#------------------------------------------------------------------------------ #$Date: 2026-09-25 10:19:11 +0100 (Fri, 25 Sep 2026) $ #$Revision: 306909 $ #$URL: svn://www.crystallography.net/cod/cif/4/51/95/4519547.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519547 loop_ _publ_author_name 'Lu, Junhao' 'Fan, Yingtong' 'Zhou, Bingyue' 'Ye, Zecong' 'Mei, Sen' 'Zhou, Dan' 'Chen, Lanhua' 'Chen, Lixi' 'Liu, Hanzhou' 'Zhu, Huifang' 'Dai, Xing' 'Wang, Yanlong' 'Diwu, Juan' 'Wang, Shuao' _publ_section_title ; A General Energy-Puzzle Strategy to Fabricate Efficient Metal--Organic Framework Scintillators for X-ray Detection ; _journal_issue 9 _journal_name_full 'ACS Materials Letters' _journal_page_first 3951 _journal_page_last 3957 _journal_paper_doi 10.1021/acsmaterialslett.4c00924 _journal_volume 6 _journal_year 2024 _chemical_formula_moiety 'C12 H12 N O5 Pb' _chemical_formula_sum 'C12 H12 N O5 Pb' _chemical_formula_weight 455.434 _space_group_crystal_system orthorhombic _space_group_IT_number 62 _space_group_name_Hall '-P 2ac 2n' _space_group_name_H-M_alt 'P n m a' _symmetry_Int_Tables_number 62 _atom_sites_solution_primary direct _audit_contact_author_name ; ; _audit_creation_date 2024-06-11 _audit_creation_method ; Olex2 1.5 (compiled 2021.11.18 svn.ra9532c28 for OlexSys, GUI svn.r6427) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 7.6706(6) _cell_length_b 18.1667(17) _cell_length_c 10.1590(9) _cell_measurement_reflns_used 9381 _cell_measurement_temperature 296.15 _cell_measurement_theta_max 27.514 _cell_measurement_theta_min 3.009 _cell_volume 1415.7(2) _computing_cell_refinement 'SAINT V8.38A (Bruker, 2018)' _computing_data_reduction 'SAINT V8.38A (Bruker, 2018)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine 1.5 (Bourhis et al., 2015)' _computing_structure_solution 'XS (Sheldrick, 2008)' _diffrn_ambient_temperature 296.15 _diffrn_measured_fraction_theta_full 0.9992 _diffrn_measured_fraction_theta_max 0.9964 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0944 _diffrn_reflns_av_unetI/netI 0.0364 _diffrn_reflns_Laue_measured_fraction_full 0.9992 _diffrn_reflns_Laue_measured_fraction_max 0.9964 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_number 28816 _diffrn_reflns_point_group_measured_fraction_full 0.9992 _diffrn_reflns_point_group_measured_fraction_max 0.9964 _diffrn_reflns_theta_full 25.2417 _diffrn_reflns_theta_max 27.57 _diffrn_reflns_theta_min 2.30 _diffrn_source_current 0.0 _diffrn_source_power 0.0 _diffrn_source_voltage 0.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 11.934 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.2357 _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1425 before and 0.1089 after correction. The Ratio of minimum to maximum transmission is 0.3161. The \l/2 correction factor is Not present. ; _exptl_crystal_density_diffrn 2.137 _exptl_crystal_description block _exptl_crystal_F_000 833.918 _refine_diff_density_max 1.1619 _refine_diff_density_min -1.7667 _refine_diff_density_rms 0.2629 _refine_ls_d_res_high 0.7677 _refine_ls_d_res_low 8.8668 _refine_ls_goodness_of_fit_ref 0.8877 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_constraints 16 _refine_ls_number_parameters 115 _refine_ls_number_reflns 1678 _refine_ls_number_restraints 54 _refine_ls_restrained_S_all 0.8728 _refine_ls_R_factor_all 0.0329 _refine_ls_R_factor_gt 0.0306 _refine_ls_shift/su_max 0.0022 _refine_ls_shift/su_mean 0.0001 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0981 _refine_ls_wR_factor_ref 0.1012 _reflns_Friedel_coverage 0.0 _reflns_limit_h_max 9 _reflns_limit_h_min 0 _reflns_limit_k_max 23 _reflns_limit_k_min 0 _reflns_limit_l_max 13 _reflns_limit_l_min 0 _reflns_number_gt 1567 _reflns_number_total 1678 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL 3 in Pnma #62 REM reset to Pnma #62 CELL 0.71073 7.6706 18.1667 10.159 90 90 90 ZERR 4 0.0006 0.0017 0.0009 0 0 0 LATT 1 SYMM 0.5-X,-Y,0.5+Z SYMM 0.5+X,0.5-Y,0.5-Z SYMM -X,0.5+Y,-Z SFAC C H N O Pb UNIT 48 40 4 20 4 SIMU C8 ISOR 0.02 0.04 C7 C6 O1 ISOR 0.002 0.004 C8 RIGU C8 ISOR 0.002 0.004 C6 C7 ISOR 0.002 0.004 C7 C6 DELU C7 N1 C6 C5 L.S. 4 PLAN 20 TEMP 23 CONF FMAP 2 MORE -1 BOND $H ACTA WGHT 0.1 FVAR 0.113672 REM REM REM Pb1 5 0.60634 0.25000 0.30715 10.50000 0.02953 0.03420 0.03725 = 0.00000 -0.00366 -0.00000 O2 4 0.87137 0.34285 0.30031 11.00000 0.06311 0.05663 0.07984 = -0.03759 0.00542 -0.00721 O3 4 0.34006 0.25000 0.45223 10.50000 0.07735 0.06840 0.06244 = 0.00000 0.02701 -0.00000 O1 4 0.69311 0.34478 0.46609 11.00000 0.09267 0.10095 0.07386 = -0.03922 0.01882 -0.04760 C1 1 0.81794 0.37065 0.40320 11.00000 0.04873 0.04140 0.05267 = -0.01780 -0.01165 0.00110 C2 1 0.90926 0.43892 0.45543 11.00000 0.04591 0.04421 0.05703 = -0.02019 -0.01089 0.00053 C4 1 1.07375 0.45267 0.41262 11.00000 0.05170 0.05901 0.08760 = -0.04415 0.00861 -0.00679 AFIX 43 H4 2 1.12432 0.42087 0.35188 11.00000 -1.20000 AFIX 0 C3 1 0.82917 0.48572 0.54201 11.00000 0.05236 0.06597 0.09747 = -0.04753 0.01515 -0.01561 PART -1 C5 1 0.30249 0.29185 0.53070 10.50000 0.07719 0.08202 0.04894 = -0.00543 0.00163 0.00295 AFIX 43 H5 2 0.36030 0.33657 0.52175 10.50000 -1.20000 AFIX 0 N1 3 0.19581 0.29035 0.63022 10.50000 0.04432 0.11768 0.05805 = -0.00873 -0.00244 0.00645 C6 1 0.15643 0.35131 0.71710 10.50000 0.09300 0.09325 0.09194 = -0.00054 0.00033 0.00053 AFIX 137 H6a 2 0.18783 0.33849 0.80566 10.50000 -1.50000 H6b 2 0.22139 0.39388 0.69006 10.50000 -1.50000 H6c 2 0.03397 0.36199 0.71318 10.50000 -1.50000 AFIX 0 C7 1 0.09179 0.22054 0.63766 10.50000 0.10588 0.10553 0.10631 = 0.00004 0.00037 -0.00059 AFIX 137 H7a 2 -0.02261 0.22892 0.60240 10.50000 -1.50000 H7b 2 0.14904 0.18282 0.58753 10.50000 -1.50000 H7c 2 0.08239 0.20520 0.72781 10.50000 -1.50000 AFIX 0 C8 1 0.64470 0.47077 0.60407 10.50000 0.12325 0.12366 0.12456 = -0.00070 -0.00006 -0.00005 AFIX 137 H8a 2 0.58959 0.43077 0.55846 10.50000 -1.50000 H8b 2 0.65788 0.45826 0.69534 10.50000 -1.50000 H8c 2 0.57403 0.51417 0.59630 10.50000 -1.50000 AFIX 0 HKLF 4 END Q1 1 0.54 0.25 0.361111 11 0.05 1.16 Q2 1 -0.06 0.25 0.722222 11 0.05 0.77 REM The information below was added by Olex2. REM REM R1 = 0.0306 for 1567 Fo > 4sig(Fo) and 0.0329 for all 1678 data REM 115 parameters refined using 54 restraints REM Highest difference peak 1.1619, deepest hole -1.7667 REM Mean Shift 0.0001, Max Shift 0.0022. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0329 REM R1_gt = 0.0306 REM wR_ref = 0.1012 REM GOOF = 0.8877 REM Shift_max = 0.0022 REM Shift_mean = 0.0001 REM Reflections_all = 1678 REM Reflections_gt = 1567 REM Parameters = 115 REM Hole = -1.7667 REM Peak = 1.1619 REM Flack = n/a ; _cod_data_source_file tz4c00924_si_006.cif _cod_data_source_block 3 _cod_database_code 4519547 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2. Rigid bond restraints C7, N1, C6, C5 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01 3. Uiso/Uaniso restraints and constraints C8: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A Uanis(C7) \\sim Ueq, Uanis(C6) \\sim Ueq, Uanis(O1) \\sim Ueq: with sigma of 0.02 and sigma for terminal atoms of 0.04 Uanis(C6) \\sim Ueq, Uanis(C7) \\sim Ueq: with sigma of 0.002 and sigma for terminal atoms of 0.004 : with sigma of 0.002 and sigma for terminal atoms of 0.004 Uanis(C8) \\sim Ueq: with sigma of 0.002 and sigma for terminal atoms of 0.004 Uanis(C7) \\sim Ueq, Uanis(C6) \\sim Ueq: with sigma of 0.002 and sigma for terminal atoms of 0.004 4. Rigid body (RIGU) restrains C8 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 5. Others Fixed Sof: C5(0.5) H5(0.5) N1(0.5) C6(0.5) C7(0.5) C8(0.5) H8a(0.5) H8b(0.5) H8c(0.5) H6a(0.5) H6b(0.5) H6c(0.5) H7a(0.5) H7b(0.5) H7c(0.5) 6.a Aromatic/amide H refined with riding coordinates: C4(H4), C5(H5) 6.b Idealised Me refined as rotating group: C8(H8a,H8b,H8c), C6(H6a,H6b,H6c), C7(H7a,H7b,H7c) ; _iucr_refine_fcf_details ; data_3 _computing_structure_refinement 'olex2.refine 1.5 (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 x+1/2,-y+1/2,-z+1/2 3 -x,y+1/2,-z 4 -x+1/2,-y,z+1/2 5 -x,-y,-z 6 -x-1/2,y-1/2,z-1/2 7 x,-y-1/2,z 8 x-1/2,y,-z-1/2 _space_group_crystal_system orthorhombic _space_group_IT_number 62 _space_group_name_H-M_alt 'P n m a' _space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_Int_Tables_number 62 _cell_length_a 7.6706(6) _cell_length_b 18.1667(17) _cell_length_c 10.1590(9) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 1415.7(2) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status 0 0 2 10250.700 9468.470 601.179 0.059 o 0 0 4 1932.090 2268.690 86.120 1.631 o 0 0 6 8008.310 7777.590 357.296 0.106 o 0 0 8 20489.300 24136.800 1494.930 0.012 o 0 0 10 6653.080 6112.460 229.069 0.170 o 0 0 12 1016.420 1108.000 157.181 2.251 o 0 1 1 96863.600 26506.000 2322.530 0.001 o 0 1 3 8292.550 7016.710 288.003 0.114 o 0 1 5 60.875 96.677 13.026 360.506 o 0 1 7 21874.700 19676.200 691.307 0.016 o 0 1 9 14232.600 13855.200 397.905 0.037 o 0 1 11 2903.740 2886.630 100.067 0.854 o 0 1 13 0.716 24.999 15.862 318.091 o 0 2 2 64169.300 57161.800 3582.080 0.002 o 0 2 4 1736.910 1758.280 54.565 2.404 o 0 2 6 14885.100 15306.900 575.131 0.031 o 0 2 8 15283.100 15278.600 497.916 0.031 o 0 2 10 6741.040 6210.290 196.067 0.171 o 0 2 12 670.118 616.218 104.930 5.260 o 0 3 1 46926.300 39366.300 2749.670 0.003 o 0 3 3 31166.300 31320.300 2133.290 0.006 o 0 3 5 2413.230 3003.470 97.533 1.034 o 0 3 7 16557.700 17606.600 652.069 0.024 o 0 3 9 12383.000 11898.300 361.627 0.049 o 0 3 11 2261.330 2342.780 128.304 1.166 o 0 3 13 8.736 39.380 14.953 353.398 o 0 4 0 78140.900 69727.600 5178.680 0.001 o 0 4 2 21379.800 20387.400 1304.040 0.013 o 0 4 4 159.244 207.890 10.301 193.935 o 0 4 6 9938.340 9268.790 320.769 0.077 o 0 4 8 14384.300 12401.500 455.156 0.038 o 0 4 10 4930.800 4489.900 200.409 0.298 o 0 4 12 585.405 526.739 63.906 11.019 o 0 5 1 45105.000 41760.900 1822.660 0.004 o 0 5 3 11984.800 12154.800 676.712 0.042 o 0 5 5 1109.890 1085.350 29.766 6.164 o 0 5 7 13278.800 11765.600 378.126 0.045 o 0 5 9 10344.000 9416.440 339.277 0.072 o 0 5 11 1870.020 1950.540 134.186 1.487 o 0 6 0 36825.100 34342.000 2288.480 0.004 o 0 6 2 27908.500 28313.000 1471.810 0.008 o 0 6 4 28.301 33.515 3.796 3425.670 o 0 6 6 6249.370 6552.550 173.067 0.185 o 0 6 8 13070.700 11933.000 349.724 0.046 o 0 6 10 4541.750 4412.800 178.604 0.343 o 0 6 12 467.363 448.944 110.353 5.612 o 0 7 1 47283.200 43038.000 2188.080 0.003 o 0 7 3 7445.290 7412.640 273.600 0.128 o 0 7 5 1014.450 1089.640 31.057 6.821 o 0 7 7 10353.700 10446.500 257.540 0.070 o 0 7 9 8715.260 7884.190 240.792 0.104 o 0 7 11 2028.850 1835.460 67.268 1.862 o 0 8 0 56634.000 52900.200 3288.930 0.002 o 0 8 2 27528.800 29454.300 1316.670 0.008 o 0 8 4 617.714 648.279 24.517 17.669 o 0 8 6 4972.020 5088.560 131.851 0.299 o 0 8 8 10811.800 10347.000 286.563 0.066 o 0 8 10 5222.720 5321.270 189.349 0.257 o 0 8 12 408.497 445.016 44.777 21.269 o 0 9 1 50007.700 51763.000 2285.460 0.003 o 0 9 3 4826.740 5638.020 135.292 0.289 o 0 9 5 594.694 608.036 23.858 19.304 o 0 9 7 8957.260 8574.350 215.415 0.097 o 0 9 9 8325.600 7839.420 266.257 0.109 o 0 9 11 2029.220 1831.290 126.646 1.471 o 0 10 0 72722.200 66091.400 8110.670 0.001 o 0 10 2 18372.900 19592.500 676.585 0.020 o 0 10 4 1139.470 1060.360 31.731 5.993 o 0 10 6 3252.570 3366.600 92.658 0.687 o 0 10 8 12567.700 11209.800 316.624 0.051 o 0 10 10 4000.910 4062.920 145.269 0.439 o 0 11 1 41390.600 39791.000 1823.120 0.004 o 0 11 3 3010.450 3259.570 76.866 0.790 o 0 11 5 37.235 51.621 7.820 1018.580 o 0 11 7 13387.900 12602.500 368.407 0.043 o 0 11 9 5260.450 5474.570 245.278 0.233 o 0 11 11 1575.670 1552.540 80.124 2.589 o 0 12 0 29472.600 32159.000 1637.760 0.007 o 0 12 2 15416.300 16316.900 569.758 0.029 o 0 12 4 2330.140 2493.910 67.816 1.306 o 0 12 6 7383.160 6666.330 201.457 0.146 o 0 12 8 7891.580 7271.390 236.492 0.124 o 0 12 10 2839.620 2627.630 183.713 0.727 o 0 13 1 19994.300 21679.700 702.837 0.017 o 0 13 3 7710.950 8004.830 193.009 0.124 o 0 13 5 2133.790 2176.070 111.160 1.373 o 0 13 7 6453.180 5691.670 166.884 0.195 o 0 13 9 4097.260 3875.470 166.180 0.424 o 0 13 11 1310.890 1338.330 58.875 3.843 o 0 14 0 15899.100 18143.300 917.103 0.022 o 0 14 2 11242.100 11852.900 316.474 0.057 o 0 14 4 18.012 76.955 16.856 269.110 o 0 14 6 2886.090 2611.550 116.417 0.876 o 0 14 8 5083.370 4364.550 142.031 0.315 o 0 14 10 2614.900 2629.110 146.008 0.893 o 0 15 1 15965.900 16618.000 457.131 0.028 o 0 15 3 1163.170 1110.410 39.887 5.456 o 0 15 5 280.993 266.371 17.955 74.005 o 0 15 7 4040.340 3835.690 173.865 0.427 o 0 15 9 3417.200 3368.590 121.686 0.615 o 0 16 0 14033.100 16286.600 555.813 0.032 o 0 16 2 4787.910 5194.650 131.050 0.309 o 0 16 4 171.332 196.091 24.424 87.355 o 0 16 6 1667.650 1603.200 62.774 2.586 o 0 16 8 3763.780 3511.840 199.531 0.458 o 0 17 1 9160.710 9923.760 248.204 0.085 o 0 17 3 1893.210 2168.640 66.057 1.834 o 0 17 5 373.464 364.882 24.297 40.880 o 0 17 7 2399.360 2348.670 121.686 1.122 o 0 17 9 2271.350 2261.910 97.836 1.316 o 0 18 0 8459.710 9095.360 346.749 0.092 o 0 18 2 5259.430 5825.830 158.900 0.249 o 0 18 4 76.140 81.167 21.643 151.771 o 0 18 6 997.073 1034.950 90.994 4.345 o 0 18 8 2402.970 2400.380 133.752 1.062 o 0 19 1 6793.240 7769.010 205.785 0.146 o 0 19 3 1332.660 1655.770 70.761 3.117 o 0 19 5 128.515 110.999 17.256 179.101 o 0 19 7 1815.870 1761.330 135.068 1.588 o 0 20 0 6936.740 7902.620 292.258 0.131 o 0 20 2 3191.600 3898.560 168.356 0.551 o 0 20 4 239.380 257.903 48.010 27.608 o 0 20 6 850.359 802.514 67.917 6.936 o 0 21 1 4406.410 5170.720 170.554 0.326 o 0 21 3 1101.900 1389.230 91.593 3.531 o 0 21 5 66.838 78.445 30.844 80.173 o 0 22 0 4336.600 4672.060 587.236 0.148 o 0 22 2 2039.520 2450.270 117.477 1.312 o 0 22 4 144.392 170.693 50.669 28.652 o 0 23 1 2765.490 3174.540 138.764 0.776 o 1 0 1 128.523 142.593 9.708 295.478 o 1 0 2 32607.200 29150.900 1282.340 0.007 o 1 0 3 17272.900 16784.200 617.452 0.024 o 1 0 4 25352.300 25570.700 1097.390 0.010 o 1 0 5 26102.600 28251.300 1258.170 0.009 o 1 0 6 12511.600 13858.300 667.310 0.038 o 1 0 7 3296.760 3116.370 84.709 0.717 o 1 0 8 475.762 524.688 17.547 29.416 o 1 0 9 135.887 205.306 15.756 160.192 o 1 0 10 213.399 200.707 14.763 122.484 o 1 0 11 1778.470 1849.520 97.966 1.908 o 1 0 12 1461.160 1381.210 68.631 3.175 o 1 0 13 1366.070 1423.330 68.644 3.359 o 1 1 1 6156.020 6701.190 217.557 0.179 o 1 1 2 19996.000 18398.900 544.980 0.020 o 1 1 3 17715.900 17863.100 442.859 0.024 o 1 1 4 29275.100 28824.500 914.889 0.009 o 1 1 5 19283.900 19081.400 564.311 0.020 o 1 1 6 12526.000 13802.500 415.199 0.043 o 1 1 7 4592.490 4829.480 89.371 0.355 o 1 1 8 346.016 396.541 16.233 50.805 o 1 1 9 6.042 25.654 8.129 1186.380 o 1 1 10 859.470 889.820 32.282 9.331 o 1 1 11 1419.540 1502.130 62.304 3.234 o 1 1 12 1717.390 1695.620 91.527 2.134 o 1 1 13 890.777 837.517 32.317 9.264 o 1 2 1 18642.100 18134.000 565.936 0.022 o 1 2 2 33422.900 32160.700 1066.430 0.007 o 1 2 3 14380.000 15314.800 440.475 0.034 o 1 2 4 19057.100 18102.700 522.524 0.021 o 1 2 5 23633.300 22893.600 671.821 0.014 o 1 2 6 8827.250 8887.420 215.853 0.097 o 1 2 7 6109.810 6529.000 122.435 0.198 o 1 2 8 434.230 374.124 14.342 41.786 o 1 2 9 235.582 270.989 18.328 84.693 o 1 2 10 332.327 313.921 15.864 61.020 o 1 2 11 1579.660 1721.680 69.175 2.568 o 1 2 12 1294.730 1247.680 68.016 3.826 o 1 2 13 1487.800 1460.710 49.441 3.302 o 1 3 1 1107.170 1235.230 24.379 5.811 o 1 3 2 42904.900 39110.100 1286.810 0.004 o 1 3 3 23114.100 23603.200 666.886 0.014 o 1 3 4 22480.900 23355.400 604.316 0.014 o 1 3 5 16562.000 16629.900 484.697 0.027 o 1 3 6 13928.800 14513.500 551.112 0.035 o 1 3 7 2688.280 2750.210 61.512 1.040 o 1 3 8 677.788 639.382 23.637 16.118 o 1 3 9 2.866 18.709 7.312 1483.190 o 1 3 10 901.116 878.283 60.458 6.898 o 1 3 11 1361.440 1549.520 49.921 3.525 o 1 3 12 1818.080 1755.370 127.479 1.654 o 1 3 13 669.751 723.470 29.611 14.322 o 1 4 1 5019.600 5634.110 147.948 0.272 o 1 4 2 1362.080 1212.380 25.158 4.497 o 1 4 3 34794.300 31591.800 1151.990 0.006 o 1 4 4 29186.200 33141.100 1107.340 0.008 o 1 4 5 25876.700 24642.500 729.464 0.011 o 1 4 6 3387.760 2793.740 59.406 0.763 o 1 4 7 5744.470 5594.600 128.806 0.236 o 1 4 8 310.465 250.012 13.893 77.504 o 1 4 9 21.987 29.414 10.534 686.482 o 1 4 10 575.110 588.254 34.932 17.535 o 1 4 11 1802.940 1716.190 43.885 2.404 o 1 4 12 890.075 1023.460 48.527 7.240 o 1 5 1 203.585 273.943 13.007 117.263 o 1 5 2 15117.900 15530.000 444.850 0.032 o 1 5 3 15756.900 16253.700 470.318 0.029 o 1 5 4 39922.100 40992.200 1361.550 0.004 o 1 5 5 11912.100 11889.000 324.275 0.053 o 1 5 6 11263.200 10584.100 250.282 0.063 o 1 5 7 2209.620 2149.740 49.885 1.592 o 1 5 8 801.686 749.446 21.053 12.175 o 1 5 9 35.093 53.554 12.556 459.617 o 1 5 10 912.292 848.781 38.776 8.500 o 1 5 11 809.294 895.341 47.239 8.676 o 1 5 12 1757.030 1525.800 96.213 2.142 o 1 6 1 3878.810 3841.030 85.207 0.512 o 1 6 2 5051.930 5437.800 147.080 0.277 o 1 6 3 30453.300 31333.800 1000.370 0.008 o 1 6 4 14642.800 14988.200 401.782 0.034 o 1 6 5 23395.700 22456.200 651.199 0.014 o 1 6 6 3933.540 4050.860 75.976 0.491 o 1 6 7 4892.670 4785.340 98.601 0.327 o 1 6 8 371.684 347.570 15.857 51.011 o 1 6 9 32.516 29.539 4.971 2317.180 o 1 6 10 425.980 533.419 20.024 31.688 o 1 6 11 1665.020 1548.020 58.361 2.690 o 1 6 12 893.809 902.143 99.011 4.500 o 1 7 1 284.006 237.081 8.979 100.250 o 1 7 2 21562.700 22981.700 648.519 0.015 o 1 7 3 16644.700 17658.300 409.836 0.026 o 1 7 4 21624.300 22349.300 536.788 0.016 o 1 7 5 7046.510 6974.660 120.784 0.158 o 1 7 6 11404.500 10939.600 206.058 0.061 o 1 7 7 2161.120 2167.730 50.520 1.627 o 1 7 8 567.130 534.644 18.318 23.404 o 1 7 9 23.800 29.618 9.951 759.831 o 1 7 10 931.068 798.517 34.065 8.894 o 1 7 11 1017.490 1099.450 31.114 6.755 o 1 7 12 1469.140 1422.970 103.658 2.518 o 1 8 1 7638.280 9291.950 217.072 0.112 o 1 8 2 7713.250 8272.820 223.535 0.119 o 1 8 3 16716.000 17899.000 463.091 0.026 o 1 8 4 14562.200 16172.600 400.791 0.033 o 1 8 5 15438.300 15178.900 370.149 0.032 o 1 8 6 3693.460 3558.970 66.310 0.584 o 1 8 7 4023.960 3896.990 71.578 0.491 o 1 8 8 1373.130 1304.360 39.837 4.051 o 1 8 9 271.926 237.865 17.750 80.761 o 1 8 10 579.003 616.792 37.440 16.378 o 1 8 11 1139.050 1062.580 63.918 4.870 o 1 8 12 807.176 859.136 104.786 4.516 o 1 9 1 5741.010 6070.390 118.588 0.225 o 1 9 2 9654.410 11103.200 301.577 0.072 o 1 9 3 11211.300 12049.100 322.860 0.056 o 1 9 4 14857.200 15393.000 386.294 0.033 o 1 9 5 7753.090 8004.740 152.981 0.126 o 1 9 6 10788.200 10762.300 184.799 0.067 o 1 9 7 2709.560 2626.140 61.665 1.060 o 1 9 8 62.626 68.948 10.644 517.286 o 1 9 9 7.938 13.307 13.422 443.335 o 1 9 10 597.929 603.436 28.047 18.313 o 1 9 11 652.767 587.964 67.141 9.454 o 1 9 12 1159.230 1168.900 38.434 5.356 o 1 10 1 1978.440 1908.100 31.773 2.046 o 1 10 2 6695.560 6455.400 112.797 0.178 o 1 10 3 11957.300 12784.100 310.487 0.050 o 1 10 4 10586.200 10160.700 201.224 0.071 o 1 10 5 12610.400 11875.400 252.864 0.050 o 1 10 6 7655.380 7672.040 131.763 0.133 o 1 10 7 1468.170 1398.880 42.810 3.534 o 1 10 8 267.400 278.314 11.783 91.913 o 1 10 9 59.454 65.326 15.637 284.444 o 1 10 10 247.587 242.506 18.503 84.774 o 1 10 11 958.032 921.686 47.119 7.189 o 1 11 1 2238.070 2174.590 43.255 1.574 o 1 11 2 6367.470 6476.590 109.264 0.190 o 1 11 3 8137.010 8330.930 142.950 0.116 o 1 11 4 12921.400 12821.400 278.027 0.046 o 1 11 5 10246.400 10202.800 191.453 0.074 o 1 11 6 4617.190 4382.060 79.743 0.378 o 1 11 7 1235.640 1156.590 27.869 5.213 o 1 11 8 386.306 361.245 24.603 39.474 o 1 11 9 5.715 11.407 8.317 1150.980 o 1 11 10 430.994 403.475 28.508 30.973 o 1 11 11 499.626 445.795 41.939 19.681 o 1 12 1 3279.670 3137.970 55.068 0.747 o 1 12 2 3256.940 3291.690 58.088 0.728 o 1 12 3 10236.400 10135.000 187.234 0.075 o 1 12 4 10146.100 10278.400 191.321 0.075 o 1 12 5 6527.920 6479.170 125.765 0.183 o 1 12 6 3986.410 3675.290 81.545 0.510 o 1 12 7 2273.720 2117.350 70.379 1.478 o 1 12 8 241.842 236.050 18.182 88.597 o 1 12 9 15.512 22.864 12.028 542.835 o 1 12 10 309.865 260.982 12.154 79.521 o 1 12 11 881.767 919.280 30.876 8.969 o 1 13 1 1170.130 1259.330 29.653 5.255 o 1 13 2 7152.480 7240.990 125.382 0.151 o 1 13 3 6121.460 5904.760 96.817 0.214 o 1 13 4 6415.930 6547.920 118.140 0.186 o 1 13 5 6395.450 6149.520 120.793 0.194 o 1 13 6 6121.570 5791.310 151.541 0.209 o 1 13 7 805.670 812.144 26.347 11.119 o 1 13 8 254.602 247.512 19.711 78.340 o 1 13 9 15.124 9.367 15.246 342.804 o 1 13 10 398.953 409.766 40.467 24.641 o 1 14 1 2005.170 1840.920 37.556 2.035 o 1 14 2 1547.540 1661.900 35.163 3.043 o 1 14 3 7234.330 7149.160 114.249 0.151 o 1 14 4 6870.430 6656.340 130.255 0.168 o 1 14 5 8053.090 8066.420 177.126 0.118 o 1 14 6 1919.490 1849.430 53.973 2.066 o 1 14 7 1641.760 1549.960 58.908 2.728 o 1 14 8 106.163 113.557 16.077 213.248 o 1 14 9 25.322 33.590 19.365 209.678 o 1 14 10 216.624 184.149 48.433 28.990 o 1 15 1 340.266 355.382 12.762 59.239 o 1 15 2 3045.570 3200.960 55.576 0.811 o 1 15 3 4881.220 4964.770 87.254 0.323 o 1 15 4 9346.480 9196.820 186.613 0.089 o 1 15 5 3066.110 2963.110 71.356 0.828 o 1 15 6 3511.360 3272.390 94.873 0.633 o 1 15 7 481.749 428.504 26.107 28.323 o 1 15 8 210.379 220.029 22.241 84.427 o 1 15 9 0.758 24.474 24.550 133.037 o 1 15 10 236.549 203.954 13.810 114.678 o 1 16 1 676.761 686.399 21.121 15.835 o 1 16 2 2096.340 2466.170 68.689 1.487 o 1 16 3 7223.440 7403.900 134.915 0.146 o 1 16 4 3049.680 3088.350 69.253 0.814 o 1 16 5 5265.500 5352.760 123.140 0.272 o 1 16 6 1067.020 1049.450 38.788 6.289 o 1 16 7 1146.270 1157.440 40.085 5.413 o 1 16 8 240.310 233.111 22.295 75.518 o 1 16 9 3.385 18.050 21.012 181.550 o 1 17 1 776.139 823.954 36.273 10.578 o 1 17 2 3365.310 3610.310 72.907 0.647 o 1 17 3 2583.190 2708.890 81.065 1.064 o 1 17 4 4971.210 5061.040 118.197 0.304 o 1 17 5 1666.620 1656.480 59.908 2.569 o 1 17 6 2731.100 2660.550 91.766 0.982 o 1 17 7 685.070 687.275 36.611 13.284 o 1 17 8 183.236 224.556 30.481 60.948 o 1 17 9 0.718 6.623 10.680 703.422 o 1 18 1 1148.830 1221.490 31.757 5.436 o 1 18 2 1167.070 1392.440 43.546 4.633 o 1 18 3 3533.530 3618.960 77.129 0.604 o 1 18 4 2406.430 2543.880 75.892 1.218 o 1 18 5 3464.520 3552.340 119.937 0.588 o 1 18 6 1107.370 1147.250 57.954 5.044 o 1 18 7 893.169 824.669 36.562 9.009 o 1 18 8 171.704 138.269 30.651 67.053 o 1 19 1 115.771 116.877 16.622 195.250 o 1 19 2 1899.630 2020.230 82.362 1.808 o 1 19 3 2051.530 2400.720 63.841 1.572 o 1 19 4 3140.570 3252.560 194.035 0.579 o 1 19 5 1665.040 1749.290 65.436 2.437 o 1 19 6 1868.750 1949.540 69.338 1.970 o 1 19 7 501.967 530.478 34.449 21.111 o 1 20 1 460.354 552.546 30.122 24.189 o 1 20 2 795.364 913.935 40.869 9.291 o 1 20 3 2319.760 2625.290 73.273 1.254 o 1 20 4 1852.060 2049.780 93.905 1.760 o 1 20 5 2158.240 2372.900 127.358 1.217 o 1 20 6 1131.250 1132.380 57.299 4.990 o 1 21 1 234.738 258.374 29.172 55.765 o 1 21 2 1178.740 1382.670 58.766 4.226 o 1 21 3 1121.040 1158.420 59.379 4.903 o 1 21 4 2079.310 2382.940 105.989 1.366 o 1 21 5 1517.040 1768.560 79.891 2.508 o 1 22 1 303.173 372.006 31.935 38.534 o 1 22 2 576.687 714.172 31.206 16.556 o 1 22 3 1497.450 1580.620 61.860 2.964 o 1 22 4 1289.230 1588.420 93.619 2.861 o 1 23 1 106.471 103.846 40.818 45.163 o 1 23 2 742.249 872.512 33.823 10.972 o 2 0 0 584.937 547.010 65.087 10.688 o 2 0 1 25318.000 25739.100 1312.310 0.010 o 2 0 2 7590.680 7776.260 491.505 0.097 o 2 0 3 9360.570 9430.560 326.918 0.081 o 2 0 4 169.880 184.323 14.895 152.323 o 2 0 5 861.287 936.967 46.824 7.987 o 2 0 6 426.521 428.450 28.980 30.130 o 2 0 7 14395.400 14490.200 425.742 0.035 o 2 0 8 1014.930 963.035 52.714 6.306 o 2 0 9 9391.490 9491.490 314.119 0.081 o 2 0 10 289.751 342.131 50.094 23.248 o 2 0 11 2056.150 2057.040 209.165 0.933 o 2 0 12 1.112 -10.818 64.135 19.517 o 2 1 0 61405.700 54855.400 2365.960 0.002 o 2 1 1 3322.000 3252.340 115.305 0.657 o 2 1 2 37971.400 36240.200 1306.070 0.005 o 2 1 3 1458.760 1488.470 44.452 3.410 o 2 1 4 180.412 234.621 12.596 145.275 o 2 1 5 695.526 865.941 22.932 12.978 o 2 1 6 8622.870 8794.850 185.586 0.102 o 2 1 7 740.665 713.379 23.162 13.634 o 2 1 8 11355.800 11886.800 265.271 0.057 o 2 1 9 473.932 481.614 40.247 20.637 o 2 1 10 5436.750 5584.710 132.075 0.252 o 2 1 11 94.333 124.660 16.448 211.474 o 2 1 12 459.183 483.603 67.051 12.019 o 2 2 0 235.777 242.531 10.093 120.102 o 2 2 1 39508.700 36982.100 1317.020 0.005 o 2 2 2 4926.820 5158.620 171.098 0.287 o 2 2 3 15297.800 16070.400 457.963 0.031 o 2 2 4 16.090 16.475 2.388 9631.740 o 2 2 5 1469.240 1469.950 33.136 3.538 o 2 2 6 814.319 830.919 25.955 10.856 o 2 2 7 13149.600 13533.900 300.028 0.043 o 2 2 8 772.751 882.401 49.338 8.936 o 2 2 9 9558.710 9838.270 211.538 0.082 o 2 2 10 333.727 341.332 23.599 47.571 o 2 2 11 2365.410 2490.540 129.152 1.076 o 2 2 12 2.078 9.589 50.938 30.939 o 2 3 0 69182.300 65715.400 2823.530 0.001 o 2 3 1 2678.940 2436.210 49.569 1.148 o 2 3 2 38654.800 38138.800 1376.310 0.005 o 2 3 3 912.705 918.136 21.709 9.087 o 2 3 4 439.153 585.074 19.271 29.185 o 2 3 5 534.408 623.885 22.150 21.850 o 2 3 6 8177.760 8078.360 146.459 0.117 o 2 3 7 627.306 625.365 17.315 18.993 o 2 3 8 12113.000 12357.300 285.362 0.051 o 2 3 9 461.696 477.933 21.276 30.473 o 2 3 10 5758.710 5755.600 143.382 0.228 o 2 3 11 143.581 172.734 30.772 67.924 o 2 3 12 553.571 561.208 61.619 11.653 o 2 4 0 6556.190 7258.260 302.654 0.145 o 2 4 1 69423.300 65901.500 2154.620 0.002 o 2 4 2 1936.010 1941.340 39.350 2.053 o 2 4 3 16067.000 15776.400 381.013 0.030 o 2 4 4 19.634 31.965 4.575 3021.920 o 2 4 5 1472.060 1516.370 36.654 3.424 o 2 4 6 264.694 295.819 10.668 92.233 o 2 4 7 10512.500 9990.440 196.797 0.072 o 2 4 8 734.205 753.830 34.015 12.083 o 2 4 9 11426.500 11505.000 239.675 0.059 o 2 4 10 428.693 512.664 27.927 28.016 o 2 4 11 2557.280 2554.920 89.344 1.095 o 2 4 12 1.609 23.041 46.900 36.485 o 2 5 0 62754.600 62419.100 2705.810 0.002 o 2 5 1 5528.390 5914.210 167.322 0.231 o 2 5 2 53415.000 52311.000 1616.440 0.003 o 2 5 3 328.780 405.146 16.336 52.758 o 2 5 4 167.690 163.894 8.653 228.171 o 2 5 5 44.624 46.961 4.817 1832.170 o 2 5 6 6297.600 6474.240 117.162 0.192 o 2 5 7 975.348 1044.340 33.118 7.256 o 2 5 8 10852.500 10213.800 210.960 0.068 o 2 5 9 465.817 474.901 19.315 31.223 o 2 5 10 7401.430 7534.520 173.778 0.137 o 2 5 11 111.840 150.673 31.660 69.322 o 2 5 12 268.708 279.017 38.815 35.724 o 2 6 0 10021.300 10264.400 330.775 0.071 o 2 6 1 57697.100 55122.000 1814.440 0.002 o 2 6 2 110.616 88.807 4.398 636.412 o 2 6 3 19279.400 19795.400 458.803 0.020 o 2 6 4 389.138 459.431 13.342 42.700 o 2 6 5 3782.180 3768.130 76.585 0.540 o 2 6 6 654.251 694.939 21.412 16.323 o 2 6 7 8274.220 7954.260 165.949 0.116 o 2 6 8 727.333 739.598 19.983 13.964 o 2 6 9 11549.900 11504.700 290.305 0.057 o 2 6 10 209.138 197.845 19.784 98.722 o 2 6 11 1839.190 1909.690 59.860 2.097 o 2 6 12 12.814 30.676 26.059 117.615 o 2 7 0 42714.200 44574.400 2267.580 0.003 o 2 7 1 906.703 889.418 18.348 9.497 o 2 7 2 30804.700 30522.800 861.162 0.008 o 2 7 3 1904.840 2183.200 41.503 1.929 o 2 7 4 1090.560 1045.980 26.828 6.532 o 2 7 5 256.084 261.984 9.082 107.274 o 2 7 6 7784.160 8104.670 138.650 0.125 o 2 7 7 1007.280 1014.010 28.825 7.284 o 2 7 8 12252.500 11841.800 248.115 0.052 o 2 7 9 286.338 310.043 18.068 67.338 o 2 7 10 4064.590 4109.700 126.015 0.440 o 2 7 11 84.985 114.945 24.381 117.260 o 2 7 12 434.103 462.528 49.558 18.149 o 2 8 0 328.741 311.621 16.291 61.334 o 2 8 1 32813.900 35406.400 992.690 0.007 o 2 8 2 2568.960 2690.550 50.376 1.137 o 2 8 3 8307.040 8331.390 197.070 0.110 o 2 8 4 39.981 39.553 7.688 1070.830 o 2 8 5 1075.170 1126.330 28.657 6.296 o 2 8 6 1102.260 1182.520 34.974 5.747 o 2 8 7 11977.700 11153.500 228.106 0.056 o 2 8 8 287.552 255.096 19.642 69.713 o 2 8 9 6210.580 5987.300 146.074 0.202 o 2 8 10 222.847 235.278 22.894 77.239 o 2 8 11 1625.360 1624.260 75.104 2.505 o 2 8 12 7.076 11.322 8.544 1089.000 o 2 9 0 31341.900 34676.300 1355.860 0.006 o 2 9 1 1282.250 1256.030 23.782 4.783 o 2 9 2 17735.600 17454.800 442.237 0.024 o 2 9 3 937.878 901.897 22.438 8.845 o 2 9 4 553.002 517.310 21.773 23.598 o 2 9 5 317.938 328.374 10.192 70.611 o 2 9 6 5882.530 5839.610 104.336 0.226 o 2 9 7 406.077 348.070 21.375 41.116 o 2 9 8 7847.470 7557.430 157.417 0.128 o 2 9 9 409.336 406.677 19.211 39.404 o 2 9 10 3607.240 3798.520 109.866 0.547 o 2 9 11 49.103 53.479 34.730 65.177 o 2 10 0 2161.210 2133.270 50.792 1.642 o 2 10 1 21431.500 22964.500 532.107 0.016 o 2 10 2 712.193 694.354 19.643 14.940 o 2 10 3 4423.410 4516.200 78.858 0.392 o 2 10 4 5.786 16.517 5.585 2503.110 o 2 10 5 1795.400 1691.950 42.052 2.449 o 2 10 6 335.230 277.967 9.525 73.641 o 2 10 7 5498.010 5429.190 107.636 0.258 o 2 10 8 368.944 320.200 21.922 46.553 o 2 10 9 5804.250 5639.590 137.041 0.230 o 2 10 10 180.144 185.559 18.601 118.577 o 2 10 11 1203.970 1167.610 54.101 4.686 o 2 11 0 23236.100 24125.500 767.169 0.013 o 2 11 1 1084.420 918.844 22.928 7.220 o 2 11 2 11481.600 11608.600 234.772 0.058 o 2 11 3 559.301 515.627 12.230 25.756 o 2 11 4 389.659 368.241 16.440 46.312 o 2 11 5 221.539 252.471 9.485 127.936 o 2 11 6 3240.430 3323.750 74.258 0.715 o 2 11 7 211.934 202.031 13.725 128.726 o 2 11 8 6170.300 5891.860 121.586 0.209 o 2 11 9 468.091 452.877 22.445 30.322 o 2 11 10 2896.000 2970.090 82.278 0.872 o 2 11 11 27.921 23.906 22.581 155.286 o 2 12 0 908.236 950.274 53.242 7.079 o 2 12 1 18551.900 19462.900 460.643 0.021 o 2 12 2 1131.680 1163.190 25.469 5.862 o 2 12 3 3776.120 3965.820 71.225 0.527 o 2 12 4 33.998 55.982 7.315 1137.360 o 2 12 5 787.590 898.530 24.378 10.858 o 2 12 6 181.759 209.425 20.515 102.192 o 2 12 7 4585.540 4475.800 88.779 0.374 o 2 12 8 309.291 278.718 19.958 62.092 o 2 12 9 4000.800 3949.360 115.764 0.466 o 2 12 10 153.353 166.265 33.597 58.289 o 2 12 11 1113.480 1088.160 34.968 5.976 o 2 13 0 18301.400 20112.000 655.073 0.020 o 2 13 1 1001.000 892.132 21.599 8.214 o 2 13 2 10433.600 10080.300 182.010 0.073 o 2 13 3 220.841 212.223 7.167 152.489 o 2 13 4 328.446 366.510 12.056 61.327 o 2 13 5 128.882 144.266 9.897 289.261 o 2 13 6 2524.950 2333.280 64.034 1.241 o 2 13 7 176.885 158.283 10.767 197.124 o 2 13 8 4331.140 4393.760 122.134 0.393 o 2 13 9 315.938 325.669 30.089 41.724 o 2 13 10 2565.270 2343.100 83.662 1.162 o 2 14 0 1443.770 1354.160 48.043 3.600 o 2 14 1 16673.300 16775.500 327.557 0.028 o 2 14 2 442.440 441.050 15.256 36.722 o 2 14 3 3607.580 3548.460 69.055 0.601 o 2 14 4 0.204 6.097 7.751 1335.270 o 2 14 5 504.384 443.329 22.044 28.380 o 2 14 6 131.624 145.470 13.911 211.750 o 2 14 7 3228.340 3280.150 89.166 0.709 o 2 14 8 250.907 236.754 18.440 84.853 o 2 14 9 3850.160 3805.340 134.147 0.486 o 2 14 10 127.750 125.037 13.937 226.052 o 2 15 0 14293.100 15191.300 420.178 0.035 o 2 15 1 691.488 681.296 19.641 15.679 o 2 15 2 8555.370 9398.350 158.728 0.100 o 2 15 3 102.228 127.059 11.423 317.829 o 2 15 4 317.851 361.544 17.375 57.064 o 2 15 5 23.082 35.399 11.579 567.514 o 2 15 6 1873.530 1728.760 48.006 2.254 o 2 15 7 239.922 240.701 25.189 66.275 o 2 15 8 4129.890 3903.040 96.574 0.462 o 2 15 9 228.047 196.991 13.355 123.081 o 2 16 0 748.262 718.207 27.439 12.943 o 2 16 1 10840.100 11273.600 201.159 0.064 o 2 16 2 252.645 235.250 11.553 108.078 o 2 16 3 3919.950 4004.090 82.350 0.494 o 2 16 4 49.205 47.824 7.997 915.201 o 2 16 5 622.889 594.948 21.221 19.046 o 2 16 6 165.910 175.539 17.332 136.905 o 2 16 7 3031.060 2956.690 100.513 0.799 o 2 16 8 311.537 234.898 22.075 61.508 o 2 16 9 2943.950 2709.970 104.901 0.862 o 2 17 0 7696.110 8368.340 225.503 0.118 o 2 17 1 348.479 362.882 15.153 54.329 o 2 17 2 7190.660 7620.620 148.145 0.143 o 2 17 3 179.947 177.253 9.586 194.635 o 2 17 4 156.839 190.048 13.509 172.858 o 2 17 5 18.388 25.337 11.705 568.186 o 2 17 6 1889.570 1831.820 74.034 1.984 o 2 17 7 369.004 349.630 21.153 45.566 o 2 17 8 3027.730 2949.070 118.673 0.771 o 2 18 0 274.167 254.623 22.255 66.257 o 2 18 1 7206.610 7729.090 151.254 0.141 o 2 18 2 284.923 283.215 23.627 58.738 o 2 18 3 1505.980 1668.380 40.519 3.090 o 2 18 4 13.521 24.045 14.835 360.067 o 2 18 5 331.847 291.214 24.190 50.229 o 2 18 6 241.723 232.786 18.386 88.411 o 2 18 7 2466.530 2341.230 89.392 1.202 o 2 18 8 50.220 35.630 27.151 105.946 o 2 19 0 7697.440 8523.320 343.977 0.106 o 2 19 1 326.245 327.884 17.710 58.109 o 2 19 2 2823.660 3103.470 76.915 0.882 o 2 19 3 74.644 68.409 11.046 459.618 o 2 19 4 58.537 49.113 12.214 446.338 o 2 19 5 87.636 95.161 10.180 434.203 o 2 19 6 1069.050 1090.340 60.041 5.287 o 2 19 7 35.389 19.311 12.119 515.011 o 2 20 0 364.885 393.261 43.519 24.363 o 2 20 1 4330.850 4931.980 112.419 0.368 o 2 20 2 129.867 137.968 20.179 137.721 o 2 20 3 692.413 850.528 47.325 10.303 o 2 20 4 7.889 23.155 19.704 205.879 o 2 20 5 227.452 219.760 32.777 50.808 o 2 20 6 15.634 18.657 10.131 761.598 o 2 21 0 3470.380 3946.740 170.156 0.500 o 2 21 1 243.641 232.742 20.407 80.889 o 2 21 2 2225.210 2430.260 64.305 1.415 o 2 21 3 9.027 11.054 15.383 337.918 o 2 21 4 14.481 35.815 25.708 120.620 o 2 21 5 1.467 14.528 34.499 67.434 o 2 22 0 160.370 161.183 60.445 20.524 o 2 22 1 2560.230 2854.320 119.805 0.944 o 2 22 2 97.222 130.287 21.544 138.099 o 2 22 3 587.981 686.104 56.904 11.322 o 2 22 4 3.119 -13.494 82.104 11.909 o 2 23 0 2463.600 2786.070 182.571 0.807 o 2 23 1 110.681 117.375 25.797 101.238 o 3 0 1 1185.560 1080.130 54.804 4.944 o 3 0 2 16707.000 17077.800 915.913 0.022 o 3 0 3 888.262 980.843 66.279 6.252 o 3 0 4 42932.400 41952.700 2175.240 0.004 o 3 0 5 5630.880 5615.150 241.180 0.214 o 3 0 6 17390.500 17432.300 559.954 0.024 o 3 0 7 1052.940 909.428 57.254 6.000 o 3 0 8 531.716 610.396 42.168 16.414 o 3 0 9 72.239 84.766 33.702 67.225 o 3 0 10 1175.660 1212.560 117.702 2.871 o 3 0 11 205.643 241.387 54.737 23.140 o 3 0 12 1909.860 1793.240 173.363 1.234 o 3 1 1 5020.390 5189.400 135.009 0.291 o 3 1 2 4301.880 3591.650 90.662 0.463 o 3 1 3 35220.500 35722.800 1447.750 0.005 o 3 1 4 3701.700 4023.250 90.106 0.524 o 3 1 5 27378.500 27376.200 702.515 0.010 o 3 1 6 3923.050 3903.440 80.496 0.502 o 3 1 7 5548.490 5235.530 101.140 0.262 o 3 1 8 49.616 42.084 16.103 285.187 o 3 1 9 126.977 130.485 12.732 246.023 o 3 1 10 68.716 109.903 15.583 258.305 o 3 1 11 1867.710 1788.060 85.550 1.948 o 3 1 12 258.094 306.536 33.491 42.845 o 3 2 1 4823.230 4623.980 112.136 0.336 o 3 2 2 23422.400 23808.200 809.525 0.013 o 3 2 3 839.240 747.338 28.752 10.900 o 3 2 4 36522.800 35491.700 1457.920 0.005 o 3 2 5 7189.850 6666.470 138.922 0.157 o 3 2 6 11000.700 11050.000 223.641 0.064 o 3 2 7 1550.540 1821.200 42.208 2.797 o 3 2 8 1404.110 1483.180 55.685 3.407 o 3 2 9 46.987 102.277 18.145 215.794 o 3 2 10 1506.180 1525.520 68.313 2.914 o 3 2 11 192.637 279.521 16.736 104.107 o 3 2 12 2037.310 2024.520 95.090 1.594 o 3 3 1 5206.550 5123.670 107.548 0.287 o 3 3 2 7100.590 6838.050 185.617 0.153 o 3 3 3 31563.800 32764.300 1113.920 0.007 o 3 3 4 5996.370 6238.710 137.954 0.207 o 3 3 5 19479.500 19793.500 518.789 0.020 o 3 3 6 2488.990 2723.180 60.533 1.154 o 3 3 7 4991.780 4923.150 92.177 0.314 o 3 3 8 410.733 352.343 18.446 42.904 o 3 3 9 47.646 62.481 10.831 553.787 o 3 3 10 88.167 134.771 20.624 150.657 o 3 3 11 2290.570 2304.700 121.532 1.190 o 3 3 12 392.429 395.012 50.780 19.460 o 3 4 1 1367.990 1328.210 29.229 4.180 o 3 4 2 15635.700 15283.100 469.356 0.031 o 3 4 3 10366.400 9932.580 236.407 0.073 o 3 4 4 25369.700 25809.900 778.786 0.011 o 3 4 5 4140.130 4504.150 82.666 0.426 o 3 4 6 11866.600 11583.300 253.302 0.055 o 3 4 7 2229.890 2313.910 46.211 1.511 o 3 4 8 483.666 516.842 24.846 26.194 o 3 4 9 58.282 55.947 16.525 262.230 o 3 4 10 1177.390 1309.560 59.193 4.358 o 3 4 11 430.465 471.121 29.899 28.017 o 3 4 12 1847.040 1881.190 129.789 1.562 o 3 5 1 6736.300 6540.580 143.361 0.172 o 3 5 2 6398.550 6156.660 130.397 0.193 o 3 5 3 16727.700 16658.800 453.061 0.027 o 3 5 4 6200.310 6334.500 122.767 0.198 o 3 5 5 21028.700 21235.400 561.035 0.017 o 3 5 6 2794.030 3020.790 56.780 0.938 o 3 5 7 3912.160 3967.180 78.165 0.500 o 3 5 8 669.988 644.738 41.660 13.134 o 3 5 9 197.369 196.770 16.286 122.758 o 3 5 10 206.271 255.621 20.004 89.579 o 3 5 11 1470.300 1468.200 85.960 2.770 o 3 5 12 345.480 363.026 45.490 24.301 o 3 6 1 1838.860 1636.920 31.097 2.482 o 3 6 2 14380.100 15155.800 354.207 0.035 o 3 6 3 6243.290 6357.590 116.468 0.197 o 3 6 4 18982.900 18328.000 444.701 0.022 o 3 6 5 5390.090 5428.670 96.766 0.266 o 3 6 6 10839.800 11224.800 206.962 0.064 o 3 6 7 2080.480 2116.260 56.430 1.709 o 3 6 8 294.450 263.562 18.528 69.765 o 3 6 9 1.448 17.921 8.970 991.811 o 3 6 10 761.958 852.602 46.093 9.557 o 3 6 11 262.761 274.918 27.613 54.451 o 3 6 12 1728.710 1721.740 105.474 1.961 o 3 7 1 4406.810 4442.430 78.492 0.399 o 3 7 2 2545.250 2467.340 45.291 1.225 o 3 7 3 18640.300 19081.900 431.628 0.022 o 3 7 4 6275.630 6387.050 111.693 0.195 o 3 7 5 16282.200 15418.300 391.893 0.030 o 3 7 6 3168.830 3322.050 65.034 0.744 o 3 7 7 3516.980 3698.670 78.591 0.598 o 3 7 8 148.862 121.635 13.067 219.264 o 3 7 9 30.155 32.313 15.045 340.354 o 3 7 10 137.403 157.872 25.925 91.217 o 3 7 11 1660.100 1647.740 71.661 2.466 o 3 7 12 257.679 145.497 113.766 5.979 o 3 8 1 423.809 409.365 13.537 41.408 o 3 8 2 11814.500 11716.300 281.537 0.055 o 3 8 3 3997.800 3839.820 67.403 0.501 o 3 8 4 21213.200 20640.200 485.870 0.017 o 3 8 5 3954.000 3954.230 76.178 0.495 o 3 8 6 8274.080 8014.320 142.474 0.116 o 3 8 7 896.959 881.731 25.939 9.305 o 3 8 8 683.093 606.448 30.110 15.349 o 3 8 9 48.577 57.822 16.083 281.339 o 3 8 10 804.271 849.801 44.034 9.277 o 3 8 11 141.072 189.288 37.586 48.373 o 3 9 1 1974.190 1759.330 33.965 2.149 o 3 9 2 2184.880 2071.210 39.391 1.685 o 3 9 3 18587.800 17981.500 429.530 0.023 o 3 9 4 2124.090 2153.580 41.053 1.700 o 3 9 5 15877.600 15910.100 344.599 0.030 o 3 9 6 3643.000 3569.210 73.134 0.589 o 3 9 7 3305.720 3370.610 90.994 0.675 o 3 9 8 9.049 26.939 13.518 433.958 o 3 9 9 61.466 74.681 12.924 381.511 o 3 9 10 57.022 114.798 23.640 130.111 o 3 9 11 1302.950 1292.350 73.205 3.609 o 3 10 1 1791.620 1642.650 32.169 2.558 o 3 10 2 9504.940 9535.900 173.741 0.086 o 3 10 3 1399.660 1519.010 33.350 3.677 o 3 10 4 18928.600 18068.300 443.244 0.022 o 3 10 5 2345.210 2310.550 48.555 1.413 o 3 10 6 8581.480 8553.060 166.044 0.105 o 3 10 7 446.137 375.803 14.163 40.398 o 3 10 8 315.812 314.275 14.232 67.087 o 3 10 9 12.017 29.745 13.267 447.919 o 3 10 10 559.650 539.734 27.603 21.015 o 3 10 11 113.659 161.048 59.589 21.590 o 3 11 1 2630.340 2512.380 47.402 1.157 o 3 11 2 1597.990 1447.400 34.306 3.194 o 3 11 3 15200.500 14425.600 269.467 0.035 o 3 11 4 1747.870 1665.730 40.498 2.570 o 3 11 5 12031.800 11713.500 222.636 0.055 o 3 11 6 1490.560 1518.640 40.979 3.321 o 3 11 7 2760.080 2738.640 81.094 0.975 o 3 11 8 107.567 87.558 10.741 369.663 o 3 11 9 46.377 40.329 9.818 691.691 o 3 11 10 33.442 43.113 17.360 255.013 o 3 11 11 1068.080 439.532 111.131 4.071 o 3 12 1 748.480 671.609 24.302 13.804 o 3 12 2 9126.300 9367.990 152.143 0.092 o 3 12 3 2015.810 1948.670 44.955 1.923 o 3 12 4 12718.300 12546.200 240.334 0.048 o 3 12 5 1251.150 1409.060 40.846 4.301 o 3 12 6 5442.540 5264.390 116.688 0.265 o 3 12 7 602.807 614.146 29.237 17.706 o 3 12 8 501.095 558.996 19.594 25.964 o 3 12 9 6.035 2.005 14.711 370.605 o 3 12 10 593.337 527.985 25.536 20.486 o 3 13 1 1436.870 1346.350 33.087 3.844 o 3 13 2 1702.170 1534.720 41.808 2.782 o 3 13 3 11944.700 11532.000 203.332 0.056 o 3 13 4 1102.200 1163.550 40.524 5.636 o 3 13 5 7458.500 7579.890 143.489 0.138 o 3 13 6 1615.600 1565.140 41.377 2.944 o 3 13 7 2142.060 1975.240 47.138 1.755 o 3 13 8 116.139 87.436 16.012 217.007 o 3 13 9 37.163 34.266 21.448 169.685 o 3 13 10 25.559 53.725 33.286 71.669 o 3 14 1 589.665 501.391 14.354 24.003 o 3 14 2 4481.880 4671.000 93.086 0.373 o 3 14 3 1779.540 1825.590 48.145 2.325 o 3 14 4 9434.200 9385.160 185.767 0.087 o 3 14 5 1725.040 1750.540 60.764 2.379 o 3 14 6 3953.140 3950.470 87.514 0.490 o 3 14 7 512.934 501.334 17.302 27.771 o 3 14 8 203.668 217.761 11.142 143.797 o 3 14 9 19.897 13.720 23.022 150.561 o 3 15 1 1140.080 1122.250 31.337 5.799 o 3 15 2 672.196 652.666 32.876 14.564 o 3 15 3 6571.220 6663.380 128.323 0.177 o 3 15 4 2130.830 2145.750 64.389 1.613 o 3 15 5 6042.620 6194.140 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4079.380 4223.100 134.598 0.426 o 4 0 7 451.655 571.516 39.573 20.157 o 4 0 8 9642.290 10228.300 358.491 0.073 o 4 0 9 2741.290 2829.350 100.297 0.925 o 4 0 10 3572.120 3321.260 152.405 0.554 o 4 0 11 214.260 282.670 72.654 13.745 o 4 0 12 505.231 467.136 91.560 7.427 o 4 1 0 9656.640 8523.240 288.022 0.085 o 4 1 1 37938.800 39242.600 1134.960 0.005 o 4 1 2 4175.340 4068.580 102.662 0.441 o 4 1 3 6630.900 5911.770 149.065 0.186 o 4 1 4 3.677 9.662 5.564 2566.750 o 4 1 5 567.559 567.039 19.259 22.361 o 4 1 6 877.745 885.401 30.796 9.230 o 4 1 7 8707.460 8636.570 168.923 0.103 o 4 1 8 2541.530 2743.400 68.975 1.103 o 4 1 9 6343.930 6524.750 145.358 0.186 o 4 1 10 950.376 987.032 86.487 4.794 o 4 1 11 1700.070 1632.050 118.766 1.901 o 4 1 12 9.584 20.800 25.807 120.224 o 4 2 0 32041.600 33655.100 1575.130 0.006 o 4 2 1 8341.260 8169.450 173.987 0.112 o 4 2 2 23797.900 26359.800 741.084 0.012 o 4 2 3 951.563 903.805 38.483 7.844 o 4 2 4 585.568 504.977 24.109 21.681 o 4 2 5 174.736 189.391 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42.188 o 4 4 5 381.894 426.186 15.946 43.926 o 4 4 6 3860.530 3927.030 86.918 0.507 o 4 4 7 2551.060 2400.830 82.925 1.156 o 4 4 8 7269.900 7359.490 167.882 0.143 o 4 4 9 1165.700 1090.620 75.334 4.296 o 4 4 10 2930.600 2950.370 86.113 0.857 o 4 4 11 193.186 219.257 26.017 74.033 o 4 5 0 12095.400 10961.200 387.971 0.053 o 4 5 1 21032.400 21474.500 529.534 0.017 o 4 5 2 2056.440 2043.640 43.274 1.825 o 4 5 3 3736.060 3682.930 80.889 0.554 o 4 5 4 238.003 222.671 11.097 120.627 o 4 5 5 250.219 253.768 12.195 102.827 o 4 5 6 1373.660 1323.460 37.400 4.052 o 4 5 7 7091.680 6988.380 160.184 0.153 o 4 5 8 2203.550 2041.620 72.248 1.561 o 4 5 9 4541.510 4844.970 104.729 0.354 o 4 5 10 547.817 565.871 43.426 16.208 o 4 5 11 1278.780 1226.030 59.406 4.131 o 4 6 0 25119.600 23766.800 744.153 0.012 o 4 6 1 6041.990 5856.330 114.686 0.217 o 4 6 2 9088.390 9099.380 181.150 0.093 o 4 6 3 378.684 363.142 18.561 46.150 o 4 6 4 508.722 530.685 18.270 26.789 o 4 6 5 52.407 83.652 10.022 573.826 o 4 6 6 3559.920 3641.280 87.356 0.589 o 4 6 7 2664.010 2467.040 87.621 1.068 o 4 6 8 5875.080 6408.550 192.781 0.199 o 4 6 9 1008.990 960.175 36.410 7.180 o 4 6 10 2573.840 2649.740 73.463 1.100 o 4 6 11 216.946 223.360 29.504 59.446 o 4 7 0 8495.410 7781.680 198.315 0.111 o 4 7 1 20129.900 19160.100 497.852 0.019 o 4 7 2 2512.600 2495.160 53.661 1.222 o 4 7 3 3749.360 3978.470 78.336 0.526 o 4 7 4 57.017 36.478 6.707 1144.330 o 4 7 5 337.494 336.929 13.260 61.117 o 4 7 6 1237.070 1283.760 31.571 4.811 o 4 7 7 5401.020 5349.020 110.639 0.266 o 4 7 8 1602.340 1478.550 93.508 2.424 o 4 7 9 4174.190 4431.410 104.293 0.417 o 4 7 10 565.406 528.071 42.034 16.640 o 4 7 11 1213.060 1158.160 63.662 4.380 o 4 8 0 23892.000 23184.800 852.974 0.013 o 4 8 1 5747.020 5263.940 101.646 0.249 o 4 8 2 11589.400 10473.600 226.096 0.061 o 4 8 3 587.879 505.272 15.066 23.845 o 4 8 4 518.763 573.947 16.293 25.479 o 4 8 5 165.365 180.347 12.334 181.488 o 4 8 6 2879.030 2970.190 61.980 0.907 o 4 8 7 1513.360 1498.870 40.222 3.294 o 4 8 8 4973.070 5263.670 120.454 0.296 o 4 8 9 1126.330 1082.960 56.693 5.154 o 4 8 10 2662.200 2707.960 77.104 1.034 o 4 8 11 208.498 257.152 36.226 44.176 o 4 9 0 8067.280 7103.640 237.098 0.122 o 4 9 1 18619.700 18186.000 499.074 0.022 o 4 9 2 2011.850 1945.120 40.053 1.949 o 4 9 3 4500.660 4721.360 87.409 0.370 o 4 9 4 39.606 58.092 5.295 1638.960 o 4 9 5 405.349 371.350 15.820 44.533 o 4 9 6 508.138 520.356 19.566 26.703 o 4 9 7 4533.950 4474.460 101.096 0.375 o 4 9 8 1407.040 1347.100 37.941 3.882 o 4 9 9 4124.560 4371.380 116.689 0.421 o 4 9 10 612.446 617.466 59.053 11.060 o 4 9 11 1080.650 1004.890 136.748 2.691 o 4 10 0 25283.500 23580.600 809.699 0.012 o 4 10 1 4647.400 4459.950 88.760 0.368 o 4 10 2 9944.950 9596.840 171.871 0.081 o 4 10 3 570.742 479.170 12.141 26.187 o 4 10 4 514.225 532.967 13.342 27.809 o 4 10 5 140.775 169.486 10.540 238.125 o 4 10 6 2233.700 2242.920 52.347 1.521 o 4 10 7 1074.370 1041.720 27.662 6.649 o 4 10 8 5104.760 5374.370 108.498 0.285 o 4 10 9 1160.920 1092.780 53.958 5.060 o 4 10 10 2204.480 2226.230 85.104 1.430 o 4 11 0 2047.060 2133.890 62.679 1.707 o 4 11 1 16431.300 16666.400 367.913 0.028 o 4 11 2 3368.180 3342.000 61.461 0.688 o 4 11 3 2812.950 2722.700 63.385 0.986 o 4 11 4 6.648 20.194 8.917 994.056 o 4 11 5 197.910 187.819 11.270 158.820 o 4 11 6 703.144 717.416 20.458 14.785 o 4 11 7 4643.400 4529.090 89.773 0.365 o 4 11 8 1149.840 1041.390 34.601 5.903 o 4 11 9 3345.600 3396.410 107.145 0.645 o 4 11 10 438.581 467.307 36.036 24.276 o 4 12 0 14558.100 13590.500 370.975 0.037 o 4 12 1 2210.780 2062.230 41.880 1.657 o 4 12 2 8167.920 7779.450 139.048 0.121 o 4 12 3 1169.150 1085.380 36.800 5.584 o 4 12 4 330.723 364.628 19.433 51.880 o 4 12 5 158.960 128.570 12.643 210.516 o 4 12 6 2402.990 2311.520 53.680 1.357 o 4 12 7 1390.910 1335.280 37.233 3.970 o 4 12 8 3830.600 3883.440 118.587 0.495 o 4 12 9 689.296 639.712 38.736 13.321 o 4 12 10 1760.040 1808.160 48.987 2.365 o 4 13 0 3067.380 2942.030 83.240 0.815 o 4 13 1 9773.610 9204.540 161.585 0.085 o 4 13 2 1293.850 1243.180 28.969 4.682 o 4 13 3 3031.750 2822.970 64.432 0.874 o 4 13 4 55.765 65.734 6.015 1129.310 o 4 13 5 674.725 700.923 20.456 15.774 o 4 13 6 690.498 654.618 26.416 15.142 o 4 13 7 2760.820 2625.230 68.680 1.023 o 4 13 8 1057.400 997.818 49.458 6.077 o 4 13 9 2714.800 2581.790 121.289 0.933 o 4 14 0 8870.900 8299.890 226.466 0.100 o 4 14 1 2275.060 2044.480 49.411 1.582 o 4 14 2 5103.120 5203.980 104.816 0.292 o 4 14 3 163.894 162.935 12.699 187.206 o 4 14 4 44.815 42.674 15.780 299.038 o 4 14 5 42.760 36.347 12.120 491.305 o 4 14 6 1351.710 1320.970 40.501 4.089 o 4 14 7 1022.090 966.248 48.493 6.463 o 4 14 8 2794.480 2538.460 72.798 1.020 o 4 14 9 356.790 326.011 31.001 37.134 o 4 15 0 2657.440 2257.010 97.968 1.095 o 4 15 1 6976.110 6430.920 127.837 0.168 o 4 15 2 972.639 851.396 22.232 8.741 o 4 15 3 1033.010 994.639 28.505 7.155 o 4 15 4 1.675 5.399 7.836 1305.520 o 4 15 5 144.914 163.562 11.829 217.957 o 4 15 6 312.074 312.277 17.128 63.328 o 4 15 7 2180.810 2131.010 76.720 1.523 o 4 15 8 540.152 464.164 46.636 16.637 o 4 16 0 6834.240 6593.840 193.180 0.163 o 4 16 1 1643.650 1451.710 34.515 3.071 o 4 16 2 2659.390 2557.120 70.658 1.086 o 4 16 3 131.793 161.391 15.453 182.679 o 4 16 4 135.958 143.563 15.075 191.576 o 4 16 5 58.898 60.401 11.099 506.618 o 4 16 6 972.504 958.078 36.808 7.490 o 4 16 7 458.806 436.634 31.876 26.289 o 4 16 8 1843.510 1914.910 83.263 1.921 o 4 17 0 2000.510 1840.160 70.234 1.874 o 4 17 1 4559.040 4518.880 89.921 0.374 o 4 17 2 516.530 486.881 17.582 27.914 o 4 17 3 992.073 1017.010 42.201 6.810 o 4 17 4 15.667 21.068 21.827 167.434 o 4 17 5 117.464 129.479 14.770 219.533 o 4 17 6 256.359 272.696 27.775 55.105 o 4 17 7 1380.360 1504.450 57.759 3.409 o 4 18 0 4583.670 4327.500 140.918 0.361 o 4 18 1 1161.670 1063.240 45.130 5.432 o 4 18 2 2400.880 2417.730 58.697 1.308 o 4 18 3 142.489 140.418 14.941 189.204 o 4 18 4 105.583 105.925 16.507 208.958 o 4 18 5 39.300 76.987 13.774 370.589 o 4 18 6 605.425 591.400 33.140 17.055 o 4 19 0 1063.670 1057.160 56.312 5.560 o 4 19 1 3381.660 3338.660 95.441 0.655 o 4 19 2 472.237 416.248 38.722 22.572 o 4 19 3 802.795 814.715 50.311 8.881 o 4 19 4 5.154 12.456 25.441 123.925 o 4 19 5 69.312 59.233 24.133 128.271 o 4 20 0 3424.420 3355.590 134.618 0.600 o 4 20 1 685.767 636.032 37.513 13.641 o 4 20 2 1759.200 1779.900 70.529 2.220 o 4 20 3 158.131 146.058 20.359 123.133 o 4 20 4 96.328 113.713 19.158 170.339 o 4 21 0 469.515 528.946 53.194 15.368 o 4 21 1 2405.720 2493.100 74.943 1.237 o 4 21 2 366.310 318.332 51.550 20.666 o 5 0 1 1582.210 1329.660 121.898 2.152 o 5 0 2 917.458 889.777 101.006 4.351 o 5 0 3 23143.800 25443.600 1418.310 0.010 o 5 0 4 1827.280 1828.590 65.628 2.129 o 5 0 5 13289.600 13171.600 397.438 0.042 o 5 0 6 417.631 566.223 43.943 19.517 o 5 0 7 2966.220 3194.220 110.925 0.766 o 5 0 8 461.099 492.435 134.487 3.953 o 5 0 9 4.471 -7.734 37.869 55.977 o 5 0 10 0.046 21.430 65.884 18.493 o 5 0 11 1798.480 1870.420 356.006 0.502 o 5 1 1 166.321 203.158 14.896 148.429 o 5 1 2 9781.870 8751.690 239.135 0.085 o 5 1 3 1422.000 1345.530 59.841 3.478 o 5 1 4 21083.500 20895.400 543.941 0.017 o 5 1 5 687.363 746.738 23.926 14.405 o 5 1 6 8070.420 8662.120 194.251 0.111 o 5 1 7 433.408 463.992 28.754 28.727 o 5 1 8 700.648 791.408 60.754 8.887 o 5 1 9 57.964 42.747 27.707 100.903 o 5 1 10 920.709 1070.560 103.151 4.002 o 5 1 11 40.717 110.675 86.473 10.678 o 5 2 1 3328.540 3071.440 74.056 0.726 o 5 2 2 541.763 606.695 29.956 19.717 o 5 2 3 20808.900 21421.900 657.354 0.017 o 5 2 4 1004.240 996.158 28.873 7.389 o 5 2 5 13951.500 13747.800 352.506 0.039 o 5 2 6 754.658 896.670 43.244 9.670 o 5 2 7 3635.980 3606.370 118.496 0.552 o 5 2 8 109.467 100.678 16.725 204.159 o 5 2 9 56.329 51.136 30.243 85.004 o 5 2 10 0.199 48.492 30.854 84.098 o 5 2 11 1451.450 1586.380 193.686 1.340 o 5 3 1 80.327 108.301 5.711 710.500 o 5 3 2 12566.100 12428.700 286.494 0.049 o 5 3 3 786.496 677.473 27.029 12.627 o 5 3 4 17867.400 17639.700 462.707 0.024 o 5 3 5 992.881 966.284 26.230 7.741 o 5 3 6 11787.300 11646.300 275.238 0.055 o 5 3 7 192.265 180.790 19.571 108.764 o 5 3 8 251.505 311.796 23.162 63.008 o 5 3 9 15.771 9.639 19.889 201.991 o 5 3 10 689.625 620.703 48.091 11.881 o 5 3 11 15.516 60.388 37.605 56.400 o 5 4 1 3763.860 3798.080 77.879 0.540 o 5 4 2 12.056 20.249 9.289 907.504 o 5 4 3 16420.700 16370.500 396.618 0.028 o 5 4 4 1167.010 1306.400 37.203 4.984 o 5 4 5 19140.500 18500.900 430.189 0.021 o 5 4 6 121.480 129.844 18.384 163.037 o 5 4 7 2845.080 2730.630 101.310 0.902 o 5 4 8 111.341 108.575 16.084 210.928 o 5 4 9 79.958 65.689 15.012 284.772 o 5 4 10 4.322 63.161 31.428 80.810 o 5 4 11 1184.510 963.572 114.804 3.146 o 5 5 1 16.764 14.284 3.501 5426.680 o 5 5 2 8433.800 8629.750 185.208 0.106 o 5 5 3 495.952 533.191 19.221 27.179 o 5 5 4 23344.300 24182.000 665.310 0.013 o 5 5 5 346.718 344.220 21.154 48.838 o 5 5 6 9078.110 9136.110 228.920 0.091 o 5 5 7 190.554 163.629 21.156 103.283 o 5 5 8 307.147 321.727 26.663 47.663 o 5 5 9 37.438 19.545 20.273 190.742 o 5 5 10 569.836 542.643 81.770 8.166 o 5 5 11 27.441 55.770 26.047 116.005 o 5 6 1 2460.130 2457.140 46.561 1.282 o 5 6 2 99.221 119.847 7.860 460.469 o 5 6 3 17428.400 17262.600 501.903 0.025 o 5 6 4 375.992 360.592 18.484 46.757 o 5 6 5 15244.400 15930.300 404.323 0.031 o 5 6 6 223.535 268.074 20.825 80.127 o 5 6 7 2698.260 2594.430 74.905 1.049 o 5 6 8 78.540 60.100 20.830 165.082 o 5 6 9 21.910 12.918 34.245 68.248 o 5 6 10 0.183 17.896 34.440 67.662 o 5 7 1 8.188 16.638 5.758 2336.030 o 5 7 2 12354.000 12130.300 229.981 0.051 o 5 7 3 422.929 409.835 21.826 36.028 o 5 7 4 14010.700 14747.300 323.771 0.038 o 5 7 5 564.860 563.834 34.232 18.419 o 5 7 6 7871.200 8253.260 190.895 0.119 o 5 7 7 132.164 140.746 13.277 223.885 o 5 7 8 410.696 456.961 28.360 30.641 o 5 7 9 44.723 25.201 28.655 96.061 o 5 7 10 619.181 622.168 32.123 16.458 o 5 8 1 5189.800 5250.290 95.775 0.286 o 5 8 2 265.661 237.932 14.156 93.579 o 5 8 3 11148.600 11821.900 223.545 0.060 o 5 8 4 674.035 691.898 31.836 14.241 o 5 8 5 11408.500 11701.000 301.128 0.057 o 5 8 6 264.001 273.577 25.924 57.925 o 5 8 7 2764.130 2853.210 78.431 0.953 o 5 8 8 164.748 143.087 22.524 106.263 o 5 8 9 59.418 44.643 24.091 131.589 o 5 8 10 0.767 14.046 24.632 132.257 o 5 9 1 435.377 457.355 15.044 36.722 o 5 9 2 7302.080 7333.020 131.614 0.145 o 5 9 3 479.555 501.859 17.706 29.899 o 5 9 4 13060.900 13502.500 280.003 0.044 o 5 9 5 328.650 355.015 27.930 41.841 o 5 9 6 5030.760 4766.890 119.665 0.310 o 5 9 7 303.277 288.936 26.683 50.083 o 5 9 8 374.750 381.512 28.354 36.077 o 5 9 9 38.870 26.806 26.995 108.360 o 5 9 10 570.286 530.009 49.877 14.365 o 5 10 1 701.643 754.422 24.921 13.856 o 5 10 2 469.770 412.225 12.720 36.623 o 5 10 3 11214.400 10880.100 212.808 0.063 o 5 10 4 581.298 569.639 23.169 20.740 o 5 10 5 8827.130 9016.040 192.113 0.097 o 5 10 6 463.519 523.214 28.802 25.354 o 5 10 7 1696.870 1766.800 64.287 2.381 o 5 10 8 153.151 134.175 19.967 130.698 o 5 10 9 17.864 15.258 55.396 26.137 o 5 11 1 4.150 7.952 8.028 1240.130 o 5 11 2 4397.840 4352.250 86.826 0.402 o 5 11 3 565.301 557.467 29.590 19.863 o 5 11 4 11339.300 11300.600 227.553 0.060 o 5 11 5 631.044 641.741 28.001 16.686 o 5 11 6 3471.310 3434.080 77.718 0.639 o 5 11 7 163.660 152.229 9.924 226.777 o 5 11 8 348.922 414.640 23.969 41.178 o 5 11 9 23.001 22.622 25.116 126.219 o 5 12 1 1220.940 1218.490 30.325 5.079 o 5 12 2 55.013 48.982 12.969 409.027 o 5 12 3 7238.310 6918.470 149.671 0.151 o 5 12 4 807.365 798.468 21.976 11.546 o 5 12 5 7091.690 6923.490 147.594 0.155 o 5 12 6 277.878 249.512 15.892 82.504 o 5 12 7 1603.110 1561.380 41.306 2.978 o 5 12 8 59.394 60.931 27.347 102.435 o 5 12 9 49.065 52.887 34.646 65.499 o 5 13 1 11.891 19.948 6.504 1806.940 o 5 13 2 4007.830 3722.820 85.273 0.501 o 5 13 3 316.580 303.044 13.025 70.206 o 5 13 4 7446.630 7335.250 144.907 0.141 o 5 13 5 376.405 335.119 23.312 43.196 o 5 13 6 3817.380 3900.000 100.408 0.508 o 5 13 7 102.719 88.074 26.309 101.895 o 5 13 8 165.523 216.265 24.666 85.293 o 5 14 1 1121.170 1030.510 30.446 6.258 o 5 14 2 79.808 62.687 9.388 561.209 o 5 14 3 5497.080 5145.750 108.577 0.267 o 5 14 4 306.770 257.322 21.102 62.332 o 5 14 5 5923.080 5550.930 128.306 0.228 o 5 14 6 83.185 84.941 16.896 225.732 o 5 14 7 1245.050 1258.730 58.173 4.225 o 5 14 8 30.164 26.036 12.814 465.453 o 5 15 1 2.073 11.309 6.779 1736.780 o 5 15 2 3179.600 3024.640 71.935 0.779 o 5 15 3 278.464 268.341 19.508 70.590 o 5 15 4 6050.910 5777.040 142.945 0.214 o 5 15 5 83.848 89.044 15.281 261.721 o 5 15 6 2785.840 2757.690 70.584 0.978 o 5 15 7 57.172 33.923 13.077 410.807 o 5 16 1 946.397 847.189 26.661 8.868 o 5 16 2 70.356 54.416 13.934 339.495 o 5 16 3 4655.390 4395.650 105.528 0.365 o 5 16 4 112.787 124.228 21.806 131.296 o 5 16 5 3949.130 3904.920 93.373 0.491 o 5 16 6 54.037 31.392 19.930 191.676 o 5 16 7 842.547 921.325 72.796 6.249 o 5 17 1 24.213 25.907 12.098 526.418 o 5 17 2 2678.590 2448.420 84.740 1.072 o 5 17 3 73.547 33.203 44.687 39.488 o 5 17 4 3946.410 3706.970 95.121 0.506 o 5 17 5 106.985 87.902 25.844 104.376 o 5 17 6 1833.560 1713.890 82.652 2.058 o 5 18 1 847.562 807.992 23.082 10.712 o 5 18 2 45.128 53.220 9.657 691.333 o 5 18 3 2891.120 2804.520 105.319 0.863 o 5 18 4 115.156 83.092 34.460 61.916 o 5 18 5 2613.940 2520.330 86.338 1.083 o 5 19 1 13.864 25.414 10.548 701.753 o 5 19 2 1480.020 1453.410 53.240 3.280 o 5 19 3 89.923 76.656 28.688 89.592 o 5 19 4 2538.060 2375.370 164.664 0.904 o 5 20 1 236.648 240.906 15.590 99.137 o 5 20 2 49.214 45.103 11.656 505.718 o 6 0 0 6634.030 6416.280 280.493 0.158 o 6 0 1 9218.500 8654.670 297.194 0.089 o 6 0 2 5067.020 5372.940 248.024 0.244 o 6 0 3 2283.760 2352.760 126.361 1.160 o 6 0 4 22.654 22.736 18.538 230.162 o 6 0 5 595.881 591.911 30.466 17.988 o 6 0 6 1780.930 1853.610 117.846 1.727 o 6 0 7 1791.260 2059.720 147.703 1.404 o 6 0 8 2645.750 2895.990 130.299 0.878 o 6 0 9 2991.680 3358.900 151.072 0.670 o 6 0 10 901.679 802.563 162.645 2.361 o 6 1 0 9635.540 9746.200 316.938 0.077 o 6 1 1 7516.590 7633.710 166.303 0.134 o 6 1 2 6434.420 6356.930 160.468 0.184 o 6 1 3 1819.020 1739.390 47.719 2.333 o 6 1 4 166.742 207.862 22.183 98.181 o 6 1 5 510.078 596.412 30.829 20.830 o 6 1 6 1130.550 1270.680 72.808 4.190 o 6 1 7 2651.220 2605.650 93.457 1.026 o 6 1 8 3246.340 3976.190 154.088 0.552 o 6 1 9 1721.660 1812.610 89.717 2.072 o 6 1 10 1638.530 1559.050 109.158 2.118 o 6 2 0 6991.310 6788.440 214.181 0.153 o 6 2 1 10784.900 10457.000 205.657 0.068 o 6 2 2 5217.930 5603.360 119.955 0.267 o 6 2 3 2078.000 2194.780 64.561 1.639 o 6 2 4 64.894 65.617 7.305 838.067 o 6 2 5 335.832 301.813 19.208 56.461 o 6 2 6 2045.120 2082.750 87.660 1.605 o 6 2 7 2268.540 2490.710 118.046 1.167 o 6 2 8 2210.340 2291.680 118.702 1.251 o 6 2 9 2571.270 2900.180 178.598 0.774 o 6 2 10 1022.230 1140.030 69.231 4.999 o 6 3 0 12296.800 12657.200 346.469 0.048 o 6 3 1 6779.820 7252.120 148.164 0.160 o 6 3 2 6383.630 7001.150 149.156 0.176 o 6 3 3 2151.410 2099.370 58.783 1.638 o 6 3 4 457.401 565.271 28.348 24.796 o 6 3 5 945.312 875.834 38.264 8.054 o 6 3 6 1515.400 1611.280 53.378 2.996 o 6 3 7 1888.160 1864.830 135.641 1.493 o 6 3 8 3203.600 3649.900 179.888 0.555 o 6 3 9 1786.520 1946.070 108.569 1.759 o 6 3 10 1534.210 1601.680 90.139 2.481 o 6 4 0 9230.550 9108.880 226.587 0.090 o 6 4 1 11055.400 11063.600 213.846 0.063 o 6 4 2 4961.520 5006.930 113.512 0.308 o 6 4 3 3278.400 3534.460 94.538 0.658 o 6 4 4 1.953 24.917 7.164 1536.680 o 6 4 5 254.563 304.214 24.008 61.219 o 6 4 6 1184.230 1228.080 44.191 4.918 o 6 4 7 2823.960 2766.730 151.507 0.790 o 6 4 8 2138.640 2203.190 119.202 1.319 o 6 4 9 2412.350 2436.210 138.050 1.034 o 6 4 10 1128.000 1101.990 115.331 3.108 o 6 5 0 12310.100 11777.900 277.115 0.052 o 6 5 1 8332.970 8464.300 152.915 0.111 o 6 5 2 6955.570 7195.600 151.218 0.155 o 6 5 3 317.933 368.224 13.085 62.164 o 6 5 4 445.838 514.756 19.035 31.358 o 6 5 5 119.764 140.098 22.608 119.602 o 6 5 6 1709.000 1661.260 50.311 2.573 o 6 5 7 2232.030 2148.790 63.587 1.525 o 6 5 8 3002.790 3167.080 116.410 0.750 o 6 5 9 1707.530 1722.130 81.589 2.231 o 6 5 10 1462.080 1424.940 117.388 2.307 o 6 6 0 10217.600 10331.200 240.437 0.072 o 6 6 1 10761.600 10555.800 198.319 0.068 o 6 6 2 2812.290 2864.800 63.008 0.955 o 6 6 3 2373.990 2377.810 84.352 1.264 o 6 6 4 123.001 146.314 16.785 177.316 o 6 6 5 182.166 195.740 12.411 159.740 o 6 6 6 1301.720 1311.440 40.230 4.305 o 6 6 7 2633.410 2643.460 77.390 1.063 o 6 6 8 2299.680 2231.800 82.916 1.367 o 6 6 9 2266.020 2226.370 130.861 1.183 o 6 6 10 728.655 642.071 96.845 5.623 o 6 7 0 12266.000 11527.300 307.602 0.052 o 6 7 1 4436.990 4320.520 87.585 0.399 o 6 7 2 4950.860 5011.550 113.525 0.309 o 6 7 3 2398.130 2385.250 74.842 1.276 o 6 7 4 157.200 206.837 10.469 195.107 o 6 7 5 684.989 639.116 22.854 16.033 o 6 7 6 1164.460 1224.890 37.782 5.193 o 6 7 7 1964.300 1965.710 77.931 1.797 o 6 7 8 2594.360 2665.620 112.647 0.988 o 6 7 9 1335.450 1401.750 56.339 3.716 o 6 8 0 2754.000 2525.630 77.657 1.033 o 6 8 1 7803.350 7632.750 151.394 0.129 o 6 8 2 5135.280 5143.160 117.971 0.289 o 6 8 3 1382.250 1410.910 48.125 3.702 o 6 8 4 12.843 30.838 9.597 839.383 o 6 8 5 125.341 124.160 13.464 237.936 o 6 8 6 1618.780 1590.500 69.395 2.614 o 6 8 7 2034.380 1994.530 97.406 1.595 o 6 8 8 1466.110 1354.780 82.534 2.948 o 6 8 9 2050.580 1946.660 100.474 1.582 o 6 9 0 7412.670 6875.990 211.896 0.141 o 6 9 1 4517.820 4122.110 88.063 0.401 o 6 9 2 4004.430 3845.520 83.162 0.492 o 6 9 3 1181.980 1064.010 28.075 5.799 o 6 9 4 65.137 57.169 8.071 770.623 o 6 9 5 410.350 439.138 23.414 34.727 o 6 9 6 896.111 860.372 62.907 6.818 o 6 9 7 1474.290 1299.850 44.480 3.644 o 6 9 8 2011.620 2127.590 70.247 1.709 o 6 9 9 1276.600 1235.950 92.677 3.271 o 6 10 0 5564.760 5243.560 195.298 0.239 o 6 10 1 4849.650 4677.950 97.376 0.336 o 6 10 2 1995.230 1785.980 51.928 2.019 o 6 10 3 1404.750 1248.070 36.009 4.098 o 6 10 4 12.297 8.992 13.036 468.993 o 6 10 5 166.488 136.558 19.138 131.349 o 6 10 6 886.661 793.012 44.424 8.640 o 6 10 7 1499.080 1525.220 60.634 3.040 o 6 10 8 1519.250 1390.580 65.609 3.076 o 6 11 0 4425.150 3798.950 139.667 0.407 o 6 11 1 3780.350 3337.640 83.221 0.578 o 6 11 2 3703.870 3688.910 87.149 0.556 o 6 11 3 750.386 683.052 28.387 13.151 o 6 11 4 31.741 54.697 9.925 704.095 o 6 11 5 248.543 209.430 15.808 99.788 o 6 11 6 658.861 682.361 37.519 13.717 o 6 11 7 1216.180 1100.670 40.042 5.189 o 6 11 8 1489.560 1480.110 139.309 1.934 o 6 12 0 3585.440 3396.680 106.962 0.592 o 6 12 1 3978.170 3725.330 76.570 0.510 o 6 12 2 2192.520 1986.490 45.990 1.700 o 6 12 3 1231.830 1198.060 40.312 4.859 o 6 12 4 3.538 4.394 7.695 1352.360 o 6 12 5 113.544 122.821 9.779 346.524 o 6 12 6 748.631 672.399 37.936 12.037 o 6 12 7 1117.450 1106.550 78.162 4.336 o 6 12 8 1029.690 930.975 65.862 5.624 o 6 13 0 4169.310 3820.560 127.499 0.445 o 6 13 1 2965.680 2604.760 64.507 0.943 o 6 13 2 2735.520 2578.440 58.190 1.065 o 6 13 3 557.027 504.924 23.638 23.129 o 6 13 4 93.742 127.592 20.917 146.547 o 6 13 5 237.932 232.032 21.616 78.396 o 6 13 6 541.420 489.050 40.504 18.304 o 6 13 7 851.674 754.953 35.386 10.077 o 6 14 0 3308.570 2907.280 120.711 0.696 o 6 14 1 3530.410 3327.970 96.211 0.621 o 6 14 2 1484.110 1302.890 65.649 3.266 o 6 14 3 994.531 902.297 26.989 8.014 o 6 14 4 9.487 29.291 23.156 149.009 o 6 14 5 35.933 32.953 7.856 1086.010 o 6 14 6 531.263 483.488 41.502 18.337 o 6 14 7 1059.740 1045.440 112.159 3.386 o 6 15 0 3710.480 3272.490 119.237 0.568 o 6 15 1 2156.360 1951.770 50.254 1.740 o 6 15 2 2129.370 1924.740 48.720 1.790 o 6 15 3 359.593 320.239 16.654 54.325 o 6 15 4 79.591 95.422 16.597 231.033 o 6 15 5 100.460 105.243 37.557 53.001 o 6 15 6 436.798 378.868 53.011 17.632 o 6 16 0 2241.440 1905.760 98.795 1.457 o 6 16 1 2966.950 2719.090 78.325 0.899 o 6 16 2 926.279 849.035 29.603 8.934 o 6 16 3 594.226 548.085 36.515 17.140 o 6 16 4 50.481 43.927 11.003 556.013 o 6 16 5 52.097 30.465 22.213 156.321 o 6 17 0 3109.450 2751.140 152.546 0.713 o 6 17 1 1310.580 1235.570 57.618 4.045 o 6 17 2 1283.570 1190.640 40.465 4.633 o 6 17 3 414.703 391.743 28.590 32.447 o 6 17 4 39.920 49.533 11.015 573.734 o 6 18 0 966.504 822.619 54.446 7.041 o 6 18 1 1892.450 1640.570 65.472 2.170 o 6 18 2 964.108 849.945 50.695 7.203 o 6 18 3 345.606 368.543 54.623 18.972 o 7 0 1 20.570 25.398 11.486 586.672 o 7 0 2 5567.620 5429.980 242.811 0.221 o 7 0 3 54.190 109.342 38.822 51.469 o 7 0 4 10663.600 12066.600 455.610 0.055 o 7 0 5 166.059 204.024 19.300 116.036 o 7 0 6 6353.730 6598.510 275.213 0.164 o 7 0 7 23.521 28.314 32.426 75.897 o 7 0 8 180.815 153.016 76.965 12.911 o 7 0 9 24.117 1.496 24.450 133.681 o 7 1 1 1787.110 1788.290 50.547 2.327 o 7 1 2 45.937 64.602 15.062 315.992 o 7 1 3 9857.720 10772.000 329.560 0.070 o 7 1 4 146.823 215.066 16.237 145.653 o 7 1 5 9416.570 9906.410 263.135 0.081 o 7 1 6 15.604 48.452 33.175 72.480 o 7 1 7 1946.340 2034.810 95.893 1.664 o 7 1 8 27.175 -1.302 16.665 285.703 o 7 1 9 38.619 21.190 17.509 252.981 o 7 2 1 67.176 88.655 10.819 465.927 o 7 2 2 5131.900 5310.580 128.368 0.281 o 7 2 3 19.192 75.468 30.226 86.507 o 7 2 4 11507.900 11584.200 342.905 0.055 o 7 2 5 4.183 56.772 10.143 746.117 o 7 2 6 4544.970 4969.820 164.318 0.325 o 7 2 7 1.477 9.734 24.160 137.492 o 7 2 8 449.633 496.739 53.352 16.018 o 7 2 9 41.399 13.051 12.699 468.179 o 7 3 1 2146.840 2278.930 84.092 1.458 o 7 3 2 147.027 158.608 14.510 183.199 o 7 3 3 9307.120 9323.480 249.080 0.086 o 7 3 4 3.589 49.469 8.981 953.254 o 7 3 5 7185.820 7604.000 214.447 0.138 o 7 3 6 2.450 22.314 23.588 144.079 o 7 3 7 2000.100 2089.820 95.782 1.593 o 7 3 8 19.001 7.392 11.447 602.163 o 7 3 9 18.839 4.573 12.761 487.039 o 7 4 1 3.447 13.187 5.841 2322.860 o 7 4 2 6580.020 6632.510 165.127 0.174 o 7 4 3 2.189 18.593 11.727 581.329 o 7 4 4 7590.960 7771.870 209.012 0.128 o 7 4 5 0.433 18.392 19.945 201.603 o 7 4 6 4964.300 5225.620 183.740 0.278 o 7 4 7 12.187 2.886 33.690 70.678 o 7 4 8 300.303 272.990 22.498 59.287 o 7 4 9 70.486 26.381 17.078 248.718 o 7 5 1 2337.480 2458.000 55.507 1.347 o 7 5 2 24.401 22.085 5.937 1966.080 o 7 5 3 7130.930 7538.790 212.250 0.140 o 7 5 4 100.851 90.016 14.721 257.928 o 7 5 5 6651.520 7245.200 198.939 0.158 o 7 5 6 67.817 92.344 28.203 94.097 o 7 5 7 1762.620 1814.070 81.416 2.096 o 7 5 8 23.485 39.010 12.480 489.645 o 7 5 9 27.788 43.340 37.148 57.721 o 7 6 1 53.153 50.559 6.179 1225.370 o 7 6 2 4732.960 4763.490 109.852 0.339 o 7 6 3 50.017 54.739 8.306 839.672 o 7 6 4 7622.890 8035.660 196.412 0.125 o 7 6 5 11.222 34.616 26.527 113.506 o 7 6 6 4244.340 4251.630 127.484 0.408 o 7 6 7 43.989 38.770 13.629 394.306 o 7 6 8 239.237 209.059 17.999 94.540 o 7 7 1 1235.110 1179.130 40.807 4.877 o 7 7 2 36.689 58.522 9.183 774.421 o 7 7 3 6469.320 6648.650 166.309 0.177 o 7 7 4 0.738 11.396 22.634 156.659 o 7 7 5 6524.730 6804.030 168.659 0.172 o 7 7 6 10.110 37.561 28.687 97.116 o 7 7 7 1581.140 1580.440 90.363 2.421 o 7 7 8 9.037 1.207 13.365 448.419 o 7 8 1 26.216 28.711 10.881 638.662 o 7 8 2 3530.520 3321.970 75.902 0.639 o 7 8 3 29.313 38.860 22.899 150.084 o 7 8 4 7559.810 7473.120 171.024 0.135 o 7 8 5 2.001 12.300 13.248 456.636 o 7 8 6 3693.640 3926.370 133.079 0.502 o 7 8 7 0.881 -9.037 27.858 103.444 o 7 8 8 179.940 168.151 17.032 133.824 o 7 9 1 596.404 546.765 17.041 21.978 o 7 9 2 0.912 8.968 7.132 1574.450 o 7 9 3 6517.190 6305.900 152.345 0.183 o 7 9 4 48.338 62.356 21.323 166.287 o 7 9 5 5800.960 5652.820 141.554 0.229 o 7 9 6 1.015 8.793 17.862 251.525 o 7 9 7 1287.180 1314.550 65.846 3.798 o 7 10 1 7.010 12.274 11.058 652.430 o 7 10 2 3388.650 3038.840 77.367 0.710 o 7 10 3 84.068 14.077 26.814 106.211 o 7 10 4 6327.270 5930.520 141.759 0.199 o 7 10 5 35.354 9.173 14.035 393.377 o 7 10 6 2956.300 2955.110 89.935 0.841 o 7 10 7 22.005 -2.010 37.654 56.538 o 7 11 1 1199.330 1040.000 36.419 5.550 o 7 11 2 17.117 22.557 10.632 688.363 o 7 11 3 4828.150 4550.220 111.725 0.339 o 7 11 4 34.050 32.548 13.044 442.572 o 7 11 5 4426.570 4178.740 118.187 0.396 o 7 11 6 0.080 2.599 14.203 397.981 o 7 11 7 1217.230 1183.260 47.174 4.788 o 7 12 1 50.118 41.340 6.248 1309.550 o 7 12 2 3224.000 2914.840 71.875 0.783 o 7 12 3 39.926 32.276 7.394 1169.500 o 7 12 4 4459.060 4169.400 121.806 0.391 o 7 12 5 0.405 2.653 8.738 1051.390 o 7 12 6 2364.610 2310.790 78.547 1.311 o 7 13 1 656.476 606.110 20.086 17.858 o 7 13 2 36.662 34.185 10.437 659.279 o 7 13 3 4125.390 3577.360 85.570 0.493 o 7 13 4 1.407 6.256 10.373 745.489 o 7 13 5 3047.100 2764.110 90.293 0.842 o 7 13 6 5.403 -6.965 32.505 75.975 o 7 14 1 6.388 0.259 7.660 1363.980 o 7 14 2 2185.940 2011.030 53.759 1.667 o 7 14 3 1.723 2.264 14.850 363.992 o 7 14 4 3350.650 2938.540 91.396 0.719 o 7 14 5 2.338 -9.986 14.412 386.464 o 7 15 1 669.385 595.876 20.987 17.456 o 7 15 2 2.358 -14.569 12.048 552.963 o 7 15 3 2291.230 2078.510 67.274 1.492 o 7 15 4 15.955 13.819 11.426 604.192 o 7 16 1 13.921 8.180 10.002 791.136 o 7 16 2 1293.640 1169.840 78.961 3.663 o 8 0 0 1981.760 2299.980 161.674 1.151 o 8 0 1 5334.570 5604.970 182.240 0.245 o 8 0 2 3003.700 3067.750 180.485 0.647 o 8 0 3 1219.550 1423.180 75.979 3.592 o 8 0 4 237.597 222.535 68.702 15.260 o 8 0 5 363.675 419.413 41.332 25.329 o 8 0 6 570.221 598.065 38.427 16.605 o 8 0 7 1551.830 1593.270 79.643 2.602 o 8 1 0 6664.970 6434.930 196.113 0.170 o 8 1 1 3130.830 3226.530 86.102 0.747 o 8 1 2 3007.450 3390.780 114.423 0.721 o 8 1 3 1091.190 1164.100 60.374 4.990 o 8 1 4 16.583 26.718 9.908 785.916 o 8 1 5 80.238 61.644 10.968 458.429 o 8 1 6 1123.350 1207.270 43.764 5.292 o 8 1 7 811.460 853.203 37.804 9.741 o 8 2 0 3601.430 3402.680 134.145 0.562 o 8 2 1 5210.340 5427.940 140.750 0.269 o 8 2 2 1723.270 2057.320 68.421 2.094 o 8 2 3 820.277 891.469 94.541 4.998 o 8 2 4 141.741 168.466 12.367 211.326 o 8 2 5 109.980 93.189 9.941 386.374 o 8 2 6 306.571 389.031 21.311 51.132 o 8 2 7 2211.220 2189.960 74.012 1.485 o 8 3 0 6379.520 6549.110 245.100 0.169 o 8 3 1 3140.750 3176.780 86.945 0.751 o 8 3 2 2621.880 2628.940 94.347 1.032 o 8 3 3 409.395 425.879 39.841 24.264 o 8 3 4 68.732 70.940 9.920 547.352 o 8 3 5 26.040 33.489 10.075 732.194 o 8 3 6 1174.910 1201.290 49.907 4.865 o 8 3 7 575.420 641.744 33.649 17.072 o 8 4 0 2703.490 3119.590 107.708 0.869 o 8 4 1 4424.470 4741.460 143.263 0.356 o 8 4 2 1517.720 1529.260 48.069 3.153 o 8 4 3 948.889 927.366 33.873 8.016 o 8 4 4 67.658 105.781 12.193 376.446 o 8 4 5 254.108 260.780 14.609 92.227 o 8 4 6 240.537 284.219 15.989 88.574 o 8 4 7 1733.170 1691.410 63.447 2.390 o 8 5 0 5274.770 5544.380 177.267 0.251 o 8 5 1 2217.570 2313.400 55.838 1.494 o 8 5 2 2769.150 2568.120 75.845 1.019 o 8 5 3 525.546 529.093 18.959 25.617 o 8 5 4 18.650 30.275 9.773 798.092 o 8 5 5 21.364 33.386 12.314 507.850 o 8 5 6 910.582 946.881 32.115 8.411 o 8 5 7 623.989 698.631 51.333 11.728 o 8 6 0 2685.180 2677.320 101.724 0.975 o 8 6 1 4152.030 4270.250 100.472 0.432 o 8 6 2 1100.370 1179.550 33.200 5.818 o 8 6 3 764.361 722.905 26.455 12.677 o 8 6 4 132.649 154.312 10.591 260.822 o 8 6 5 232.163 222.034 13.450 113.980 o 8 6 6 309.570 367.563 26.322 45.239 o 8 6 7 1491.610 1479.940 71.025 2.954 o 8 7 0 4520.420 4038.470 160.900 0.372 o 8 7 1 2009.470 1894.480 51.305 1.935 o 8 7 2 2448.460 2367.380 79.381 1.236 o 8 7 3 553.997 585.287 27.958 20.235 o 8 7 4 27.963 36.212 20.142 193.380 o 8 7 5 19.580 23.223 13.079 457.730 o 8 7 6 905.942 943.519 51.326 7.252 o 8 8 0 2015.580 1773.050 67.667 1.911 o 8 8 1 3856.880 3652.520 85.025 0.532 o 8 8 2 1437.800 1264.190 37.813 3.922 o 8 8 3 662.492 631.925 32.167 15.177 o 8 8 4 89.128 125.628 18.285 183.732 o 8 8 5 190.438 194.946 14.726 137.170 o 8 8 6 235.807 288.214 28.208 55.861 o 8 9 0 4460.770 4296.640 127.206 0.382 o 8 9 1 1673.360 1584.300 46.268 2.753 o 8 9 2 1734.160 1693.490 46.276 2.529 o 8 9 3 799.437 852.267 26.295 10.897 o 8 9 4 31.897 35.357 10.584 653.017 o 8 9 5 17.412 34.752 15.256 337.134 o 8 9 6 708.515 678.493 48.750 11.065 o 8 10 0 1899.470 1723.450 66.897 2.093 o 8 10 1 3220.850 2989.450 94.874 0.745 o 8 10 2 1299.920 1201.250 33.779 4.669 o 8 10 3 582.853 541.041 21.781 21.633 o 8 10 4 110.571 115.201 12.023 297.059 o 8 10 5 177.270 166.508 17.977 128.483 o 8 11 0 2809.250 2692.910 78.056 0.969 o 8 11 1 1612.610 1508.260 61.062 2.805 o 8 11 2 1730.300 1623.350 56.002 2.520 o 8 11 3 541.127 489.663 23.329 24.404 o 8 11 4 21.692 25.758 13.620 420.734 o 8 12 0 1956.700 1753.230 64.854 2.013 o 8 12 1 2379.870 2113.590 65.749 1.413 o 8 12 2 919.647 752.259 36.456 9.132 o 8 12 3 454.867 462.335 31.473 26.046 o 8 12 4 8.265 7.700 15.591 329.398 o 8 13 0 2872.460 2423.210 139.970 0.857 o 8 13 1 1293.610 1089.120 51.004 4.557 o 8 13 2 917.731 863.157 38.709 8.371 o 8 13 3 188.551 185.193 33.666 54.074 o 8 14 0 1296.670 1252.420 144.770 2.147 o 8 14 1 1809.440 1495.580 337.379 0.562 o 9 0 1 783.784 734.489 39.350 10.795 o 9 0 2 336.918 359.746 29.351 39.191 o 9 0 3 3499.800 3794.020 214.698 0.457 o 9 0 4 167.897 186.267 24.766 87.627 o 9 0 5 2969.160 3540.940 220.521 0.541 o 9 1 1 77.805 79.972 9.730 513.514 o 9 1 2 2135.950 2173.080 72.144 1.563 o 9 1 3 204.790 267.378 17.182 99.803 o 9 1 4 3897.300 4452.790 146.231 0.427 o 9 1 5 202.117 243.077 21.112 88.096 o 9 2 1 473.160 489.923 20.484 29.607 o 9 2 2 280.073 291.137 21.349 63.666 o 9 2 3 3449.600 3882.460 127.671 0.552 o 9 2 4 284.598 358.517 22.514 54.869 o 9 2 5 3381.940 3678.380 161.444 0.545 o 9 3 1 22.044 43.839 10.931 626.803 o 9 3 2 1917.060 2058.000 78.222 1.796 o 9 3 3 333.349 391.241 24.830 43.159 o 9 3 4 3840.590 4258.150 161.037 0.436 o 9 3 5 230.409 255.533 25.687 65.270 o 9 4 1 649.069 666.181 31.617 15.185 o 9 4 2 175.922 236.460 16.306 123.427 o 9 4 3 3074.610 3238.470 117.004 0.719 o 9 4 4 433.664 428.086 30.082 28.988 o 9 4 5 3297.270 3671.940 160.871 0.561 o 9 5 1 31.966 39.329 8.003 1057.750 o 9 5 2 1807.940 1766.180 69.930 2.165 o 9 5 3 279.322 309.110 35.586 38.175 o 9 5 4 3874.370 3995.180 266.636 0.358 o 9 6 1 385.915 391.295 18.177 43.784 o 9 6 2 213.420 194.948 30.394 59.320 o 9 6 3 3291.220 3143.020 112.738 0.681 o 9 6 4 314.325 372.660 31.526 38.086 o 9 7 1 82.207 94.141 11.085 407.221 o 9 7 2 1716.670 1610.370 72.321 2.397 o 9 7 3 320.604 298.196 43.949 27.569 o 9 7 4 3118.730 3019.070 334.720 0.387 o 9 8 1 555.743 542.818 28.123 20.952 o 9 8 2 175.138 172.642 19.581 116.814 o 9 8 3 2516.020 2691.800 109.072 1.027 o 9 9 1 66.274 73.934 13.533 348.278 o 9 9 2 1397.220 1466.360 81.573 2.993 o 9 10 1 315.535 290.284 51.608 22.259 o ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 x+1/2,-y+1/2,-z+1/2 3 -x,y+1/2,-z 4 -x+1/2,-y,z+1/2 5 -x,-y,-z 6 -x-1/2,y-1/2,z-1/2 7 x,-y-1/2,z 8 x-1/2,y,-z-1/2 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_group Pb1 Pb 0.60634(3) 0.25 0.307150(19) 0.03366(15) Uani 1.000000 2 S T P . O2 O 0.8714(7) 0.3429(4) 0.3003(5) 0.0665(17) Uani 1.000000 1 . . . . O3 O 0.3401(10) 0.25 0.4522(6) 0.0694(16) Uani 1.000000 2 S T P . O1 O 0.6931(7) 0.3448(3) 0.4661(5) 0.0892(17) Uani 1.000000 1 . U . . C1 C 0.8179(7) 0.3707(3) 0.4032(5) 0.0476(11) Uani 1.000000 1 . . . . C2 C 0.9093(6) 0.4389(3) 0.4554(6) 0.0490(12) Uani 1.000000 1 . . . . C4 C 1.0738(8) 0.4527(4) 0.4126(7) 0.0661(18) Uani 1.000000 1 . . . . H4 H 1.1243(8) 0.4209(4) 0.3519(7) 0.079(2) Uiso 1.000000 1 R . . . C3 C 0.8292(8) 0.4857(4) 0.5420(7) 0.0719(19) Uani 1.000000 1 . . . . C5 C 0.3025(19) 0.2918(7) 0.5307(13) 0.069(3) Uani 0.500000 1 . U . -1 H5 H 0.3603(19) 0.3366(7) 0.5218(13) 0.083(4) Uiso 0.500000 1 R . . -1 N1 N 0.1958(13) 0.2903(7) 0.6302(11) 0.073(3) Uani 0.500000 1 . U . -1 C6 C 0.156(3) 0.3513(14) 0.717(2) 0.093(4) Uani 0.500000 1 . U . -1 C7 C 0.092(3) 0.2205(12) 0.638(3) 0.106(5) Uani 0.500000 1 . U . -1 C8 C 0.645(3) 0.4708(17) 0.604(3) 0.124(8) Uani 0.500000 1 . U . -1 H8a H 0.590(12) 0.431(8) 0.558(15) 0.186(11) Uiso 0.500000 1 GR . . -1 H8b H 0.658(3) 0.458(12) 0.695(6) 0.186(11) Uiso 0.500000 1 GR . . -1 H8c H 0.574(10) 0.514(4) 0.596(19) 0.186(11) Uiso 0.500000 1 GR . . -1 H6a H 0.188(18) 0.338(3) 0.806(3) 0.139(6) Uiso 0.500000 1 GR . . -1 H6b H 0.221(13) 0.394(3) 0.690(8) 0.139(6) Uiso 0.500000 1 GR . . -1 H6c H 0.034(3) 0.362(5) 0.713(11) 0.139(6) Uiso 0.500000 1 GR . . -1 H7a H -0.023(5) 0.229(2) 0.602(12) 0.159(7) Uiso 0.500000 1 GR . . -1 H7b H 0.149(8) 0.183(2) 0.588(11) 0.159(7) Uiso 0.500000 1 GR . . -1 H7c H 0.082(16) 0.205(4) 0.728(3) 0.159(7) Uiso 0.500000 1 GR . . -1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Pb1 0.0295(2) 0.0342(2) 0.0372(2) -0.000000 -0.00366(6) 0.000000 O2 0.063(3) 0.057(3) 0.080(4) -0.007(2) 0.0054(17) -0.038(2) O3 0.077(4) 0.068(4) 0.062(4) -0.000000 0.027(3) 0.000000 O1 0.093(4) 0.101(4) 0.074(3) -0.048(3) 0.019(3) -0.039(3) C1 0.049(3) 0.041(2) 0.053(3) 0.0011(19) -0.012(2) -0.018(2) C2 0.046(3) 0.044(3) 0.057(3) 0.0005(18) -0.011(2) -0.020(2) C4 0.052(2) 0.059(3) 0.088(5) -0.007(3) 0.009(3) -0.044(3) C3 0.052(3) 0.066(4) 0.097(5) -0.016(3) 0.015(3) -0.048(4) C5 0.077(8) 0.082(8) 0.049(5) 0.003(6) 0.002(5) -0.005(5) N1 0.044(5) 0.118(8) 0.058(6) 0.006(4) -0.002(4) -0.009(5) C6 0.093(4) 0.093(4) 0.092(4) 0.0005(7) 0.0003(7) -0.0005(7) C7 0.106(5) 0.106(5) 0.106(5) -0.0006(7) 0.0004(7) 0.0000(7) C8 0.123(8) 0.124(8) 0.125(8) -0.0001(10) -0.0001(10) -0.0007(10) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source C 0.00347 0.00161 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.21560 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.00304 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' N 0.00653 0.00323 12.21260 3.13220 2.01250 1.16630 0.00570 9.89330 28.99750 0.58260 -11.52900 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' O 0.01158 0.00611 3.04850 2.28680 1.54630 0.86700 13.27710 5.70110 0.32390 32.90890 0.25080 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' Pb -3.20855 10.15389 31.06170 13.06370 18.44200 5.96960 0.69020 2.35760 8.61800 47.25790 13.41180 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u 1 0 0 0.01 0.35 -1 0 0 0.06 0.03 -1 0 0 0.32 0.13 -1 0 0 0.63 0.4 1 0 0 0.1 0.11 2 0 0 6.64 0.61 2 0 0 10.09 1.76 2 0 0 6.95 0.61 3 0 0 0.09 0.08 -3 0 0 0.25 0.32 -3 0 0 0.63 0.96 -3 0 0 0.26 0.09 3 0 0 0.43 0.32 3 0 0 0.39 1.11 3 0 0 0.18 0.09 4 0 0 1000 78.35 -4 0 0 792.76 77.43 5 0 0 0.28 0.47 5 0 0 0.01 0.15 -5 0 0 -0.62 1.25 5 0 0 0.3 0.14 -5 0 0 -0.22 0.47 -6 0 0 87.39 7.45 6 0 0 79.59 7.08 6 0 0 79.71 7.08 6 0 0 85.03 7.41 -7 0 0 -0.04 0.54 7 0 0 0.23 0.21 7 0 0 1.34 0.26 -7 0 0 0.88 2.32 7 0 0 0.58 0.68 7 0 0 -0.07 3.15 8 0 0 28.33 2.56 8 0 0 47.33 8 8 0 0 30.52 3.2 -8 0 0 28.59 3.08 8 0 0 29.35 2.57 -8 0 0 22.99 5.95 9 0 0 -0.65 0.8 0 0 -1 0.13 0.1 0 0 -1 0.19 0.03 0 0 1 0.42 0.13 0 0 -1 0.78 0.53 0 0 -1 0.29 0.05 -1 0 1 2.24 0.41 -1 0 1 2.06 0.92 1 0 -1 1.82 0.18 1 0 -1 2.64 0.39 1 0 -1 2.34 1.01 1 0 -1 1.7 0.18 -1 0 1 1.96 0.18 -1 0 1 1.38 0.18 2 0 -1 315.52 29.79 -2 0 1 328.44 29.87 -2 0 1 350.2 28.51 3 0 -1 16.11 3.26 -3 0 1 14.3 2.88 -3 0 1 15.17 1.6 -3 0 1 12.3 1.2 -3 0 1 14.27 1.2 -4 0 -1 158.24 13.1 4 0 1 160.82 13.09 4 0 -1 153.47 13.22 4 0 -1 162.59 15.72 -4 0 1 138.66 13.27 -4 0 1 136.33 14.84 5 0 -1 31.07 7.85 5 0 -1 14.72 1.47 5 0 1 17.81 1.45 -5 0 1 20.34 2.08 -5 0 -1 21.18 3.14 -5 0 1 11.59 3.31 5 0 -1 14.54 1.47 5 0 -1 18.15 1.94 6 0 -1 108.42 9.56 -6 0 -1 111.62 11.17 -6 0 -1 115.77 9.76 6 0 -1 116.38 9.94 -6 0 1 101.5 12.13 6 0 -1 105.69 9.55 6 0 1 118.53 9.77 7 0 -1 0.47 0.72 7 0 -1 0.41 0.24 7 0 -1 0.21 0.25 -7 0 -1 0.1 0.43 7 0 1 0.35 0.61 -7 0 -1 0.22 2.05 -7 0 1 0.69 0.75 -8 0 1 69.3 6.72 8 0 1 69.61 6.12 8 0 -1 80.54 6.76 8 0 -1 65.97 6.15 8 0 1 73.18 6.44 8 0 -1 96.19 12.99 8 0 1 67.92 6.11 8 0 -1 72.57 6.16 9 0 -1 9.47 0.97 9 0 -1 8.79 1.69 9 0 1 8.84 0.88 -9 0 1 12.66 2.64 9 0 -1 9.89 0.99 0 0 -2 120.6 11.48 0 0 -2 123.78 10.55 1 0 2 392.26 32.82 -1 0 -2 381.9 32.62 1 0 -2 359.09 33.53 -1 0 2 370.74 33.62 2 0 -2 82.21 10.25 -2 0 2 90.81 10.36 2 0 -2 110.74 8.81 -2 0 2 106.28 8.87 -3 0 2 222.2 21.2 -3 0 2 224.88 19.2 3 0 -2 213.59 21.31 4 0 -2 202.19 19.25 -4 0 2 236.03 19.39 -4 0 2 218.59 21.58 4 0 -2 235.29 22.28 5 0 -2 11.38 1.66 -5 0 2 13.24 1.84 -5 0 2 9.71 3.72 5 0 -2 9.8 1.04 5 0 -2 23.54 5.57 -5 0 2 11.62 1.03 -6 0 2 70.38 6.51 6 0 -2 63.01 5.85 6 0 -2 67.06 6.32 6 0 -2 88.84 10.89 -6 0 2 68.97 9.5 -7 0 2 80.12 6.78 7 0 -2 67.63 6.48 7 0 -2 69.47 5.98 7 0 -2 63.46 5.97 8 0 -2 56.17 10.26 8 0 -2 41.08 4.14 -8 0 2 39.41 4.26 8 0 -2 35.09 3.41 8 0 -2 40.21 3.43 -9 0 -2 5.01 0.71 9 0 -2 5.58 1.43 9 0 -2 4.09 0.7 -9 0 2 4.16 1.4 9 0 -2 4.6 0.72 0 0 3 0.08 0.08 0 0 -3 0.34 0.28 0 0 -3 0.09 0.07 0 0 -3 0.21 0.05 0 0 3 0.28 0.06 0 0 -3 0.12 0.07 0 0 3 0.11 0.09 0 0 -3 0.85 1.03 0 0 3 0.21 0.29 -1 0 -3 215.41 19.45 1 0 -3 231.32 18.66 -1 0 -3 197.83 18.52 -1 0 3 225.94 20.71 1 0 -3 202.11 20.37 1 0 3 224.99 19.85 -2 0 -3 121.2 10.36 2 0 3 136.07 11.47 2 0 -3 108.93 12.67 -2 0 -3 106.32 10.39 -2 0 3 114.29 12.79 2 0 -3 134.17 10.66 -2 0 3 122.65 10.71 3 0 -3 21.87 4.86 -3 0 -3 12.69 1.09 -3 0 3 12.93 1.81 -3 0 3 11.95 1.14 -3 0 3 12.46 1.14 -3 0 3 11.59 3.55 4 0 -3 13.78 1.27 -4 0 3 21.14 5.27 4 0 -3 20 4.98 -4 0 3 14.1 2.3 4 0 -3 12.84 1.27 -4 0 3 14.12 1.28 4 0 -3 16.47 1.9 -5 0 3 349.48 35.97 -5 0 3 310 28.39 5 0 -3 333.8 32.21 6 0 -3 27.2 3.26 -6 0 3 32.2 3.56 -6 0 3 27.74 2.62 6 0 -3 43.87 8.41 6 0 -3 28.6 2.64 6 0 -3 31.13 2.65 -6 0 3 40.64 7.62 -6 0 -3 31.06 2.61 -7 0 -3 1.63 0.31 7 0 -3 1.5 0.37 7 0 -3 -2.3 4.09 7 0 -3 1.11 0.97 -7 0 3 3.13 5.05 -7 0 3 0.72 1.04 8 0 -3 18.87 1.75 -8 0 -3 18.67 1.7 8 0 -3 15.02 2.55 -8 0 3 19.2 2.9 8 0 -3 19.14 1.71 -8 0 3 10.91 5.97 -9 0 3 55.47 5.4 -9 0 -3 51.78 4.25 9 0 -3 42.86 5.02 9 0 -3 45.17 4.24 0 0 -4 32 2.53 0 0 4 28.67 2.51 0 0 -4 29.6 2.53 0 0 4 29.15 2.53 0 0 -4 27.99 4.36 0 0 -4 26.63 2.8 -1 0 -4 306.3 29.26 1 0 4 350.26 30.08 -1 0 4 349.67 30.9 -1 0 -4 289.09 28.01 1 0 -4 290.4 30.13 1 0 4 376.1 28.01 2 0 -4 2.71 0.74 -2 0 4 3.28 0.95 -2 0 4 2.68 0.37 2 0 4 2.26 0.28 -2 0 4 1.75 0.3 -2 0 4 1.89 0.26 -2 0 -4 2.8 0.24 2 0 4 5.44 2.03 2 0 -4 1.73 2.18 -2 0 -4 2.72 0.52 -2 0 4 2.18 2.51 -2 0 -4 2.16 0.24 -3 0 4 566.25 49.93 3 0 -4 520.72 49.69 -3 0 4 538.1 46.64 -4 0 4 8.98 0.98 4 0 -4 10.8 1.75 4 0 -4 12.48 4.46 -4 0 4 11.74 0.99 -4 0 4 12.05 4.77 -4 0 4 10.97 1.97 -4 0 4 11.14 0.95 4 0 -4 8.55 0.97 -5 0 4 22.51 5.89 5 0 -4 20.18 2.06 -5 0 4 20.73 2.07 5 0 -4 24.38 2.83 5 0 -4 27.12 6.61 -5 0 4 23.41 2.06 -5 0 4 27.19 3.14 -5 0 4 25.96 2.06 -5 0 -4 27.14 2.05 5 0 -4 19.52 2.06 6 0 -4 0.2 0.21 6 0 -4 0.41 0.28 6 0 -4 1.78 3.64 6 0 -4 0.18 0.26 -6 0 4 3.15 4.18 -6 0 4 0.54 1 -6 0 4 0.29 0.26 -6 0 -4 0.14 0.18 -7 0 -4 158.46 13.22 7 0 -4 156.6 13.26 7 0 -4 161.53 13.27 7 0 -4 131.16 13.76 -7 0 4 161.61 14.21 7 0 -4 172.99 25.55 8 0 -4 4.12 1.32 8 0 -4 2.84 0.51 -8 0 -4 3.08 0.52 -8 0 4 3.48 1.43 -8 0 4 -6.77 7.06 8 0 -4 2.7 0.48 -9 0 -4 1.92 0.45 9 0 -4 2.06 1.3 -9 0 4 3.36 1.6 9 0 -4 2.75 0.51 0 0 5 0.24 0.16 0 0 -5 0.11 0.07 0 0 5 0.02 0.08 0 0 5 0.21 1.58 0 0 5 -0.01 0.17 0 0 -5 0.1 0.45 0 0 -5 0.05 0.11 0 0 5 0.02 0.43 0 0 -5 2 1.81 -1 0 -5 326.6 30.9 -1 0 -5 320.76 32.4 1 0 -5 347.18 31.01 1 0 5 419.99 33.82 1 0 -5 311.82 33.29 1 0 5 413.12 30.89 -1 0 5 386.96 34.53 -2 0 -5 12.67 1.05 -2 0 5 10.06 1.06 -2 0 5 15.33 4.86 2 0 -5 10.62 1.09 -2 0 -5 13.5 1.04 2 0 5 18.46 4.05 -2 0 5 14.62 1.99 -2 0 -5 15.07 3.22 2 0 -5 11.76 1.75 -2 0 5 10.76 1.11 -2 0 -5 11.98 1.42 -2 0 5 11.1 1.11 2 0 5 13.72 1.32 2 0 -5 6.55 3.43 -3 0 -5 69.69 6.15 3 0 -5 59.63 6.09 -3 0 5 74.34 6.08 3 0 -5 60.33 6.09 -3 0 -5 81.2 6.05 -3 0 5 76.33 6.9 -3 0 5 87.5 11.09 3 0 -5 81.35 10.5 -4 0 5 27.52 3.21 -4 0 5 20.19 2.04 -4 0 5 25.39 2.01 4 0 -5 21.05 2.03 4 0 -5 22.62 5.96 -4 0 5 21.08 2.03 -4 0 -5 26.08 1.97 4 0 -5 23.37 2.8 4 0 -5 19.7 2.02 -4 0 5 37.84 8 5 0 -5 174.82 14.94 -5 0 5 163.97 14.34 -5 0 5 180.94 14.35 5 0 -5 193.3 20.24 -5 0 5 190.88 20.18 5 0 -5 172.12 14.36 5 0 -5 144.03 14.35 -5 0 5 150.11 14.35 -5 0 5 173.74 15.32 6 0 -5 8.02 0.88 -6 0 5 7.09 0.87 6 0 -5 4.83 4.69 -6 0 5 9.85 5.94 -6 0 5 8.05 1.96 6 0 -5 7.49 0.87 -6 0 -5 7.51 0.73 6 0 -5 9.3 1.8 7 0 -5 2.51 0.49 7 0 -5 3.22 5.89 7 0 -5 2.16 0.44 -7 0 -5 2.85 0.38 -7 0 5 3.73 1.55 8 0 -5 4.22 0.77 -8 0 -5 5.87 0.65 -8 0 5 5.72 1.86 8 0 -5 6.28 0.84 8 0 -5 2.89 1.29 -9 0 -5 45.21 4 9 0 -5 46.3 4.06 0 0 -6 96.97 11.5 0 0 6 107.11 8.61 0 0 -6 99.87 8.6 0 0 -6 95.29 9 -1 0 6 163.95 15.05 1 0 6 202.47 15.37 1 0 -6 146.84 17.98 -1 0 -6 149.73 19.03 -1 0 -6 162.7 15.38 -1 0 6 201.5 19.95 1 0 -6 166.28 15.48 -1 0 6 209.9 15.65 -2 0 -6 6.18 0.52 2 0 -6 6.27 3.67 -2 0 6 4.01 3.87 -2 0 -6 6.56 1.16 2 0 -6 5.4 0.59 -2 0 6 4.25 0.65 -2 0 6 4.96 0.64 -2 0 6 4.53 0.55 2 0 6 6.45 0.49 -2 0 6 7.44 1.5 2 0 6 7.22 1.08 2 0 -6 3.81 0.99 2 0 6 12.15 4.34 -2 0 -6 4.92 0.49 2 0 -6 4.91 0.6 -3 0 -6 241.93 19.26 3 0 6 229.44 20.51 -3 0 6 205.97 19.01 -3 0 -6 199.05 19.1 3 0 -6 203.32 23.3 -3 0 6 264.5 25.02 -3 0 6 231.82 20.13 3 0 -6 225.21 19.56 -4 0 6 71.01 11.09 -4 0 -6 61.89 4.79 4 0 -6 49.87 4.69 -4 0 -6 55.99 4.62 -4 0 6 52.93 5.8 -4 0 6 57.59 4.67 -4 0 6 50.13 4.69 4 0 -6 47.48 9.27 -4 0 6 54.06 4.71 4 0 -6 48.97 4.69 -5 0 6 9.46 6.46 5 0 -6 10.27 1.92 -5 0 6 6.32 0.88 5 0 -6 7.69 0.86 -5 0 6 7.81 0.88 5 0 -6 2 4.61 5 0 -6 6.99 0.83 -5 0 6 5.49 1.68 -5 0 -6 7.34 0.69 -6 0 -6 23.67 2.07 6 0 -6 16.23 3.92 -6 0 6 22.1 2.17 6 0 -6 24.25 2.18 -6 0 6 35.43 8.83 6 0 -6 24.92 2.18 -6 0 6 27.46 3.83 -7 0 6 108.52 17.23 7 0 -6 84.01 7.3 7 0 -6 89.15 7.31 -7 0 6 89.45 8.68 7 0 -6 72.51 8.06 -7 0 -6 82.89 7.23 -8 0 6 6.14 2.01 8 0 -6 8.58 1.03 8 0 -6 7.78 0.99 -8 0 -6 7.69 0.82 8 0 -6 5.44 1.67 0 0 7 0.02 0.71 0 0 -7 -0.01 0.69 0 0 7 1.79 2.59 0 0 7 0.5 0.31 0 0 -7 0.46 2.06 0 0 7 0.51 0.3 0 0 -7 0.57 0.18 -1 0 7 45.02 8.56 -1 0 -7 44.07 3.45 -1 0 7 44.31 4.27 1 0 7 44.68 3.94 1 0 -7 38.01 3.46 1 0 -7 39.59 3.47 -1 0 -7 33.83 5.98 -1 0 -7 44.12 3.45 -1 0 -7 40.4 4.05 -1 0 7 34.99 3.48 -1 0 7 34.98 3.43 1 0 -7 35.21 4.07 1 0 -7 33.1 7.22 1 0 7 42.36 3.41 2 0 -7 166.12 15.81 -2 0 7 226.81 22.32 -2 0 7 193.51 15.79 2 0 7 198.63 16.08 -2 0 7 171.08 15.82 -2 0 7 197.14 16.61 2 0 -7 180.36 15.82 2 0 -7 180.68 16.38 -2 0 -7 181.01 16.19 -3 0 -7 11.83 1.03 3 0 7 26.53 6.01 -3 0 -7 9.39 1.32 3 0 -7 11.54 1.14 3 0 -7 10.79 1.12 -3 0 7 17.56 6.43 -3 0 7 10.06 1.19 -3 0 7 11.48 1.18 -3 0 -7 12.51 1.03 -3 0 -7 11.84 1.65 3 0 7 13.54 1.09 3 0 -7 16.43 2.96 -3 0 7 11.33 1.09 -3 0 7 7.71 1.82 3 0 -7 8.17 4.44 4 0 -7 7.09 0.82 -4 0 -7 5.45 0.87 -4 0 -7 6.07 1.1 4 0 -7 7.91 0.87 4 0 -7 9.23 1.85 -4 0 7 11.14 2.45 4 0 -7 6.61 4.75 -4 0 7 13.63 7.39 -4 0 7 8.62 0.76 -4 0 -7 5.85 0.63 -4 0 7 7.96 0.91 -4 0 7 7.7 0.93 -5 0 7 40.04 3.66 -5 0 7 56.71 12.71 5 0 -7 34.06 9.06 -5 0 7 43.92 5.15 -5 0 7 43.43 3.63 -5 0 -7 39.04 3.52 5 0 -7 42.42 3.64 5 0 -7 40.51 3.62 5 0 -7 38.84 4.58 -6 0 7 26.05 2.43 6 0 -7 28.31 2.42 6 0 -7 17.22 8.1 6 0 -7 26.08 2.42 -6 0 7 31.32 4.22 -6 0 7 36.09 10.9 6 0 -7 20.26 3.42 -7 0 7 -7.3 5.76 7 0 -7 0.33 0.38 7 0 -7 0.3 0.54 -7 0 7 0.8 0.44 7 0 -7 0.68 1.22 7 0 -7 0.4 6.05 -7 0 -7 0.39 0.23 -7 0 7 0.66 1.53 8 0 -7 22.85 2.01 -8 0 -7 20.16 1.85 8 0 -7 20.18 2 8 0 -7 17.72 3.29 -8 0 7 17.3 4.01 0 0 8 331.82 26.91 0 0 8 328.25 26.37 0 0 -8 266.24 26.84 -1 0 8 6.5 1.65 -1 0 8 7.77 5.46 -1 0 -8 7.56 3.3 1 0 -8 5.48 1.36 -1 0 -8 6.17 1.42 -1 0 -8 7.11 0.69 1 0 -8 5.1 3.48 -1 0 8 8.86 0.9 -1 0 -8 6.15 0.69 -1 0 8 6.24 0.66 1 0 -8 6.31 0.71 1 0 -8 6.28 0.73 1 0 8 7.64 0.61 1 0 8 8.63 5.06 1 0 8 6.62 0.82 1 0 8 5.98 1.27 -1 0 8 5.85 0.84 2 0 -8 12.03 1.2 2 0 8 24.7 7.11 -2 0 -8 14.13 4.49 -2 0 -8 11.91 1.12 -2 0 8 12.77 1.59 -2 0 -8 13.5 2.02 -2 0 8 9.96 2.6 2 0 8 13.62 1.83 -2 0 8 17.02 7.41 -2 0 8 12.32 1.15 2 0 -8 7.06 4.38 -2 0 -8 12.4 1.12 2 0 -8 11.83 2.2 3 0 -8 9.06 2.01 3 0 -8 7.45 0.89 3 0 8 12.39 5.06 3 0 -8 7.68 0.88 3 0 -8 2.91 4.33 -3 0 -8 7.73 0.74 -3 0 -8 8.92 1.4 -3 0 8 8.13 0.86 -3 0 8 10.42 2.27 -3 0 8 7.54 1.06 -3 0 -8 7.88 0.74 -3 0 -8 6.45 1.17 -3 0 8 15.37 6.93 4 0 -8 122.6 11.29 -4 0 8 131.82 11.32 4 0 -8 105.97 19.96 -4 0 8 147.96 12.71 -4 0 -8 132.85 11.21 -4 0 -8 130.26 11.52 4 0 -8 135.64 12.16 5 0 -8 6.86 0.89 5 0 -8 -4.99 4.63 -5 0 8 9.55 2.58 -5 0 8 5.41 0.98 -5 0 8 12.72 9.72 5 0 -8 7.33 1.94 6 0 -8 36.58 3.37 -6 0 8 38.07 3.38 -6 0 8 36.47 5.3 6 0 -8 35.42 4.58 6 0 -8 37.82 3.36 -6 0 8 51.29 13.67 -7 0 8 0.86 2.08 -7 0 8 -2.79 7.28 7 0 -8 2.27 0.54 7 0 -8 2.69 1.65 0 0 9 6.82 4.41 0 0 -9 3.18 3.01 0 0 -9 1.18 1.01 0 0 9 -0.66 1.02 0 0 -9 1.38 0.31 -1 0 -9 1.28 2.81 -1 0 9 2.72 0.39 1 0 9 2.55 0.31 1 0 -9 1.84 3.14 1 0 -9 3.74 1.37 -1 0 9 1.13 5.38 1 0 -9 2.62 0.4 -1 0 -9 2.15 0.35 1 0 9 5.17 5.42 -1 0 -9 2.63 0.44 -1 0 -9 2.57 1.08 -1 0 9 2.03 1.24 1 0 -9 3.53 0.47 1 0 9 2 1.11 2 0 -9 106.15 15.27 2 0 9 116.62 11.06 -2 0 9 125.83 10.48 2 0 -9 125.63 10.52 -2 0 -9 131.01 10.47 2 0 -9 132.05 11.37 -2 0 9 123.49 11.56 -2 0 -9 97.31 13.18 -3 0 9 1.26 0.55 -3 0 9 -5.11 6.29 3 0 -9 1.44 0.37 -3 0 -9 0.59 0.63 3 0 -9 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0.9 4 21 1 34.31 2.84 -4 -21 1 36.93 11.26 4 -21 -1 31.86 2.86 4 -21 -1 32.27 2.87 -4 21 -1 32.83 2.93 4 21 1 40.36 5.51 -4 -21 1 29.95 4.02 4 21 -1 34.57 2.87 -4 -21 -1 30.06 4.05 4 -21 1 32.15 2.85 4 21 -1 27.77 4.62 -4 21 1 27.61 2.91 4 21 -1 21.72 10.44 0 21 2 0.22 1.41 0 21 -2 -0.13 0.36 0 -21 -2 1.74 5.87 0 21 2 0.33 0.37 0 -21 -2 0.28 1.18 0 21 -2 -0.03 1.75 0 -21 2 -0.51 4.97 0 21 -2 0.34 0.37 0 -21 2 0.58 1.05 0 -21 -2 -0.09 0.37 0 21 -2 1.14 4.58 0 -21 -2 -0.14 0.33 0 21 2 4 4.4 1 21 2 19.98 3.21 1 -21 -2 18.94 1.69 1 21 2 18.78 1.69 1 21 2 8.3 6.23 -1 21 -2 15.33 2.95 -1 21 -2 10.05 5.96 1 -21 -2 19.16 1.71 -1 -21 2 13.17 2.81 -1 21 -2 16.65 1.7 1 -21 -2 18.7 3.24 -1 21 -2 20.93 1.99 1 -21 -2 28.76 10.21 1 21 -2 15.85 1.7 1 -21 2 12.54 6.93 -1 -21 -2 15.49 2.99 1 21 -2 14.63 3.09 -1 -21 -2 18.29 1.7 1 -21 2 12.05 2.57 -1 -21 -2 20.29 1.74 -1 21 2 11.78 9.07 -1 -21 -2 15.31 7.96 -1 21 2 17.59 1.71 2 -21 -2 33.77 2.81 -2 21 -2 30.37 2.81 2 -21 -2 24.02 7.74 -2 21 -2 32.79 9.72 -2 -21 2 35.78 10.5 2 21 2 17.05 8.78 -2 -21 2 29.63 3.95 2 -21 -2 29.82 3.99 2 -21 -2 31.83 2.81 -2 21 -2 30.55 2.83 2 21 2 34.53 4.26 2 21 -2 31.44 2.84 -2 21 2 30.66 2.82 -2 21 2 30.08 2.82 -2 21 2 24.53 8.35 -2 21 2 34.4 3.99 2 21 -2 19.91 7.85 2 21 -2 24.06 4.19 -2 -21 -2 35.97 2.87 -2 -21 -2 31.66 4.05 2 -21 2 28.36 15.59 -3 -21 2 11.36 6.72 3 21 2 4.69 1.92 3 -21 -2 5.01 0.72 -3 21 -2 4.05 0.64 -3 21 -2 3.1 5.2 -3 -21 2 3.09 1.33 3 -21 -2 6.73 0.77 3 21 2 0.23 5.53 3 21 2 4.8 0.68 -3 -21 -2 5.16 1.67 -3 -21 -2 7.32 6.69 -3 21 2 5.49 0.71 3 -21 2 9.78 6.75 -3 21 2 4.94 0.81 3 21 -2 3.09 0.59 -3 21 2 -0.68 5.19 3 21 -2 4.43 2.09 -4 21 -2 4 0.65 4 -21 -2 5.18 0.74 -4 -21 2 2.42 1.39 -4 -21 2 11.98 7.77 4 -21 -2 4.17 0.69 4 21 2 3.77 0.62 4 21 2 3.58 1.85 4 21 -2 4.31 0.69 -4 -21 -2 4.84 1.81 4 21 -2 -8.21 5.87 4 21 -2 2.64 1.8 -4 21 2 4.23 0.67 0 21 -3 6.62 6.28 0 -21 -3 20.95 1.75 0 -21 3 15.02 2.87 0 21 3 19.2 1.69 0 21 3 17.74 3.07 0 -21 3 20.14 8.24 0 21 3 10.89 6.55 0 21 -3 16.79 1.71 0 -21 -3 17.7 1.72 0 21 -3 15.28 2.96 0 -21 -3 14.22 2.88 0 -21 -3 29.27 9.23 1 -21 -3 16.42 1.49 1 -21 -3 5.76 7.03 1 21 3 10.04 9.21 -1 21 -3 4.25 5.13 1 21 3 17.11 3.06 -1 -21 3 12.08 2.35 -1 -21 3 18.66 7.96 -1 21 -3 13.71 1.47 1 -21 -3 16.15 2.88 -1 21 -3 15.15 1.49 1 -21 -3 16.96 1.49 -1 -21 -3 13.73 2.78 1 -21 3 9.32 6.75 -1 21 3 9.39 5.82 1 21 -3 12.89 1.69 -1 -21 -3 18.28 7.71 1 21 -3 11.93 6.87 1 21 -3 16.05 1.48 -1 21 3 15.2 3.03 -2 21 -3 0.06 0.29 -2 21 -3 3.67 5.25 2 21 3 -3.47 4.92 2 21 3 -0.81 2.47 2 -21 -3 1.2 1.3 2 -21 -3 -0.01 0.33 2 -21 -3 -0.03 0.31 2 21 3 0.26 0.35 -2 -21 3 0.41 1.14 -2 -21 3 -0.39 6.4 -2 -21 -3 -0.24 0.35 -2 -21 -3 0.34 0.42 -2 -21 -3 -1.66 5.26 -2 21 3 1.31 4.01 2 21 -3 0.97 1.26 -2 -21 -3 0.26 1.12 2 -21 3 2.2 6.07 -2 21 3 -0.04 0.28 -2 21 3 -0.11 0.39 2 21 -3 0.88 5.47 2 21 -3 0.61 0.39 -3 -21 3 25.76 10.5 3 21 3 33.05 4.01 3 -21 -3 25.61 3.75 -3 21 -3 27.18 2.56 -3 21 -3 28.61 2.56 3 -21 -3 28.99 2.53 -3 -21 3 22.01 3.52 3 -21 -3 27.48 2.53 -3 21 -3 13.15 6.5 3 21 3 32.47 2.47 -3 21 3 18.94 7.91 3 21 -3 12.25 8.76 3 21 -3 26.59 2.59 -3 21 3 27.54 2.66 -3 -21 -3 27.34 3.8 0 21 4 -1.05 1.49 0 -21 4 -1.29 5.33 0 21 -4 -0.16 1.27 0 -21 -4 0.03 1.16 0 21 -4 -0.05 0.29 0 21 4 0.51 0.38 0 21 -4 -2.62 5.85 0 -21 -4 -0.17 5.24 0 -21 -4 -0.27 0.37 0 -21 -4 -0.21 0.37 0 21 4 0.62 5.14 -1 -21 4 22.44 3.71 1 -21 -4 26.77 3.98 -1 -21 4 16.46 8.97 1 -21 -4 32.03 2.79 1 21 4 31.39 9.9 1 -21 -4 35.05 2.79 1 21 4 33.74 4.13 -1 21 -4 28.42 2.78 -1 21 4 35.25 2.77 1 -21 4 33.61 10.14 -1 -21 -4 32.04 2.78 -1 -21 -4 26.26 3.82 1 21 -4 21.66 4.16 -1 21 4 21.97 7.8 2 -21 -4 0.6 0.42 2 -21 -4 0.97 1.48 2 -21 -4 0.64 0.39 -2 21 -4 4.25 5.56 -2 -21 4 1.69 6.68 -2 -21 4 0.38 1.09 2 21 4 5.59 7.92 2 21 4 0.78 0.36 -2 21 -4 0.62 0.39 2 21 4 -1.07 1.38 -2 21 4 -0.21 0.4 -2 -21 -4 0.5 0.39 2 21 -4 1.21 2.8 2 21 -4 -1.47 4.91 -2 -21 -4 0.53 1.68 -2 21 4 7.11 6.18 -2 -21 -4 0.22 0.4 -2 -21 -4 -4 4.81 2 -21 4 -0.47 5.07 2 21 -4 0.3 0.39 3 21 4 4.09 0.62 3 21 4 4.18 1.94 3 -21 -4 4.09 0.61 -3 -21 4 9.39 8.2 3 -21 -4 2.56 1.46 -3 21 -4 3.87 0.64 -3 -21 4 3.37 1.95 3 -21 -4 5.2 0.79 -3 -21 -4 5.19 0.77 -3 21 4 3.26 0.68 3 21 -4 3.62 0.6 3 21 -4 -2.53 6.28 -3 21 4 -4.14 6.25 -3 -21 -4 4.53 1.76 0 21 -5 0.32 5.98 0 21 5 1.52 0.43 0 -21 -5 0.78 0.38 0 21 -5 1.17 0.43 0 -21 5 2.91 6.52 0 -21 -5 -0.19 1.23 0 21 5 -1.13 6.44 1 21 5 29.84 9.84 1 -21 -5 21.51 3.5 -1 21 -5 4.78 8.94 1 -21 -5 21.78 2.15 -1 -21 5 17.71 9.91 1 21 5 24.14 3.56 1 -21 -5 21.84 2.16 -1 21 -5 19.89 2.12 -1 -21 -5 24.83 2.17 -1 21 5 25.66 2.13 -1 -21 -5 20.7 9.13 -1 -21 -5 20.63 3.38 -1 -21 -5 24.32 2.15 1 -21 5 19.25 10.3 2 -21 -5 0.35 1.31 -2 -21 5 0.56 6.8 -2 -21 5 0.08 1.55 2 -21 -5 0.19 0.4 2 -21 -5 -1.65 1.32 -2 21 -5 0.01 0.41 2 -21 -5 0.02 0.38 2 21 5 -0.84 1.43 2 21 -5 -0.27 0.37 -2 -21 -5 0.4 0.4 2 21 -5 10.83 8.06 -2 -21 -5 -0.48 1.03 2 21 -5 0.84 1.49 -2 21 5 0.42 0.43 -2 21 5 10.45 5.52 -2 21 5 3.33 5.72 -2 -21 -5 0 0.39 0 -21 -6 0.42 0.39 0 21 6 0.02 0.39 0 21 6 1.46 4.81 0 21 6 -3.31 5.54 0 21 -6 0.07 0.4 0 -21 -6 -0.03 1.19 0 22 0 36.06 10.99 0 -22 0 79.53 19.37 0 22 0 64.6 5.21 0 -22 0 55.5 6.27 -1 22 0 0.39 0.27 -1 22 0 0.85 1.48 1 22 0 1.35 1.36 1 22 0 6.69 6.01 1 22 0 -0.08 0.41 1 -22 0 0.52 1.36 1 -22 0 8.01 7.52 -1 -22 0 -0.17 1.51 1 -22 0 -0.02 0.33 -1 -22 0 1.6 5.26 -1 22 0 10.37 5.74 2 22 0 1 6.24 -2 -22 0 9.56 6.34 2 22 0 1.58 0.47 -2 -22 0 1.9 1.3 2 22 0 1.02 1.74 -2 22 0 2.37 0.44 2 -22 0 1.74 0.41 -2 22 0 2.97 0.53 2 -22 0 -3.57 4.5 -2 22 0 -3.87 6.49 3 -22 0 0.27 0.34 -3 -22 0 0.62 1.28 3 22 0 0.59 6.06 -3 22 0 -2.43 11.86 3 22 0 0.13 1.72 -3 -22 0 4.38 6.11 -3 22 0 -0.18 0.4 0 22 1 -0.79 5.02 0 22 -1 -0.65 1.82 0 -22 -1 -1.87 2.07 0 -22 1 -0.13 1.28 0 -22 -1 -0.12 0.34 0 -22 1 3.23 5.53 0 22 -1 -0.25 0.33 0 22 1 -0.11 0.39 0 22 -1 -0.2 0.47 0 22 -1 0.61 6.44 0 -22 -1 2.14 6.04 -1 -22 1 4.04 1.76 -1 22 -1 7.32 6.1 -1 -22 1 5.52 5.98 1 -22 -1 5.51 1.81 1 22 1 0.76 6.06 1 -22 -1 7.46 6.11 1 -22 -1 4.21 0.74 -1 22 -1 3.67 0.63 1 22 1 5.83 1.93 1 22 1 5.81 0.83 1 -22 -1 5.84 0.83 -1 22 -1 4.15 1.83 -1 22 -1 6.44 1.1 -1 22 1 4.98 1.88 1 22 -1 6.7 6.48 -1 22 1 4.9 0.81 -1 -22 -1 -2.39 5.41 -1 22 1 4.33 0.79 -1 -22 -1 3.82 1.63 -1 22 1 3.53 5.55 1 -22 1 -3.37 5.91 -2 -22 1 32.65 4.38 2 -22 -1 39.79 3.27 2 22 1 39.9 4.74 -2 22 -1 29.18 9.63 2 -22 -1 42.8 3.29 2 22 1 27.35 9.86 -2 -22 1 29.52 10.18 2 -22 -1 36.09 11.6 -2 22 1 32.45 3.26 2 22 -1 36.12 3.27 -2 22 1 27.51 9.63 2 -22 1 53.77 14.63 2 22 -1 22.26 8.38 2 22 -1 34.35 4.83 -2 -22 -1 32.68 4.49 -2 22 1 38.54 3.3 3 22 1 1.05 0.41 -3 -22 1 1.35 6.97 3 22 1 1.08 1.84 -3 -22 1 1.4 1.42 -3 22 -1 1.16 0.46 3 -22 -1 1.8 0.39 3 22 1 8.5 7.17 3 -22 -1 3.51 6.49 3 -22 -1 1.23 0.42 3 22 -1 2.98 6.7 3 22 -1 0.84 1.68 -3 22 1 -1.39 7.09 3 22 -1 1.34 0.42 -3 -22 -1 1.74 1.35 -3 -22 -1 3.05 6.23 -3 22 1 1.19 0.48 0 -22 -2 41.63 12 0 -22 -2 35.75 2.87 0 22 2 32.68 4.25 0 22 -2 28.53 2.83 0 -22 -2 29.85 4.1 0 -22 2 28.38 9.85 0 22 2 32.97 2.83 0 22 -2 26.1 4.01 0 22 2 23.19 7.52 1 -22 -2 10.39 1.08 1 22 2 5.79 6.28 1 22 2 8.85 2.43 1 -22 -2 8.95 1.06 1 -22 -2 7.49 2.11 -1 -22 2 10.87 7.85 -1 -22 2 8.07 2.02 -1 22 -2 8.9 1.05 -1 22 -2 -3.26 5 1 22 2 10.09 1.1 1 -22 -2 10.78 6.26 1 22 -2 8.37 1.08 -1 22 2 9.75 1.12 -1 22 2 9.22 2.14 1 22 -2 9.59 6.27 -1 22 2 7.08 6.61 -1 -22 -2 9.25 2.2 -1 -22 -2 12.64 7.74 1 -22 2 13.95 7.9 1 22 -2 8.57 4.18 -1 -22 -2 9.36 1.06 -2 22 -2 4.45 5.78 2 22 2 1.05 1.54 2 22 2 1.47 0.44 2 -22 -2 1.78 0.44 2 22 2 -3.32 6.29 2 -22 -2 1.82 0.43 -2 -22 2 0.68 1.18 -2 -22 2 2.01 6.54 -2 22 -2 2.47 0.52 2 -22 -2 1.33 6.11 -2 -22 -2 -3.02 7.87 2 22 -2 1.42 0.78 -2 -22 -2 1.38 1.52 2 -22 2 -2.19 5.43 -2 22 2 1.95 0.4 -2 22 2 1.74 1.89 -2 22 2 3.01 6.34 2 22 -2 1.59 5.04 -2 22 2 1.45 0.5 3 22 2 18.2 1.58 3 -22 -2 19.18 1.65 3 -22 -2 16.14 1.61 -3 -22 2 14.76 2.91 -3 22 -2 15.98 1.68 3 22 2 12.25 2.77 3 22 -2 7.5 7.44 -3 -22 -2 15.49 3.09 -3 22 2 15.15 1.69 3 22 -2 16.85 1.61 0 -22 3 0 5.97 0 22 3 1.54 1.5 0 -22 -3 -0.29 0.36 0 22 3 -0.57 5.02 0 -22 -3 -4.95 5.79 0 -22 -3 0.39 0.4 0 22 -3 0.16 0.27 0 22 -3 0.05 0.4 0 22 3 0.2 0.4 0 -22 -3 -0.12 1.36 0 22 -3 0.15 5.88 1 -22 -3 18.74 8.37 -1 22 -3 9.6 6.36 1 22 3 9.05 6.35 1 -22 -3 18.72 3.36 -1 22 -3 20.34 1.94 1 -22 -3 19.39 1.98 -1 -22 3 22.9 12.25 -1 -22 3 20.91 3.19 1 22 3 22.03 3.59 -1 22 3 18.21 7.53 -1 22 3 22.75 3.59 1 22 -3 17.22 3.37 1 22 -3 19.42 1.92 -1 -22 -3 19.97 3.31 -1 -22 -3 24.49 2 1 -22 3 15.43 7.37 2 22 3 10.39 1 -2 -22 3 7.61 2.58 -2 22 -3 8.12 1.04 2 22 3 10.24 6.08 2 -22 -3 8.76 1.04 -2 -22 3 -3.59 7.11 2 22 3 7.73 2.3 2 -22 -3 8.64 1.07 -2 22 3 -1.12 6.3 -2 -22 -3 10.75 7.17 2 22 -3 6.99 1.03 -2 -22 -3 11.36 1.07 2 22 -3 9.36 6.48 2 22 -3 5.13 2.24 -2 -22 -3 6.89 1.93 0 22 4 2.31 0.5 0 -22 4 -5.56 7.03 0 22 -4 7.24 6.99 0 -22 -4 3.92 5.84 0 22 -4 1.96 0.51 0 -22 -4 2.99 0.57 0 22 4 1.26 1.48 0 -22 -4 0.89 1.59 0 22 4 0.59 6.61 0 -22 -4 2.09 0.51 1 -22 -4 21.21 1.97 1 22 4 18.18 3.43 1 22 4 10.41 7.43 -1 22 -4 17.59 1.93 1 -22 -4 23 2.17 -1 -22 4 18.03 9.61 1 22 4 23.73 1.92 -1 -22 -4 20.41 1.96 -1 22 4 11.43 7.37 -1 22 4 23.41 1.95 1 22 -4 8.5 9.42 -1 -22 -4 20.54 1.98 1 22 -4 16.54 1.9 -1 -22 -4 30.51 10.59 -1 -22 -4 14.99 3.14 2 22 4 -1 2.5 -2 -22 4 -0.18 1.24 -2 -22 4 6.37 8.44 -2 22 4 -0.19 4.78 2 22 -4 -3.24 7.01 0 23 0 0.14 0.43 0 23 0 -1.96 6.74 0 -23 0 -5.2 5.75 0 23 0 -0.25 2.06 0 -23 0 0.64 1.49 1 23 0 0.37 6.76 -1 23 0 -8.14 5.02 -1 -23 0 -4.98 6.39 -1 23 0 0.11 0.49 -1 -23 0 -0.25 1.4 1 -23 0 6.68 7.89 1 23 0 0.05 0.43 2 -23 0 38.18 3.22 2 23 0 18.71 10.46 2 23 0 36.32 3.24 -2 23 0 38.01 3.27 2 23 0 30.92 4.67 -2 -23 0 31.23 6.01 0 23 -1 39.48 4.96 0 -23 -1 41.43 4.96 0 -23 -1 46.53 13.5 0 -23 -1 44.74 3.63 0 23 1 43.04 5.04 0 23 1 40.03 3.62 0 -23 1 60.77 16.65 0 23 1 36.96 10.07 0 23 -1 36.31 3.65 0 23 -1 29.94 12.39 -1 23 -1 0.73 0.45 1 23 1 -2.98 6.68 -1 23 -1 3.61 7.61 -1 -23 1 1.5 1.4 -1 -23 1 -5.83 5.97 1 23 1 2.39 1.85 1 -23 -1 1.65 0.44 1 23 -1 0.82 1.33 -1 23 1 2.31 1.81 -1 -23 -1 2.07 1.66 -1 -23 -1 4.3 6.74 1 23 -1 1.6 6.24 -1 23 1 -5.27 6.94 1 -23 1 -2.46 5.39 -1 23 1 1.69 0.54 1 23 -1 1.94 0.55 2 -23 -1 1.74 0.45 2 23 1 0.18 1.66 2 -23 -1 1.56 0.43 2 23 1 -3.16 5.78 -2 -23 1 3.51 2.17 -2 23 -1 1.68 0.52 -2 -23 -1 0.57 1.42 2 23 -1 1.76 0.49 -2 23 1 1.36 0.51 2 23 -1 1.3 8.6 0 -23 2 -2.04 6.15 0 23 -2 -0.56 5.64 0 23 2 0.49 5.48 0 23 2 0.46 2.36 0 23 -2 -0.22 0.42 0 -23 -2 -1 1.08 0 -23 -2 1.23 6.72 0 -23 -2 -0.04 0.47 0 -23 -2 0.28 0.42 1 -23 -2 11.01 1.49 1 23 2 11.85 1.24 1 23 2 15.88 2.97 1 23 2 13.49 7.86 1 -23 -2 10.8 1.21 -1 -23 2 9.96 8.06 -1 23 -2 11.89 1.26 -1 -23 2 9.62 2.36 1 -23 -2 14.48 7.7 -1 23 2 11.57 1.25 1 23 -2 10.18 1.23 1 -23 2 14.75 11.41 1 23 -2 11.86 2.78 1 23 -2 15.04 8.25 -1 -23 -2 8.04 2.84 -1 -23 -2 11.34 1.24 -1 23 2 7.7 2.06 -1 23 2 11.55 7.49 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 O2 Pb1 O2 79.3(3) 7_565 . O2 Pb1 O2 96.0(2) 8_556 . O2 Pb1 O2 96.0(2) 7_565 2_455 O2 Pb1 O2 77.4(3) 8_556 2_455 O3 Pb1 O2 129.74(14) . . O3 Pb1 O2 72.25(16) . 2_455 O3 Pb1 O2 129.74(14) . 7_565 O3 Pb1 O2 72.25(16) . 8_556 O1 Pb1 O2 50.24(14) . . O1 Pb1 O2 104.9(2) 7_565 . O1 Pb1 O2 152.40(15) 7_565 8_556 O1 Pb1 O2 104.9(2) . 7_565 O1 Pb1 O2 90.5(2) 7_565 2_455 O1 Pb1 O2 152.40(15) . 2_455 O1 Pb1 O2 90.5(2) . 8_556 O1 Pb1 O2 50.24(14) 7_565 7_565 O1 Pb1 O3 80.49(17) 7_565 . O1 Pb1 O3 80.49(17) . . O1 Pb1 O1 89.2(3) 7_565 . C1 O2 Pb1 145.3(5) . 2 C1 O2 Pb1 89.0(4) . . C5 O3 Pb1 127.9(8) 7_565 . C5 O3 Pb1 127.9(8) . . C5 O3 C5 83.8(14) . 7_565 C1 O1 Pb1 97.8(3) . . O1 C1 O2 122.5(5) . . C2 C1 O2 118.5(5) . . C2 C1 O1 118.9(5) . . C4 C2 C1 117.8(5) . . C3 C2 C1 121.6(5) . . C3 C2 C4 120.6(5) . . H4 C4 C2 119.1(3) . . C3 C4 C2 121.9(5) 5_766 . C3 C4 H4 119.1(3) 5_766 . C4 C3 C2 117.5(5) 5_766 . C8 C3 C2 123.7(12) . . C8 C3 C4 118.5(12) . 5_766 H5 C5 O3 113.2(8) . 7_565 N1 C5 O3 133.6(14) . 7_565 N1 C5 H5 113.2(8) . . C6 N1 C5 126.1(16) . . C7 N1 C5 113.0(15) . . C7 N1 C6 120.3(14) . . H6a C6 N1 109.5 . . H6b C6 N1 109.5 . . H6b C6 H6a 109.5 . . H6c C6 N1 109.5 . . H6c C6 H6a 109.5 . . H6c C6 H6b 109.5 . . H7a C7 N1 109.5 . . H7b C7 N1 109.5 . . H7b C7 H7a 109.5 . . H7c C7 N1 109.5 . . H7c C7 H7a 109.5 . . H7c C7 H7b 109.5 . . H8a C8 C3 109.5 . . H8b C8 C3 109.5 . . H8b C8 H8a 109.5 . . H8c C8 C3 109.5 . . H8c C8 H8a 109.5 . . H8c C8 H8b 109.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Pb1 O2 2.643(6) . Pb1 O2 2.699(6) 2_455 Pb1 O2 2.643(6) 7_565 Pb1 O2 2.699(6) 8_556 Pb1 O3 2.519(6) . Pb1 O1 2.453(4) . Pb1 O1 2.453(4) 7_565 O2 C1 1.231(6) . O3 C5 1.139(12) . O3 C5 1.139(12) 7_565 O1 C1 1.243(7) . C1 C2 1.520(6) . C2 C4 1.358(8) . C2 C3 1.369(8) . C4 H4 0.9300 . C4 C3 1.421(7) 5_766 C3 C8 1.57(2) . C5 H5 0.9300 . C5 N1 1.301(17) . N1 C6 1.45(3) . N1 C7 1.50(2) . C6 H6a 0.9600 . C6 H6b 0.9600 . C6 H6c 0.9600 . C7 H7a 0.9600 . C7 H7b 0.9600 . C7 H7c 0.9600 . C8 H8a 0.9600 . C8 H8b 0.9600 . C8 H8c 0.9600 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 Pb1 O2 C1 O1 6.1(5) . . . . Pb1 O2 C1 O1 -95.2(8) 2 . . . Pb1 O2 C1 O1 6.1(5) 7_565 . . . Pb1 O2 C1 O1 -95.2(8) 8_656 . . . Pb1 O2 C1 C2 -174.3(3) . . . . Pb1 O2 C1 C2 -174.3(3) 7_565 . . . Pb1 O2 C1 C2 84.3(8) 2 . . . Pb1 O2 C1 C2 84.3(8) 8_656 . . . Pb1 O3 C5 N1 -161.2(10) . . . . Pb1 O3 C5 N1 161.2(10) . . 7_565 7_565 Pb1 O1 C1 O2 -6.6(6) . . . . Pb1 O1 C1 O2 -6.6(6) 7_565 . . . Pb1 O1 C1 C2 173.8(3) . . . . Pb1 O1 C1 C2 173.8(3) 7_565 . . . O2 C1 C2 C4 -20.3(7) . . . . O2 C1 C2 C3 159.2(7) . . . . O3 C5 N1 C6 -176.2(18) . . . . O3 C5 N1 C6 -176.2(18) 7_565 . . . O3 C5 N1 C7 -5(2) . . . . O3 C5 N1 C7 -5(2) 7_565 . . . O1 C1 C2 C4 159.3(7) . . . . O1 C1 C2 C3 -21.2(7) . . . . C1 C2 C4 C3 -178.7(6) . . . 5_766 C1 C2 C3 C4 178.8(7) . . . 5_766 C1 C2 C3 C8 5.1(14) . . . . C2 C4 C3 C2 -1.8(8) . . 5_766 5_766 C2 C4 C3 C8 -175.8(14) . . 5_766 5_766 C2 C3 C4 C2 1.8(8) . . 5_766 5_766 loop_ _restr_U_iso_atom_site_label _restr_U_iso_weight_param O1 0.0200 C6 0.0020 C6 0.0200 C6 0.0020 C7 0.0020 C7 0.0020 C7 0.0200 C8 0.0020 loop_ _restr_U_rigid_atom_site_label_1 _restr_U_rigid_atom_site_label_2 _restr_U_rigid_target_weight_param _restr_U_rigid_U_parallel _restr_U_rigid_diff C5 N1 0.0100 0.0571 0.0033 C5 C6 0.0100 0.0734 -0.0364 C5 C7 0.0100 0.0909 -0.0286 N1 C6 0.0100 0.0874 -0.0092 N1 C7 0.0100 0.1043 -0.0016 C6 C7 0.0100 0.0992 -0.0125