#------------------------------------------------------------------------------ #$Date: 2023-11-01 19:09:25 +0000 (Wed, 01 Nov 2023) $ #$Revision: 287216 $ #$URL: svn://www.crystallography.net/cod/hkl/4/51/94/4519467.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519467 _cell_angle_alpha 90.000 _cell_angle_beta 109.490 _cell_angle_gamma 90.000 _cell_length_a 9.1681 _cell_length_b 16.0667 _cell_length_c 11.3762 _exptl_crystal_F_000 698.48 _reflns_d_resolution_high 0.7701 _cod_data_source_file S22_Pq-Br_0_59_Cl_1_41_3H2O.fcf _cod_data_source_block jw2262b _shelx_title ' jw2262b_a.res in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 129.72 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 417.91 452.06 29.03 o 3 0 0 4.96 6.57 0.47 o 5 0 0 287.71 309.08 9.69 o 6 0 0 1765.80 1705.81 29.42 o 7 0 0 957.19 912.35 15.12 o 8 0 0 12.93 21.70 0.97 o 9 0 0 634.47 641.53 12.55 o 10 0 0 378.72 400.00 9.07 o 11 0 0 225.63 225.11 5.18 o 1 1 0 95.63 105.17 2.39 o 2 1 0 399.33 401.78 9.87 o 3 1 0 1324.44 1424.99 38.86 o 4 1 0 1699.27 1871.86 87.03 o 5 1 0 1641.87 1517.56 18.95 o 6 1 0 2208.46 2139.20 25.41 o 7 1 0 9.92 8.25 0.32 o 8 1 0 1595.94 1566.39 20.20 o 9 1 0 63.08 62.45 1.05 o 10 1 0 105.70 106.69 1.86 o 11 1 0 58.26 59.21 1.14 o 1 2 0 976.54 1186.04 96.57 o 2 2 0 1565.93 1470.97 80.05 o 3 2 0 223.67 235.14 5.88 o 4 2 0 789.23 794.00 25.17 o 5 2 0 490.81 466.01 5.90 o 6 2 0 2010.99 1929.91 22.42 o 7 2 0 509.01 472.93 6.04 o 8 2 0 649.54 647.97 8.46 o 9 2 0 5.19 5.35 0.27 o 10 2 0 995.55 1008.51 15.96 o 11 2 0 12.94 10.54 1.00 o 1 3 0 69.45 84.46 2.41 o 2 3 0 911.27 874.76 24.80 o 3 3 0 687.04 721.59 23.41 o 4 3 0 4900.11 4655.70 180.70 o 5 3 0 348.17 343.13 4.42 o 6 3 0 55.48 64.29 0.94 o 7 3 0 504.55 505.53 6.45 o 8 3 0 22.37 25.16 0.52 o 9 3 0 74.62 74.56 1.29 o 10 3 0 96.40 101.70 1.95 o 11 3 0 29.42 35.26 0.81 o 0 4 0 905.76 1089.36 42.66 o 1 4 0 12.42 9.03 0.60 o 3 4 0 9.11 7.87 0.36 o 4 4 0 5738.55 5047.07 138.92 o 5 4 0 150.58 151.21 2.12 o 6 4 0 4090.86 3880.18 74.49 o 7 4 0 99.98 103.09 1.45 o 8 4 0 1456.45 1431.15 23.70 o 9 4 0 33.13 33.13 0.70 o 10 4 0 345.33 348.81 6.48 o 11 4 0 11.18 11.91 0.57 o 1 5 0 104.97 123.71 2.86 o 2 5 0 110.15 138.65 3.38 o 3 5 0 432.49 447.50 8.71 o 4 5 0 2597.04 2708.73 44.58 o 5 5 0 216.70 208.43 2.72 o 6 5 0 16.60 18.77 0.39 o 7 5 0 164.14 146.58 2.10 o 8 5 0 46.90 45.31 0.89 o 9 5 0 9.85 11.10 0.41 o 10 5 0 2.93 4.65 0.27 o 1 6 0 52.79 57.19 1.51 o 3 6 0 750.68 773.15 13.40 o 4 6 0 5526.47 5279.14 143.51 o 5 6 0 0.67 1.70 0.14 o 6 6 0 1756.73 1671.36 22.15 o 7 6 0 41.87 38.01 0.70 o 8 6 0 530.02 529.83 7.63 o 9 6 0 206.86 208.75 3.49 o 10 6 0 90.73 83.54 2.10 o 1 7 0 6.71 6.60 0.34 o 2 7 0 52.00 72.50 1.54 o 3 7 0 270.79 260.70 4.41 o 4 7 0 1432.48 1519.40 21.41 o 5 7 0 455.92 448.42 6.24 o 6 7 0 429.87 393.81 5.34 o 7 7 0 13.52 13.33 0.40 o 8 7 0 514.79 517.53 8.02 o 9 7 0 41.70 36.95 1.09 o 10 7 0 7.21 4.46 0.42 o 0 8 0 1170.97 1199.92 29.29 o 1 8 0 456.89 470.54 9.13 o 2 8 0 380.16 428.67 8.95 o 3 8 0 491.51 464.12 7.41 o 4 8 0 844.20 786.21 11.98 o 5 8 0 415.90 418.30 6.24 o 6 8 0 858.48 822.66 12.58 o 7 8 0 114.71 99.39 1.90 o 8 8 0 255.14 283.73 5.15 o 9 8 0 12.78 12.70 0.58 o 10 8 0 436.58 448.53 11.08 o 1 9 0 362.67 358.72 7.51 o 2 9 0 369.00 367.07 8.03 o 3 9 0 483.72 463.59 7.42 o 4 9 0 960.98 945.22 14.38 o 5 9 0 472.13 467.67 6.98 o 6 9 0 772.40 794.35 12.67 o 7 9 0 548.55 520.28 9.23 o 8 9 0 191.19 226.58 4.40 o 9 9 0 116.69 122.03 3.58 o 10 9 0 254.39 277.77 6.95 o 1 10 0 335.18 346.22 6.82 o 3 10 0 402.86 375.80 6.07 o 4 10 0 4194.87 4039.13 69.51 o 5 10 0 4.09 3.12 0.25 o 6 10 0 2056.17 1936.77 31.88 o 7 10 0 104.36 99.24 2.12 o 8 10 0 194.42 204.63 4.83 o 9 10 0 113.69 110.67 2.69 o 1 11 0 114.50 116.89 3.04 o 2 11 0 266.26 265.15 5.29 o 3 11 0 141.56 132.95 2.53 o 4 11 0 575.77 558.78 9.39 o 5 11 0 157.71 153.31 2.65 o 6 11 0 538.64 506.88 8.55 o 7 11 0 246.74 252.12 5.16 o 8 11 0 281.90 272.96 6.26 o 9 11 0 44.06 51.23 1.68 o 0 12 0 293.51 236.58 7.70 o 1 12 0 548.68 564.66 15.58 o 2 12 0 21.93 25.06 0.79 o 3 12 0 1525.13 1515.49 27.67 o 4 12 0 1432.85 1367.87 25.00 o 5 12 0 30.19 25.97 0.79 o 6 12 0 859.93 814.68 15.03 o 7 12 0 0.04 0.15 0.30 o 8 12 0 428.01 411.55 9.31 o 9 12 0 0.80 0.92 0.36 o 1 13 0 4.88 6.35 0.61 o 2 13 0 40.39 35.64 1.29 o 3 13 0 301.41 302.90 13.80 o 4 13 0 595.36 602.54 11.91 o 5 13 0 32.28 33.38 0.96 o 6 13 0 74.02 77.19 2.06 o 7 13 0 101.18 106.70 2.86 o 8 13 0 43.20 42.28 1.34 o 0 14 0 186.13 192.94 7.88 o 1 14 0 15.19 14.19 0.68 o 2 14 0 1591.88 1610.07 39.54 o 3 14 0 134.54 135.75 4.62 o 4 14 0 1911.55 1878.06 41.94 o 5 14 0 13.62 13.30 0.91 o 6 14 0 582.76 581.06 14.61 o 7 14 0 0.91 0.72 0.39 o 8 14 0 407.71 420.90 13.41 o 1 15 0 3.77 3.91 0.42 o 2 15 0 155.20 157.93 3.92 o 3 15 0 141.29 142.62 3.92 o 4 15 0 29.32 30.75 1.10 o 5 15 0 6.35 6.46 0.51 o 6 15 0 47.42 49.40 1.77 o 7 15 0 2.88 2.18 0.45 o 0 16 0 794.49 914.23 35.65 o 1 16 0 0.28 0.63 0.34 o 2 16 0 2872.52 2855.08 69.63 o 3 16 0 54.36 54.22 1.64 o 4 16 0 678.24 665.01 17.72 o 5 16 0 14.08 11.24 0.68 o 6 16 0 190.79 172.93 5.00 o 7 16 0 2.32 0.13 0.47 o 1 17 0 114.54 122.51 3.15 o 2 17 0 230.06 227.88 7.38 o 3 17 0 190.67 197.50 4.87 o 4 17 0 124.81 125.60 3.35 o 5 17 0 83.52 81.40 3.61 o 6 17 0 96.76 91.94 3.91 o 0 18 0 59.19 62.01 2.35 o 1 18 0 315.73 321.34 10.42 o 2 18 0 4.35 5.36 0.57 o 3 18 0 141.60 139.83 3.70 o 4 18 0 58.22 58.10 1.79 o 5 18 0 30.72 30.61 1.74 o 1 19 0 14.41 16.92 1.10 o 2 19 0 208.34 198.22 5.70 o 3 19 0 81.84 76.31 2.49 o 4 19 0 292.02 307.41 8.78 o 0 20 0 1206.66 1168.50 63.87 o 1 20 0 114.27 115.30 4.06 o 2 20 0 952.01 906.84 28.71 o 3 20 0 16.09 12.84 1.70 o -11 1 1 396.50 399.00 6.66 o -10 1 1 13.27 14.28 0.42 o -9 1 1 504.23 488.27 6.80 o -8 1 1 200.64 200.43 2.90 o -7 1 1 4.56 8.63 0.38 o -6 1 1 59.84 54.03 0.75 o -5 1 1 3139.74 3067.23 50.23 o -4 1 1 86.33 86.53 1.72 o -3 1 1 1624.43 1507.15 41.07 o -2 1 1 1313.35 1293.86 28.71 o -1 1 1 177.19 283.95 6.93 o 0 1 1 262.78 316.33 8.60 o 2 1 1 918.93 971.03 26.49 o 3 1 1 209.80 203.32 5.13 o 4 1 1 332.56 329.84 7.52 o 5 1 1 1164.80 1036.90 14.17 o 6 1 1 0.62 0.53 0.13 o 7 1 1 5002.61 4646.97 89.44 o 8 1 1 49.56 46.32 0.88 o 9 1 1 741.04 729.80 10.07 o 10 1 1 53.86 61.37 1.24 o -11 2 1 1.51 0.85 0.22 o -10 2 1 0.69 0.49 0.19 o -9 2 1 310.60 303.32 4.29 o -8 2 1 1032.97 1013.23 13.13 o -7 2 1 2482.63 2414.82 29.46 o -6 2 1 593.75 548.56 6.62 o -5 2 1 148.79 152.39 2.18 o -4 2 1 120.22 126.42 2.43 o -2 2 1 0.43 1.30 0.16 o 0 2 1 12.53 12.76 0.43 o 2 2 1 549.12 563.82 11.64 o 3 2 1 130.04 117.85 2.78 o 4 2 1 44.61 50.30 1.47 o 5 2 1 168.41 133.15 1.87 o 6 2 1 2.68 3.23 0.17 o 7 2 1 87.74 89.73 1.67 o 8 2 1 58.18 57.05 0.99 o 9 2 1 167.32 161.77 2.47 o 10 2 1 111.39 118.63 2.11 o -11 3 1 10.60 7.37 0.37 o -10 3 1 62.09 63.20 1.29 o -9 3 1 343.83 343.30 5.19 o -8 3 1 32.75 33.71 0.63 o -7 3 1 913.10 950.11 11.68 o -6 3 1 832.04 824.10 10.12 o -5 3 1 4488.62 4338.01 136.35 o -4 3 1 30.71 27.81 0.80 o -2 3 1 378.17 485.62 18.48 o 0 3 1 407.50 477.18 13.07 o 2 3 1 1199.99 1280.55 26.36 o 4 3 1 90.52 72.13 1.26 o 5 3 1 7218.81 5996.64 326.14 o 6 3 1 5.03 5.66 0.20 o 7 3 1 2091.49 2061.66 27.29 o 8 3 1 62.54 62.23 0.96 o 9 3 1 573.52 569.20 8.14 o 10 3 1 17.17 14.38 0.48 o -11 4 1 344.40 385.53 7.56 o -10 4 1 5.34 5.53 0.39 o -9 4 1 159.60 152.85 2.50 o -8 4 1 434.00 455.19 6.57 o -7 4 1 828.28 809.95 9.97 o -6 4 1 798.58 778.64 9.82 o -5 4 1 389.54 348.53 4.57 o -4 4 1 1146.62 1236.00 25.58 o -3 4 1 880.57 950.34 18.53 o -2 4 1 87.86 112.22 4.74 o 0 4 1 0.67 1.34 0.18 o 1 4 1 510.94 534.13 13.03 o 2 4 1 388.73 431.74 9.71 o 4 4 1 11.66 17.68 0.44 o 5 4 1 1757.23 1707.04 23.24 o 6 4 1 937.81 918.19 11.58 o 7 4 1 476.82 502.85 6.60 o 8 4 1 601.98 596.83 8.27 o 9 4 1 190.18 185.37 2.98 o 10 4 1 79.32 78.35 1.77 o -11 5 1 763.49 800.86 17.90 o -10 5 1 69.77 79.67 2.36 o -9 5 1 986.88 1012.66 16.03 o -8 5 1 0.18 0.54 0.19 o -7 5 1 974.92 971.45 12.25 o -6 5 1 8.48 9.07 0.28 o -5 5 1 5.30 9.49 0.28 o -4 5 1 173.17 184.43 3.78 o -3 5 1 2475.76 2673.21 85.37 o -2 5 1 1422.37 1505.61 57.76 o -1 5 1 115.13 115.51 3.76 o 0 5 1 3450.65 3094.89 168.27 o 1 5 1 54.58 54.76 1.17 o 2 5 1 2142.62 2180.99 44.86 o 3 5 1 2128.98 2169.20 44.61 o 4 5 1 412.08 377.08 6.61 o 5 5 1 314.91 336.21 4.83 o 6 5 1 96.39 85.95 1.33 o 7 5 1 902.62 856.05 12.17 o 8 5 1 127.30 122.00 1.91 o 9 5 1 942.79 914.23 14.03 o 10 5 1 3.20 2.23 0.29 o -10 6 1 31.83 25.50 0.71 o -9 6 1 148.28 151.70 2.49 o -8 6 1 209.81 221.36 3.56 o -7 6 1 293.12 312.26 4.41 o -6 6 1 497.99 464.25 6.09 o -5 6 1 852.45 741.79 9.89 o -4 6 1 633.24 625.75 9.67 o -3 6 1 3087.74 3182.27 136.25 o -2 6 1 60.83 58.39 1.62 o -1 6 1 2325.46 2320.72 81.12 o 0 6 1 15.24 13.54 0.45 o 1 6 1 142.02 134.39 2.53 o 2 6 1 6.30 7.63 0.38 o 3 6 1 39.80 35.00 0.70 o 4 6 1 440.93 427.91 7.14 o 5 6 1 1520.83 1557.47 21.93 o 6 6 1 483.41 473.10 7.02 o 7 6 1 1386.96 1265.72 17.92 o 8 6 1 241.32 235.67 3.73 o 9 6 1 322.12 312.15 5.63 o 10 6 1 192.23 215.54 5.44 o -10 7 1 9.11 6.91 0.43 o -9 7 1 120.55 128.11 2.75 o -8 7 1 10.22 14.32 0.46 o -7 7 1 351.23 399.66 5.60 o -6 7 1 15.57 15.44 0.38 o -5 7 1 2318.47 2174.21 28.74 o -4 7 1 29.47 24.93 0.52 o -3 7 1 2165.94 2228.08 42.87 o -2 7 1 37.24 41.94 1.39 o -1 7 1 11609.27 10554.31 587.41 o 0 7 1 724.66 728.04 14.05 o 1 7 1 11497.91 9990.41 556.41 o 2 7 1 418.37 421.62 8.24 o 3 7 1 9765.55 9180.62 352.61 o 4 7 1 46.07 45.69 0.81 o 5 7 1 3117.92 3062.79 48.09 o 6 7 1 4.16 3.66 0.22 o 7 7 1 2412.86 2308.22 34.88 o 8 7 1 93.88 86.34 1.62 o 9 7 1 339.59 324.28 10.62 o 10 7 1 157.89 171.13 4.37 o -10 8 1 128.89 148.17 3.82 o -9 8 1 69.19 71.58 1.67 o -8 8 1 0.92 0.75 0.24 o -7 8 1 0.78 1.35 0.22 o -6 8 1 105.62 106.02 1.69 o -5 8 1 658.88 689.55 10.18 o -4 8 1 382.00 366.71 5.68 o -3 8 1 165.93 167.33 3.27 o -2 8 1 31.35 28.94 0.82 o -1 8 1 37.69 50.39 1.10 o 0 8 1 186.41 186.20 4.29 o 1 8 1 252.33 266.80 5.25 o 2 8 1 15.83 16.84 0.51 o 3 8 1 328.45 325.53 5.77 o 4 8 1 570.11 567.11 8.71 o 5 8 1 355.91 358.59 5.59 o 6 8 1 182.13 173.51 3.11 o 7 8 1 122.98 124.64 2.32 o 8 8 1 77.35 70.99 1.51 o 9 8 1 21.13 24.63 0.86 o 10 8 1 21.21 31.03 1.12 o -10 9 1 7.89 9.17 0.59 o -9 9 1 452.99 464.89 12.88 o -8 9 1 15.34 18.04 0.65 o -7 9 1 263.04 306.39 5.49 o -6 9 1 335.17 305.53 4.63 o -5 9 1 1007.35 946.70 13.91 o -4 9 1 129.09 129.23 2.04 o -3 9 1 4601.96 4560.29 144.54 o -2 9 1 144.67 157.30 4.76 o -1 9 1 115.26 119.76 2.83 o 0 9 1 314.72 319.57 6.70 o 1 9 1 2501.54 2406.84 49.48 o 2 9 1 19.18 19.50 0.58 o 3 9 1 174.42 181.44 3.33 o 4 9 1 15.16 15.94 0.50 o 5 9 1 1106.76 1107.96 19.28 o 6 9 1 72.56 76.56 1.59 o 7 9 1 824.54 774.53 13.58 o 8 9 1 83.09 77.06 1.62 o 9 9 1 445.36 467.71 10.52 o -10 10 1 25.74 24.07 0.90 o -9 10 1 54.28 49.81 1.46 o -8 10 1 4.54 6.89 0.60 o -7 10 1 2.29 0.33 0.24 o -6 10 1 0.14 0.49 0.20 o -5 10 1 48.18 51.91 1.00 o -4 10 1 68.63 69.53 1.36 o -3 10 1 17.62 22.57 0.66 o -2 10 1 0.75 0.47 0.19 o -1 10 1 2289.67 2467.31 60.03 o 0 10 1 44.69 47.02 1.09 o 1 10 1 167.78 198.03 3.95 o 2 10 1 2.12 2.02 0.21 o 3 10 1 1026.93 971.08 16.87 o 4 10 1 63.27 58.13 1.25 o 5 10 1 278.60 277.53 4.78 o 6 10 1 53.10 48.87 1.21 o 7 10 1 28.17 23.15 0.78 o 8 10 1 40.36 39.36 1.05 o 9 10 1 22.53 23.42 0.98 o -9 11 1 750.87 766.33 17.16 o -8 11 1 0.38 -0.05 0.29 o -7 11 1 617.93 618.95 14.04 o -6 11 1 28.60 23.96 0.78 o -5 11 1 268.68 291.59 5.02 o -4 11 1 55.84 50.98 1.23 o -3 11 1 19.16 18.94 0.62 o -2 11 1 175.11 179.95 4.22 o -1 11 1 68.74 71.18 1.65 o 0 11 1 414.84 400.78 8.40 o 1 11 1 1273.11 1312.18 27.08 o 2 11 1 372.31 363.35 6.46 o 3 11 1 299.88 295.13 5.30 o 4 11 1 91.37 86.98 1.78 o 5 11 1 289.93 292.77 5.03 o 6 11 1 104.97 92.82 1.87 o 7 11 1 308.63 306.61 5.54 o 8 11 1 15.80 13.06 0.64 o 9 11 1 376.97 395.76 10.94 o -9 12 1 183.25 162.25 4.13 o -8 12 1 97.57 90.80 2.70 o -7 12 1 178.38 176.84 4.24 o -6 12 1 259.93 242.69 6.28 o -5 12 1 232.95 220.85 5.34 o -4 12 1 38.81 36.93 1.24 o -3 12 1 2112.13 2101.94 43.39 o -2 12 1 1.40 0.93 0.26 o -1 12 1 36.32 32.82 1.04 o 0 12 1 57.93 57.80 1.67 o 1 12 1 34.57 39.32 1.00 o 2 12 1 9.56 8.74 0.50 o 3 12 1 0.77 3.55 0.40 o 4 12 1 242.41 250.42 4.57 o 5 12 1 877.97 874.69 16.18 o 6 12 1 68.74 68.02 1.48 o 7 12 1 144.01 131.78 3.01 o 8 12 1 56.49 61.72 1.96 o -9 13 1 78.85 67.68 2.73 o -8 13 1 117.71 110.91 2.95 o -7 13 1 408.12 412.88 10.46 o -6 13 1 19.77 17.03 0.82 o -5 13 1 310.60 287.08 8.01 o -4 13 1 14.42 19.01 1.18 o -3 13 1 256.33 284.85 6.74 o -2 13 1 24.68 25.95 1.14 o 0 13 1 516.97 511.61 39.06 o 1 13 1 4245.84 4073.37 154.82 o 2 13 1 346.69 354.34 7.12 o 3 13 1 6254.18 5829.82 112.15 o 4 13 1 2.56 2.85 0.33 o 5 13 1 2092.65 2087.78 40.37 o 6 13 1 0.64 1.29 0.32 o 7 13 1 313.05 315.23 8.99 o 8 13 1 27.65 31.97 1.19 o -8 14 1 56.53 55.52 1.88 o -7 14 1 147.30 153.09 5.14 o -6 14 1 350.83 346.20 9.64 o -5 14 1 1834.21 1803.64 40.26 o -4 14 1 178.83 185.15 4.96 o -3 14 1 26.77 33.02 1.13 o -2 14 1 1.23 0.95 0.36 o -1 14 1 1.59 2.64 0.41 o 0 14 1 1.09 1.00 0.25 o 1 14 1 61.17 63.99 1.93 o 2 14 1 246.57 246.62 6.43 o 3 14 1 458.82 458.83 9.18 o 4 14 1 303.90 293.00 5.63 o 5 14 1 17.37 19.46 0.70 o 6 14 1 179.13 171.95 4.07 o 7 14 1 377.43 387.74 9.63 o 8 14 1 87.62 73.19 2.33 o -8 15 1 0.53 0.12 0.47 o -7 15 1 348.77 373.52 10.47 o -6 15 1 77.86 75.02 3.02 o -5 15 1 80.13 76.83 2.63 o -4 15 1 319.71 334.44 8.58 o -3 15 1 5.51 6.81 0.55 o -2 15 1 648.06 665.28 16.67 o -1 15 1 4.18 5.20 0.71 o 1 15 1 3.89 3.29 0.43 o 2 15 1 76.93 81.82 2.42 o 3 15 1 182.00 191.21 4.64 o 4 15 1 36.88 34.98 1.11 o 5 15 1 374.23 369.81 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19.91 0.85 o 3 18 1 0.11 0.00 0.42 o 4 18 1 26.10 24.86 1.13 o 5 18 1 1.78 1.73 0.46 o -4 19 1 12.18 10.32 0.69 o -3 19 1 107.61 104.78 3.17 o -2 19 1 4.32 3.62 0.57 o -1 19 1 426.61 416.95 16.32 o 0 19 1 4.26 3.63 0.73 o 1 19 1 75.25 82.76 3.09 o 2 19 1 41.29 37.51 1.75 o 3 19 1 185.17 173.25 5.02 o 4 19 1 47.11 45.86 1.93 o -3 20 1 0.11 1.01 0.77 o -2 20 1 9.33 11.06 1.56 o -1 20 1 0.05 0.53 0.62 o 0 20 1 24.75 26.33 1.71 o 1 20 1 3.70 3.76 0.76 o 2 20 1 0.64 1.52 0.76 o -11 0 2 81.52 81.01 2.05 o -10 0 2 242.83 245.77 6.98 o -9 0 2 145.08 148.09 3.30 o -8 0 2 4570.10 4358.00 106.09 o -7 0 2 24.27 28.33 0.74 o -5 0 2 91.68 79.47 1.86 o -4 0 2 5786.03 4866.10 265.85 o -3 0 2 504.04 542.92 17.24 o -1 0 2 431.88 496.96 27.08 o 1 0 2 1529.42 1809.71 98.60 o 3 0 2 244.61 276.04 11.02 o 5 0 2 12.13 25.26 1.13 o 6 0 2 3678.11 3628.84 130.71 o 7 0 2 476.17 442.06 8.72 o 8 0 2 857.81 866.70 18.10 o 9 0 2 211.63 210.69 4.66 o 10 0 2 2.31 1.32 0.34 o -11 1 2 45.64 47.70 0.97 o -10 1 2 233.89 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