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Information card for entry 5000372
Preview
| Coordinates | 5000372.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C108 H152 Mo2 N2 O12 |
|---|---|
| Calculated formula | C103.6 H133.6 Mo2 N2 O10.2 |
| Title of publication | Dinuclear Molybdenum and Tungsten Complexes with Metal-Metal Triple Bonds Supported by p-tert-Butylcalix[4]arene Ligands |
| Authors of publication | Malcolm H. Chisholm; Kirsten Folting; William E. Streib; De-Dong Wu |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 1999 |
| Journal volume | 38 |
| Pages of publication | 5219 - 5229 |
| a | 13.105 ± 0.004 Å |
| b | 18.631 ± 0.006 Å |
| c | 20.543 ± 0.006 Å |
| α | 90° |
| β | 94.035 ± 0.016° |
| γ | 90° |
| Cell volume | 5003 ± 3 Å3 |
| Cell temperature | 104 K |
| Ambient diffraction temperature | 104 K |
| Number of distinct elements | 5 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for significantly intense reflections | 0.067 |
| Weighted residual factors for all reflections included in the refinement | 0.0662 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.5027 |
| Diffraction radiation wavelength | 0.71069 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
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