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Information card for entry 7051206
Preview
| Coordinates | 7051206.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C5 H14 N8 Ni |
|---|---|
| Calculated formula | C5 H14 N8 Ni |
| Title of publication | Synthesis of N3−/SCN− bridged polynuclear complexes of nickel(II) using N,N,N'-trimethylethane-1,2-diamine as a blocking ligand: low temperature magnetic study and single crystal structure of [Ni(μ1,1-N3)(μ1,3-N3)(N,N,N'-Me3en)]n |
| Authors of publication | Montserrat Monfort; Inmaculada Resino; Joan Ribas; Xavier Solans; Mercé Font-Bardia |
| Journal of publication | New J. Chem. |
| Year of publication | 2001 |
| Journal volume | 25 |
| Journal issue | 12 |
| Pages of publication | 1577 - 1582 |
| a | 7.132 ± 0.004 Å |
| b | 10.122 ± 0.002 Å |
| c | 14.614 ± 0.005 Å |
| α | 90° |
| β | 102.22 ± 0.02° |
| γ | 90° |
| Cell volume | 1031.1 ± 0.7 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.1373 |
| Residual factor for significantly intense reflections | 0.0504 |
| Weighted residual factors for all reflections | 0.1395 |
| Weighted residual factors for significantly intense reflections | 0.1008 |
| Goodness-of-fit parameter for all reflections | 1.005 |
| Goodness-of-fit parameter for significantly intense reflections | 1.07 |
| Diffraction radiation wavelength | 0.71069 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
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