#------------------------------------------------------------------------------ #$Date: 2026-09-24 07:48:01 +0100 (Thu, 24 Sep 2026) $ #$Revision: 306902 $ #$URL: svn://www.crystallography.net/cod/cif/4/51/95/4519530.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519530 loop_ _publ_author_name 'Kapustin, Eugene A.' 'Lee, Seungkyu' 'Alshammari, Ahmad S.' 'Yaghi, Omar M.' _publ_contact_author_address ;Department of Chemistry, University of California, Berkeley, Berkeley, CA 94720 USA ; _publ_contact_author_email yaghi@berkeley.edu _publ_contact_author_name 'Omar M. Yaghi' _publ_section_title ; Molecular Retrofitting Adapts a Metal--Organic Framework to Extreme Pressure ; _journal_issue 6 _journal_name_full 'ACS Central Science' _journal_page_first 662 _journal_page_last 667 _journal_paper_doi 10.1021/acscentsci.7b00169 _journal_volume 3 _journal_year 2017 _chemical_absolute_configuration ad _chemical_formula_moiety 'C34 H21 Al2 O10' _chemical_formula_sum 'C34 H21 Al2 O10' _chemical_formula_weight 643.47 _chemical_name_common MOF-520-BPDC_100K _space_group_crystal_system tetragonal _space_group_IT_number 94 _space_group_name_Hall 'P 4n 2n' _space_group_name_H-M_alt 'P 42 21 2' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 19.1813(7) _cell_length_b 19.1813(7) _cell_length_c 36.6658(13) _cell_measurement_reflns_used 9961 _cell_measurement_temperature 298(2) _cell_measurement_theta_max 38.51 _cell_measurement_theta_min 2.72 _cell_volume 13490.2(8) _computing_cell_refinement 'SAINT V8.34A Bruker-AXS, Madison WI' _computing_data_collection 'Bruker APEX2 Bruker-AXS, Madison WI' _computing_data_reduction 'SAINT V8.34A Bruker-AXS, Madison WI' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2015)' _computing_structure_solution 'XS (Sheldrick, 2008)' _diffrn_ambient_temperature 298(2) _diffrn_detector_area_resol_mean 10.42 _diffrn_measured_fraction_theta_full 0.990 _diffrn_measured_fraction_theta_max 0.990 _diffrn_measurement_device_type 'Bruker D8 with PHOTON 100 detector' _diffrn_measurement_method '\f and \w shutterless scans' _diffrn_radiation_monochromator 'silicon 111' _diffrn_radiation_type synchrotron _diffrn_radiation_wavelength 1.0332 _diffrn_reflns_av_R_equivalents 0.0335 _diffrn_reflns_av_unetI/netI 0.0482 _diffrn_reflns_Laue_measured_fraction_full 0.990 _diffrn_reflns_Laue_measured_fraction_max 0.986 _diffrn_reflns_limit_h_max 23 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 37 _diffrn_reflns_limit_l_min -43 _diffrn_reflns_number 46877 _diffrn_reflns_point_group_measured_fraction_full 0.969 _diffrn_reflns_point_group_measured_fraction_max 0.965 _diffrn_reflns_theta_full 38.564 _diffrn_reflns_theta_max 38.564 _diffrn_reflns_theta_min 2.183 _diffrn_source ; Advanced Light Source, station 11.3.1 ; _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.190 _exptl_absorpt_correction_T_max 0.7476 _exptl_absorpt_correction_T_min 0.6824 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2014/4 (Bruker,2014/4) was used for absorption correction. wR2(int) was 0.0676 before and 0.0511 after correction. The Ratio of minimum to maximum transmission is 0.9128. The \l/2 correction factor is Not present. ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 0.634 _exptl_crystal_description block _exptl_crystal_F_000 2648 _exptl_crystal_size_max 0.08 _exptl_crystal_size_mid 0.06 _exptl_crystal_size_min 0.06 _refine_diff_density_max 0.174 _refine_diff_density_min -0.179 _refine_diff_density_rms 0.025 _refine_ls_abs_structure_details ; Flack x determined using 3834 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.08(2) _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.045 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 424 _refine_ls_number_reflns 11988 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.045 _refine_ls_R_factor_all 0.0397 _refine_ls_R_factor_gt 0.0315 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0380P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0732 _refine_ls_wR_factor_ref 0.0750 _reflns_Friedel_coverage 0.740 _reflns_Friedel_fraction_full 0.943 _reflns_Friedel_fraction_max 0.938 _reflns_number_gt 10083 _reflns_number_total 11988 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file oc7b00169_si_003.cif _cod_data_source_block MOF520_BPDC_100K _cod_original_cell_volume 13490.2(11) _cod_database_code 4519530 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.7476 _shelx_estimated_absorpt_t_min 0.6824 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All O(H) groups 2.a Aromatic/amide H refined with riding coordinates: O2(H2), O1(H1), C26(H26), C23(H23), C25(H25), C22(H22), C7(H7), C16(H16), C18(H18), C3(H3), C4(H4), C6(H6), C13(H13), C19(H19), C15(H15), C11(H11), C9(H9), C6G(H6G), C5G(H5G), C2G(H2G), C3G(H3G) ; _shelx_res_file ; TITL ek_mof5x_bridged_ambient_model in P42212 #94 REM reset to P42212 #94 CELL 1.0332 19.1813 19.1813 36.6658 90 90 90 ZERR 8 0.0007 0.0007 0.0013 0 0 0 LATT -1 SYMM 0.5-Y,0.5+X,0.5+Z SYMM -X,-Y,+Z SYMM 0.5+Y,0.5-X,0.5+Z SYMM 0.5+X,0.5-Y,0.5-Z SYMM 0.5-X,0.5+Y,0.5-Z SYMM +Y,+X,-Z SYMM -Y,-X,-Z SFAC C H O Al DISP Al 0.12 0.11 744.346 DISP C 0.009 0.004 30.879 DISP H -0 0 0.639 DISP O 0.025 0.014 100.516 UNIT 272 168 80 16 L.S. 24 PLAN 10 TEMP 25 BOND fmap 2 acta ABIN REM REM REM WGHT 0.038000 FVAR 0.11361 AL1 4 0.660843 0.339157 0.500000 10.50000 0.02081 0.02081 = 0.01594 -0.00152 -0.00152 0.00044 AL2 4 0.625467 0.401890 0.417408 11.00000 0.01874 0.02207 = 0.01456 0.00043 -0.00063 -0.00031 AL3 4 0.500000 0.500000 0.382888 10.50000 0.02063 0.01972 = 0.01477 0.00000 0.00000 0.00199 O2 3 0.566412 0.477260 0.417923 11.00000 0.02328 0.01705 = 0.01214 -0.00091 -0.00086 0.00136 AFIX 43 H2 2 0.570085 0.507205 0.437779 11.00000 -1.20000 AFIX 0 O3 3 0.655389 0.422869 0.369579 11.00000 0.02535 0.03146 = 0.02246 0.00453 0.00440 0.00413 O1 3 0.601242 0.373489 0.464327 11.00000 0.01556 0.02252 = 0.01301 0.00116 -0.00349 -0.00154 AFIX 43 H1 2 0.554357 0.376858 0.470543 11.00000 -1.20000 AFIX 0 O4 3 0.563394 0.478677 0.344281 11.00000 0.02829 0.03062 = 0.01525 0.00205 0.00280 0.00563 C1 1 0.623864 0.451641 0.343047 11.00000 0.02755 0.01816 = 0.01580 0.00211 0.00690 -0.00032 C26 1 0.806787 0.643730 0.145168 11.00000 0.06202 0.03184 = 0.01510 0.00664 0.00886 0.00942 AFIX 43 H26 2 0.809018 0.645777 0.170483 11.00000 0.07340 AFIX 0 C23 1 0.798277 0.639117 0.070363 11.00000 0.05494 0.03741 = 0.01685 0.00145 0.00360 -0.00274 AFIX 43 H23 2 0.794909 0.637933 0.045068 11.00000 0.06908 AFIX 0 C20 1 0.995422 0.151341 0.115544 11.00000 0.02774 0.02916 = 0.01455 -0.00155 0.00246 0.00454 C25 1 0.807172 0.705843 0.125752 11.00000 0.04626 0.02767 = 0.02203 0.00155 0.00313 0.00445 AFIX 43 H25 2 0.810288 0.748351 0.137842 11.00000 0.48769 AFIX 0 C22 1 0.798668 0.578145 0.089415 11.00000 0.07474 0.02143 = 0.03269 -0.00184 0.02192 0.00518 AFIX 43 H22 2 0.795982 0.535833 0.077110 11.00000 0.05238 AFIX 0 C24 1 0.802846 0.703455 0.088143 11.00000 0.03103 0.02590 = 0.02399 0.00342 0.00505 0.00132 C27 1 0.807669 0.770021 0.067380 11.00000 0.01839 0.03109 = 0.01535 0.00190 -0.00039 -0.00481 C17 1 0.956331 0.214305 0.126880 11.00000 0.03279 0.02501 = 0.01733 0.00235 0.01083 0.00649 C7 1 0.631418 0.484673 0.277025 11.00000 0.03686 0.03721 = 0.02377 0.01283 0.00810 0.01346 AFIX 43 H7 2 0.588471 0.506821 0.279105 11.00000 -1.20000 AFIX 0 C21 1 0.803263 0.579228 0.128792 11.00000 0.05538 0.02562 = 0.02769 0.00986 0.02280 0.01367 C5 1 0.730583 0.452223 0.240557 11.00000 0.05932 0.03262 = 0.03269 0.01159 0.02587 0.02284 C16 1 0.891127 0.206321 0.142798 11.00000 0.03839 0.02600 = 0.04633 0.00561 0.01806 0.00706 AFIX 43 H16 2 0.872361 0.162153 0.146418 11.00000 -1.20000 AFIX 0 C8 1 0.768332 0.452771 0.204976 11.00000 0.06945 0.03540 = 0.03123 0.01312 0.02399 0.01903 C2 1 0.660431 0.451749 0.307603 11.00000 0.03230 0.03220 = 0.02266 0.00535 0.00874 0.00808 C18 1 0.984304 0.280242 0.121776 11.00000 0.04653 0.02662 = 0.03654 -0.00318 0.02225 0.00286 AFIX 43 H18 2 1.028643 0.285055 0.111826 11.00000 -1.20000 AFIX 0 C3 1 0.724658 0.418727 0.303962 11.00000 0.04360 0.03494 = 0.02362 0.01190 0.01063 0.01717 AFIX 43 H3 2 0.743941 0.395598 0.323841 11.00000 -1.20000 AFIX 0 C4 1 0.760195 0.419896 0.271095 11.00000 0.04560 0.03920 = 0.03691 0.00663 0.01366 0.01885 AFIX 43 H4 2 0.803878 0.399141 0.269296 11.00000 0.05482 AFIX 0 C14 1 0.882418 0.333216 0.148264 11.00000 0.06407 0.02503 = 0.03611 0.01052 0.03010 0.01459 C6 1 0.665160 0.484755 0.244260 11.00000 0.05651 0.04101 = 0.02946 0.00572 0.01165 0.02431 AFIX 43 H6 2 0.644799 0.506452 0.224233 11.00000 0.03233 AFIX 0 C13 1 0.767590 0.512158 0.183530 11.00000 0.07534 0.03010 = 0.03006 0.01345 0.03256 0.02812 AFIX 43 H13 2 0.742758 0.551038 0.191334 11.00000 0.06381 AFIX 0 C19 1 0.946642 0.338853 0.131396 11.00000 0.05309 0.02419 = 0.04355 0.00038 0.02416 0.00817 AFIX 43 H19 2 0.964795 0.382802 0.126443 11.00000 -1.20000 AFIX 0 C10 1 0.842190 0.394785 0.159799 11.00000 0.06125 0.02887 = 0.03715 0.00667 0.02397 0.01473 C15 1 0.854033 0.266151 0.153331 11.00000 0.03998 0.03548 = 0.05719 0.00896 0.02723 0.00900 AFIX 43 H15 2 0.810121 0.261443 0.163798 11.00000 0.06170 AFIX 0 C12 1 0.804126 0.514864 0.149741 11.00000 0.05867 0.03792 = 0.02168 0.00316 0.02108 0.01906 C11 1 0.840406 0.455574 0.138935 11.00000 0.07159 0.03134 = 0.03152 0.00543 0.03155 0.01622 AFIX 43 H11 2 0.864444 0.456494 0.116912 11.00000 -1.20000 AFIX 0 C9 1 0.805331 0.394444 0.193219 11.00000 0.06730 0.03369 = 0.03724 0.01507 0.02692 0.02144 AFIX 43 H9 2 0.805807 0.354528 0.207615 11.00000 -1.20000 AFIX 0 O8 3 0.812611 0.825338 0.086296 11.00000 0.02630 0.02421 = 0.01815 0.00115 0.00291 -0.00697 O10 3 0.731130 0.400866 0.485319 11.00000 0.01933 0.04179 = 0.01533 -0.00031 -0.00161 -0.00339 O5 3 1.056007 0.159699 0.102620 11.00000 0.02633 0.01812 = 0.01950 -0.00198 0.00493 0.00000 O6 3 0.965236 0.092197 0.119511 11.00000 0.02219 0.01961 = 0.03112 -0.00369 0.00352 -0.00272 O9 3 0.704327 0.456477 0.433477 11.00000 0.02155 0.02849 = 0.02449 0.00592 -0.00211 -0.00615 O7 3 0.805968 0.768042 0.032892 11.00000 0.03890 0.02364 = 0.01630 0.00167 -0.00200 -0.00951 C28 1 0.746398 0.438876 0.458247 11.00000 0.03254 0.03011 = 0.02125 -0.00189 -0.00485 -0.00661 C6G 1 0.848787 0.490117 0.425260 11.00000 0.02544 0.06615 = 0.03281 0.00716 -0.00442 -0.00598 AFIX 43 H6G 2 0.820491 0.501036 0.405471 11.00000 -1.20000 AFIX 0 C1G 1 0.820320 0.460111 0.455535 11.00000 0.03261 0.05294 = 0.03818 0.00394 0.00226 -0.01154 C5G 1 0.919569 0.504453 0.423772 11.00000 0.03834 0.07838 = 0.04288 0.01156 0.00280 -0.02600 AFIX 43 H5G 2 0.938619 0.521992 0.402328 11.00000 -1.20000 AFIX 0 C2G 1 0.864186 0.445544 0.485182 11.00000 0.03079 0.13388 = 0.04499 0.02943 -0.00975 -0.02778 AFIX 43 H2G 2 0.846514 0.423397 0.505765 11.00000 -1.20000 AFIX 0 C4G 1 0.962090 0.493295 0.453289 11.00000 0.02963 0.09287 = 0.04987 0.00763 -0.00417 -0.02606 C3G 1 0.933740 0.464187 0.483731 11.00000 0.02136 0.15025 = 0.05594 0.02826 -0.01271 -0.02340 AFIX 43 H3G 2 0.961830 0.456667 0.504027 11.00000 -1.20000 AFIX 0 HKLF 4 REM ek_mof5x_bridged_ambient_model in P42212 #94 REM R1 = 0.0315 for 10083 Fo > 4sig(Fo) and 0.0397 for all 11988 data REM 424 parameters refined using 0 restraints END WGHT 0.0383 0.0000 REM Highest difference peak 0.174, deepest hole -0.179, 1-sigma level 0.025 Q1 1 0.5217 0.3668 0.4718 11.00000 0.05 0.17 Q2 1 0.8967 0.1011 0.1322 11.00000 0.05 0.17 Q3 1 1.1020 0.3052 0.1238 11.00000 0.05 0.15 Q4 1 0.9140 0.0762 0.1609 11.00000 0.05 0.15 Q5 1 0.5314 0.3780 0.5016 11.00000 0.05 0.14 Q6 1 0.8661 0.1393 0.1423 11.00000 0.05 0.14 Q7 1 0.9025 0.0669 0.1021 11.00000 0.05 0.13 Q8 1 1.0765 0.2841 0.1018 11.00000 0.05 0.12 Q9 1 0.5978 0.3858 0.4877 11.00000 0.05 0.12 Q10 1 1.0991 0.2368 0.1200 11.00000 0.05 0.12 ; _shelx_res_checksum 78515 _shelx_hkl_file ; 1 1 0 1000.00 29.65 -1 1 0 976.45 30.10 2 0 0 31.96 1.01 0 2 0 32.37 1.02 0 -2 0 29.67 1.05 0 -2 0 30.83 1.01 2 1 0 709.33 22.36 1 -2 0 710.69 23.04 2 -1 0 760.40 22.88 -2 1 0 719.21 22.70 -1 2 0 714.70 23.00 2 2 0 165.60 4.85 -2 2 0 158.59 4.83 2 -2 0 161.44 4.84 -2 -2 0 164.56 4.86 0 -3 0 -0.18 0.27 0 -3 0 -0.19 0.25 3 0 0 0.11 0.23 3 0 0 -0.12 0.26 0 3 0 0.34 0.27 1 -3 0 4.62 0.42 -1 3 0 4.66 0.36 -3 -1 0 4.18 0.54 1 3 0 4.16 0.35 3 -1 0 4.83 0.41 3 1 0 4.23 0.41 -1 -3 0 4.38 0.37 1 -3 0 5.28 0.46 3 -1 0 6.02 0.38 -1 -3 0 4.80 0.44 3 2 0 320.58 9.21 3 -2 0 312.20 9.19 2 -3 0 308.88 9.17 3 -2 0 309.22 9.11 -3 2 0 315.73 9.20 -3 -2 0 304.45 9.20 -2 3 0 306.15 9.18 -2 -3 0 319.23 9.20 2 3 0 309.59 9.19 -3 -3 0 33.45 1.28 3 -3 0 32.56 1.24 3 3 0 31.88 1.20 -3 3 0 33.77 1.25 4 0 0 11.18 0.75 0 -4 0 11.45 0.67 4 0 0 9.87 0.63 0 -4 0 10.08 0.56 0 4 0 11.46 0.66 1 4 0 -0.69 0.33 4 -1 0 0.21 0.41 4 -1 0 0.41 0.33 -1 -4 0 -0.05 0.25 -1 -4 0 0.11 0.42 1 -4 0 0.88 0.28 1 -4 0 0.89 0.45 -4 -1 0 -0.10 0.30 -1 4 0 0.61 0.36 4 1 0 -0.20 0.29 4 1 0 -0.40 0.31 -2 4 0 162.66 4.79 2 -4 0 144.89 4.84 -4 -2 0 159.52 4.84 2 4 0 161.07 4.79 4 -2 0 160.28 4.71 -2 -4 0 158.34 4.88 2 -4 0 153.14 4.77 4 -2 0 165.31 4.81 4 2 0 157.04 4.83 -2 -4 0 155.63 4.78 4 -3 0 72.90 2.38 4 3 0 75.40 2.41 -3 -4 0 69.26 2.35 -3 4 0 68.61 2.35 3 4 0 73.86 2.38 3 -4 0 74.15 2.37 -4 -3 0 73.73 2.42 -4 3 0 69.01 2.34 -4 4 0 3.16 0.48 -4 -4 0 2.51 0.41 4 4 0 3.00 0.51 4 -4 0 3.70 0.48 0 5 0 0.64 0.29 5 0 0 0.07 0.33 5 0 0 -0.67 0.36 0 -5 0 -0.43 0.42 0 -5 0 -0.14 0.26 1 -5 0 192.24 5.88 5 -1 0 196.86 5.95 -1 -5 0 204.84 6.01 5 1 0 198.98 5.95 5 1 0 192.34 5.89 1 -5 0 199.87 5.99 -1 5 0 195.79 5.89 5 -1 0 191.28 5.85 1 5 0 194.49 5.88 -1 -5 0 190.67 5.88 5 2 0 44.80 1.66 -2 -5 0 46.04 1.61 2 5 0 43.95 1.54 2 -5 0 40.90 1.63 5 -2 0 44.62 1.50 -2 -5 0 44.49 1.73 5 -2 0 44.52 1.64 -5 -2 0 45.48 1.62 -2 5 0 43.71 1.54 -5 -2 0 42.08 1.32 2 -5 0 44.65 1.59 5 -3 0 15.86 0.74 -3 -5 0 15.67 0.80 5 3 0 15.02 0.94 -5 3 0 14.84 0.80 3 -5 0 16.73 0.90 -5 -3 0 14.75 0.83 3 -5 0 15.40 0.87 -3 5 0 17.00 0.88 3 5 0 15.51 0.78 5 -3 0 15.37 0.80 -4 5 0 16.66 0.83 -4 -5 0 17.47 0.87 -5 4 0 16.56 0.95 -5 -4 0 18.03 0.90 5 -4 0 16.60 0.84 4 5 0 17.12 0.85 4 -5 0 16.19 0.82 5 4 0 16.07 0.96 5 -5 0 106.24 3.45 -5 -5 0 108.51 3.50 -5 5 0 106.30 3.46 5 5 0 106.61 3.44 6 0 0 149.39 4.54 0 -6 0 147.36 4.58 0 -6 0 138.23 4.46 0 6 0 145.43 4.45 6 0 0 144.20 4.46 6 1 0 543.24 15.99 1 -6 0 559.12 16.06 -1 -6 0 560.00 15.94 1 -6 0 528.89 15.91 6 1 0 494.91 15.94 -1 -6 0 535.12 16.06 6 -1 0 546.40 15.90 6 -1 0 547.10 15.98 1 6 0 544.44 15.92 -1 6 0 560.08 15.93 6 2 0 136.82 4.40 -6 -2 0 142.80 4.47 -2 6 0 143.31 4.39 6 2 0 138.93 4.43 6 -2 0 143.10 4.41 -2 -6 0 145.72 4.53 2 -6 0 147.11 4.51 -2 -6 0 134.29 4.38 6 -2 0 140.32 4.32 2 6 0 143.49 4.38 2 -6 0 137.61 4.35 6 3 0 70.80 2.43 3 -6 0 75.27 2.42 6 -3 0 69.47 2.30 -3 -6 0 70.41 2.40 -3 6 0 71.70 2.42 -6 -3 0 69.98 2.45 3 6 0 72.73 2.39 3 -6 0 67.03 2.53 6 -3 0 77.18 2.48 -6 4 0 3.55 0.56 4 6 0 3.33 0.53 -6 -4 0 3.70 0.58 4 -6 0 3.39 0.66 -4 -6 0 3.91 0.55 6 -4 0 2.98 0.45 4 -6 0 3.75 0.51 -4 6 0 3.14 0.49 -6 5 0 5.36 0.58 -5 -6 0 5.24 0.76 5 -6 0 4.46 0.70 5 6 0 4.80 0.56 6 -5 0 4.39 0.73 -6 -5 0 3.84 0.60 -5 6 0 4.72 0.70 6 5 0 5.48 0.60 -6 6 0 1.55 0.41 6 6 0 1.24 0.40 6 -6 0 0.96 0.39 -6 -6 0 1.29 0.64 0 -7 0 -0.37 0.60 0 -7 0 0.25 0.40 7 0 0 0.43 0.45 0 7 0 0.18 0.41 -1 -7 0 80.40 2.66 7 1 0 80.85 2.70 -1 -7 0 84.96 2.84 1 -7 0 81.87 2.68 7 -1 0 82.87 2.73 1 -7 0 75.16 2.78 1 7 0 84.50 2.70 -1 7 0 78.66 2.68 -2 7 0 19.60 0.98 2 -7 0 17.74 0.96 7 -2 0 18.50 1.05 -2 -7 0 18.45 1.05 7 2 0 17.42 1.07 2 -7 0 17.97 1.11 7 2 0 18.32 0.92 -2 -7 0 17.06 0.96 7 -2 0 18.83 0.90 2 7 0 16.73 0.86 -7 -3 0 51.09 1.96 3 -7 0 52.46 1.98 -3 -7 0 50.96 1.84 7 -3 0 49.40 1.76 7 3 0 51.31 1.94 7 -3 0 47.20 1.90 7 3 0 48.92 1.92 -3 -7 0 50.95 2.01 3 -7 0 52.32 1.86 -3 7 0 50.02 1.86 3 7 0 52.71 1.87 -4 -7 0 56.94 2.12 7 -4 0 58.61 2.13 7 4 0 56.00 2.09 4 -7 0 59.06 2.23 4 -7 0 58.62 2.04 -7 -4 0 60.29 2.19 4 7 0 55.65 2.04 -4 7 0 57.42 2.09 7 -4 0 58.20 1.97 -5 7 0 11.46 0.87 5 -7 0 9.79 0.98 -7 -5 0 11.81 0.96 5 7 0 10.18 0.74 7 5 0 11.36 0.79 -7 5 0 10.80 0.76 5 -7 0 11.85 0.88 -5 -7 0 10.80 0.78 -7 -6 0 253.88 7.74 -6 -7 0 252.61 7.72 7 -6 0 254.88 7.70 -6 7 0 252.74 7.70 6 -7 0 247.93 7.89 -7 6 0 238.47 7.73 6 -7 0 250.08 7.66 7 6 0 258.10 7.73 -7 -7 0 111.29 3.70 -7 7 0 108.74 3.68 7 -7 0 110.24 3.67 7 7 0 112.06 3.69 8 0 0 38.53 1.53 8 0 0 39.53 1.57 0 -8 0 39.56 1.53 0 -8 0 36.99 1.66 0 8 0 37.81 1.56 -1 8 0 23.95 1.23 8 1 0 25.68 1.20 8 -1 0 27.24 1.21 -1 -8 0 26.05 1.20 8 -1 0 26.01 1.29 -1 -8 0 25.35 1.36 1 -8 0 24.51 1.25 1 -8 0 26.45 1.18 8 -1 0 26.31 1.17 -2 8 0 177.61 5.59 8 2 0 181.83 5.62 8 2 0 185.60 5.69 2 -8 0 177.41 5.76 8 -2 0 183.99 5.56 -2 -8 0 178.51 5.60 2 -8 0 179.52 5.58 2 8 0 181.22 5.59 3 8 0 37.47 1.48 8 3 0 35.72 1.58 8 -3 0 36.93 1.45 -3 8 0 39.01 1.49 8 -3 0 38.74 1.62 -3 -8 0 39.67 1.52 8 3 0 37.65 1.63 -3 -8 0 38.11 1.69 -8 -3 0 37.95 1.58 3 -8 0 36.64 1.54 4 -8 0 46.92 1.99 8 4 0 46.79 1.91 4 -8 0 50.98 1.89 -4 8 0 48.05 1.87 8 4 0 48.23 1.95 4 8 0 48.81 1.82 -8 -4 0 50.19 1.91 8 -4 0 52.37 1.89 5 -8 0 1.50 0.66 -8 -5 0 1.29 0.46 -5 -8 0 1.45 0.42 -5 8 0 1.02 0.48 8 -5 0 0.97 0.41 8 5 0 0.60 0.61 5 8 0 1.19 0.47 5 -8 0 1.24 0.41 8 5 0 1.56 0.56 6 -8 0 63.86 2.31 -6 8 0 62.28 2.31 6 -8 0 59.34 2.48 8 -6 0 65.98 2.29 6 8 0 63.27 2.26 -8 -6 0 63.35 2.40 -6 -8 0 62.15 2.35 8 6 0 59.72 2.27 8 7 0 173.68 5.46 8 -7 0 179.35 5.49 -7 8 0 164.80 5.43 -8 -7 0 172.86 5.53 -7 -8 0 174.18 5.50 7 8 0 165.49 5.44 -8 7 0 165.57 5.46 7 -8 0 172.94 5.68 7 -8 0 177.63 5.45 8 8 0 4.24 0.63 -8 8 0 4.19 0.63 -8 -8 0 5.39 0.88 8 -8 0 6.13 0.68 9 0 0 -0.48 0.54 0 9 0 -0.34 0.43 0 -9 0 0.09 0.56 0 -9 0 0.13 0.42 9 0 0 -0.40 0.48 9 -1 0 48.02 1.85 9 -1 0 50.63 1.97 9 1 0 50.06 1.92 1 -9 0 47.71 1.80 9 1 0 47.84 1.82 1 9 0 49.58 1.83 9 -1 0 49.62 1.91 -1 9 0 50.08 1.82 -1 -9 0 47.84 1.87 1 -9 0 49.98 2.00 9 -2 0 131.96 4.20 2 -9 0 126.61 4.10 9 -2 0 132.34 4.22 9 -2 0 126.33 4.09 2 -9 0 131.26 4.33 -2 9 0 126.13 4.13 -2 -9 0 126.42 4.35 9 2 0 133.12 4.24 2 9 0 124.60 4.12 9 2 0 126.04 4.15 -3 -9 0 31.92 1.44 3 -9 0 33.38 1.54 3 -9 0 30.74 1.41 9 3 0 31.48 1.41 3 9 0 32.01 1.34 -3 9 0 32.47 1.42 9 3 0 30.62 1.45 9 -3 0 32.25 1.40 -3 -9 0 27.84 1.55 9 -3 0 33.18 1.39 4 -9 0 151.55 4.84 9 -4 0 156.40 4.91 9 4 0 144.77 4.88 9 4 0 152.70 4.94 4 -9 0 157.30 5.08 -4 -9 0 154.13 4.91 9 -4 0 158.02 4.80 -9 -4 0 154.32 4.98 4 9 0 149.12 4.86 9 5 0 181.74 5.75 5 -9 0 183.43 5.92 -5 9 0 180.90 5.72 5 -9 0 180.95 5.69 9 5 0 177.28 5.73 9 -5 0 183.19 5.76 5 9 0 177.89 5.71 -5 -9 0 180.98 5.76 -9 -5 0 189.13 5.81 6 -9 0 22.05 1.23 6 -9 0 23.55 1.45 6 9 0 22.75 1.23 -9 -6 0 24.17 1.34 9 -6 0 21.79 1.24 -6 9 0 21.46 1.21 -6 -9 0 22.97 1.18 9 6 0 23.18 1.17 9 6 0 20.52 1.24 -7 9 0 0.73 0.40 -7 -9 0 1.08 0.46 -9 -7 0 0.23 0.42 7 9 0 0.83 0.53 9 -7 0 0.74 0.55 7 -9 0 0.56 0.40 9 7 0 0.71 0.42 7 -9 0 1.32 0.71 9 7 0 0.54 0.63 -9 8 0 10.79 0.99 9 8 0 10.45 0.82 8 -9 0 8.77 0.80 9 -8 0 9.91 0.97 -8 -9 0 10.27 1.02 -9 -8 0 11.06 1.04 8 9 0 10.62 0.95 -8 9 0 9.13 0.80 8 -9 0 8.18 0.94 9 8 0 9.16 0.96 -9 -9 0 94.39 3.31 9 -9 0 87.40 3.49 9 -9 0 92.93 3.28 -9 9 0 92.13 3.28 9 9 0 94.77 3.28 0 10 0 0.46 0.55 10 0 0 1.31 0.46 0 -10 0 1.48 0.67 10 0 0 1.34 0.57 0 -10 0 1.36 0.39 -1 -10 0 21.81 1.35 -1 -10 0 20.84 1.15 10 1 0 22.09 1.15 1 10 0 22.62 1.17 -1 10 0 20.02 1.07 10 1 0 21.08 1.15 10 -1 0 20.36 1.13 1 -10 0 21.88 1.33 10 -1 0 19.38 1.22 1 -10 0 20.99 1.12 10 -1 0 20.07 1.18 10 -2 0 24.21 1.21 -2 -10 0 24.77 1.38 2 -10 0 22.21 1.34 2 10 0 24.03 1.24 -2 10 0 25.62 1.24 10 2 0 22.54 1.26 10 -2 0 24.26 1.21 10 2 0 24.47 1.23 10 -2 0 23.37 1.21 -2 -10 0 24.90 1.16 2 -10 0 25.31 1.22 3 -10 0 168.13 5.80 10 -3 0 180.83 5.66 -3 -10 0 180.94 5.65 10 -3 0 182.13 5.57 3 10 0 180.12 5.61 -3 -10 0 173.29 5.86 10 3 0 177.53 5.67 3 -10 0 176.90 5.60 -3 10 0 183.00 5.62 10 3 0 177.64 5.62 -4 10 0 2.02 0.54 10 -4 0 1.87 0.61 10 -4 0 2.24 0.57 -4 -10 0 1.18 0.43 4 10 0 1.89 0.55 10 4 0 1.63 0.49 4 -10 0 1.60 0.52 4 -10 0 2.35 0.74 10 4 0 1.64 0.65 5 -10 0 3.24 0.63 10 -5 0 2.09 0.48 -10 -5 0 2.62 0.67 10 5 0 2.29 0.51 5 10 0 2.61 0.48 10 5 0 2.35 0.66 5 -10 0 2.67 0.74 -5 -10 0 2.62 0.61 -5 10 0 2.73 0.58 6 10 0 1.22 0.41 10 -6 0 1.41 0.46 6 -10 0 2.01 0.70 10 6 0 1.31 0.66 -10 -6 0 1.12 0.63 -6 10 0 1.01 0.52 -6 -10 0 0.46 0.41 10 6 0 0.93 0.43 6 -10 0 0.89 0.54 10 -7 0 7.86 0.79 7 -10 0 9.95 0.97 -10 -7 0 8.12 0.84 10 7 0 8.34 0.96 7 -10 0 9.25 0.97 10 7 0 8.65 0.95 7 10 0 8.27 0.89 -7 10 0 8.68 0.94 -7 -10 0 8.26 0.96 10 8 0 70.49 2.64 10 8 0 70.40 2.58 -10 -8 0 71.54 2.72 8 10 0 67.85 2.54 8 -10 0 68.86 2.60 -8 -10 0 68.88 2.67 -8 10 0 65.24 2.59 10 -8 0 67.50 2.56 8 -10 0 73.01 2.90 -9 10 0 23.34 1.35 9 -10 0 23.03 1.24 -10 -9 0 20.56 1.26 10 9 0 20.77 1.33 9 -10 0 22.17 1.45 10 9 0 22.26 1.32 9 10 0 20.41 1.30 10 -9 0 21.54 1.36 -9 -10 0 21.80 1.44 -10 10 0 7.83 0.85 10 10 0 8.54 0.84 10 10 0 6.40 0.96 10 -10 0 8.51 1.06 10 -10 0 8.64 0.89 0 11 0 0.06 0.36 11 0 0 -0.61 0.50 11 0 0 -0.35 0.53 0 -11 0 0.58 0.62 11 0 0 -0.05 0.37 0 -11 0 -0.01 0.32 1 -11 0 0.13 0.34 11 -1 0 0.22 0.52 11 -1 0 0.81 0.57 -1 11 0 0.28 0.47 11 1 0 0.25 0.56 11 1 0 0.42 0.43 -1 -11 0 0.40 0.36 -1 -11 0 0.41 0.62 11 -1 0 0.50 0.57 1 -11 0 0.53 0.63 1 11 0 0.16 0.37 11 -2 0 47.59 1.95 2 -11 0 48.62 1.92 -2 11 0 47.43 1.93 -2 -11 0 49.45 1.95 11 2 0 47.62 1.91 2 11 0 46.20 1.93 11 -2 0 47.99 1.92 11 2 0 49.69 1.97 11 -2 0 48.21 2.00 -2 -11 0 51.88 2.15 -3 -11 0 3.19 0.95 11 -3 0 3.07 0.66 3 -11 0 2.66 0.49 -3 -11 0 3.68 0.65 3 -11 0 3.62 0.82 -3 11 0 2.94 0.60 11 -3 0 4.03 0.67 11 3 0 3.55 0.73 11 3 0 2.50 0.67 3 11 0 3.19 0.51 11 -3 0 3.80 0.71 11 4 0 2.37 0.67 11 -4 0 1.27 0.61 11 -4 0 3.81 0.68 4 -11 0 4.18 0.86 -4 -11 0 3.09 0.54 11 4 0 2.45 0.54 4 -11 0 2.25 0.48 -4 11 0 2.87 0.61 4 11 0 2.50 0.57 11 5 0 77.31 2.92 11 -5 0 84.10 2.82 5 -11 0 79.44 3.14 11 -5 0 81.22 2.90 5 -11 0 85.17 2.93 -5 11 0 80.52 2.86 -5 -11 0 81.43 2.96 11 5 0 84.41 2.99 5 11 0 77.56 2.84 11 6 0 40.13 1.75 -6 11 0 40.68 1.80 6 -11 0 43.45 2.07 -11 -6 0 41.89 1.83 6 11 0 41.47 1.72 11 -6 0 39.95 1.74 -6 -11 0 40.60 1.77 11 6 0 39.77 1.75 6 -11 0 42.49 1.82 -7 11 0 154.10 5.03 11 7 0 151.23 5.03 11 7 0 150.59 5.00 -11 -7 0 151.18 5.10 7 -11 0 155.22 4.98 11 -7 0 147.12 4.98 -7 -11 0 156.42 5.05 7 -11 0 156.86 5.30 7 11 0 152.26 4.97 -8 -11 0 76.42 2.87 11 8 0 77.38 2.82 8 11 0 75.58 2.78 11 8 0 78.47 2.91 -8 11 0 77.99 2.83 8 -11 0 78.22 2.81 11 -8 0 75.86 2.89 -11 -8 0 74.18 2.95 8 -11 0 77.28 3.12 9 11 0 0.97 0.48 9 -11 0 2.03 1.02 11 -9 0 0.82 0.54 9 -11 0 -0.28 0.64 11 9 0 0.92 0.71 -9 11 0 0.92 0.63 11 9 0 1.02 0.72 10 -11 0 12.45 1.70 10 11 0 16.89 1.22 -10 11 0 18.78 1.56 11 -10 0 10.84 1.42 11 10 0 16.88 1.24 11 11 0 29.87 1.66 11 -11 0 33.98 1.89 12 0 0 0.07 0.56 12 0 0 1.29 0.63 12 0 0 0.29 0.59 0 -12 0 0.68 0.67 0 12 0 0.49 0.40 0 -12 0 0.94 0.40 12 -1 0 7.95 0.98 12 -1 0 8.79 0.92 -1 -12 0 8.20 0.89 12 1 0 8.96 0.93 12 1 0 8.16 1.00 1 -12 0 6.57 1.01 12 -1 0 8.67 0.80 -1 12 0 6.92 0.88 1 -12 0 8.21 0.86 -1 -12 0 6.45 0.87 1 12 0 7.23 0.89 12 -2 0 44.57 1.95 2 12 0 44.66 1.88 12 -2 0 44.43 1.90 12 2 0 44.90 1.92 -2 12 0 44.80 1.88 12 2 0 46.26 1.98 12 -2 0 43.07 1.96 2 -12 0 48.33 1.88 -2 -12 0 48.28 2.11 -2 -12 0 45.27 1.91 2 -12 0 42.28 2.01 -3 12 0 3.94 0.57 12 3 0 4.29 0.77 -3 -12 0 4.68 0.95 -3 -12 0 4.01 0.66 12 -3 0 3.60 0.62 3 -12 0 4.90 0.80 3 12 0 3.91 0.69 12 3 0 4.59 0.71 12 -3 0 4.79 0.71 12 -3 0 3.72 0.69 3 -12 0 3.47 0.81 12 -4 0 28.35 1.49 4 12 0 28.36 1.40 -4 -12 0 24.68 1.39 4 -12 0 27.80 1.39 12 -4 0 26.07 1.34 12 4 0 26.28 1.46 12 -4 0 23.85 1.46 4 -12 0 26.49 1.52 12 4 0 26.27 1.44 -4 12 0 25.78 1.39 5 12 0 2.27 0.61 5 -12 0 1.04 0.57 12 -5 0 1.46 0.51 -5 -12 0 1.65 0.52 12 -5 0 2.20 0.65 -5 12 0 2.14 0.60 5 -12 0 1.13 0.86 12 5 0 0.78 0.53 12 5 0 1.13 0.63 12 -6 0 66.30 2.75 6 -12 0 76.51 2.78 12 6 0 75.30 2.80 -6 12 0 75.42 2.73 6 12 0 71.44 2.68 12 6 0 71.10 2.73 -6 -12 0 73.83 2.76 6 -12 0 81.51 3.08 7 -12 0 6.56 0.90 7 -12 0 7.09 0.99 -7 -12 0 8.12 1.06 -7 12 0 6.89 0.98 12 7 0 7.03 0.82 7 12 0 7.53 0.76 12 -7 0 6.71 0.85 8 12 0 8.68 0.84 12 8 0 8.59 1.03 8 -12 0 7.90 1.06 8 -12 0 5.95 0.90 -8 12 0 9.13 1.04 -9 12 0 -0.01 0.66 12 9 0 -0.10 0.65 9 -12 0 -0.06 0.77 9 12 0 0.62 0.69 12 -10 0 37.96 2.09 10 -12 0 42.38 2.13 12 10 0 38.43 1.80 10 12 0 38.90 1.88 12 -11 0 2.47 0.88 11 -12 0 3.91 1.05 11 12 0 1.94 0.64 12 11 0 2.60 0.70 12 12 0 6.68 1.00 12 -12 0 5.30 1.31 13 0 0 -0.55 0.55 0 -13 0 -0.06 0.49 0 13 0 -0.80 0.34 0 -13 0 -0.39 0.60 13 0 0 0.04 0.42 13 0 0 0.52 0.58 13 1 0 17.91 1.15 13 -1 0 17.61 1.13 13 -1 0 18.43 1.30 1 -13 0 18.65 1.29 -1 -13 0 18.81 1.20 -1 -13 0 19.60 1.33 -1 13 0 20.37 1.20 13 1 0 19.23 1.24 1 13 0 17.27 1.17 1 -13 0 19.60 1.10 13 -1 0 18.68 1.22 2 -13 0 4.25 0.90 13 -2 0 2.84 0.70 2 -13 0 3.36 0.56 2 13 0 2.99 0.56 -2 13 0 2.71 0.66 13 2 0 4.57 0.79 13 2 0 3.44 0.77 -2 -13 0 4.14 0.92 -2 -13 0 4.60 0.68 13 -2 0 3.21 0.73 13 -2 0 2.88 0.60 13 -3 0 3.37 0.76 13 -3 0 4.55 0.81 3 13 0 4.11 0.74 13 3 0 4.68 0.80 13 -3 0 4.80 0.78 -3 -13 0 4.68 0.87 3 -13 0 4.31 1.00 -3 13 0 3.59 0.70 3 -13 0 4.28 0.69 13 3 0 5.51 0.84 -3 -13 0 6.08 0.90 4 -13 0 0.80 0.44 -4 13 0 0.76 0.55 13 -4 0 -0.22 0.63 13 -4 0 0.68 0.49 4 -13 0 -0.08 0.64 -4 -13 0 0.77 0.61 13 -4 0 -0.66 0.64 13 4 0 -0.13 0.61 13 4 0 0.12 0.51 4 13 0 0.33 0.45 -5 13 0 24.31 1.29 5 -13 0 25.02 1.56 -5 -13 0 25.86 1.49 5 13 0 25.37 1.41 13 5 0 25.71 1.71 5 -13 0 23.89 1.38 13 5 0 25.40 1.47 13 -5 0 23.86 1.52 13 -5 0 26.23 1.41 6 -13 0 7.95 1.20 -6 -13 0 9.04 1.13 -6 13 0 9.77 1.07 6 -13 0 8.67 1.07 13 6 0 8.92 0.88 6 13 0 12.14 1.04 7 -13 0 49.84 2.36 7 -13 0 44.77 2.47 7 13 0 53.70 2.17 13 7 0 50.20 2.09 -7 13 0 50.37 2.19 13 8 0 6.67 0.98 8 -13 0 6.42 1.78 9 -13 0 32.97 1.89 13 9 0 32.40 1.73 9 13 0 32.33 1.68 13 -10 0 0.78 0.74 10 13 0 1.07 0.77 13 10 0 1.29 0.80 10 -13 0 1.21 0.93 11 13 0 14.63 1.27 13 -11 0 15.28 1.49 13 11 0 16.22 1.29 11 -13 0 15.09 1.40 13 -12 0 31.18 2.04 12 -13 0 27.27 2.02 13 12 0 36.57 1.80 12 13 0 33.72 1.77 13 13 0 27.27 1.60 13 -13 0 22.62 1.72 0 14 0 6.55 0.77 14 0 0 6.60 0.98 0 -14 0 7.30 0.96 0 -14 0 6.32 0.94 1 -14 0 0.17 0.68 14 1 0 0.82 0.69 1 -14 0 0.54 0.55 -1 -14 0 -0.70 0.57 14 -1 0 1.25 0.73 1 14 0 -0.25 0.53 -1 14 0 0.60 0.57 -1 -14 0 -0.24 0.86 2 14 0 64.94 2.51 2 -14 0 62.97 2.70 -2 -14 0 63.53 2.76 -2 -14 0 61.71 2.45 -2 14 0 62.94 2.51 14 -2 0 62.90 2.50 14 2 0 67.00 2.55 2 -14 0 64.75 2.51 3 -14 0 21.44 1.32 3 14 0 17.77 1.30 -3 14 0 20.56 1.34 3 -14 0 17.72 1.47 14 -3 0 18.57 1.27 14 3 0 20.42 1.34 -3 -14 0 20.27 1.44 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9.54 1.28 16 -3 -4 12.71 1.25 16 3 4 12.91 1.17 3 16 -4 12.52 1.19 16 3 -4 12.14 1.28 16 -3 4 8.57 1.29 -3 -16 4 12.20 1.28 3 -16 -4 10.96 1.35 4 16 -4 1.89 0.77 4 -16 4 -0.27 0.80 16 4 -4 1.49 0.86 4 -16 -4 0.88 1.68 5 -16 4 7.49 1.14 16 5 4 7.58 1.11 5 16 -4 9.28 1.09 16 5 -4 9.20 1.20 5 -16 -4 12.64 1.43 6 16 -4 77.95 3.08 16 6 4 83.22 3.14 16 6 -4 80.89 3.15 16 7 4 3.53 0.90 7 -16 4 3.15 1.02 7 16 -4 3.73 0.92 16 7 -4 4.39 0.93 7 -16 -4 2.93 1.02 16 8 4 3.98 0.93 8 -16 4 2.13 0.97 8 16 -4 4.79 0.93 16 8 -4 4.27 0.97 8 -16 -4 1.67 0.92 9 16 -4 1.15 0.80 16 9 4 -1.29 0.67 9 -16 4 0.29 0.87 16 9 -4 0.60 0.84 9 -16 -4 1.36 1.17 10 16 -4 2.90 0.89 16 10 4 3.13 0.84 10 -16 4 2.63 1.03 10 -16 -4 3.89 1.32 16 -10 4 2.01 0.97 16 10 -4 3.30 0.78 11 16 -4 7.25 1.12 11 -16 4 5.78 1.44 16 -11 -4 6.79 1.17 16 11 4 5.84 0.98 11 -16 -4 3.66 1.42 11 16 4 7.95 1.10 16 11 -4 7.53 1.17 16 -11 4 6.09 1.20 16 12 4 23.32 1.54 12 16 -4 22.96 1.57 16 -12 -4 23.55 1.77 12 -16 4 21.01 1.72 16 12 -4 21.51 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39.20 1.45 0 -6 -9 38.98 1.28 0 6 9 37.09 1.27 0 -6 9 39.28 1.50 6 0 -9 39.03 1.51 6 0 -9 38.98 1.59 6 0 9 38.05 1.47 0 6 -9 38.19 1.35 0 -6 9 39.23 1.69 0 6 -9 39.32 1.51 -6 0 9 37.92 1.54 1 6 -9 92.53 2.94 6 1 9 87.70 3.04 -6 -1 9 91.02 3.06 1 -6 9 97.80 3.28 -1 6 9 90.11 2.83 -1 -6 -9 93.67 2.87 6 -1 -9 92.34 3.07 1 6 -9 97.16 3.12 6 -1 -9 94.54 3.04 1 -6 9 89.29 3.05 -1 6 -9 86.88 2.83 6 1 -9 91.77 3.10 -1 6 -9 96.84 3.11 1 -6 -9 95.30 2.90 6 1 -9 92.57 3.03 6 -1 9 94.72 3.09 -1 -6 9 99.31 3.29 -1 -6 9 93.49 3.07 1 6 9 93.43 2.85 1 -6 -9 90.81 2.83 2 6 -9 28.25 1.30 2 -6 9 30.63 1.43 -2 6 9 27.00 1.01 2 -6 9 28.30 1.23 -6 -2 9 27.43 1.22 2 6 -9 28.59 1.17 -6 2 -9 29.40 1.23 6 -2 -9 28.17 1.20 6 2 9 28.06 1.23 6 2 9 26.74 1.14 -2 -6 -9 27.49 1.06 6 -2 9 28.26 1.29 2 6 9 26.64 1.04 -2 6 -9 28.95 1.23 -2 -6 9 25.69 1.41 6 2 -9 30.28 1.33 6 2 -9 29.53 1.28 2 -6 -9 28.58 1.07 2 -6 -9 27.05 1.00 -2 -6 9 27.70 1.31 -6 -3 9 8.03 0.69 6 -3 -9 7.61 0.67 6 -3 -9 7.45 0.64 3 6 -9 7.70 0.72 3 6 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108.03 3.51 6 -6 9 103.99 3.37 6 6 -9 96.24 3.35 6 -6 -9 98.05 3.23 6 6 -9 99.86 3.38 6 -6 9 97.06 3.60 -6 6 -9 100.32 3.37 0 -7 -9 223.52 6.85 7 0 -9 224.78 7.05 -7 0 9 232.84 7.08 7 0 -9 227.87 7.05 0 -7 -9 236.89 6.95 7 0 9 242.87 7.09 0 -7 9 230.30 7.07 0 7 9 229.56 6.84 0 -7 9 230.89 7.29 0 7 -9 232.77 7.07 0 7 -9 221.85 6.86 -1 -7 -9 58.28 1.96 7 1 9 63.04 2.17 -7 -1 9 57.57 2.14 7 -1 -9 62.24 2.15 1 7 -9 62.94 2.16 1 -7 9 59.35 2.14 -1 7 9 59.07 1.93 1 7 -9 59.05 2.00 1 -7 9 59.91 2.35 -1 7 -9 58.07 1.89 -1 -7 9 57.55 2.18 7 -1 9 59.46 2.14 1 7 9 58.36 1.95 7 1 -9 57.89 2.20 1 -7 -9 60.57 2.01 -1 7 -9 61.45 2.21 7 1 -9 59.25 2.12 1 -7 -9 58.13 1.91 2 7 -9 2.04 0.50 -7 -2 9 3.28 0.52 7 2 9 3.35 0.48 2 -7 9 2.84 0.59 2 -7 9 3.97 0.82 7 -2 -9 4.14 0.63 7 2 9 2.78 0.45 -2 -7 -9 3.53 0.48 -2 7 9 2.77 0.42 7 2 -9 3.89 0.71 -2 -7 9 2.84 0.59 -2 -7 9 3.05 0.79 7 2 -9 2.95 0.57 2 -7 -9 3.44 0.43 2 -7 -9 2.86 0.44 2 7 9 3.06 0.46 7 -2 9 3.45 0.61 3 -7 9 53.20 1.97 -3 7 9 52.02 1.79 3 7 -9 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32.33 1.66 6 13 9 35.29 1.66 7 13 -9 1.28 0.75 -7 13 9 0.41 0.70 7 -13 9 1.89 0.93 -7 -13 -9 1.93 0.77 13 -7 -9 1.64 0.74 7 -13 -9 1.11 0.70 13 7 -9 1.10 0.85 7 13 9 2.36 0.69 7 -13 -9 0.72 0.69 -8 -13 -9 20.47 1.54 8 13 -9 22.20 1.43 8 -13 9 22.87 1.63 8 -13 -9 20.45 1.46 13 8 -9 23.38 1.51 8 13 9 24.39 1.45 9 13 -9 9.02 1.13 9 -13 9 10.63 1.42 9 13 9 12.89 1.45 13 -9 9 8.83 1.29 9 -13 -9 8.98 1.30 13 9 -9 9.96 1.18 10 -13 9 28.90 1.86 10 13 -9 27.72 1.64 13 -10 9 28.32 1.82 13 10 -9 28.06 1.69 10 -13 -9 26.31 1.74 11 13 -9 6.12 1.04 13 -11 -9 8.12 1.15 11 -13 9 5.74 1.12 13 11 -9 5.26 0.89 13 -11 9 7.02 1.19 11 -13 -9 6.66 1.41 12 -13 9 10.69 1.31 12 13 -9 9.80 1.25 13 -12 -9 11.49 1.51 13 12 -9 9.36 1.23 13 -12 9 7.63 1.25 12 -13 -9 10.66 1.29 13 -13 -9 -0.93 1.14 13 -13 9 0.38 0.93 13 13 -9 -0.80 0.78 14 0 9 67.04 2.66 14 0 -9 69.44 2.76 0 -14 -9 69.32 2.88 0 -14 -9 74.05 2.70 0 14 9 68.84 2.65 1 -14 9 63.21 2.89 14 1 9 63.52 2.54 -1 -14 -9 64.70 2.50 14 -1 -9 65.47 2.62 -1 14 9 65.09 2.52 14 -1 9 65.68 2.52 1 -14 -9 67.07 2.50 1 14 9 65.68 2.53 14 1 -9 66.22 2.62 1 -14 -9 62.36 2.76 2 -14 9 16.60 1.35 14 -2 -9 11.30 1.39 -2 14 9 15.12 1.20 14 2 9 15.03 1.18 -2 -14 -9 14.65 1.22 14 2 -9 12.24 1.07 2 -14 -9 16.75 1.21 14 -2 9 16.30 1.20 2 14 9 13.46 1.21 3 14 -9 41.16 1.87 -3 -14 -9 43.35 2.01 3 -14 9 41.01 2.20 -3 14 9 42.91 1.95 14 3 -9 43.14 2.03 14 -3 9 43.16 1.94 3 14 9 43.23 1.90 3 -14 -9 45.55 1.89 -4 -14 -9 2.55 0.73 -4 14 9 2.73 0.74 4 14 -9 2.70 0.74 4 -14 9 4.06 1.03 14 4 9 2.45 0.73 -4 -14 9 2.94 1.15 4 -14 -9 2.83 0.71 4 14 9 2.56 0.77 14 4 -9 2.47 0.88 5 14 -9 13.32 1.22 -5 14 9 10.38 1.50 14 5 9 14.35 1.18 -5 -14 -9 14.70 1.37 5 -14 9 12.98 1.28 5 14 9 11.60 1.20 14 5 -9 14.59 1.29 -6 -14 -9 13.60 1.48 6 14 -9 10.76 1.16 14 6 9 12.69 1.18 6 -14 9 13.57 1.31 6 14 9 12.87 1.30 14 6 -9 14.43 1.32 7 14 -9 22.31 1.53 7 -14 9 20.88 1.63 -7 -14 -9 24.12 1.70 7 14 9 24.62 1.50 14 7 -9 24.06 1.56 8 -14 9 4.86 1.18 8 14 -9 3.38 0.86 14 8 -9 4.66 0.85 9 14 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15.78 1.17 5 15 -9 18.57 1.43 15 5 9 18.55 1.33 5 -15 9 18.49 1.64 15 5 -9 17.95 1.44 6 15 -9 9.50 1.13 6 -15 9 11.32 1.26 15 6 9 10.58 1.13 15 6 -9 11.77 1.29 15 7 9 17.11 1.28 7 15 -9 13.76 1.26 7 -15 9 14.54 1.44 15 7 -9 15.88 1.41 8 -15 9 44.75 2.34 8 15 -9 43.39 2.11 15 8 -9 44.16 2.17 9 15 -9 1.97 0.85 9 -15 9 1.74 1.02 15 9 9 1.66 0.80 15 9 -9 1.94 0.93 15 -9 9 1.41 0.85 10 15 -9 31.28 1.77 15 10 9 28.95 1.67 10 -15 9 27.50 1.88 15 10 -9 32.08 1.83 15 11 9 2.23 0.81 11 -15 9 0.66 0.94 11 15 -9 2.21 0.87 15 -11 -9 1.46 1.18 15 -11 9 2.60 1.11 15 11 -9 1.34 0.88 15 12 9 2.40 0.81 15 -12 -9 1.80 1.06 12 -15 9 0.75 0.96 12 15 -9 0.92 0.88 15 -12 9 1.38 1.04 15 12 -9 0.66 0.92 15 13 9 2.15 0.70 13 15 -9 1.18 0.91 15 -13 -9 2.81 1.47 13 -15 9 1.00 1.01 15 13 -9 1.81 0.98 15 -13 9 1.45 1.02 15 14 9 18.58 1.39 14 15 -9 17.19 1.45 14 -15 9 13.54 1.51 15 14 -9 15.94 1.44 15 -14 9 13.52 1.53 14 15 9 16.54 1.34 15 -15 9 0.62 1.27 15 15 9 0.46 0.80 16 0 9 12.10 1.31 0 -16 9 9.77 1.22 16 0 -9 11.21 1.26 1 -16 9 5.41 1.16 16 1 9 3.44 0.90 16 -1 -9 3.81 0.98 -1 -16 9 5.39 1.18 16 -1 9 4.65 0.96 16 1 -9 3.83 0.95 2 -16 9 0.12 0.78 16 2 9 0.62 0.76 16 -2 -9 0.61 0.87 -2 -16 9 0.67 0.91 16 2 -9 1.00 0.85 16 -2 9 0.35 0.90 16 3 9 1.73 0.81 3 -16 9 2.97 1.01 16 3 -9 1.81 0.88 -3 -16 9 2.06 1.03 4 -16 9 39.94 2.22 16 4 -9 44.72 2.13 16 5 9 2.51 0.82 5 -16 9 1.89 0.91 16 5 -9 2.15 0.94 6 16 -9 10.42 1.22 16 6 9 12.72 1.20 6 -16 9 15.79 1.43 16 6 -9 14.61 1.37 16 7 9 24.31 1.50 7 16 -9 20.18 1.50 7 -16 9 19.78 1.65 16 7 -9 23.18 1.43 16 8 9 7.86 1.10 8 -16 9 7.63 1.19 8 16 -9 6.60 1.06 16 8 -9 8.15 1.21 9 -16 9 2.50 1.08 9 16 -9 2.47 0.95 16 9 9 2.64 0.83 16 9 -9 3.25 0.99 16 -9 9 2.04 0.95 16 10 9 21.51 1.43 10 16 -9 20.26 1.61 10 -16 9 16.77 1.58 16 -10 9 18.41 1.60 16 10 -9 23.14 1.60 16 11 9 3.84 0.88 11 16 -9 3.02 0.99 11 -16 9 4.16 1.23 16 -11 -9 2.82 1.08 16 11 -9 2.73 1.01 16 -11 9 2.89 1.01 12 16 -9 -0.07 0.88 16 -12 -9 0.53 1.35 16 12 9 0.75 0.77 12 -16 9 -0.09 1.16 16 -12 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9.73 1.31 6 -18 9 2.86 0.99 18 6 9 4.89 0.98 18 6 -9 6.37 1.13 18 7 9 7.83 1.15 7 -18 9 5.59 1.13 18 7 -9 5.72 1.13 18 8 9 -0.15 0.80 8 -18 9 0.62 0.94 8 18 -9 0.57 0.99 18 8 -9 0.78 0.90 18 9 9 0.80 0.75 9 -18 9 1.09 0.96 9 18 -9 -0.42 0.92 18 -9 9 1.66 0.91 18 9 -9 1.32 0.95 10 -18 9 7.76 1.51 18 10 9 9.29 1.18 10 18 -9 7.40 1.31 18 -10 9 7.54 1.23 18 10 -9 7.79 1.23 11 18 -9 5.44 1.21 18 -11 -9 4.70 1.26 18 11 9 7.14 1.15 11 -18 9 7.10 1.27 18 -11 9 7.01 1.22 18 11 -9 6.14 1.13 12 -18 9 2.86 1.16 18 -12 -9 1.32 1.40 18 12 9 1.84 0.85 18 -12 9 2.05 1.07 18 12 -9 2.05 1.01 12 18 9 2.37 0.89 13 -18 9 21.46 1.76 13 18 -9 14.94 1.73 18 13 9 19.17 1.50 18 -13 9 15.21 1.63 13 18 9 18.69 1.43 19 0 9 9.96 1.45 19 0 -9 12.24 1.33 0 -19 9 9.81 1.30 19 1 9 5.40 1.14 1 -19 9 7.51 1.23 19 1 -9 5.70 1.09 -1 -19 9 7.19 1.20 2 -19 9 6.24 1.22 19 2 9 10.52 1.46 -2 -19 9 8.37 1.25 19 2 -9 9.67 1.30 19 3 9 8.42 1.25 3 -19 9 9.01 1.47 19 3 -9 8.98 1.31 19 4 9 0.62 0.89 4 -19 9 -0.26 0.91 19 4 -9 0.55 0.85 19 5 9 9.54 1.26 5 -19 9 7.14 1.44 19 5 -9 8.95 1.33 19 6 9 15.91 1.38 6 -19 9 13.42 1.46 19 6 -9 16.60 1.47 19 7 9 2.64 0.89 7 -19 9 2.01 1.04 19 7 -9 1.85 0.89 8 -19 9 1.45 1.02 19 8 9 2.49 0.90 19 8 -9 2.15 0.95 9 19 -9 -2.37 1.00 9 -19 9 0.78 0.99 19 9 -9 -0.31 0.90 19 -9 9 0.59 1.25 19 10 9 1.49 0.86 10 19 -9 -1.21 1.04 10 -19 9 0.85 1.03 19 10 -9 0.48 0.91 19 -10 9 1.02 0.83 11 19 -9 -0.83 1.50 11 -19 9 1.58 1.03 19 11 9 0.73 0.79 19 -11 9 1.20 0.89 19 11 -9 0.47 0.93 12 -19 9 15.61 1.53 19 -12 -9 16.70 2.02 12 19 -9 10.14 1.51 12 19 9 14.78 1.36 19 12 -9 12.28 1.44 19 -12 9 9.30 1.42 20 0 -9 17.57 1.52 0 -20 9 15.48 1.56 20 1 9 3.11 1.17 1 -20 9 1.98 1.00 -1 -20 9 4.75 1.23 20 1 -9 5.01 1.10 2 -20 9 8.59 1.51 20 2 9 5.45 1.26 20 2 -9 5.69 1.11 -2 -20 9 4.09 1.19 3 -20 9 2.53 1.10 20 3 9 3.87 1.09 20 3 -9 3.61 1.05 20 4 9 17.08 1.60 4 -20 9 14.72 1.71 20 4 -9 16.66 1.51 5 -20 9 3.66 1.19 20 5 9 5.59 1.11 20 5 -9 5.36 1.10 20 6 9 2.13 0.94 6 -20 9 1.72 1.08 20 6 -9 2.18 0.97 7 -20 9 2.25 1.15 20 7 -9 0.28 0.92 20 8 9 6.42 1.11 8 -20 9 8.02 1.28 20 8 -9 6.58 1.15 9 -20 9 1.45 1.08 20 9 9 2.87 0.94 20 9 -9 2.80 0.99 20 -9 9 1.77 1.00 10 -20 9 4.92 1.25 20 10 9 3.20 0.96 20 10 -9 3.60 1.03 20 -10 9 4.74 1.24 0 -21 9 0.55 0.98 21 1 9 3.44 1.26 1 -21 9 8.04 1.55 -1 -21 9 3.83 1.20 21 1 -9 5.96 1.14 21 2 9 12.75 1.81 2 -21 9 15.67 1.60 21 2 -9 14.18 1.58 3 -21 9 3.33 1.52 21 3 9 0.64 1.18 21 3 -9 3.89 1.06 21 4 9 11.52 1.58 4 -21 9 13.56 1.68 21 4 -9 12.77 1.48 5 -21 9 12.60 1.45 21 5 9 6.65 1.40 21 5 -9 10.55 1.47 21 6 9 10.70 1.36 6 -21 9 11.82 1.44 21 6 -9 10.70 1.40 21 7 9 4.32 1.03 7 -21 9 5.40 1.30 21 7 -9 3.93 1.11 8 -21 9 11.67 1.46 21 8 9 8.90 1.32 21 8 -9 9.30 1.35 21 -8 9 10.77 1.35 0 -22 9 1.49 1.33 1 -22 9 3.56 1.21 2 -22 9 0.57 1.26 22 2 9 -4.54 1.60 22 2 -9 -1.22 0.89 22 3 9 33.93 2.37 3 -22 9 39.61 2.38 22 3 -9 41.54 2.23 4 -22 9 0.63 1.07 22 4 9 -2.25 1.01 22 4 -9 0.35 0.89 22 5 9 -0.50 0.99 5 -22 9 2.01 1.36 22 5 -9 2.76 1.03 0 0 10 394.85 11.64 0 0 -10 406.39 11.65 0 0 -10 401.77 11.58 0 0 10 380.81 11.57 1 0 -10 212.68 6.29 1 0 -10 214.84 6.36 1 0 10 217.48 6.37 1 0 10 217.98 6.31 0 -1 10 216.97 6.42 0 1 -10 209.40 6.33 -1 0 -10 219.96 6.31 0 -1 10 203.73 6.33 -1 0 10 219.11 6.37 0 -1 -10 202.70 6.24 0 1 10 199.98 6.23 0 1 10 209.60 6.27 0 -1 -10 220.67 6.39 -1 0 10 213.83 6.30 -1 -1 -10 83.77 2.76 -1 -1 10 89.11 2.80 1 -1 -10 82.52 2.76 1 1 10 84.86 2.63 -1 1 -10 89.03 2.73 1 -1 -10 88.50 2.62 1 -1 10 89.40 2.80 1 1 10 88.43 2.68 -1 -1 -10 89.19 2.64 -1 -1 10 84.55 2.71 -1 1 10 83.47 2.62 1 1 -10 90.21 2.72 1 -1 10 85.61 2.72 2 0 10 34.34 1.23 2 0 -10 35.78 1.29 0 -2 -10 33.80 1.28 -2 0 -10 33.97 1.23 0 -2 10 34.41 1.29 0 2 10 32.40 1.05 0 2 -10 35.81 1.31 0 -2 10 36.44 1.41 0 2 10 34.28 1.04 2 0 10 36.42 1.31 -2 0 10 34.49 1.22 2 0 -10 35.51 1.20 -2 -1 10 251.38 7.47 1 -2 10 255.90 7.60 -2 1 -10 248.20 7.47 2 1 10 248.59 7.40 1 -2 10 244.59 7.48 -2 -1 10 261.81 7.58 2 -1 -10 246.36 7.38 -1 -2 -10 250.74 7.49 1 2 -10 255.69 7.49 -1 2 -10 255.25 7.49 -1 -2 10 260.76 7.60 1 2 10 243.25 7.33 -2 1 10 244.89 7.39 -2 -1 -10 240.14 7.48 2 -1 10 267.75 7.58 -1 -2 10 251.76 7.48 2 1 -10 241.78 7.45 2 1 -10 254.82 7.45 -2 -1 -10 247.39 7.41 1 2 10 251.77 7.36 2 -1 10 248.28 7.46 2 -2 10 2.34 0.54 -2 -2 10 2.06 0.52 2 2 -10 1.17 0.30 2 2 10 1.47 0.26 2 -2 10 1.93 0.33 -2 2 -10 2.00 0.43 2 -2 -10 1.62 0.26 -2 -2 10 1.98 0.40 -2 -2 -10 1.51 0.44 0 -3 10 488.14 14.78 3 0 10 515.54 14.63 -3 0 -10 477.81 14.62 0 -3 10 498.25 14.66 0 3 -10 518.19 14.67 3 0 -10 495.94 14.59 -3 0 10 493.96 14.61 1 -3 10 46.19 1.65 3 -1 -10 45.58 1.51 3 1 10 46.54 1.55 1 -3 10 44.60 1.77 -3 1 -10 44.48 1.61 -3 -1 10 42.92 1.60 1 3 -10 46.14 1.64 3 -1 10 43.78 1.56 1 3 10 44.35 1.37 -1 -3 10 44.13 1.72 3 1 -10 46.48 1.54 1 3 10 43.55 1.37 3 1 -10 46.94 1.59 -1 -3 10 45.76 1.64 -3 1 10 45.10 1.53 -1 3 -10 45.83 1.60 2 3 -10 22.07 1.01 2 -3 10 18.37 1.27 -3 2 -10 24.49 1.06 -3 -2 10 23.76 0.99 3 -2 -10 23.83 0.87 2 -3 10 23.87 1.00 -2 -3 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1.38 4 2 10 34.14 1.27 -4 -2 10 33.77 1.31 2 4 -10 31.16 1.29 -4 2 -10 34.23 1.37 4 -2 -10 32.98 1.22 4 2 10 34.22 1.26 2 4 -10 33.73 1.30 -2 4 -10 35.59 1.33 4 2 -10 32.56 1.38 -2 -4 10 32.33 1.31 2 -4 -10 32.84 1.07 2 4 10 32.81 1.12 -4 -2 -10 32.85 1.29 4 -2 10 31.78 1.28 -2 -4 10 35.84 1.50 4 2 -10 32.53 1.33 2 -4 -10 33.16 1.05 4 2 -10 33.89 1.21 2 -4 -10 33.53 1.06 4 3 10 51.82 1.81 -4 -3 10 52.97 1.91 4 3 10 52.97 1.83 4 -3 -10 51.38 1.76 4 -3 -10 53.53 1.78 3 -4 10 53.96 2.08 -4 3 -10 51.49 1.89 3 4 -10 52.78 1.93 3 -4 10 55.00 1.91 3 4 -10 52.41 1.90 4 3 -10 54.20 1.90 4 3 -10 52.62 1.76 -3 -4 10 56.16 2.15 3 4 10 54.13 1.77 4 -3 10 50.13 2.04 3 -4 -10 53.43 1.70 -4 -3 -10 54.88 1.87 3 -4 -10 54.48 1.71 -3 -4 10 55.84 1.97 4 3 -10 54.60 1.89 -3 4 -10 57.65 1.98 4 -3 10 52.63 1.90 4 -4 -10 5.58 0.49 -4 -4 10 4.60 0.73 4 -4 -10 4.99 0.48 -4 4 -10 4.96 0.58 4 4 10 5.65 0.50 4 -4 10 4.47 0.57 4 4 -10 4.12 0.54 4 4 -10 5.93 0.72 0 -5 10 74.31 2.45 0 -5 10 71.13 2.62 0 5 10 73.37 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0.20 0.91 3 -20 13 9.37 1.34 20 3 13 11.31 1.47 20 3 -13 10.30 1.35 4 -20 13 -0.44 0.92 20 4 13 -0.32 0.90 20 5 13 3.87 1.08 5 -20 13 4.39 1.93 20 5 -13 3.25 1.03 6 -20 13 0.41 1.20 20 6 -13 -0.59 0.87 20 7 13 -0.29 0.89 7 -20 13 -0.44 1.16 20 7 -13 -0.85 0.84 20 -7 13 -0.08 0.94 20 8 13 4.81 1.02 8 -20 13 6.70 1.25 20 8 -13 4.40 1.06 9 -20 13 2.43 1.14 20 9 13 1.44 0.90 20 9 -13 1.82 1.01 20 -9 13 3.14 1.07 0 -21 13 34.12 2.17 1 -21 13 -0.16 0.92 -1 -21 13 0.03 0.97 2 -21 13 15.03 1.56 21 3 13 -2.66 1.06 3 -21 13 1.69 1.29 21 3 -13 0.51 0.89 21 4 13 3.36 1.23 4 -21 13 3.78 1.12 21 4 -13 2.90 1.02 5 -21 13 2.78 1.12 21 5 13 2.55 1.08 21 5 -13 3.87 1.04 6 -21 13 6.69 1.26 21 6 13 4.93 1.16 21 6 -13 5.49 1.07 0 -22 13 0.54 1.07 1 -22 13 13.05 1.73 2 -22 13 3.12 1.15 0 0 -14 318.82 9.24 0 0 14 302.23 9.23 0 0 -14 314.20 9.34 0 0 14 316.51 9.32 1 0 -14 50.70 1.81 -1 0 14 51.93 1.68 0 1 -14 52.89 1.75 0 1 14 49.40 1.62 0 -1 14 49.70 1.83 -1 0 14 51.66 1.78 -1 0 -14 52.50 1.71 0 -1 -14 49.44 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-14 35.14 1.46 2 4 14 36.23 1.18 -2 -4 14 37.25 1.50 -2 4 -14 36.62 1.51 4 -2 14 37.75 1.47 4 -3 -14 46.47 1.54 3 -4 14 46.48 1.80 -4 -3 14 47.24 1.79 4 3 14 46.30 1.64 3 4 -14 47.04 1.77 3 -4 14 48.33 1.99 4 3 14 46.66 1.63 -4 3 -14 50.94 1.77 4 3 -14 47.77 1.67 -3 4 -14 46.56 1.81 3 -4 -14 45.48 1.42 3 4 14 45.24 1.55 -4 -3 -14 43.88 1.74 -3 -4 14 47.88 1.81 4 -3 14 46.06 1.97 4 3 -14 46.59 1.82 -3 -4 14 41.94 1.94 3 4 14 45.74 1.55 3 -4 -14 44.70 1.42 4 3 -14 44.78 1.70 4 -3 14 49.60 1.80 4 4 14 59.33 1.97 4 -4 14 60.65 2.12 -4 4 -14 59.45 2.17 4 -4 -14 56.36 1.87 4 -4 14 57.91 2.30 4 -4 -14 58.56 1.87 4 4 -14 57.52 2.13 4 4 14 59.46 1.97 4 4 -14 58.46 2.16 0 5 -14 83.61 2.82 5 0 14 81.27 2.71 0 -5 14 80.32 2.96 -5 0 14 81.65 2.73 5 0 -14 83.19 2.70 -5 -1 14 67.47 2.33 1 -5 14 56.36 2.44 1 -5 14 71.35 2.57 1 5 -14 70.84 2.40 5 1 14 66.88 2.28 5 -1 -14 70.35 2.25 -5 1 -14 68.12 2.33 -1 5 -14 67.60 2.38 -5 1 14 65.23 2.27 -1 -5 14 61.79 2.54 5 1 -14 65.53 2.28 5 -1 14 66.19 2.31 5 2 14 92.60 3.00 -5 -2 14 92.37 3.09 2 -5 14 82.20 3.26 2 -5 14 89.14 3.09 2 5 -14 93.17 3.07 5 -2 -14 92.40 2.94 -5 2 -14 95.30 3.09 2 5 14 90.12 2.76 5 -2 14 90.90 3.06 -2 -5 14 92.58 3.11 -2 -5 14 93.85 3.33 -5 -2 -14 95.14 3.04 2 5 14 89.32 2.75 5 2 -14 97.21 2.98 5 -2 14 94.37 3.30 5 2 -14 94.06 3.05 -2 5 -14 90.36 3.11 -5 -3 14 14.45 0.97 5 -3 -14 14.23 0.74 3 -5 14 14.48 1.00 3 5 -14 13.24 0.96 -5 3 -14 14.31 0.85 3 5 -14 15.11 0.94 5 3 14 14.62 0.81 5 3 14 14.30 0.84 5 3 -14 13.55 0.89 5 -3 14 15.19 0.97 -3 -5 14 12.37 0.95 -3 -5 14 14.58 1.15 3 5 14 14.62 0.64 3 5 14 14.18 0.66 -3 5 -14 14.94 0.90 5 3 -14 14.25 0.76 5 3 -14 13.37 0.91 5 -3 14 14.17 1.02 -5 -3 -14 15.73 0.91 3 -5 -14 13.49 0.48 4 5 -14 84.57 2.95 5 4 14 89.33 2.88 4 -5 14 89.25 3.23 5 4 14 86.80 2.86 -5 4 -14 91.34 3.04 5 -4 -14 88.17 2.78 5 -4 -14 89.17 2.79 4 -5 14 90.55 2.99 -5 -4 14 89.19 3.03 4 5 -14 89.29 2.99 -4 -5 14 84.15 3.25 5 4 -14 86.96 3.02 5 -4 14 91.68 2.98 4 5 14 89.65 2.81 -5 -4 -14 88.24 2.94 4 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26.23 1.73 6 -9 21 23.69 1.64 9 -6 21 25.18 1.68 7 -9 21 12.35 1.33 7 9 -21 15.86 1.32 9 7 -21 15.70 1.33 9 -7 21 14.31 1.34 8 -9 21 7.37 1.14 8 9 -21 5.94 1.01 9 -8 21 5.55 1.16 9 8 -21 6.19 1.03 9 9 -21 3.43 0.95 9 -9 21 3.62 1.14 10 0 21 15.78 1.20 0 -10 21 12.89 1.25 10 0 -21 16.01 1.15 10 1 21 32.24 1.68 1 -10 21 32.99 1.89 10 1 21 32.19 1.74 10 -1 -21 37.03 1.64 10 1 -21 35.20 1.66 -10 -1 -21 33.49 1.62 10 -1 21 32.99 1.71 -1 -10 21 30.51 1.90 10 2 21 27.04 1.56 10 2 21 26.23 1.50 2 -10 21 24.83 1.69 10 -2 -21 29.53 1.49 -10 -2 21 27.38 1.62 10 -2 21 22.88 1.67 -10 -2 -21 26.98 1.41 -2 -10 21 26.06 1.81 10 2 -21 27.45 1.48 10 -3 -21 4.73 0.75 -10 -3 21 3.85 0.86 10 3 21 4.61 0.79 10 -3 -21 6.54 0.94 3 -10 21 5.64 1.02 10 3 21 7.62 1.03 10 3 -21 5.17 0.75 -10 -3 -21 3.26 0.75 10 -3 21 2.82 0.90 -3 -10 21 5.71 1.15 10 4 21 8.60 1.09 4 -10 21 6.73 1.07 10 4 21 8.50 1.05 10 -4 21 7.08 1.06 -10 -4 -21 7.51 0.95 -4 -10 21 7.83 1.12 10 4 -21 6.43 0.99 10 5 21 1.19 0.76 5 -10 21 1.44 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26.91 1.28 0 -8 22 24.47 1.40 0 8 -22 23.15 1.41 0 -8 22 19.08 1.49 8 0 22 24.58 1.35 -8 0 -22 24.23 1.32 8 1 22 30.05 1.52 1 -8 22 31.88 1.79 1 8 -22 29.37 1.61 8 -1 -22 32.89 1.49 1 -8 22 29.86 1.49 -8 -1 22 32.60 1.62 -1 -8 22 33.36 1.84 8 -1 22 35.91 1.82 -8 -1 -22 34.96 1.58 -1 -8 22 31.46 1.53 8 1 -22 34.46 1.57 8 -1 22 33.06 1.61 -1 8 -22 30.91 1.52 2 -8 22 7.18 1.00 8 2 22 10.26 1.08 8 2 22 9.25 1.01 -8 -2 22 8.51 1.00 2 -8 22 8.36 0.99 2 8 -22 7.33 0.83 8 -2 -22 9.24 0.84 8 -2 22 8.14 0.97 -2 -8 22 7.67 1.03 -8 -2 -22 8.65 0.92 -2 8 -22 8.12 1.02 8 2 -22 9.52 0.91 -2 -8 22 8.35 1.02 8 -2 22 8.09 0.96 -8 -3 22 9.95 1.09 8 3 22 7.88 0.92 3 -8 22 9.32 1.08 8 -3 -22 10.75 0.85 3 8 -22 7.88 0.87 8 3 22 8.95 1.04 3 -8 22 8.62 1.24 8 -3 -22 10.56 0.91 -3 8 -22 8.08 0.86 8 -3 22 7.66 1.00 -8 -3 -22 7.28 0.93 -3 -8 22 7.65 1.08 8 3 -22 9.55 0.94 8 -3 22 10.35 1.07 -3 -8 22 7.46 1.07 -8 4 -22 4.45 0.68 4 8 -22 2.67 0.73 -8 -4 22 4.27 0.75 8 4 22 5.56 0.77 4 -8 22 5.14 1.07 8 4 22 4.73 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1.37 5 -2 28 21.30 1.38 3 -5 28 2.61 1.02 -5 3 -28 2.85 0.79 -5 -3 28 3.81 0.82 3 5 -28 3.84 0.84 3 -5 28 3.03 0.75 3 5 -28 3.14 0.76 5 -3 28 5.02 1.13 -3 5 -28 4.45 0.83 -3 -5 28 3.49 0.81 -5 -3 -28 3.22 0.78 5 -3 28 6.46 1.01 -5 4 -28 0.51 0.72 -5 -4 28 2.17 0.82 4 5 -28 -0.04 0.73 4 -5 28 1.14 0.82 4 5 -28 0.50 0.67 5 4 -28 -1.27 0.68 5 -4 28 1.20 0.79 -4 -5 28 0.99 0.72 5 -4 28 2.17 0.71 -4 5 -28 0.00 0.69 5 5 -28 8.91 1.38 5 5 -28 9.54 1.59 -5 -5 28 10.52 1.35 5 -5 28 9.10 1.44 0 6 -28 46.01 2.16 0 -6 28 50.01 2.36 -6 0 -28 47.46 1.98 1 6 -28 26.86 1.63 -6 1 -28 26.42 1.46 1 -6 28 24.93 1.78 1 6 -28 27.79 1.44 6 -1 28 25.60 1.71 -1 -6 28 29.19 1.73 -6 -1 -28 26.70 1.49 2 6 -28 12.20 1.23 2 -6 28 15.47 1.30 2 6 -28 13.93 1.12 -6 2 -28 13.70 1.14 6 -2 28 13.89 1.37 -2 6 -28 11.46 1.27 6 -2 28 14.64 1.22 -2 -6 28 12.20 1.41 -6 -2 -28 12.53 1.12 3 6 -28 32.69 1.62 -6 3 -28 31.49 1.75 -6 -3 -28 29.61 1.61 6 -3 28 32.13 1.75 6 -3 28 33.97 1.87 4 6 -28 22.99 1.39 -6 -4 28 28.08 2.19 -6 4 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1.09 8 -3 28 1.04 1.07 4 -8 28 9.14 1.16 4 8 -28 8.01 1.10 8 -4 28 6.29 1.12 5 -8 28 28.03 1.94 5 8 -28 28.48 1.60 8 -5 28 24.69 1.90 6 -8 28 14.18 1.54 6 8 -28 14.38 1.33 8 -6 28 16.70 1.46 7 -8 28 16.37 1.46 8 -7 28 16.31 1.67 8 -8 28 16.32 1.66 -9 0 -28 20.55 1.33 0 -9 28 21.80 1.62 -9 1 -28 1.13 0.70 1 -9 28 0.99 1.04 -9 -1 -28 0.72 0.73 9 -1 28 0.92 1.27 -1 -9 28 0.83 0.91 2 -9 28 20.90 1.57 -9 2 -28 21.18 1.35 -2 -9 28 21.01 1.63 9 -2 28 21.38 1.58 -9 -2 -28 19.73 1.34 3 -9 28 2.57 0.98 -9 -3 -28 3.23 0.84 -3 -9 28 3.78 1.16 9 -3 28 4.72 1.33 4 9 -28 43.93 2.05 4 -9 28 44.21 2.34 9 -4 28 42.62 2.32 5 -9 28 10.88 1.29 5 9 -28 11.88 1.25 9 -5 28 11.09 1.31 6 9 -28 1.09 0.83 6 -9 28 0.65 0.89 9 -6 28 0.59 1.19 7 -9 28 13.76 1.58 9 -7 28 14.70 1.64 8 -9 28 2.88 1.08 9 -8 28 2.94 1.08 9 -9 28 2.72 1.05 0 -10 28 19.30 1.56 -10 0 -28 17.79 1.30 1 -10 28 25.32 1.73 -10 1 -28 22.63 1.41 -1 -10 28 21.42 1.72 -10 -1 -28 23.57 1.46 -10 2 -28 7.18 0.99 2 -10 28 8.09 1.17 10 -2 28 7.01 1.47 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10.40 1.36 11 -10 28 9.60 1.55 11 -11 28 -0.23 1.19 0 -12 28 2.00 1.01 -12 0 -28 0.58 0.75 1 -12 28 5.56 1.25 -12 1 -28 5.02 0.92 12 -1 28 4.00 1.21 -12 -1 -28 4.67 0.93 -1 -12 28 1.95 1.21 2 -12 28 13.48 1.41 -12 2 -28 12.92 1.21 -12 -2 -28 14.11 1.33 12 -2 28 14.21 1.48 -2 -12 28 15.00 1.47 3 -12 28 7.40 1.18 -3 -12 28 6.14 1.22 -12 -3 -28 7.59 1.08 12 -3 28 7.65 1.46 4 -12 28 5.32 1.23 12 -4 28 2.98 1.32 5 12 -28 8.58 1.21 5 -12 28 7.76 1.41 12 -5 28 8.09 1.27 6 -12 28 2.61 1.05 12 -6 28 1.03 1.01 7 -12 28 11.35 1.33 12 -7 28 9.43 1.36 8 -12 28 4.82 1.25 12 -8 28 2.43 1.13 9 -12 28 24.00 1.78 12 -9 28 23.03 1.81 10 -12 28 8.12 1.27 12 -10 28 7.08 1.27 11 -12 28 11.80 1.41 12 -11 28 9.53 1.41 12 -12 28 1.41 0.99 0 -13 28 6.26 1.16 -13 0 -28 6.58 1.00 -13 1 -28 5.18 0.94 1 -13 28 5.76 1.28 -1 -13 28 4.09 1.14 13 -1 28 7.54 1.45 -13 -1 -28 5.37 0.97 -13 2 -28 4.65 0.88 2 -13 28 3.55 1.13 -2 -13 28 3.16 1.27 -13 -2 -28 4.19 0.94 13 -2 28 5.32 1.50 3 -13 28 15.96 1.51 -3 -13 28 20.65 1.65 -13 -3 -28 19.25 1.45 13 -3 28 17.41 1.87 4 -13 28 1.14 1.21 13 -4 28 0.65 0.97 5 -13 28 0.18 0.92 13 -5 28 0.76 0.97 6 -13 28 6.01 1.16 13 -6 28 4.18 1.25 7 -13 28 8.73 1.46 13 -7 28 6.75 1.28 8 -13 28 9.14 1.49 13 -8 28 7.80 1.30 9 -13 28 14.93 1.54 13 -9 28 17.12 1.66 10 -13 28 9.82 1.35 13 -10 28 10.38 1.42 11 -13 28 7.23 1.27 13 -11 28 5.91 1.34 12 -13 28 1.31 1.26 13 -12 28 0.21 0.95 0 -14 28 0.38 0.91 14 0 28 -0.12 0.96 -14 0 -28 0.18 0.77 -14 1 -28 1.99 0.87 1 -14 28 1.72 1.04 14 -1 28 3.31 1.19 -14 -1 -28 2.64 0.92 -1 -14 28 1.94 1.09 2 -14 28 8.60 1.31 -14 2 -28 8.74 1.16 -14 -2 -28 9.79 1.23 -2 -14 28 8.56 1.30 14 -2 28 9.09 1.61 3 -14 28 2.74 1.10 -14 3 -28 2.57 0.85 -3 -14 28 2.00 1.02 14 -3 28 1.49 1.28 4 -14 28 8.09 1.25 14 -4 28 9.92 1.41 5 -14 28 12.94 1.41 14 -5 28 9.73 1.40 6 -14 28 8.88 1.50 14 -6 28 8.75 1.36 7 -14 28 11.34 1.60 14 -7 28 16.84 1.59 8 -14 28 3.99 1.35 14 -8 28 2.17 1.17 9 -14 28 1.87 1.08 14 -9 28 0.97 1.09 10 -14 28 1.41 1.06 14 -10 28 0.91 1.02 11 -14 28 4.86 1.29 14 -11 28 1.67 1.07 -15 0 -28 8.99 1.23 0 -15 28 8.07 1.25 -15 1 -28 1.02 0.84 1 -15 28 0.57 1.17 -15 -1 -28 2.91 0.93 15 -1 28 2.71 1.10 -1 -15 28 1.98 1.04 2 -15 28 6.98 1.23 -15 2 -28 8.37 1.18 -2 -15 28 5.75 1.33 -15 -2 -28 6.00 1.17 15 -2 28 7.38 1.44 -15 3 -28 5.72 0.98 3 -15 28 3.85 1.12 15 -3 28 6.91 1.61 4 -15 28 3.49 1.16 15 -4 28 2.39 1.43 15 -5 28 2.52 1.31 6 -15 28 1.94 1.06 15 -6 28 1.51 1.05 7 -15 28 16.27 1.61 15 -7 28 14.27 1.55 8 -15 28 13.91 1.68 15 -8 28 13.18 1.55 9 -15 28 9.08 1.33 15 -9 28 8.83 1.41 -16 0 -28 -0.14 0.90 0 -16 28 0.68 1.35 -16 1 -28 18.39 1.62 1 -16 28 24.31 1.81 -16 -1 -28 20.68 1.75 -1 -16 28 18.47 1.73 16 -1 28 23.34 2.01 -16 2 -28 0.32 0.89 2 -16 28 0.71 0.99 16 -2 28 -0.48 1.26 -2 -16 28 0.72 1.06 -16 -2 -28 1.33 1.03 -16 3 -28 0.59 0.86 3 -16 28 0.89 0.98 16 -3 28 0.41 0.98 4 -16 28 2.36 1.32 -16 4 -28 1.65 1.00 16 -4 28 3.02 1.19 5 -16 28 4.23 1.21 16 -5 28 7.42 1.50 6 -16 28 15.65 1.53 16 -6 28 16.13 1.65 7 -16 28 1.57 1.08 16 -7 28 -0.09 1.04 -17 0 -28 28.68 2.09 0 -17 28 29.19 1.99 1 -17 28 0.18 0.94 -17 1 -28 1.24 0.99 17 -1 28 0.49 2.14 -1 -17 28 -0.07 1.15 2 -17 28 20.83 1.71 -2 -17 28 14.93 1.57 17 -2 28 16.91 1.71 -17 3 -28 1.23 1.02 3 -17 28 0.90 1.22 4 -17 28 1.57 1.07 -17 4 -28 3.16 0.99 17 -4 28 1.29 1.19 5 -17 28 3.11 1.15 17 -5 28 3.97 1.50 0 0 -29 -0.14 0.64 1 0 -29 135.16 4.50 0 1 -29 130.38 4.48 -1 0 -29 136.47 4.51 -1 1 -29 1.66 0.70 -1 -1 -29 0.77 0.67 1 1 -29 0.22 0.65 -2 0 -29 5.54 0.89 0 2 -29 7.28 0.79 -2 1 -29 42.56 1.89 1 2 -29 43.18 1.90 -2 -1 -29 42.57 1.82 2 1 -29 41.85 1.88 -1 2 -29 41.28 1.79 2 2 -29 0.22 0.62 -2 2 -29 0.00 0.67 0 3 -29 58.42 2.27 0 -3 29 59.50 2.41 0 -3 29 58.84 2.55 -3 0 -29 57.45 2.34 1 3 -29 18.02 1.25 1 -3 29 20.30 1.47 -3 1 -29 19.79 1.15 1 -3 29 21.74 1.32 -1 -3 29 20.19 1.42 -1 3 -29 17.56 1.22 -3 -1 -29 18.57 1.29 -1 -3 29 18.69 1.46 2 -3 29 0.87 0.88 -3 2 -29 1.23 0.57 2 3 -29 0.62 0.65 2 -3 29 1.61 0.62 3 2 -29 1.01 0.68 3 -2 29 1.53 0.87 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1 -5 29 16.44 1.45 1 5 -29 17.19 1.19 -1 -5 29 16.23 1.34 -1 5 -29 16.35 1.35 -5 -1 -29 15.06 1.20 -1 5 -29 16.88 1.19 -1 -5 29 16.73 1.34 2 -5 29 15.06 1.28 2 5 -29 12.36 1.28 2 5 -29 11.86 1.10 2 -5 29 13.30 1.39 -5 2 -29 14.29 1.15 -2 -5 29 14.85 1.34 -2 5 -29 10.80 1.27 -2 -5 29 14.92 1.28 -5 -2 -29 12.39 1.13 3 5 -29 7.75 1.19 3 -5 29 10.64 1.16 -5 3 -29 10.55 1.02 3 5 -29 10.17 1.04 -3 -5 29 12.07 1.28 5 -3 29 11.05 1.30 -3 5 -29 10.86 1.27 -5 4 -29 10.63 1.50 4 -5 29 13.68 1.25 4 5 -29 13.39 1.14 -4 5 -29 13.41 1.38 5 4 -29 12.73 1.11 -4 -5 29 13.44 1.55 5 -4 29 13.29 1.32 5 -4 29 12.41 1.22 5 -5 29 1.60 0.91 5 5 -29 -0.14 0.70 -6 0 -29 55.80 2.26 0 6 -29 54.79 2.24 0 -6 29 52.87 2.63 1 -6 29 1.30 0.82 1 6 -29 1.30 0.69 1 6 -29 -0.77 0.78 -6 1 -29 0.02 0.51 -1 -6 29 0.93 0.81 -6 -1 -29 0.63 0.70 -1 6 -29 1.69 1.04 2 -6 29 9.77 1.43 2 6 -29 12.41 1.52 -6 2 -29 10.53 0.92 2 6 -29 11.75 1.04 -2 -6 29 11.12 1.42 -6 -2 -29 10.73 0.93 6 -2 29 12.73 1.38 3 -6 29 4.18 1.22 3 6 -29 3.27 0.73 -6 3 -29 3.16 0.76 6 -3 29 3.71 1.18 -6 -3 -29 1.91 0.78 4 -6 29 20.35 1.64 4 6 -29 20.17 1.38 6 -4 29 20.31 2.49 5 -6 29 6.59 1.05 5 6 -29 6.97 1.00 6 -5 29 6.65 1.26 6 6 -29 47.76 2.13 6 -6 29 43.66 2.44 -7 0 -29 20.04 1.34 0 -7 29 22.26 1.61 1 7 -29 0.53 0.63 -7 1 -29 -0.09 0.67 1 -7 29 0.80 0.82 -7 -1 -29 1.17 0.56 -1 -7 29 0.40 1.05 7 -1 29 0.06 1.30 2 7 -29 -0.38 0.65 2 -7 29 0.16 0.78 -7 2 -29 0.20 0.68 -7 -2 -29 1.11 0.75 -2 -7 29 0.09 0.83 7 -2 29 0.34 1.03 3 -7 29 9.22 1.15 3 7 -29 8.51 1.01 -7 -3 -29 6.83 0.85 7 -3 29 10.43 1.76 4 7 -29 15.35 1.17 4 -7 29 11.89 1.26 7 -4 29 13.52 1.33 5 -7 29 2.67 0.98 5 7 -29 2.30 0.79 7 -5 29 2.16 1.01 6 7 -29 3.15 0.82 6 -7 29 4.19 1.09 7 -6 29 3.61 1.25 7 -7 29 36.33 2.11 -8 0 -29 0.17 0.69 0 -8 29 0.36 0.83 -8 1 -29 23.82 1.40 1 -8 29 21.21 1.61 -8 -1 -29 24.40 1.43 -1 -8 29 21.32 1.62 2 8 -29 5.79 0.89 -8 2 -29 5.41 0.89 2 -8 29 4.67 1.25 -2 -8 29 6.76 1.08 -8 -2 -29 5.98 0.91 3 8 -29 4.50 0.85 3 -8 29 6.78 1.10 8 -3 29 6.50 1.42 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21 3 13 0.0419 -0.4093 21 3 14 4.1759 0.2163 21 3 15 2.1429 0.2089 21 3 16 -0.2438 0.6473 21 3 17 4.9995 -1.1065 21 4 0 6.3962 -0.0000 21 4 1 -3.0275 -0.9261 21 4 2 -0.1692 -0.3947 21 4 3 0.7485 -2.4219 21 4 4 3.8111 -1.2142 21 4 5 2.4105 -0.8291 21 4 6 3.1767 0.6937 21 4 7 -0.4963 -2.7529 21 4 8 -1.9367 -1.9358 21 4 9 4.0319 0.0813 21 4 10 0.6998 0.0903 21 4 11 0.6210 -1.0599 21 4 12 -1.0814 1.7417 21 4 13 -1.1921 -1.8887 21 4 14 -0.9630 -3.3205 21 4 15 -5.4208 -1.9684 21 4 16 -3.8778 0.5876 21 5 0 -0.3068 0.0000 21 5 1 -1.8127 2.1183 21 5 2 -3.3148 1.1995 21 5 3 0.5458 0.9551 21 5 4 -0.9314 -3.6819 21 5 5 -1.8317 2.5395 21 5 6 1.4234 -2.2965 21 5 7 -1.6470 2.1187 21 5 8 1.1603 2.4954 21 5 9 0.9022 -1.5530 21 5 10 1.1403 1.3870 21 5 11 -0.3949 1.8347 21 5 12 -0.5701 1.0018 21 5 13 -0.5007 0.8128 21 5 14 -0.8881 3.3949 21 5 15 2.0538 2.0592 21 6 0 0.2134 -0.0000 21 6 1 -2.0625 1.3911 21 6 2 -0.1086 -0.2718 21 6 3 -2.1697 -2.6871 21 6 4 2.0797 -2.7371 21 6 5 -1.0747 -0.6968 21 6 6 1.9957 0.2196 21 6 7 -1.4443 -1.2606 21 6 8 0.1450 -1.0196 21 6 9 -0.9959 0.8273 21 6 10 -2.4405 2.7448 21 6 11 0.0160 -1.8892 21 6 12 -2.8328 1.9526 21 6 13 0.9242 -1.4597 21 6 14 1.1747 2.1524 21 7 0 1.9364 -0.0000 21 7 1 0.1417 0.4202 21 7 2 4.6979 0.3531 21 7 3 -2.7190 -0.8086 21 7 4 0.2480 -3.9206 21 7 5 0.0079 -0.3512 21 7 6 -0.2948 -1.2349 21 7 7 -2.5983 1.5734 21 7 8 -0.0138 -2.6804 21 7 9 -0.2163 1.7390 21 7 10 -0.3354 2.1161 21 7 11 -2.0412 0.2069 21 7 12 -2.1399 -4.7540 21 8 0 3.1716 -0.0000 21 8 1 0.6579 -0.5050 21 8 2 -0.8707 -0.6573 21 8 3 3.8700 -2.0983 21 8 4 -0.3052 0.6386 21 8 5 -1.9265 -1.2792 21 8 6 -1.4131 -0.0531 21 8 7 -1.5481 1.4489 21 8 8 -1.0929 -1.1574 21 8 9 -3.2317 2.9361 21 8 10 -2.0160 1.3909 21 9 0 -1.7699 0.0000 21 9 1 1.5608 -0.1643 21 9 2 1.5882 -0.2963 21 9 3 0.1817 -1.4004 21 9 4 -5.5965 2.4877 21 9 5 -1.2020 -1.5553 21 9 6 1.9859 -1.2031 22 0 0 5.3526 -0.0000 22 0 1 0.0000 7.1788 22 0 2 3.1994 -0.0000 22 0 3 0.0000 4.8979 22 0 4 -1.4728 0.0000 22 0 5 -0.0000 -2.6862 22 0 6 0.1403 -0.0000 22 0 7 0.0000 1.0316 22 0 8 -3.7734 -0.0000 22 0 9 0.0000 1.1014 22 0 10 -2.9090 -0.0000 22 0 11 0.0000 1.7918 22 0 12 -2.7873 0.0000 22 0 13 -0.0000 -4.4856 22 1 0 -1.6437 0.0000 22 1 1 0.3742 -0.8969 22 1 2 0.4992 -4.9933 22 1 3 -1.1477 0.0527 22 1 4 0.7939 -0.6469 22 1 5 2.9713 -1.5343 22 1 6 -1.4507 2.6159 22 1 7 0.6296 3.7657 22 1 8 0.2711 1.2389 22 1 9 2.8120 2.4161 22 1 10 -2.3463 -2.3382 22 1 11 -3.7413 -1.7051 22 1 12 -0.2537 0.3544 22 1 13 -3.4106 -0.3854 22 2 0 0.1787 0.0000 22 2 1 -1.9361 7.6419 22 2 2 -0.1516 -5.6034 22 2 3 -0.0889 4.8748 22 2 4 -4.8576 0.1293 22 2 5 0.8652 -1.3694 22 2 6 -0.3821 -1.9186 22 2 7 -1.7055 1.1296 22 2 8 0.8156 -3.9071 22 2 9 -1.5835 1.5243 22 2 10 2.6270 1.8844 22 2 11 1.1000 1.8110 22 2 12 3.2553 -3.3214 22 2 13 -0.9321 -1.1235 22 3 0 -1.5588 0.0000 22 3 1 -1.7883 0.6108 22 3 2 1.2135 -0.2995 22 3 3 -0.3475 -0.5891 22 3 4 -5.2396 -0.9252 22 3 5 -2.4738 -2.2086 22 3 6 -1.0842 -0.9221 22 3 7 2.6506 0.9212 22 3 8 0.8675 -2.8994 22 3 9 -1.9171 -5.0513 22 3 10 -2.5919 -3.3398 22 3 11 -0.4105 -0.5930 22 3 12 -1.5449 5.1723 22 4 0 -6.3179 0.0000 22 4 1 -0.1345 2.1034 22 4 2 -0.0915 1.4674 22 4 3 -2.6044 -0.6674 22 4 4 -5.2650 -2.6335 22 4 5 3.3588 2.9356 22 4 6 -3.0502 3.4086 22 4 7 -1.1825 -0.8187 22 4 8 -0.0286 -2.0706 22 4 9 -0.6786 5.8025 22 4 10 0.2210 2.2097 22 4 11 1.6155 -2.0695 22 5 0 0.0407 -0.0000 22 5 1 0.0731 3.1515 22 5 2 0.7129 -1.8879 22 5 3 5.7314 -0.2564 22 5 4 2.9215 3.4601 22 5 5 2.8568 2.5438 22 5 6 1.5698 2.1110 22 5 7 5.2740 -1.4490 22 5 8 3.2485 0.1616 22 5 9 -0.4731 -2.2335 22 6 0 -1.2382 0.0000 22 6 1 0.3010 1.5293 22 6 2 0.0700 2.7525 22 6 3 2.1147 -1.2035 22 6 4 -1.7342 3.4068 22 6 5 -1.2458 -1.1473 22 6 6 0.9177 1.8189 22 6 7 3.7163 2.9716 22 7 0 -5.2811 0.0000 22 7 1 -0.4014 -3.0041 22 7 2 -5.5255 0.5915 23 0 1 -1.1604 0.0000 23 0 2 -0.0000 -0.2382 23 0 3 -1.3417 -0.0000 23 0 4 0.0000 0.2627 23 1 0 -2.3483 0.0000 23 1 1 1.8470 -1.9677 23 1 2 1.4423 3.5223 23 1 3 3.7620 3.9433 23 2 0 8.7432 -0.0000 23 2 1 -2.0664 -6.2436 23 2 2 -3.2586 -4.3095 ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-y+1/2, x+1/2, z+1/2' '-x, -y, z' 'y+1/2, -x+1/2, z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x+1/2, y+1/2, -z+1/2' 'y, x, -z' '-y, -x, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Al1 Al 0.66084(3) 0.33916(3) 0.5000 0.01919(19) Uani 1 2 d S T P . . Al2 Al 0.62547(3) 0.40189(3) 0.41741(2) 0.01846(14) Uani 1 1 d . . . . . Al3 Al 0.5000 0.5000 0.38289(2) 0.01838(19) Uani 1 2 d S T P . . O2 O 0.56641(6) 0.47726(6) 0.41792(3) 0.0175(3) Uani 1 1 d . . . . . H2 H 0.5701 0.5072 0.4378 0.021 Uiso 1 1 calc R . . . . O3 O 0.65539(7) 0.42287(7) 0.36958(3) 0.0264(3) Uani 1 1 d . . . . . O1 O 0.60124(6) 0.37349(6) 0.46433(3) 0.0170(3) Uani 1 1 d . . . . . H1 H 0.5544 0.3769 0.4705 0.020 Uiso 1 1 calc R . . . . O4 O 0.56339(7) 0.47868(7) 0.34428(3) 0.0247(3) Uani 1 1 d . . . . . C1 C 0.62386(11) 0.45164(10) 0.34305(5) 0.0205(5) Uani 1 1 d . . . . . C26 C 0.80679(12) 0.64373(11) 0.14517(6) 0.0363(6) Uani 1 1 d . . . . . H26 H 0.8090 0.6458 0.1705 0.073(8) Uiso 1 1 calc R . . . . C23 C 0.79828(12) 0.63912(12) 0.07036(6) 0.0364(6) Uani 1 1 d . . . . . H23 H 0.7949 0.6379 0.0451 0.069(8) Uiso 1 1 calc R . . . . C20 C 0.99542(11) 0.15134(11) 0.11554(5) 0.0238(5) Uani 1 1 d . . . . . C25 C 0.80717(12) 0.70584(11) 0.12575(5) 0.0320(5) Uani 1 1 d . . . . . H25 H 0.8103 0.7484 0.1378 0.49(6) Uiso 1 1 calc R . . . . C22 C 0.79867(13) 0.57814(12) 0.08942(6) 0.0430(6) Uani 1 1 d . . . . . H22 H 0.7960 0.5358 0.0771 0.052(7) Uiso 1 1 calc R . . . . C24 C 0.80285(11) 0.70346(10) 0.08814(6) 0.0270(5) Uani 1 1 d . . . . . C27 C 0.80767(10) 0.77002(11) 0.06738(5) 0.0216(5) Uani 1 1 d . . . . . C17 C 0.95633(11) 0.21430(10) 0.12688(5) 0.0250(5) Uani 1 1 d . . . . . C7 C 0.63142(11) 0.48467(11) 0.27702(5) 0.0326(5) Uani 1 1 d . . . . . H7 H 0.5885 0.5068 0.2791 0.039 Uiso 1 1 calc R . . . . C21 C 0.80326(12) 0.57923(11) 0.12879(6) 0.0362(6) Uani 1 1 d . . . . . C5 C 0.73058(13) 0.45222(11) 0.24056(6) 0.0415(6) Uani 1 1 d . . . . . C16 C 0.89113(11) 0.20632(11) 0.14280(6) 0.0369(6) Uani 1 1 d . . . . . H16 H 0.8724 0.1622 0.1464 0.044 Uiso 1 1 calc R . . . . C8 C 0.76833(13) 0.45277(12) 0.20498(6) 0.0454(7) Uani 1 1 d . . . . . C2 C 0.66043(11) 0.45175(11) 0.30760(5) 0.0291(5) Uani 1 1 d . . . . . C18 C 0.98430(12) 0.28024(11) 0.12178(5) 0.0366(6) Uani 1 1 d . . . . . H18 H 1.0286 0.2851 0.1118 0.044 Uiso 1 1 calc R . . . . C3 C 0.72466(11) 0.41873(11) 0.30396(5) 0.0341(6) Uani 1 1 d . . . . . H3 H 0.7439 0.3956 0.3238 0.041 Uiso 1 1 calc R . . . . C4 C 0.76020(13) 0.41990(11) 0.27109(6) 0.0406(6) Uani 1 1 d . . . . . H4 H 0.8039 0.3991 0.2693 0.055(7) Uiso 1 1 calc R . . . . C14 C 0.88242(13) 0.33322(11) 0.14826(6) 0.0417(6) Uani 1 1 d . . . . . C6 C 0.66516(12) 0.48475(12) 0.24426(6) 0.0423(6) Uani 1 1 d . . . . . H6 H 0.6448 0.5065 0.2242 0.032(6) Uiso 1 1 calc R . . . . C13 C 0.76759(13) 0.51216(12) 0.18353(6) 0.0452(7) Uani 1 1 d . . . . . H13 H 0.7428 0.5510 0.1913 0.064(8) Uiso 1 1 calc R . . . . C19 C 0.94664(12) 0.33885(12) 0.13140(6) 0.0403(6) Uani 1 1 d . . . . . H19 H 0.9648 0.3828 0.1264 0.048 Uiso 1 1 calc R . . . . C10 C 0.84219(13) 0.39478(12) 0.15980(6) 0.0424(6) Uani 1 1 d . . . . . C15 C 0.85403(13) 0.26615(12) 0.15333(6) 0.0442(6) Uani 1 1 d . . . . . H15 H 0.8101 0.2614 0.1638 0.062(8) Uiso 1 1 calc R . . . . C12 C 0.80413(13) 0.51486(12) 0.14974(5) 0.0394(6) Uani 1 1 d . . . . . C11 C 0.84041(13) 0.45557(11) 0.13893(6) 0.0448(7) Uani 1 1 d . . . . . H11 H 0.8644 0.4565 0.1169 0.054 Uiso 1 1 calc R . . . . C9 C 0.80533(13) 0.39444(12) 0.19322(6) 0.0461(7) Uani 1 1 d . . . . . H9 H 0.8058 0.3545 0.2076 0.055 Uiso 1 1 calc R . . . . O8 O 0.81261(6) 0.82534(7) 0.08630(3) 0.0229(3) Uani 1 1 d . . . . . O10 O 0.73113(6) 0.40087(7) 0.48532(3) 0.0255(3) Uani 1 1 d . . . . . O5 O 1.05601(7) 0.15970(6) 0.10262(3) 0.0213(3) Uani 1 1 d . . . . . O6 O 0.96524(6) 0.09220(6) 0.11951(3) 0.0243(3) Uani 1 1 d . . . . . O9 O 0.70433(7) 0.45648(7) 0.43348(3) 0.0248(3) Uani 1 1 d . . . . . O7 O 0.80597(7) 0.76804(6) 0.03289(3) 0.0263(3) Uani 1 1 d . . . . . C28 C 0.74640(11) 0.43888(11) 0.45825(6) 0.0280(5) Uani 1 1 d . . . . . C6G C 0.84879(11) 0.49012(13) 0.42526(6) 0.0415(6) Uani 1 1 d . . . . . H6G H 0.8205 0.5010 0.4055 0.050 Uiso 1 1 calc R . . . . C1G C 0.82032(12) 0.46011(12) 0.45554(6) 0.0412(6) Uani 1 1 d . . . . . C5G C 0.91957(12) 0.50445(14) 0.42377(7) 0.0532(7) Uani 1 1 d . . . . . H5G H 0.9386 0.5220 0.4023 0.064 Uiso 1 1 calc R . . . . C2G C 0.86419(13) 0.44554(17) 0.48518(7) 0.0699(9) Uani 1 1 d . . . . . H2G H 0.8465 0.4234 0.5058 0.084 Uiso 1 1 calc R . . . . C4G C 0.96209(12) 0.49330(16) 0.45329(7) 0.0575(8) Uani 1 1 d . . . . . C3G C 0.93374(13) 0.46419(17) 0.48373(7) 0.0758(10) Uani 1 1 d . . . . . H3G H 0.9618 0.4567 0.5040 0.091 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Al1 0.0208(3) 0.0208(3) 0.0159(4) -0.0015(3) -0.0015(3) 0.0004(3) Al2 0.0187(3) 0.0221(3) 0.0146(3) 0.0004(3) -0.0006(3) -0.0003(2) Al3 0.0206(4) 0.0197(4) 0.0148(4) 0.000 0.000 0.0020(3) O2 0.0233(7) 0.0170(7) 0.0121(6) -0.0009(6) -0.0009(6) 0.0014(5) O3 0.0253(8) 0.0315(8) 0.0225(7) 0.0045(7) 0.0044(7) 0.0041(7) O1 0.0156(7) 0.0225(7) 0.0130(6) 0.0012(6) -0.0035(6) -0.0015(5) O4 0.0283(8) 0.0306(8) 0.0153(7) 0.0020(6) 0.0028(6) 0.0056(6) C1 0.0275(12) 0.0182(11) 0.0158(11) 0.0021(9) 0.0069(10) -0.0003(9) C26 0.0620(17) 0.0318(14) 0.0151(12) 0.0066(11) 0.0089(11) 0.0094(12) C23 0.0549(16) 0.0374(15) 0.0168(12) 0.0015(11) 0.0036(11) -0.0027(12) C20 0.0277(12) 0.0292(12) 0.0145(10) -0.0016(10) 0.0025(10) 0.0045(10) C25 0.0463(14) 0.0277(13) 0.0220(12) 0.0016(10) 0.0031(11) 0.0044(10) C22 0.0747(18) 0.0214(13) 0.0327(13) -0.0018(11) 0.0219(13) 0.0052(12) C24 0.0310(12) 0.0259(12) 0.0240(12) 0.0034(10) 0.0051(10) 0.0013(9) C27 0.0184(11) 0.0311(13) 0.0153(11) 0.0019(10) -0.0004(9) -0.0048(9) C17 0.0328(13) 0.0250(12) 0.0173(10) 0.0023(9) 0.0108(10) 0.0065(9) C7 0.0369(13) 0.0372(14) 0.0238(12) 0.0128(10) 0.0081(11) 0.0135(11) C21 0.0554(16) 0.0256(13) 0.0277(12) 0.0099(11) 0.0228(12) 0.0137(11) C5 0.0593(17) 0.0326(13) 0.0327(13) 0.0116(11) 0.0259(12) 0.0228(12) C16 0.0384(14) 0.0260(13) 0.0463(14) 0.0056(11) 0.0181(12) 0.0071(10) C8 0.0695(18) 0.0354(14) 0.0312(13) 0.0131(12) 0.0240(13) 0.0190(12) C2 0.0323(13) 0.0322(13) 0.0227(11) 0.0053(10) 0.0087(10) 0.0081(10) C18 0.0465(15) 0.0266(13) 0.0365(13) -0.0032(11) 0.0222(12) 0.0029(10) C3 0.0436(14) 0.0349(14) 0.0236(12) 0.0119(10) 0.0106(11) 0.0172(11) C4 0.0456(15) 0.0392(14) 0.0369(14) 0.0066(12) 0.0137(12) 0.0189(12) C14 0.0641(17) 0.0250(13) 0.0361(13) 0.0105(11) 0.0301(13) 0.0146(12) C6 0.0565(16) 0.0410(15) 0.0295(13) 0.0057(12) 0.0116(12) 0.0243(12) C13 0.0753(18) 0.0301(14) 0.0301(12) 0.0134(11) 0.0326(13) 0.0281(13) C19 0.0531(16) 0.0242(13) 0.0436(14) 0.0004(11) 0.0242(13) 0.0082(11) C10 0.0612(17) 0.0289(13) 0.0372(13) 0.0067(12) 0.0240(13) 0.0147(12) C15 0.0400(15) 0.0355(15) 0.0572(16) 0.0090(13) 0.0272(13) 0.0090(12) C12 0.0587(16) 0.0379(15) 0.0217(11) 0.0032(11) 0.0211(11) 0.0191(12) C11 0.0716(18) 0.0313(14) 0.0315(13) 0.0054(11) 0.0316(13) 0.0162(13) C9 0.0673(17) 0.0337(14) 0.0372(14) 0.0151(12) 0.0269(13) 0.0214(13) O8 0.0263(8) 0.0242(8) 0.0182(7) 0.0011(7) 0.0029(6) -0.0070(6) O10 0.0193(7) 0.0418(9) 0.0153(7) -0.0003(7) -0.0016(6) -0.0034(6) O5 0.0263(8) 0.0181(7) 0.0195(7) -0.0020(6) 0.0049(6) 0.0000(6) O6 0.0222(7) 0.0196(8) 0.0311(8) -0.0037(7) 0.0035(6) -0.0027(6) O9 0.0215(8) 0.0285(8) 0.0245(7) 0.0059(6) -0.0021(7) -0.0062(6) O7 0.0389(9) 0.0236(8) 0.0163(7) 0.0017(6) -0.0020(7) -0.0095(6) C28 0.0325(13) 0.0301(13) 0.0212(12) -0.0019(10) -0.0048(11) -0.0066(10) C6G 0.0254(13) 0.0661(17) 0.0328(13) 0.0072(12) -0.0044(11) -0.0060(12) C1G 0.0326(14) 0.0529(16) 0.0382(14) 0.0039(13) 0.0023(12) -0.0115(11) C5G 0.0383(15) 0.0784(19) 0.0429(15) 0.0116(15) 0.0028(13) -0.0260(14) C2G 0.0308(15) 0.134(3) 0.0450(16) 0.0294(17) -0.0098(13) -0.0278(16) C4G 0.0296(14) 0.093(2) 0.0499(16) 0.0076(16) -0.0042(13) -0.0261(15) C3G 0.0214(15) 0.150(3) 0.0559(18) 0.028(2) -0.0127(13) -0.0234(17) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0090 0.0040 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0250 0.0140 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Al Al 0.1200 0.1100 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 O1 Al1 O1 93.41(8) . 8_666 O1 Al1 O10 93.94(5) 8_666 . O1 Al1 O10 90.95(5) 8_666 8_666 O1 Al1 O10 90.95(5) . . O1 Al1 O10 93.93(5) . 8_666 O1 Al1 O7 172.92(5) 8_666 6_645 O1 Al1 O7 90.77(5) 8_666 2_645 O1 Al1 O7 172.92(6) . 2_645 O1 Al1 O7 90.78(5) . 6_645 O10 Al1 O10 172.88(9) . 8_666 O10 Al1 O7 91.70(6) 8_666 2_645 O10 Al1 O7 83.07(6) . 2_645 O10 Al1 O7 83.06(6) 8_666 6_645 O10 Al1 O7 91.70(6) . 6_645 O7 Al1 O7 85.65(8) 6_645 2_645 O2 Al2 O3 91.68(6) . . O2 Al2 O1 93.83(5) . . O2 Al2 O8 176.36(6) . 6_645 O2 Al2 O5 93.44(6) . 5_455 O2 Al2 O9 93.05(6) . . O3 Al2 O8 84.72(6) . 6_645 O3 Al2 O5 89.25(6) . 5_455 O3 Al2 O9 85.97(6) . . O1 Al2 O3 174.48(6) . . O1 Al2 O8 89.77(6) . 6_645 O1 Al2 O5 90.01(5) . 5_455 O1 Al2 O9 94.14(6) . . O8 Al2 O5 86.04(6) 6_645 5_455 O8 Al2 O9 87.19(6) 6_645 . O5 Al2 O9 172.05(6) 5_455 . O2 Al3 O2 92.69(8) . 3_665 O2 Al3 O4 175.83(6) 3_665 . O2 Al3 O4 175.84(6) . 3_665 O2 Al3 O4 91.46(5) 3_665 3_665 O2 Al3 O4 91.47(5) . . O2 Al3 O6 93.11(5) . 5_455 O2 Al3 O6 90.57(5) 3_665 5_455 O2 Al3 O6 90.57(5) . 6_655 O2 Al3 O6 93.11(5) 3_665 6_655 O4 Al3 O4 84.38(8) 3_665 . O6 Al3 O4 86.64(6) 5_455 3_665 O6 Al3 O4 86.64(6) 6_655 . O6 Al3 O4 89.42(6) 6_655 3_665 O6 Al3 O4 89.42(6) 5_455 . O6 Al3 O6 174.68(9) 5_455 6_655 Al2 O2 Al3 126.84(7) . . C1 O3 Al2 131.18(12) . . Al1 O1 Al2 126.88(7) . . C1 O4 Al3 133.98(12) . . O3 C1 C2 116.62(17) . . O4 C1 O3 125.71(16) . . O4 C1 C2 117.65(17) . . C21 C26 C25 123.22(19) . . C22 C23 C24 121.21(19) . . O5 C20 C17 117.83(18) . . O5 C20 O6 124.71(17) . . O6 C20 C17 117.46(18) . . C24 C25 C26 118.9(2) . . C23 C22 C21 120.0(2) . . C23 C24 C27 121.47(18) . . C25 C24 C23 119.87(19) . . C25 C24 C27 118.54(19) . . O8 C27 C24 116.19(16) . . O7 C27 C24 118.91(18) . . O7 C27 O8 124.90(18) . . C16 C17 C20 118.95(19) . . C18 C17 C20 120.67(18) . . C18 C17 C16 120.39(19) . . C6 C7 C2 121.1(2) . . C26 C21 C22 116.82(19) . . C26 C21 C12 122.14(19) . . C22 C21 C12 121.0(2) . . C4 C5 C8 120.36(19) . . C4 C5 C6 118.73(19) . . C6 C5 C8 120.9(2) . . C17 C16 C15 118.8(2) . . C13 C8 C5 119.83(19) . . C13 C8 C9 119.36(19) . . C9 C8 C5 120.80(19) . . C7 C2 C1 121.05(18) . . C3 C2 C1 120.28(18) . . C3 C2 C7 118.66(18) . . C19 C18 C17 120.3(2) . . C4 C3 C2 120.79(19) . . C3 C4 C5 120.2(2) . . C19 C14 C10 122.2(2) . . C19 C14 C15 118.3(2) . . C15 C14 C10 119.5(2) . . C7 C6 C5 120.5(2) . . C8 C13 C12 121.3(2) . . C18 C19 C14 121.1(2) . . C11 C10 C14 121.71(19) . . C11 C10 C9 117.8(2) . . C9 C10 C14 120.46(19) . . C16 C15 C14 120.9(2) . . C13 C12 C21 119.00(19) . . C11 C12 C21 123.33(18) . . C11 C12 C13 117.7(2) . . C12 C11 C10 122.65(19) . . C8 C9 C10 121.3(2) . . C27 O8 Al2 130.91(12) . 6_655 C28 O10 Al1 139.09(12) . . C20 O5 Al2 134.46(13) . 5 C20 O6 Al3 131.51(12) . 5 C28 O9 Al2 125.15(13) . . C27 O7 Al1 126.52(13) . 4_564 O10 C28 C1G 115.67(19) . . O9 C28 O10 124.81(18) . . O9 C28 C1G 119.44(19) . . C1G C6G C5G 120.5(2) . . C6G C1G C28 123.7(2) . . C6G C1G C2G 118.3(2) . . C2G C1G C28 117.9(2) . . C4G C5G C6G 121.3(2) . . C3G C2G C1G 119.8(2) . . C5G C4G C4G 123.94(16) . 3_765 C3G C4G C5G 118.2(2) . . C3G C4G C4G 117.69(18) . 3_765 C4G C3G C2G 121.5(2) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Al1 O1 1.8578(12) . Al1 O1 1.8579(12) 8_666 Al1 O10 1.8731(13) . Al1 O10 1.8731(13) 8_666 Al1 O7 1.9288(14) 6_645 Al1 O7 1.9288(14) 2_645 Al2 O2 1.8367(13) . Al2 O3 1.8886(14) . Al2 O1 1.8634(12) . Al2 O8 1.8935(13) 6_645 Al2 O5 1.9262(14) 5_455 Al2 O9 1.9317(14) . Al3 O2 1.8610(12) . Al3 O2 1.8611(12) 3_665 Al3 O4 1.9104(13) . Al3 O4 1.9104(13) 3_665 Al3 O6 1.8921(12) 5_455 Al3 O6 1.8921(12) 6_655 O3 C1 1.271(2) . O4 C1 1.271(2) . C1 C2 1.477(3) . C26 C25 1.388(3) . C26 C21 1.377(3) . C23 C22 1.362(3) . C23 C24 1.398(3) . C20 C17 1.481(3) . C20 O5 1.265(2) . C20 O6 1.282(2) . C25 C24 1.382(3) . C22 C21 1.447(3) . C24 C27 1.489(3) . C27 O8 1.271(2) . C27 O7 1.265(2) . C17 C16 1.389(3) . C17 C18 1.387(3) . C7 C2 1.402(3) . C7 C6 1.365(3) . C21 C12 1.454(3) . C5 C8 1.492(3) . C5 C4 1.400(3) . C5 C6 1.408(3) . C16 C15 1.404(3) . C8 C13 1.384(3) . C8 C9 1.393(3) . C2 C3 1.392(3) . C18 C19 1.382(3) . C3 C4 1.385(3) . C14 C19 1.383(3) . C14 C10 1.473(3) . C14 C15 1.409(3) . C13 C12 1.424(3) . C10 C11 1.395(3) . C10 C9 1.415(3) . C12 C11 1.391(3) . O8 Al2 1.8934(13) 6_655 O10 C28 1.266(2) . O5 Al2 1.9261(14) 5 O6 Al3 1.8920(12) 5 O9 C28 1.261(2) . O7 Al1 1.9288(14) 4_564 C28 C1G 1.479(3) . C6G C1G 1.364(3) . C6G C5G 1.386(3) . C1G C2G 1.403(3) . C5G C4G 1.372(3) . C2G C3G 1.382(3) . C4G C4G 1.477(4) 3_765 C4G C3G 1.361(3) . loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons 1 -0.198 -0.714 -0.493 9052.2 5819.9