.06 2960.55 79.20 o -2 6 1 51.01 44.68 1.50 o -1 6 1 2242.87 2199.65 41.70 o 0 6 1 13.50 12.92 0.69 o 1 6 1 157.63 144.80 4.14 o 2 6 1 3.22 1.99 0.42 o 3 6 1 22.33 17.76 0.96 o 4 6 1 405.52 380.49 6.45 o 5 6 1 1491.52 1466.85 25.24 o 6 6 1 478.66 475.64 8.71 o 7 6 1 1435.77 1291.67 25.32 o 8 6 1 251.83 254.24 5.70 o 9 6 1 341.29 331.45 7.46 o 10 6 1 223.97 252.06 6.49 o -10 7 1 7.30 5.42 0.86 o -9 7 1 115.58 121.50 3.46 o -8 7 1 8.88 14.87 1.01 o -7 7 1 320.16 353.71 7.10 o -6 7 1 24.10 21.68 1.05 o -5 7 1 2226.97 1957.11 39.82 o -4 7 1 30.16 26.63 1.42 o -3 7 1 1893.86 1787.86 43.10 o -2 7 1 24.85 28.56 1.36 o -1 7 1 10944.53 10459.28 307.35 o 0 7 1 683.05 713.51 13.07 o 1 7 1 10945.77 11771.45 286.42 o 2 7 1 387.04 384.81 9.62 o 3 7 1 9610.69 9156.94 343.01 o 4 7 1 42.67 41.49 1.13 o 5 7 1 3044.93 2911.27 47.16 o 6 7 1 3.38 2.14 0.73 o 7 7 1 2582.28 2382.09 43.06 o 8 7 1 91.53 84.74 3.04 o 9 7 1 372.08 361.50 8.06 o 10 7 1 178.99 197.17 5.78 o -10 8 1 151.81 176.45 5.20 o -9 8 1 75.08 74.38 3.11 o -8 8 1 0.38 0.18 0.46 o -7 8 1 1.93 0.67 0.42 o -6 8 1 95.59 92.96 2.08 o -5 8 1 675.18 667.74 15.11 o -4 8 1 373.36 357.51 8.78 o -3 8 1 146.62 150.82 6.30 o -2 8 1 33.50 28.13 1.30 o -1 8 1 36.79 43.10 1.47 o 0 8 1 194.81 203.54 4.38 o 1 8 1 269.51 286.87 5.89 o 2 8 1 13.60 14.68 1.38 o 3 8 1 302.08 289.01 6.21 o 4 8 1 587.74 575.50 11.21 o 5 8 1 359.91 349.47 6.15 o 6 8 1 183.94 171.62 3.55 o 7 8 1 122.18 119.79 3.06 o 8 8 1 75.67 71.60 2.11 o 9 8 1 22.46 27.20 1.22 o 10 8 1 27.00 37.45 2.09 o -10 9 1 8.54 8.64 1.14 o -9 9 1 450.44 439.63 13.15 o -8 9 1 21.91 20.90 1.14 o -7 9 1 237.83 268.58 6.31 o -6 9 1 355.99 329.16 6.49 o -5 9 1 952.95 894.74 18.60 o -4 9 1 124.46 126.94 3.12 o -3 9 1 4634.74 4379.59 95.31 o -2 9 1 136.31 141.65 3.28 o -1 9 1 77.95 81.11 2.17 o 0 9 1 296.93 314.09 10.05 o 1 9 1 2472.09 2375.46 45.18 o 2 9 1 12.36 13.12 0.80 o 3 9 1 126.34 137.12 3.21 o 4 9 1 13.92 14.39 0.77 o 5 9 1 1135.84 1034.76 17.22 o 6 9 1 78.61 79.62 1.98 o 7 9 1 855.24 771.35 14.55 o 8 9 1 90.70 88.47 3.66 o 9 9 1 497.46 524.48 18.25 o -10 10 1 32.72 35.15 2.12 o -9 10 1 58.67 50.95 2.16 o -8 10 1 5.77 7.09 0.78 o -7 10 1 1.75 0.55 0.52 o -6 10 1 0.19 0.56 0.46 o -5 10 1 57.56 63.63 2.06 o -4 10 1 74.64 71.02 2.13 o -3 10 1 14.05 17.45 0.84 o -2 10 1 0.16 0.07 0.59 o -1 10 1 2441.77 2573.56 45.97 o 0 10 1 47.04 51.08 1.39 o 1 10 1 180.04 211.70 4.05 o 2 10 1 2.51 2.57 0.42 o 3 10 1 1111.98 1036.35 21.26 o 4 10 1 73.19 68.29 1.73 o 5 10 1 301.93 287.48 5.21 o 6 10 1 64.42 54.87 1.62 o 7 10 1 30.08 24.64 1.03 o 8 10 1 52.18 51.98 1.86 o 9 10 1 26.28 28.51 1.43 o -9 11 1 815.21 839.29 23.83 o -8 11 1 1.03 0.88 0.59 o -7 11 1 608.06 600.40 12.31 o -6 11 1 31.38 27.02 1.17 o -5 11 1 248.58 259.40 5.86 o -4 11 1 66.22 59.25 1.92 o -3 11 1 5.11 6.44 0.62 o -2 11 1 154.20 158.31 4.43 o -1 11 1 55.29 47.97 1.49 o 0 11 1 413.17 391.45 7.45 o 1 11 1 1251.41 1302.89 23.64 o 2 11 1 363.01 350.97 6.48 o 3 11 1 266.86 262.37 5.34 o 4 11 1 86.91 84.64 1.96 o 5 11 1 251.74 247.79 4.85 o 6 11 1 120.51 109.55 2.84 o 7 11 1 303.24 300.64 6.67 o 8 11 1 18.03 16.15 1.05 o 9 11 1 407.71 428.98 17.68 o -9 12 1 209.77 199.87 7.36 o -8 12 1 106.43 100.75 3.29 o -7 12 1 186.28 176.51 4.16 o -6 12 1 269.59 248.83 5.72 o -5 12 1 229.11 211.98 4.92 o -4 12 1 36.60 33.40 1.72 o -3 12 1 2236.31 2163.90 50.59 o -2 12 1 2.86 2.84 0.49 o -1 12 1 30.28 28.09 1.03 o 0 12 1 63.67 60.81 1.66 o 1 12 1 35.42 37.71 1.08 o 2 12 1 6.08 6.33 0.53 o 3 12 1 2.34 2.95 0.60 o 4 12 1 249.15 255.62 5.03 o 5 12 1 932.59 873.09 17.34 o 6 12 1 70.54 74.68 2.18 o 7 12 1 146.54 134.17 3.18 o 8 12 1 62.62 72.44 2.83 o -8 13 1 129.57 128.68 3.54 o -7 13 1 444.53 431.99 10.00 o -6 13 1 15.32 12.61 0.92 o -5 13 1 308.46 290.04 6.52 o -4 13 1 15.31 19.12 1.31 o -3 13 1 208.35 209.40 4.83 o -2 13 1 19.69 19.70 0.97 o -1 13 1 4664.60 4413.48 89.25 o 0 13 1 536.01 521.44 11.78 o 1 13 1 4358.08 4299.67 66.33 o 2 13 1 357.65 351.94 6.21 o 3 13 1 6580.40 6491.39 109.80 o 4 13 1 1.79 2.15 0.53 o 5 13 1 2217.25 2161.98 37.32 o 6 13 1 1.37 0.54 0.44 o 7 13 1 344.57 318.81 11.09 o 8 13 1 27.96 30.52 1.59 o -8 14 1 62.50 60.34 2.12 o -7 14 1 159.44 149.23 4.51 o -6 14 1 372.60 362.72 11.15 o -5 14 1 1996.47 1938.55 40.13 o -4 14 1 179.42 179.43 4.37 o -3 14 1 23.21 23.71 1.28 o -2 14 1 2.65 1.96 0.52 o -1 14 1 0.43 -0.16 0.49 o 0 14 1 0.95 0.85 0.47 o 1 14 1 61.12 61.48 1.68 o 2 14 1 260.69 257.62 4.95 o 3 14 1 463.38 477.33 9.96 o 4 14 1 327.25 319.74 6.85 o 5 14 1 15.24 17.47 1.02 o 6 14 1 193.33 191.55 4.97 o 7 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14 311.72 283.81 9.20 o -5 2 14 30.33 32.69 2.09 o -4 2 14 85.89 86.34 2.89 o -3 2 14 39.21 35.97 1.85 o -2 2 14 106.55 108.28 3.36 o -1 2 14 167.54 161.75 4.92 o -6 3 14 19.65 15.95 1.86 o -5 3 14 25.02 19.99 1.32 o -4 3 14 0.92 1.63 0.88 o -3 3 14 48.61 45.91 2.86 o -2 3 14 44.35 44.20 2.19 o -1 3 14 65.36 57.91 2.13 o -6 4 14 114.91 105.49 4.90 o -5 4 14 1.30 0.63 0.92 o -4 4 14 303.85 290.05 13.93 o -3 4 14 3.03 1.25 0.84 o -2 4 14 242.16 247.34 9.69 o -1 4 14 2.99 2.24 0.86 o -6 5 14 107.68 81.26 8.21 o -5 5 14 3.99 3.05 1.09 o -4 5 14 2.45 1.36 0.89 o -3 5 14 0.23 0.62 0.76 o -2 5 14 2.31 1.99 0.75 o -5 6 14 11.88 7.83 1.28 o -4 6 14 345.11 339.14 12.94 o -3 6 14 0.89 1.78 1.43 o