A new synthetic method to Mn carboxylate clusters: reductive fragmentation of [Mn~12~O~12~(O~2~CR)~16~(H~2~O)~4~] to [Mn~8~O~2~(O~2~CR)~14~(RCO~2~H)~4~] (R = CH2But)
Authors of publication
Boskovic, Colette; Huffman, John C.; Christou, George
Journal of publication
Chemical Communications
Year of publication
2002
Journal issue
21
Pages of publication
2502 - 2503
a
14.7812 ± 0.0004 Å
b
15.0833 ± 0.0004 Å
c
35.2358 ± 0.0009 Å
α
78.7348 ± 0.0012°
β
84.8151 ± 0.0012°
γ
61.9138 ± 0.0006°
Cell volume
6797.2 ± 0.3 Å3
Cell temperature
117 ± 2 K
Ambient diffraction temperature
117 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for significantly intense reflections
0.0441
Weighted residual factors for all reflections included in the refinement
0.0436
Goodness-of-fit parameter for all reflections included in the refinement
1.5095
Diffraction radiation wavelength
0.71073 Å
Diffraction radiation type
MoKα
Has coordinates
Yes
Has disorder
Yes
Has Fobs
No
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