#------------------------------------------------------------------------------ #$Date: 2026-04-24 05:57:51 +0100 (Fri, 24 Apr 2026) $ #$Revision: 305615 $ #$URL: svn://www.crystallography.net/cod/cif/7/06/43/7064385.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7064385 loop_ _publ_author_name 'Caltagirone, Claudia' 'Lippolis, Vito' 'Olmos, Maria Elena' 'Coconubo, Laura' 'Moreno, Sonia' 'Picci, Giacomo' 'Monge, Miguel' 'L\'opez-de-Luzuriaga, Jos\'e Maria' _publ_section_title ; Structural and computational evidence of rare synergic N(amide)H•••Au(I) and N(amidate)•••Au(I) secondary bonding interactions ; _journal_name_full 'New Journal of Chemistry' _journal_paper_doi 10.1039/D6NJ00558F _journal_year 2026 _chemical_formula_moiety 'C43 H33 Au2 Cl2 N3 O2 P2' _chemical_formula_sum 'C43 H33 Au2 Cl2 N3 O2 P2' _chemical_formula_weight 1150.546 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_Int_Tables_number 2 _atom_sites_solution_primary iterative _audit_creation_date 2026-03-16 _audit_creation_method ; Olex2 1.5 (compiled 2025.07.13 svn.rb7424aed for OlexSys, GUI svn.r7314) ; _audit_update_record ; 2026-03-19 deposited with the CCDC. 2026-04-21 downloaded from the CCDC. ; _cell_angle_alpha 94.721(1) _cell_angle_beta 90.624(1) _cell_angle_gamma 106.150(1) _cell_formula_units_Z 2 _cell_length_a 11.1966(4) _cell_length_b 11.5477(4) _cell_length_c 16.5303(5) _cell_measurement_reflns_used 9871 _cell_measurement_temperature 296.00 _cell_measurement_theta_max 26.85 _cell_measurement_theta_min 2.31 _cell_volume 2044.70(12) _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine 1.5 (Bourhis et al., 2015)' _computing_structure_solution 'olex2.solve 1.5 (Bourhis et al., 2015)' _diffrn_ambient_temperature 296.00 _diffrn_measured_fraction_theta_full 0.9977 _diffrn_measured_fraction_theta_max 0.9977 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0321 _diffrn_reflns_av_unetI/netI 0.0242 _diffrn_reflns_Laue_measured_fraction_full 0.9977 _diffrn_reflns_Laue_measured_fraction_max 0.9977 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 51359 _diffrn_reflns_point_group_measured_fraction_full 0.9977 _diffrn_reflns_point_group_measured_fraction_max 0.9977 _diffrn_reflns_theta_full 24.7112 _diffrn_reflns_theta_max 24.71 _diffrn_reflns_theta_min 2.30 _exptl_absorpt_coefficient_mu 7.441 _exptl_absorpt_correction_T_max 0.0210 _exptl_absorpt_correction_T_min 0.0049 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0871 before and 0.0478 after correction. The Ratio of minimum to maximum transmission is 0.2333. The \l/2 correction factor is Not present. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.869 _exptl_crystal_description prism _exptl_crystal_F_000 1096.051 _exptl_crystal_size_max 0.197 _exptl_crystal_size_mid 0.127 _exptl_crystal_size_min 0.075 _refine_diff_density_max 0.3934 _refine_diff_density_min -0.4523 _refine_diff_density_rms 0.0683 _refine_ls_d_res_high 0.8501 _refine_ls_d_res_low 8.8580 _refine_ls_goodness_of_fit_ref 1.0447 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_constraints 62 _refine_ls_number_parameters 545 _refine_ls_number_reflns 6971 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.0447 _refine_ls_R_factor_all 0.0282 _refine_ls_R_factor_gt 0.0205 _refine_ls_shift/su_max -0.0003 _refine_ls_shift/su_mean 0.0000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0102P)^2^+1.2685P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0413 _refine_ls_wR_factor_ref 0.0443 _reflns_Friedel_coverage 0.0 _reflns_limit_h_max 13 _reflns_limit_h_min -13 _reflns_limit_k_max 13 _reflns_limit_k_min -13 _reflns_limit_l_max 19 _reflns_limit_l_min 0 _reflns_number_gt 5936 _reflns_number_total 6971 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL 1_a.res in P-1 CELL 0.71073 11.1966 11.5477 16.5303 94.721 90.624 106.15 ZERR 2 0.0004 0.0004 0.0005 0.001 0.001 0.001 LATT 1 SFAC C H Au Cl N O P UNIT 86 66 4 4 6 4 4 EQIV $1 1-X,1-Y,1-Z EQIV $2 1-X,-Y,1-Z EQIV $3 1-X,1-Y,-Z L.S. 20 PLAN 7 SIZE 0.075 0.127 0.197 TEMP 22.85 HTAB N1 Au1 HTAB C21 Au1 HTAB C31 Au1 HTAB C43 Au2 HTAB C33 Cl1_$1 HTAB C16 O2_$2 HTAB C36 O1_$3 CONF MORE -1 FMAP 2 ACTA BOND $H LIST 4 MERG 2 SHEL 0.85 99 OMIT 1 -1 2 WGHT 0.010191 1.268462 FVAR 0.367536 REM REM REM REM > REM REM Au1 3 0.767872 0.512710 0.343741 11.00000 0.08169 0.08759 = 0.08204 0.00447 0.00783 0.02022 Au2 3 0.210391 0.087080 0.210888 11.00000 0.08779 0.10551 = 0.07823 -0.00500 0.00535 0.01758 Cl1 4 0.659624 0.451293 0.455340 11.00000 0.09033 0.10953 = 0.07838 0.00528 0.02167 0.01748 Cl2 4 0.189947 -0.046058 0.099643 11.00000 0.14206 0.14573 = 0.10844 -0.04508 0.03576 -0.00308 P1 7 0.893009 0.585058 0.244513 11.00000 0.06461 0.06992 = 0.07045 0.00926 0.00544 0.01702 P2 7 0.229873 0.227430 0.314728 11.00000 0.06422 0.08139 = 0.06054 0.00711 0.00018 0.02228 C1 1 0.827043 0.661700 0.171625 11.00000 0.07158 0.06651 = 0.07727 0.01094 0.01139 0.02107 C2 1 0.881366 0.781445 0.157315 11.00000 0.08997 0.06955 = 0.10311 0.01571 0.00128 0.01551 AFIX 43 H2 2 0.951920 0.826227 0.187687 11.00000 -1.20000 AFIX 0 C3 1 0.831815 0.835138 0.098344 11.00000 0.11060 0.07259 = 0.12487 0.03115 0.01376 0.02773 AFIX 43 H3 2 0.870979 0.914513 0.088073 11.00000 -1.20000 AFIX 0 C4 1 0.725114 0.771559 0.055036 11.00000 0.11967 0.08619 = 0.10686 0.03115 0.00242 0.04485 AFIX 43 H4 2 0.691749 0.808180 0.015885 11.00000 -1.20000 AFIX 0 C5 1 0.667235 0.653172 0.069572 11.00000 0.08945 0.08528 = 0.09342 0.01892 0.00005 0.03202 AFIX 43 H5 2 0.593783 0.610857 0.041237 11.00000 -1.20000 AFIX 0 C6 1 0.718935 0.597433 0.126586 11.00000 0.07091 0.06845 = 0.07341 0.01550 0.00732 0.02099 N1 5 0.663697 0.473453 0.136826 11.00000 0.07291 0.07366 = 0.06524 0.01409 0.00447 0.01672 C7 1 0.645802 0.385779 0.075427 11.00000 0.07781 0.08182 = 0.06408 0.01309 0.00093 0.01911 O1 6 0.657454 0.405542 0.004402 11.00000 0.18542 0.09485 = 0.06418 0.01881 0.00637 0.02897 C8 1 0.618332 0.259363 0.100003 11.00000 0.07118 0.07539 = 0.06259 0.00803 0.00146 0.01727 C9 1 0.635520 0.170225 0.044538 11.00000 0.10240 0.09129 = 0.06805 0.00538 0.01086 0.02901 AFIX 43 H9 2 0.656368 0.186499 -0.008475 11.00000 -1.20000 AFIX 0 C10 1 0.621111 0.056573 0.069431 11.00000 0.13387 0.08547 = 0.08297 0.00142 0.02147 0.04219 AFIX 43 H10 2 0.634430 -0.004775 0.033694 11.00000 -1.20000 AFIX 0 C11 1 0.587101 0.034390 0.147005 11.00000 0.11465 0.07025 = 0.08488 0.01082 0.01987 0.03153 AFIX 43 H11 2 0.576826 -0.041979 0.164834 11.00000 -1.20000 AFIX 0 C12 1 0.568342 0.127420 0.198269 11.00000 0.06494 0.07006 = 0.06849 0.00868 0.00472 0.01956 N2 5 0.584151 0.239565 0.176780 11.00000 0.05977 0.06933 = 0.06363 0.00785 0.00337 0.01846 C13 1 0.525195 0.101941 0.282079 11.00000 0.06513 0.06773 = 0.07290 0.01365 0.00495 0.01867 O2 6 0.524136 0.007233 0.309144 11.00000 0.12162 0.07802 = 0.08897 0.02412 0.02054 0.04095 N3 5 0.485742 0.190180 0.322144 11.00000 0.06791 0.06673 = 0.07144 0.01776 0.00964 0.02364 C14 1 0.427368 0.179907 0.398021 11.00000 0.06344 0.06223 = 0.06404 0.01117 0.00489 0.01706 C15 1 0.483267 0.148380 0.463803 11.00000 0.06439 0.07180 = 0.07854 0.01384 0.00059 0.01916 AFIX 43 H15 2 0.560933 0.134568 0.458852 11.00000 -1.20000 AFIX 0 C16 1 0.425622 0.136979 0.537036 11.00000 0.08683 0.07175 = 0.06641 0.01291 -0.00764 0.02183 AFIX 43 H16 2 0.463406 0.113824 0.580921 11.00000 -1.20000 AFIX 0 C17 1 0.312674 0.159788 0.545077 11.00000 0.09003 0.08386 = 0.06105 0.01209 0.01026 0.02724 AFIX 43 H17 2 0.274495 0.153730 0.594844 11.00000 -1.20000 AFIX 0 C18 1 0.255299 0.191645 0.479893 11.00000 0.07472 0.08593 = 0.06177 0.00990 0.00717 0.02955 AFIX 43 H18 2 0.178900 0.207837 0.486087 11.00000 -1.20000 AFIX 0 C19 1 0.310596 0.199921 0.404511 11.00000 0.06431 0.06259 = 0.06067 0.00718 0.00060 0.01766 C20 1 0.946444 0.472629 0.182712 11.00000 0.06321 0.08667 = 0.06234 0.01653 0.00130 0.02322 C21 1 0.909502 0.353775 0.199513 11.00000 0.07815 0.08818 = 0.07129 0.00376 0.00178 0.03174 AFIX 43 H21 2 0.861637 0.332566 0.244462 11.00000 -1.20000 AFIX 0 C22 1 0.941952 0.265301 0.151085 11.00000 0.11171 0.10197 = 0.09280 -0.00942 -0.00774 0.05073 AFIX 43 H22 2 0.914707 0.184908 0.162706 11.00000 -1.20000 AFIX 0 C23 1 1.014243 0.296009 0.085967 11.00000 0.12238 0.14078 = 0.08625 -0.01282 -0.00576 0.07309 AFIX 43 H23 2 1.035268 0.236432 0.052510 11.00000 -1.20000 AFIX 0 C24 1 1.055597 0.414403 0.070085 11.00000 0.11344 0.17914 = 0.07376 0.01410 0.01935 0.07548 AFIX 43 H24 2 1.107625 0.435558 0.026995 11.00000 -1.20000 AFIX 0 C25 1 1.020463 0.504314 0.118025 11.00000 0.09995 0.12078 = 0.08045 0.02201 0.01219 0.04666 AFIX 43 H25 2 1.047028 0.584617 0.106128 11.00000 -1.20000 AFIX 0 C26 1 1.025721 0.697422 0.293177 11.00000 0.06801 0.07436 = 0.08387 0.00877 0.00248 0.01718 C27 1 1.145535 0.700520 0.280778 11.00000 0.07702 0.10067 = 0.17444 -0.02975 -0.00593 0.02053 AFIX 43 H27 2 1.164227 0.644237 0.243159 11.00000 -1.20000 AFIX 0 C28 1 1.241577 0.788060 0.324305 11.00000 0.07135 0.11877 = 0.24590 -0.04904 -0.02612 0.01920 AFIX 43 H28 2 1.323695 0.789156 0.315226 11.00000 -1.20000 AFIX 0 C29 1 1.217975 0.869127 0.378000 11.00000 0.09619 0.08461 = 0.14497 -0.00142 -0.03803 0.01130 AFIX 43 H29 2 1.283227 0.926599 0.406309 11.00000 -1.20000 AFIX 0 C30 1 1.098221 0.868870 0.392093 11.00000 0.11057 0.09308 = 0.11250 -0.01380 -0.00355 0.01057 AFIX 43 H30 2 1.080918 0.926503 0.429258 11.00000 -1.20000 AFIX 0 C31 1 1.004012 0.782273 0.350553 11.00000 0.08403 0.10932 = 0.10688 -0.01598 0.00450 0.01460 AFIX 43 H31 2 0.922214 0.780490 0.361375 11.00000 -1.20000 AFIX 0 C32 1 0.316035 0.375810 0.287147 11.00000 0.06450 0.08428 = 0.06571 0.01132 0.00441 0.03174 C33 1 0.392960 0.460698 0.342310 11.00000 0.09049 0.07719 = 0.07514 0.00972 0.00552 0.02573 AFIX 43 H33 2 0.401186 0.442264 0.395435 11.00000 -1.20000 AFIX 0 C34 1 0.457506 0.572009 0.319793 11.00000 0.10498 0.07689 = 0.10727 0.01085 0.00744 0.01969 AFIX 43 H34 2 0.509644 0.627846 0.357677 11.00000 -1.20000 AFIX 0 C35 1 0.446177 0.601676 0.242774 11.00000 0.09955 0.08658 = 0.13083 0.03458 0.02764 0.02988 AFIX 43 H35 2 0.489528 0.677650 0.228093 11.00000 -1.20000 AFIX 0 C36 1 0.370335 0.518661 0.186984 11.00000 0.10845 0.13012 = 0.09688 0.05568 0.02106 0.05038 AFIX 43 H36 2 0.361570 0.538931 0.134383 11.00000 -1.20000 AFIX 0 C37 1 0.306075 0.403991 0.208229 11.00000 0.08544 0.11392 = 0.07676 0.02606 -0.00363 0.02601 AFIX 43 H37 2 0.256969 0.347037 0.169587 11.00000 -1.20000 AFIX 0 C38 1 0.081268 0.240058 0.350945 11.00000 0.06992 0.09161 = 0.06969 0.01552 -0.00232 0.02791 C39 1 0.068653 0.342318 0.394186 11.00000 0.07286 0.10931 = 0.08712 -0.00333 -0.00489 0.03265 AFIX 43 H39 2 0.137233 0.409704 0.403774 11.00000 -1.20000 AFIX 0 C40 1 -0.045244 0.345624 0.423490 11.00000 0.08955 0.14727 = 0.09715 0.00280 0.00690 0.05850 AFIX 43 H40 2 -0.052953 0.415113 0.453041 11.00000 -1.20000 AFIX 0 C41 1 -0.146521 0.247864 0.409467 11.00000 0.07656 0.15680 = 0.13560 0.05792 0.03295 0.05312 AFIX 43 H41 2 -0.223021 0.251264 0.429256 11.00000 -1.20000 AFIX 0 C42 1 -0.136742 0.144767 0.366556 11.00000 0.07156 0.11335 = 0.17115 0.05794 0.02270 0.02310 AFIX 43 H42 2 -0.206168 0.078158 0.357232 11.00000 -1.20000 AFIX 0 C43 1 -0.022573 0.140201 0.337029 11.00000 0.07421 0.09485 = 0.11473 0.02821 0.00522 0.02598 AFIX 43 H43 2 -0.015317 0.070257 0.307847 11.00000 -1.20000 AFIX 0 H1 2 0.658443 0.453776 0.182355 11.00000 0.07168 H3a 2 0.494964 0.250721 0.301195 11.00000 0.06924 HKLF 4 END Q2 1 0.2 0.175 0.166667 11 0.05 0.36 Q5 1 0.15 0.25 0.333333 11 0.05 0.31 Q6 1 0.8 0.525 0.266667 11 0.05 0.29 Q4 1 0.65 0.425 0.383333 11 0.05 0.32 Q1 1 0.2 -0.125 0.133333 11 0.05 0.39 Q3 1 0.175 -0.025 0.1 11 0.05 0.36 Q7 1 0.2 0.175 0.266667 11 0.05 0.26 REM The information below was added by Olex2. REM REM R1 = 0.0205 for 5936 Fo > 4sig(Fo) and 0.0282 for all 6971 data REM 545 parameters refined using 0 restraints REM Highest difference peak 0.3934, deepest hole -0.4523 REM Mean Shift 0.0000, Max Shift -0.0003. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0282 REM R1_gt = 0.0205 REM wR_ref = 0.0443 REM GOOF = 1.0447 REM Shift_max = -0.0003 REM Shift_mean = 0.0000 REM Reflections_all = 6971 REM Reflections_gt = 5936 REM Parameters = 545 REM Hole = -0.4523 REM Peak = 0.3934 REM Flack = n/a ; _cod_data_source_file d6nj00558f2.cif _cod_data_source_block bsm139lc154aw1 _cod_database_code 7064385 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2.a Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3), C4(H4), C5(H5), C9(H9), C10(H10), C11(H11), C15(H15), C16(H16), C17(H17), C18(H18), C21(H21), C22(H22), C23(H23), C24(H24), C25(H25), C27(H27), C28(H28), C29(H29), C30(H30), C31(H31), C33(H33), C34(H34), C35(H35), C36(H36), C37(H37), C39(H39), C40(H40), C41(H41), C42(H42), C43(H43) ; _iucr_refine_fcf_details ; data_bsm139lc154aw1_CCDC1 _computing_structure_refinement 'olex2.refine 1.5 (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_Int_Tables_number 2 _cell_length_a 11.1966(4) _cell_length_b 11.5477(4) _cell_length_c 16.5303(5) _cell_angle_alpha 94.721(1) _cell_angle_beta 90.624(1) _cell_angle_gamma 106.150(1) _cell_volume 2044.70(12) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status -13 2 1 271.282 243.666 77.730 8.112 o -13 2 2 122.142 147.343 32.563 42.168 o -13 3 1 116.411 146.033 30.025 48.684 o -13 3 2 38.330 14.235 18.724 133.037 o -13 3 3 41.204 -5.271 18.227 141.008 o -13 4 1 36.179 21.788 19.109 127.801 o -13 4 2 131.509 96.525 21.406 84.627 o -13 4 3 123.617 82.094 19.922 96.337 o -13 5 1 282.841 230.914 25.557 51.909 o -13 5 2 9.707 25.363 18.532 142.858 o -12 -1 1 403.620 355.094 29.075 38.279 o -12 -1 2 365.787 342.751 29.312 39.018 o -12 -1 3 63.067 93.553 24.059 77.001 o -12 -1 4 109.801 129.454 33.175 41.429 o -12 -1 5 38.441 36.622 22.200 95.696 o -12 0 1 5.582 33.796 18.499 143.304 o -12 0 2 11.009 38.519 16.906 166.220 o -12 0 3 364.301 388.258 30.762 36.127 o -12 0 4 2.592 -11.432 25.430 79.778 o -12 0 5 1003.950 1025.190 41.706 16.550 o -12 0 6 174.739 191.582 22.755 69.031 o -12 1 1 32.602 36.851 19.785 119.088 o -12 1 2 1087.550 1064.640 70.240 8.058 o -12 1 3 64.053 92.227 40.554 29.781 o -12 1 4 302.535 250.375 40.867 25.373 o -12 1 5 251.189 278.106 32.136 37.794 o -12 1 6 85.895 97.526 31.395 47.048 o -12 1 7 6.083 19.485 28.501 62.697 o -12 2 1 580.106 590.926 37.631 23.618 o -12 2 2 17.805 -5.957 20.098 123.551 o -12 2 3 37.911 41.436 34.893 40.851 o -12 2 4 6.899 -2.245 20.509 121.388 o -12 2 5 685.333 650.376 43.248 18.675 o -12 2 6 385.749 397.127 34.750 30.143 o -12 2 7 314.792 350.263 34.590 31.919 o -12 2 8 471.839 481.039 67.002 10.121 o -12 3 1 44.622 19.049 17.374 148.850 o -12 3 2 320.117 322.178 28.829 41.457 o -12 3 3 340.703 305.325 33.983 32.697 o -12 3 4 164.799 142.727 23.639 68.020 o -12 3 5 423.626 340.469 29.555 37.190 o -12 3 6 0.924 -2.910 18.700 147.719 o -12 3 7 30.484 58.294 19.028 125.453 o -12 3 8 20.096 7.821 21.493 107.341 o -12 4 1 531.402 532.412 30.149 32.098 o -12 4 2 202.892 147.552 20.653 77.959 o -12 4 3 34.082 1.931 15.491 191.971 o -12 4 4 104.177 131.304 24.255 70.601 o -12 4 5 57.812 44.670 20.007 110.530 o -12 4 6 758.648 723.260 38.997 20.494 o -12 4 7 5.805 43.341 18.573 140.582 o -12 4 8 870.401 1041.840 43.939 16.195 o -12 5 1 58.669 36.833 16.299 156.336 o -12 5 2 114.622 62.780 23.812 74.865 o -12 5 3 722.213 782.404 37.755 21.355 o -12 5 4 10.041 35.665 16.019 184.754 o -12 5 5 807.246 901.723 41.642 18.032 o -12 5 6 44.227 30.145 17.709 142.254 o -12 5 7 88.528 89.273 20.366 98.012 o -12 6 1 133.984 143.367 20.778 85.201 o -12 6 2 593.093 610.204 31.473 28.965 o -12 6 3 1.427 -2.903 15.322 219.374 o -12 6 4 83.798 96.778 18.344 115.273 o -12 6 5 0.582 -15.268 15.268 221.593 o -12 6 6 124.255 84.909 20.033 95.238 o -12 7 1 15.027 26.607 18.947 135.173 o -12 7 2 22.817 43.370 15.739 181.372 o -12 7 3 279.530 254.027 24.925 53.223 o -12 7 4 184.003 201.289 26.569 54.471 o -12 7 5 220.264 199.895 20.254 75.492 o -12 8 1 26.627 37.368 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436.107 27.165 38.224 o 9 4 1 1301.640 1313.990 44.579 13.550 o 9 4 2 647.271 730.553 34.562 24.674 o 9 4 3 2110.010 2203.430 54.877 8.345 o 9 4 4 1.955 -18.137 23.614 92.563 o 9 4 5 304.700 297.627 28.710 42.529 o 9 4 6 32.488 41.336 26.376 69.885 o 9 4 7 110.522 85.742 21.140 89.608 o 9 4 8 26.636 54.778 18.702 130.861 o 9 4 9 488.021 484.603 31.371 31.831 o 9 5 0 681.120 631.993 28.942 29.980 o 9 5 1 82.949 96.868 19.778 102.905 o 9 5 2 109.019 110.312 20.944 89.451 o 9 5 3 23.089 47.423 18.564 134.711 o 9 5 4 479.596 537.187 38.568 24.122 o 9 5 5 15.488 14.652 26.137 73.697 o 9 5 6 625.206 551.699 71.652 8.725 o 9 5 7 136.503 151.839 21.674 79.460 o 9 6 0 1.643 19.421 12.694 303.194 o 9 6 1 316.803 308.783 24.976 50.139 o 9 6 2 14.364 30.391 16.002 184.159 o 9 6 3 828.869 794.998 41.109 18.512 o 9 6 4 267.052 295.159 29.782 41.564 o 10 -11 0 270.615 252.586 29.698 42.264 o 10 -11 1 216.337 212.524 23.828 61.238 o 10 -11 2 140.565 196.186 24.576 64.037 o 10 -11 3 223.807 247.230 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74.392 o 10 -8 6 270.943 294.636 20.239 67.112 o 10 -8 7 585.883 548.502 25.430 36.761 o 10 -8 8 16.403 38.962 15.198 198.060 o 10 -8 9 124.372 114.762 18.309 105.555 o 10 -8 10 2.213 -2.486 14.485 244.563 o 10 -7 0 4.068 -1.229 10.601 446.948 o 10 -7 1 368.481 340.589 17.863 65.687 o 10 -7 2 230.191 223.946 15.841 94.867 o 10 -7 3 532.741 534.164 21.870 43.716 o 10 -7 4 550.847 591.880 25.422 37.098 o 10 -7 5 9.362 -2.199 11.918 345.196 o 10 -7 6 40.319 39.216 13.054 233.994 o 10 -7 7 110.398 140.923 15.436 131.820 o 10 -7 8 194.681 210.969 13.186 119.876 o 10 -7 9 2.357 -8.622 14.254 252.303 o 10 -7 10 399.799 405.134 26.404 42.318 o 10 -7 11 84.712 72.416 17.624 125.189 o 10 -6 0 1247.840 1227.790 35.071 17.464 o 10 -6 1 761.107 785.527 31.983 25.129 o 10 -6 2 125.099 138.052 20.788 86.565 o 10 -6 3 22.107 0.651 16.196 184.039 o 10 -6 4 26.326 34.274 14.650 205.875 o 10 -6 5 656.641 656.582 31.120 28.041 o 10 -6 6 8.274 2.225 13.416 275.450 o 10 -6 7 1614.820 1609.820 45.587 11.780 o 10 -6 8 333.397 391.478 32.026 34.836 o 10 -6 9 287.863 269.702 25.762 50.289 o 10 -6 10 230.802 226.919 22.869 63.164 o 10 -6 11 11.605 24.830 14.987 211.335 o 10 -5 0 411.794 382.026 21.050 53.389 o 10 -5 1 349.624 331.097 19.337 62.993 o 10 -5 2 235.359 250.043 17.535 83.737 o 10 -5 3 109.342 113.969 15.185 138.973 o 10 -5 4 1943.220 1909.180 40.682 11.522 o 10 -5 5 105.412 100.065 16.127 131.843 o 10 -5 6 794.782 832.022 32.770 23.907 o 10 -5 7 179.196 172.806 16.007 106.944 o 10 -5 8 38.029 23.883 14.560 203.522 o 10 -5 9 6.708 15.578 12.414 311.138 o 10 -5 10 231.526 245.217 13.427 106.619 o 10 -5 11 286.840 260.072 23.380 57.067 o 10 -5 12 91.994 103.227 18.471 111.674 o 10 -4 0 632.639 653.987 27.282 32.389 o 10 -4 1 3776.400 3793.610 73.627 4.423 o 10 -4 2 299.021 330.531 20.776 62.055 o 10 -4 3 1188.240 1164.430 31.407 19.697 o 10 -4 4 13.680 3.179 13.140 278.944 o 10 -4 5 101.704 84.952 16.170 134.687 o 10 -4 6 97.569 95.794 15.499 142.136 o 10 -4 7 246.673 236.925 22.733 62.244 o 10 -4 8 665.501 717.091 29.989 28.543 o 10 -4 9 16.721 26.740 12.999 266.228 o 10 -4 10 250.874 216.377 16.787 87.536 o 10 -4 11 0.742 2.844 11.698 373.335 o 10 -4 12 6.279 8.132 19.022 139.696 o 10 -3 0 1233.370 1269.700 33.823 17.945 o 10 -3 1 163.675 155.587 17.274 102.453 o 10 -3 2 18.106 30.674 14.347 221.076 o 10 -3 3 112.410 76.861 15.424 141.248 o 10 -3 4 566.813 638.757 25.905 35.538 o 10 -3 5 875.177 878.590 30.523 24.385 o 10 -3 6 686.827 712.749 40.059 20.404 o 10 -3 7 1245.260 1212.270 44.105 14.109 o 10 -3 8 35.910 9.051 13.694 233.420 o 10 -3 9 44.486 24.285 14.434 201.934 o 10 -3 10 0.566 -10.807 10.807 441.467 o 10 -3 11 717.636 787.347 31.890 25.708 o 10 -3 12 163.571 162.712 13.203 134.742 o 10 -2 0 37.472 38.077 15.077 188.083 o 10 -2 1 2861.240 2825.390 50.766 7.359 o 10 -2 2 1007.790 1013.090 29.589 22.887 o 10 -2 3 891.742 936.977 30.427 23.950 o 10 -2 4 1172.790 1060.280 33.246 19.322 o 10 -2 5 23.844 7.934 18.319 144.147 o 10 -2 6 38.461 9.010 20.123 117.294 o 10 -2 7 124.644 127.160 18.790 100.739 o 10 -2 8 746.960 703.772 27.337 29.884 o 10 -2 9 20.449 39.483 14.001 224.989 o 10 -2 10 1033.820 1032.770 33.910 20.130 o 10 -2 11 463.614 517.378 25.720 39.932 o 10 -2 12 142.265 176.185 22.118 75.414 o 10 -1 0 2151.500 2184.330 41.895 10.387 o 10 -1 1 841.656 883.686 30.623 24.661 o 10 -1 2 42.718 45.169 18.743 127.280 o 10 -1 3 61.747 34.214 22.185 92.582 o 10 -1 4 181.960 164.958 18.113 93.285 o 10 -1 5 836.280 884.653 29.381 25.629 o 10 -1 6 16.470 30.762 17.130 161.565 o 10 -1 7 923.244 923.085 33.971 21.449 o 10 -1 8 29.456 59.356 30.291 53.496 o 10 -1 9 64.862 56.466 18.469 123.189 o 10 -1 10 3.164 6.026 14.425 242.691 o 10 -1 11 91.611 76.977 18.950 110.168 o 10 0 0 37.706 49.546 18.277 133.742 o 10 0 1 378.775 468.965 31.782 33.484 o 10 0 2 2340.540 2302.970 50.547 8.527 o 10 0 3 40.119 65.698 19.640 115.638 o 10 0 4 1281.950 1246.340 39.561 15.482 o 10 0 5 14.993 20.483 21.225 109.712 o 10 0 6 211.255 207.405 23.056 64.509 o 10 0 7 3.118 2.019 17.890 160.008 o 10 0 8 187.827 177.480 23.338 66.192 o 10 0 9 678.372 693.773 32.702 26.080 o 10 0 10 145.001 177.845 30.443 45.929 o 10 0 11 798.279 863.955 48.865 14.800 o 10 1 0 463.245 518.711 24.738 41.511 o 10 1 1 2248.840 2199.120 46.572 9.382 o 10 1 2 129.180 132.849 19.171 96.814 o 10 1 3 141.464 151.862 20.003 88.319 o 10 1 4 117.799 101.794 19.021 102.358 o 10 1 5 511.999 484.684 33.810 28.644 o 10 1 6 221.451 239.310 26.269 52.618 o 10 1 7 573.822 588.766 43.702 19.325 o 10 1 8 652.343 617.015 35.672 24.332 o 10 1 9 63.850 75.706 18.951 116.169 o 10 1 10 252.227 227.485 24.630 56.131 o 10 2 0 110.042 81.059 23.064 78.395 o 10 2 1 77.788 110.906 28.636 55.455 o 10 2 2 1094.150 1072.260 44.502 14.869 o 10 2 3 327.482 399.891 32.663 33.930 o 10 2 4 1696.270 1834.680 57.587 8.862 o 10 2 5 960.864 1026.380 55.045 11.828 o 10 2 6 267.501 314.217 34.096 33.838 o 10 2 7 140.653 136.176 25.929 60.844 o 10 2 8 0.264 9.751 18.951 142.418 o 10 2 9 69.312 46.068 18.401 124.120 o 10 3 0 19.203 20.718 17.975 148.693 o 10 3 1 1253.000 1282.630 55.836 10.597 o 10 3 2 567.788 619.543 45.658 18.086 o 10 3 3 281.900 355.078 35.244 31.558 o 10 3 4 179.312 221.478 23.503 64.586 o 10 3 5 25.701 51.946 23.706 85.457 o 10 3 6 65.696 88.377 19.865 106.061 o 10 3 7 91.843 123.042 26.820 60.899 o 10 3 8 702.514 694.041 37.096 22.367 o 10 4 0 348.964 354.586 51.061 16.890 o 10 4 1 41.109 9.231 22.491 95.058 o 10 4 2 24.462 15.511 17.617 153.326 o 10 4 3 320.687 301.307 27.442 44.555 o 10 4 4 65.769 121.473 24.611 72.564 o 10 4 5 1006.820 949.613 48.781 13.865 o 10 4 6 6.789 6.922 20.921 115.983 o 10 5 0 122.935 119.888 16.234 123.339 o 10 5 1 191.287 164.958 18.643 88.867 o 10 5 2 790.294 689.753 35.738 22.541 o 10 5 3 3.116 11.339 18.216 152.593 o 11 -10 0 101.406 80.041 16.052 136.891 o 11 -10 1 127.682 199.873 27.503 54.419 o 11 -10 2 294.062 293.563 25.619 49.869 o 11 -10 3 28.382 36.248 10.379 351.792 o 11 -9 0 24.780 33.527 17.050 158.843 o 11 -9 1 23.707 -7.479 11.909 319.763 o 11 -9 2 26.306 15.898 13.520 244.398 o 11 -9 3 88.842 71.845 13.599 177.807 o 11 -9 4 6.361 6.498 14.345 242.009 o 11 -9 5 278.579 270.598 17.466 78.086 o 11 -9 6 169.661 183.146 18.111 93.772 o 11 -8 0 324.145 340.886 21.953 56.797 o 11 -8 1 0.366 -1.252 11.963 360.921 o 11 -8 2 452.649 482.733 30.679 33.392 o 11 -8 3 108.215 108.537 19.498 99.787 o 11 -8 4 20.938 21.227 12.876 268.891 o 11 -8 5 55.925 55.489 12.973 216.267 o 11 -8 6 175.932 206.725 16.013 104.331 o 11 -8 7 106.390 119.759 15.525 135.202 o 11 -8 8 137.983 156.439 16.011 117.297 o 11 -7 0 99.385 118.024 17.836 114.221 o 11 -7 1 331.789 314.361 20.675 60.761 o 11 -7 2 90.234 74.750 17.660 123.105 o 11 -7 3 84.028 65.594 13.667 180.883 o 11 -7 4 34.851 56.557 14.982 186.203 o 11 -7 5 351.521 349.027 21.873 55.306 o 11 -7 6 622.611 667.179 42.370 19.565 o 11 -7 7 22.632 39.846 13.032 251.435 o 11 -7 8 338.288 336.385 19.544 62.971 o 11 -7 9 75.504 82.844 20.040 103.311 o 11 -6 0 195.574 191.514 20.302 78.149 o 11 -6 1 12.139 -8.560 16.002 194.385 o 11 -6 2 349.569 312.435 23.060 53.299 o 11 -6 3 493.410 429.643 23.019 44.940 o 11 -6 4 275.901 316.243 30.869 38.964 o 11 -6 5 356.107 381.110 23.445 50.468 o 11 -6 6 17.973 13.791 13.799 244.811 o 11 -6 7 28.201 37.661 13.904 221.993 o 11 -6 8 2.160 5.751 23.968 89.452 o 11 -6 9 348.328 327.713 18.403 66.040 o 11 -5 0 1217.820 1312.420 47.342 12.980 o 11 -5 1 315.341 336.252 22.230 56.651 o 11 -5 2 575.989 565.365 29.162 32.143 o 11 -5 3 1.380 -0.005 13.816 269.573 o 11 -5 4 32.625 28.619 13.991 219.778 o 11 -5 5 2.055 0.749 13.746 271.042 o 11 -5 6 476.619 439.968 23.491 44.501 o 11 -5 7 274.741 279.655 19.906 68.589 o 11 -5 8 248.847 233.517 19.618 73.932 o 11 -5 9 345.474 342.774 22.551 54.040 o 11 -5 10 10.271 5.022 11.892 340.059 o 11 -4 0 261.951 284.001 20.903 65.857 o 11 -4 1 108.429 128.921 15.673 131.653 o 11 -4 2 215.193 225.849 17.137 89.859 o 11 -4 3 1098.740 1060.230 36.572 18.245 o 11 -4 4 114.621 157.966 17.252 111.788 o 11 -4 5 921.351 927.560 36.748 19.832 o 11 -4 6 300.564 332.129 24.884 50.561 o 11 -4 7 41.124 39.425 13.885 211.800 o 11 -4 8 5.360 -13.905 13.905 261.611 o 11 -4 9 192.165 203.579 17.822 90.789 o 11 -4 10 245.681 221.212 26.499 51.289 o 11 -3 0 2448.380 2408.370 64.277 6.606 o 11 -3 1 8.599 55.781 17.963 146.402 o 11 -3 2 2029.790 2080.700 44.402 10.348 o 11 -3 3 221.440 226.013 19.335 78.220 o 11 -3 4 70.733 85.103 16.171 144.646 o 11 -3 5 12.150 3.471 23.638 90.740 o 11 -3 6 161.081 100.748 18.853 96.527 o 11 -3 7 350.320 342.510 23.844 50.646 o 11 -3 8 91.941 36.822 15.314 157.633 o 11 -3 9 765.116 768.446 30.846 26.088 o 11 -3 10 2.873 16.040 13.802 259.200 o 11 -2 0 79.573 122.993 18.502 111.925 o 11 -2 1 103.665 99.302 18.715 107.632 o 11 -2 2 1.521 7.570 16.269 192.325 o 11 -2 3 524.568 500.228 32.052 30.271 o 11 -2 4 394.936 403.214 32.541 32.769 o 11 -2 5 494.613 552.299 32.188 30.180 o 11 -2 6 792.102 787.132 31.521 25.116 o 11 -2 7 0.177 -5.576 19.554 135.343 o 11 -2 8 100.012 60.347 18.559 113.695 o 11 -2 9 7.255 -1.554 20.602 120.231 o 11 -2 10 160.726 170.198 25.936 58.604 o 11 -1 0 628.505 725.545 39.414 21.242 o 11 -1 1 693.702 823.409 35.488 23.002 o 11 -1 2 673.084 700.406 41.414 19.693 o 11 -1 3 1171.200 1236.600 47.668 13.162 o 11 -1 4 104.041 95.344 19.091 104.828 o 11 -1 5 165.283 190.158 24.676 62.206 o 11 -1 6 10.927 -10.523 21.095 113.962 o 11 -1 7 110.759 61.342 22.715 81.331 o 11 -1 8 1.540 -4.495 18.632 148.562 o 11 -1 9 577.661 560.844 62.590 11.069 o 11 0 0 1184.800 1213.730 49.089 12.710 o 11 0 1 34.431 31.576 18.749 131.354 o 11 0 2 156.508 180.339 29.102 48.916 o 11 0 3 177.343 193.835 26.848 54.139 o 11 0 4 576.840 592.740 38.867 22.663 o 11 0 5 1.802 20.093 23.832 89.566 o 11 0 6 1116.330 1111.550 63.254 9.338 o 11 0 7 25.983 52.175 23.615 86.016 o 11 0 8 517.333 472.614 37.030 25.442 o 11 1 0 21.147 15.205 19.151 132.359 o 11 1 1 199.335 183.145 29.384 46.499 o 11 1 2 32.368 38.104 24.458 80.663 o 11 1 3 1648.990 1677.120 63.922 7.995 o 11 1 4 111.089 196.256 30.716 46.122 o 11 1 5 736.189 674.687 54.685 13.101 o 11 1 6 44.453 64.714 30.096 53.316 o 11 1 7 9.498 9.208 25.585 77.666 o 11 2 0 686.150 650.939 51.288 14.652 o 11 2 1 3.160 -19.759 20.710 119.953 o 11 2 2 322.340 323.654 35.277 31.097 o 11 2 3 43.808 41.322 23.048 88.353 o 11 2 4 56.422 76.147 25.195 72.394 o 11 2 5 86.999 98.202 29.544 52.354 o 11 2 6 221.737 245.784 36.116 32.329 o 11 3 0 25.226 25.808 18.062 144.377 o 11 3 1 23.607 18.829 19.394 128.112 o 11 3 2 50.859 63.175 23.818 81.226 o 11 3 3 454.933 450.707 38.564 24.843 o 11 3 4 748.486 852.742 39.393 19.842 o 12 -8 0 313.305 319.513 35.925 30.434 o 12 -8 1 35.438 31.630 13.446 230.845 o 12 -8 2 0.945 13.671 20.619 119.906 o 12 -8 3 7.609 -9.913 13.455 276.148 o 12 -8 4 241.328 244.250 22.805 62.108 o 12 -7 0 52.259 54.102 17.625 136.955 o 12 -7 1 448.962 426.127 23.551 45.622 o 12 -7 2 52.408 44.715 15.013 179.207 o 12 -7 3 322.932 295.086 24.377 51.650 o 12 -7 4 127.112 100.789 18.838 102.221 o 12 -7 5 19.881 15.047 15.152 204.794 o 12 -7 6 1.510 8.158 13.724 268.115 o 12 -6 0 507.062 471.622 27.624 36.540 o 12 -6 1 243.434 227.804 21.045 68.936 o 12 -6 2 1.213 3.672 13.950 262.533 o 12 -6 3 5.360 -13.645 13.645 271.450 o 12 -6 4 142.436 148.577 21.100 82.086 o 12 -6 5 235.334 212.171 21.050 70.223 o 12 -6 6 7.554 32.764 16.777 171.574 o 12 -6 7 409.837 419.398 23.410 47.510 o 12 -5 0 9.411 -6.951 15.759 201.975 o 12 -5 1 523.339 556.232 30.037 32.162 o 12 -5 2 450.977 440.936 25.252 42.217 o 12 -5 3 120.943 114.932 21.215 85.933 o 12 -5 4 900.651 955.787 35.297 20.713 o 12 -5 5 1.453 36.208 17.503 160.326 o 12 -5 6 157.139 139.648 23.770 68.177 o 12 -5 7 27.875 9.385 14.445 219.132 o 12 -4 0 405.263 481.364 49.001 17.450 o 12 -4 1 1365.190 1390.790 46.856 12.523 o 12 -4 2 8.884 8.566 17.429 164.395 o 12 -4 3 151.411 104.062 17.110 110.928 o 12 -4 4 4.595 -10.411 14.370 246.054 o 12 -4 5 63.988 48.656 17.481 136.012 o 12 -4 6 13.257 9.325 15.640 199.284 o 12 -4 7 254.666 183.459 25.623 54.207 o 12 -3 0 110.355 100.904 19.291 101.646 o 12 -3 1 41.847 18.020 25.390 75.270 o 12 -3 2 507.158 567.374 31.896 30.186 o 12 -3 3 78.354 94.956 19.936 102.600 o 12 -3 4 641.124 625.421 36.652 23.617 o 12 -3 5 254.157 226.475 24.913 55.214 o 12 -3 6 118.851 80.371 24.288 71.351 o 12 -3 7 53.180 0.471 34.612 41.639 o 12 -2 0 32.195 15.054 18.702 135.012 o 12 -2 1 1259.010 1312.660 48.818 12.408 o 12 -2 2 495.224 568.368 42.773 20.570 o 12 -2 3 332.626 338.256 34.964 31.216 o 12 -2 4 286.057 262.384 30.983 39.194 o 12 -2 5 24.010 54.315 31.996 48.512 o 12 -2 6 70.233 66.513 30.408 51.122 o 12 -2 7 58.749 31.676 24.761 76.530 o 12 -1 0 471.424 424.218 51.430 15.955 o 12 -1 1 116.966 91.556 26.024 63.435 o 12 -1 2 44.210 19.767 30.658 52.516 o 12 -1 3 44.110 18.590 23.476 86.799 o 12 -1 4 124.146 105.542 25.716 63.725 o 12 -1 5 713.085 682.642 53.637 13.552 o 12 -1 6 15.269 72.509 29.782 55.625 o 12 0 0 36.258 -1.842 17.677 150.832 o 12 0 1 196.697 162.137 27.773 51.266 o 12 0 2 621.788 631.036 43.163 19.200 o 12 0 3 14.591 15.616 22.980 94.630 o 12 0 4 396.455 321.673 32.811 33.139 o 12 0 5 25.002 52.147 29.049 58.355 o 12 1 0 95.647 73.770 20.327 98.407 o 12 1 1 214.724 226.044 26.357 52.998 o 12 1 2 12.489 16.018 21.501 107.929 o 12 1 3 34.992 68.079 24.261 79.987 o 13 -5 0 276.823 261.617 26.704 48.587 o 13 -5 1 49.423 34.938 19.726 116.106 o 13 -5 2 42.781 45.492 21.701 98.317 o 13 -4 0 57.529 64.166 20.904 100.891 o 13 -4 1 171.054 194.741 24.956 60.680 o 13 -4 2 37.678 41.815 19.158 124.226 o 13 -3 0 526.608 504.933 38.611 23.772 o 13 -3 1 0.895 7.570 18.096 156.202 o 13 -3 2 309.452 299.810 28.724 42.320 o 13 -2 0 1.166 -5.979 30.352 56.135 o 13 -2 1 10.843 -9.425 30.722 54.321 o ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_refinement_flags_posn Au1 Au 0.76787(4) 0.51271(4) 0.34374(2) 0.0846(3) Uani 1.000000 . Au2 Au 0.21039(4) 0.08708(4) 0.21089(2) 0.0932(2) Uani 1.000000 . Cl1 Cl 0.65962(11) 0.45129(11) 0.45534(7) 0.0949(3) Uani 1.000000 . Cl2 Cl 0.18995(15) -0.04606(15) 0.09964(9) 0.1438(6) Uani 1.000000 . P1 P 0.89301(9) 0.58506(9) 0.24451(6) 0.0685(3) Uani 1.000000 . P2 P 0.22987(9) 0.22743(9) 0.31473(6) 0.0683(3) Uani 1.000000 . C1 C 0.8270(4) 0.6617(3) 0.1716(2) 0.0711(10) Uani 1.000000 . C2 C 0.8814(4) 0.7814(4) 0.1573(3) 0.0885(12) Uani 1.000000 . H2 H 0.9519(4) 0.8262(4) 0.1877(3) 0.1062(14) Uiso 1.000000 R C3 C 0.8318(5) 0.8351(4) 0.0983(3) 0.1009(14) Uani 1.000000 . H3 H 0.8710(5) 0.9145(4) 0.0881(3) 0.1211(17) Uiso 1.000000 R C4 C 0.7251(5) 0.7716(4) 0.0550(3) 0.0997(14) Uani 1.000000 . H4 H 0.6917(5) 0.8082(4) 0.0159(3) 0.1197(17) Uiso 1.000000 R C5 C 0.6672(4) 0.6532(4) 0.0696(3) 0.0873(12) Uani 1.000000 . H5 H 0.5938(4) 0.6109(4) 0.0412(3) 0.1047(14) Uiso 1.000000 R C6 C 0.7189(4) 0.5974(3) 0.1266(2) 0.0701(9) Uani 1.000000 . N1 N 0.6637(3) 0.4735(3) 0.1368(2) 0.0709(8) Uani 1.000000 . C7 C 0.6458(4) 0.3858(4) 0.0754(2) 0.0749(10) Uani 1.000000 . O1 O 0.6575(4) 0.4055(3) 0.00440(18) 0.1162(11) Uani 1.000000 . C8 C 0.6183(3) 0.2594(3) 0.1000(2) 0.0703(9) Uani 1.000000 . C9 C 0.6355(4) 0.1702(4) 0.0445(3) 0.0869(12) Uani 1.000000 . H9 H 0.6564(4) 0.1865(4) -0.0085(3) 0.1043(14) Uiso 1.000000 R C10 C 0.6211(5) 0.0566(4) 0.0694(3) 0.0987(14) Uani 1.000000 . H10 H 0.6344(5) -0.0048(4) 0.0337(3) 0.1184(17) Uiso 1.000000 R C11 C 0.5871(4) 0.0344(4) 0.1470(3) 0.0884(12) Uani 1.000000 . H11 H 0.5768(4) -0.0420(4) 0.1648(3) 0.1061(15) Uiso 1.000000 R C12 C 0.5683(3) 0.1274(3) 0.1983(2) 0.0675(9) Uani 1.000000 . N2 N 0.5842(3) 0.2396(3) 0.17678(17) 0.0640(7) Uani 1.000000 . C13 C 0.5252(3) 0.1019(3) 0.2821(2) 0.0681(9) Uani 1.000000 . O2 O 0.5241(3) 0.0072(3) 0.30914(17) 0.0925(8) Uani 1.000000 . N3 N 0.4857(3) 0.1902(3) 0.32214(19) 0.0670(8) Uani 1.000000 . C14 C 0.4274(3) 0.1799(3) 0.3980(2) 0.0630(8) Uani 1.000000 . C15 C 0.4833(3) 0.1484(3) 0.4638(2) 0.0712(10) Uani 1.000000 . H15 H 0.5609(3) 0.1346(3) 0.4589(2) 0.0854(11) Uiso 1.000000 R C16 C 0.4256(4) 0.1370(3) 0.5370(2) 0.0748(10) Uani 1.000000 . H16 H 0.4634(4) 0.1138(3) 0.5809(2) 0.0897(12) Uiso 1.000000 R C17 C 0.3127(4) 0.1598(4) 0.5451(2) 0.0773(10) Uani 1.000000 . H17 H 0.2745(4) 0.1537(4) 0.5948(2) 0.0928(12) Uiso 1.000000 R C18 C 0.2553(4) 0.1916(3) 0.4799(2) 0.0725(10) Uani 1.000000 . H18 H 0.1789(4) 0.2078(3) 0.4861(2) 0.0870(12) Uiso 1.000000 R C19 C 0.3106(3) 0.1999(3) 0.4045(2) 0.0625(8) Uani 1.000000 . C20 C 0.9464(3) 0.4726(4) 0.1827(2) 0.0697(9) Uani 1.000000 . C21 C 0.9095(4) 0.3538(4) 0.1995(2) 0.0777(10) Uani 1.000000 . H21 H 0.8616(4) 0.3326(4) 0.2445(2) 0.0932(13) Uiso 1.000000 R C22 C 0.9420(5) 0.2653(5) 0.1511(3) 0.0991(14) Uani 1.000000 . H22 H 0.9147(5) 0.1849(5) 0.1627(3) 0.1189(17) Uiso 1.000000 R C23 C 1.0142(5) 0.2960(6) 0.0860(3) 0.1105(17) Uani 1.000000 . H23 H 1.0353(5) 0.2364(6) 0.0525(3) 0.133(2) Uiso 1.000000 R C24 C 1.0556(5) 0.4144(6) 0.0701(3) 0.1149(18) Uani 1.000000 . H24 H 1.1076(5) 0.4356(6) 0.0270(3) 0.138(2) Uiso 1.000000 R C25 C 1.0205(4) 0.5043(5) 0.1180(3) 0.0964(13) Uani 1.000000 . H25 H 1.0470(4) 0.5846(5) 0.1061(3) 0.1157(16) Uiso 1.000000 R C26 C 1.0257(4) 0.6974(4) 0.2932(2) 0.0759(10) Uani 1.000000 . C27 C 1.1455(5) 0.7005(5) 0.2808(4) 0.1208(19) Uani 1.000000 . H27 H 1.1642(5) 0.6442(5) 0.2432(4) 0.145(2) Uiso 1.000000 R C28 C 1.2416(5) 0.7881(6) 0.3243(5) 0.151(3) Uani 1.000000 . H28 H 1.3237(5) 0.7892(6) 0.3152(5) 0.181(3) Uiso 1.000000 R C29 C 1.2180(5) 0.8691(5) 0.3780(4) 0.1124(17) Uani 1.000000 . H29 H 1.2832(5) 0.9266(5) 0.4063(4) 0.135(2) Uiso 1.000000 R C30 C 1.0982(5) 0.8689(4) 0.3921(3) 0.1104(16) Uani 1.000000 . H30 H 1.0809(5) 0.9265(4) 0.4293(3) 0.1325(19) Uiso 1.000000 R C31 C 1.0040(5) 0.7823(5) 0.3506(3) 0.1041(15) Uani 1.000000 . H31 H 0.9222(5) 0.7805(5) 0.3614(3) 0.1249(18) Uiso 1.000000 R C32 C 0.3160(3) 0.3758(4) 0.2871(2) 0.0690(9) Uani 1.000000 . C33 C 0.3930(4) 0.4607(4) 0.3423(3) 0.0803(11) Uani 1.000000 . H33 H 0.4012(4) 0.4423(4) 0.3954(3) 0.0964(13) Uiso 1.000000 R C34 C 0.4575(4) 0.5720(4) 0.3198(3) 0.0974(13) Uani 1.000000 . H34 H 0.5096(4) 0.6278(4) 0.3577(3) 0.1168(16) Uiso 1.000000 R C35 C 0.4462(5) 0.6017(5) 0.2428(4) 0.1033(15) Uani 1.000000 . H35 H 0.4895(5) 0.6777(5) 0.2281(4) 0.1239(18) Uiso 1.000000 R C36 C 0.3703(5) 0.5187(5) 0.1870(3) 0.1056(15) Uani 1.000000 . H36 H 0.3616(5) 0.5389(5) 0.1344(3) 0.1268(19) Uiso 1.000000 R C37 C 0.3061(4) 0.4040(4) 0.2082(3) 0.0915(13) Uani 1.000000 . H37 H 0.2570(4) 0.3470(4) 0.1696(3) 0.1098(15) Uiso 1.000000 R C38 C 0.0813(4) 0.2401(4) 0.3509(2) 0.0756(10) Uani 1.000000 . C39 C 0.0687(4) 0.3423(4) 0.3942(3) 0.0891(12) Uani 1.000000 . H39 H 0.1372(4) 0.4097(4) 0.4038(3) 0.1069(15) Uiso 1.000000 R C40 C -0.0452(5) 0.3456(6) 0.4235(3) 0.1066(16) Uani 1.000000 . H40 H -0.0530(5) 0.4151(6) 0.4530(3) 0.1280(19) Uiso 1.000000 R C41 C -0.1465(5) 0.2479(6) 0.4095(4) 0.1160(18) Uani 1.000000 . H41 H -0.2230(5) 0.2513(6) 0.4293(4) 0.139(2) Uiso 1.000000 R C42 C -0.1367(4) 0.1448(5) 0.3666(4) 0.1165(18) Uani 1.000000 . H42 H -0.2062(4) 0.0782(5) 0.3572(4) 0.140(2) Uiso 1.000000 R C43 C -0.0226(4) 0.1402(4) 0.3370(3) 0.0930(13) Uani 1.000000 . H43 H -0.0153(4) 0.0703(4) 0.3078(3) 0.1116(16) Uiso 1.000000 R H1 H 0.658(3) 0.454(3) 0.182(2) 0.072(12) Uiso 1.000000 . H3a H 0.495(3) 0.251(3) 0.301(2) 0.069(12) Uiso 1.000000 . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Au1 0.0817(4) 0.0876(4) 0.0820(4) 0.0202(3) 0.0078(3) 0.0045(3) Au2 0.0878(4) 0.1055(4) 0.0782(4) 0.0176(3) 0.0053(3) -0.0050(3) Cl1 0.0903(8) 0.1095(8) 0.0784(7) 0.0175(6) 0.0217(6) 0.0053(6) Cl2 0.1421(12) 0.1457(12) 0.1084(10) -0.0031(10) 0.0358(9) -0.0451(9) P1 0.0646(6) 0.0699(6) 0.0705(6) 0.0170(5) 0.0054(5) 0.0093(5) P2 0.0642(6) 0.0814(6) 0.0605(5) 0.0223(5) 0.0002(4) 0.0071(5) C1 0.072(2) 0.067(2) 0.077(2) 0.0211(19) 0.011(2) 0.0109(19) C2 0.090(3) 0.070(3) 0.103(3) 0.016(2) 0.001(2) 0.016(2) C3 0.111(4) 0.073(3) 0.125(4) 0.028(3) 0.014(3) 0.031(3) C4 0.120(4) 0.086(3) 0.107(4) 0.045(3) 0.002(3) 0.031(3) C5 0.089(3) 0.085(3) 0.093(3) 0.032(2) 0.000(2) 0.019(2) C6 0.071(2) 0.068(2) 0.073(2) 0.021(2) 0.0073(19) 0.0155(19) N1 0.073(2) 0.074(2) 0.065(2) 0.0167(16) 0.0045(16) 0.0141(18) C7 0.078(3) 0.082(3) 0.064(2) 0.019(2) 0.0009(19) 0.013(2) O1 0.185(4) 0.095(2) 0.0642(19) 0.029(2) 0.006(2) 0.0188(16) C8 0.071(2) 0.075(2) 0.063(2) 0.0173(19) 0.0015(18) 0.0080(19) C9 0.102(3) 0.091(3) 0.068(3) 0.029(3) 0.011(2) 0.005(2) C10 0.134(4) 0.085(3) 0.083(3) 0.042(3) 0.021(3) 0.001(2) C11 0.115(3) 0.070(3) 0.085(3) 0.032(2) 0.020(2) 0.011(2) C12 0.065(2) 0.070(2) 0.068(2) 0.0196(18) 0.0047(17) 0.0087(18) N2 0.0598(17) 0.0693(19) 0.0636(18) 0.0185(14) 0.0034(14) 0.0078(14) C13 0.065(2) 0.068(2) 0.073(2) 0.0187(19) 0.0049(18) 0.0136(19) O2 0.122(2) 0.0780(18) 0.089(2) 0.0409(17) 0.0205(17) 0.0241(15) N3 0.068(2) 0.067(2) 0.071(2) 0.0236(16) 0.0096(15) 0.0178(17) C14 0.063(2) 0.062(2) 0.064(2) 0.0171(17) 0.0049(17) 0.0112(17) C15 0.064(2) 0.072(2) 0.079(3) 0.0192(19) 0.0006(19) 0.0138(19) C16 0.087(3) 0.072(2) 0.066(2) 0.022(2) -0.008(2) 0.0129(18) C17 0.090(3) 0.084(3) 0.061(2) 0.027(2) 0.010(2) 0.0121(19) C18 0.075(2) 0.086(3) 0.062(2) 0.030(2) 0.0072(18) 0.0099(19) C19 0.064(2) 0.063(2) 0.061(2) 0.0177(17) 0.0006(16) 0.0072(16) C20 0.063(2) 0.087(3) 0.062(2) 0.023(2) 0.0013(17) 0.0165(19) C21 0.078(3) 0.088(3) 0.071(2) 0.032(2) 0.002(2) 0.004(2) C22 0.112(4) 0.102(3) 0.093(3) 0.051(3) -0.008(3) -0.009(3) C23 0.122(4) 0.141(5) 0.086(4) 0.073(4) -0.006(3) -0.013(3) C24 0.113(4) 0.179(6) 0.074(3) 0.075(4) 0.019(3) 0.014(3) C25 0.100(3) 0.121(4) 0.080(3) 0.047(3) 0.012(2) 0.022(3) C26 0.068(3) 0.074(2) 0.084(3) 0.017(2) 0.002(2) 0.009(2) C27 0.077(3) 0.101(4) 0.174(5) 0.021(3) -0.006(3) -0.030(4) C28 0.071(3) 0.119(4) 0.246(8) 0.019(3) -0.026(4) -0.049(5) C29 0.096(4) 0.085(3) 0.145(5) 0.011(3) -0.038(3) -0.001(3) C30 0.111(4) 0.093(3) 0.112(4) 0.011(3) -0.004(3) -0.014(3) C31 0.084(3) 0.109(4) 0.107(4) 0.015(3) 0.005(3) -0.016(3) C32 0.064(2) 0.084(3) 0.066(2) 0.032(2) 0.0044(18) 0.0113(19) C33 0.090(3) 0.077(3) 0.075(3) 0.026(2) 0.006(2) 0.010(2) C34 0.105(4) 0.077(3) 0.107(4) 0.020(3) 0.007(3) 0.011(3) C35 0.100(4) 0.087(3) 0.131(4) 0.030(3) 0.028(3) 0.035(3) C36 0.108(4) 0.130(4) 0.097(4) 0.050(3) 0.021(3) 0.056(3) C37 0.085(3) 0.114(4) 0.077(3) 0.026(3) -0.004(2) 0.026(3) C38 0.070(3) 0.092(3) 0.070(2) 0.028(2) -0.0023(19) 0.016(2) C39 0.073(3) 0.109(3) 0.087(3) 0.033(3) -0.005(2) -0.003(3) C40 0.090(4) 0.147(5) 0.097(3) 0.059(4) 0.007(3) 0.003(3) C41 0.077(3) 0.157(5) 0.136(5) 0.053(4) 0.033(3) 0.058(4) C42 0.072(3) 0.113(4) 0.171(5) 0.023(3) 0.023(3) 0.058(4) C43 0.074(3) 0.095(3) 0.115(4) 0.026(2) 0.005(3) 0.028(3) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source Au -1.91220 8.83481 16.88190 18.59130 25.55820 5.86000 0.46110 8.62160 1.48260 36.39560 12.06580 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' C 0.00313 0.00162 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.21560 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' Cl 0.14908 0.15974 11.46040 7.19640 6.25560 1.64550 0.01040 1.16620 18.51940 47.77840 -9.55740 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.00304 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' N 0.00612 0.00332 12.21260 3.13220 2.01250 1.16630 0.00570 9.89330 28.99750 0.58260 -11.52900 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' O 0.01085 0.00610 3.04850 2.28680 1.54630 0.86700 13.27710 5.70110 0.32390 32.90890 0.25080 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' P 0.10265 0.09519 6.43450 4.17910 1.78000 1.49080 1.90670 27.15700 0.52600 68.16450 1.11490 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u -2 0 0 7409.66 211.88 -2 0 0 7062.89 211.68 -3 0 0 965.6 33.4 -3 0 0 1040.5 34.4 -3 0 0 972.4 33.6 -3 0 0 951.4 33.9 3 0 0 1012.5 34.4 3 0 0 989.5 34 3 0 0 996.9 33.6 3 0 0 975.3 33.5 -4 0 0 2385.26 76.69 -4 0 0 2433.06 76.39 -4 0 0 2501.35 77.19 -4 0 0 2384.26 75.99 4 0 0 2440.36 76.19 4 0 0 2461.75 77.09 4 0 0 2298.87 76.59 4 0 0 2504.45 76.39 -5 0 0 1962.3 65.59 -5 0 0 1962.4 68.79 -5 0 0 2024.7 66.69 5 0 0 2075.69 65.99 5 0 0 2337.47 78.39 5 0 0 1947.31 66.49 -6 0 0 414.06 19.5 -6 0 0 397.16 19.7 -6 0 0 398.76 22.2 6 0 0 393.06 19.2 6 0 0 393.06 19.1 6 0 0 408.56 20.3 -7 0 0 1622.74 55.49 -7 0 0 1657.93 55.09 -7 0 0 1555.14 54.29 -7 0 0 1641.74 55.69 7 0 0 1595.84 54.89 7 0 0 1567.34 55.29 7 0 0 1630.94 54.59 7 0 0 1595.04 55.89 -8 0 0 22.3 6.4 -8 0 0 24.3 6.6 -8 0 0 14.5 6.2 -8 0 0 17.1 6.6 8 0 0 28.5 7.9 8 0 0 31.2 7 8 0 0 31.9 6.8 -9 0 0 703.93 28.5 -9 0 0 682.93 28.2 -9 0 0 696.73 28.9 -9 0 0 654.83 28.7 9 0 0 649.04 29 9 0 0 698.63 28.2 9 0 0 684.93 27.8 -10 0 0 6 7.2 -10 0 0 1.2 5.4 -10 0 0 8 6.3 10 0 0 9.3 5 10 0 0 8.5 4.7 -11 0 0 170.08 13 -11 0 0 141.09 12.2 11 0 0 176.08 14.4 11 0 0 168.78 12.5 -12 0 0 0.4 5 -12 0 0 -4.9 4.7 12 0 0 0.3 4.4 12 0 0 3.5 5.1 -13 0 0 14.5 6.3 -13 0 0 29.4 7.3 13 0 0 31.4 7.2 -14 0 0 8.2 5.4 -14 0 0 0.1 4.5 14 0 0 6.1 5.3 14 -1 0 6.5 5.5 -14 1 0 25.7 11.5 13 -1 0 44.9 8 -13 1 0 41.5 8 -13 1 0 31.7 6.8 12 -1 0 63.09 8.9 -12 1 0 65.69 9.4 -12 1 0 42 7.7 11 -1 0 100.39 10.6 11 -1 0 92.69 10.2 -11 1 0 106.19 11.4 -11 1 0 93.19 10.5 10 -1 0 301.47 16.8 10 -1 0 273.07 16.9 10 -1 0 286.37 17.7 10 -1 0 308.47 16.8 10 -1 0 295.47 16.4 -10 1 0 307.37 18.6 -10 1 0 305.67 17.1 -10 1 0 307.97 17 -10 1 0 267.97 15.9 9 -1 0 181.98 12.2 9 -1 0 161.58 12.1 9 -1 0 173.78 13.2 9 -1 0 152.28 12.9 9 -1 0 192.18 13.3 -9 1 0 193.68 13.5 -9 1 0 183.88 12.6 -9 1 0 176.28 13.4 -9 1 0 166.48 13.6 8 -1 0 831.12 32.4 8 -1 0 821.02 33.5 8 -1 0 859.41 33 8 -1 0 862.31 32.9 8 -1 0 860.51 34 -8 1 0 893.01 34.1 -8 1 0 880.01 33.1 -8 1 0 840.32 32.6 -8 1 0 807.82 33.1 7 -1 0 -6.1 4.2 7 -1 0 -3 4.1 7 -1 0 -3.2 4.2 7 -1 0 -4.6 4.6 7 -1 0 1.2 5.3 -7 1 0 -6 4.2 -7 1 0 3.5 5.1 -7 1 0 -5.4 4.4 -7 1 0 -2.1 4.6 6 -1 0 592.04 23.4 6 -1 0 507.85 23 6 -1 0 541.65 24.1 6 -1 0 548.95 22.7 -6 1 0 495.35 22.9 -6 1 0 553.94 23.4 -6 1 0 533.05 23.4 -6 1 0 511.65 22.1 5 -1 0 1271.77 45.6 5 -1 0 1316.67 44.8 5 -1 0 1346.17 46.3 5 -1 0 1404.56 45.8 -5 1 0 1299.17 44.8 -5 1 0 1388.36 46.4 -5 1 0 1344.67 45.3 -5 1 0 1320.37 45.8 4 -1 0 119.19 8.4 4 -1 0 119.29 9.2 4 -1 0 120.89 9.6 4 -1 0 130.79 8.4 -4 1 0 105.79 8.5 -4 1 0 105.29 8 -4 1 0 109.99 8.9 -4 1 0 120.79 9 3 -1 0 9858.71 290.27 -3 1 0 9999 290.17 2 -1 0 877.71 28.2 2 -1 0 848.92 27.1 2 -1 0 829.32 27.4 2 -1 0 819.42 27.7 -2 1 0 875.91 27.3 -2 1 0 845.72 27.4 -2 1 0 836.22 27.8 -2 1 0 894.61 28.2 -1 -1 0 2352.36 69.49 -1 -1 0 2260.17 69.29 -1 -1 0 2262.57 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114.39 -2 2 0 3848.72 112.49 -2 2 0 3757.52 114.29 1 -2 0 252.27 9.7 1 -2 0 240.68 9.7 1 -2 0 251.37 9.7 1 -2 0 245.28 10 -1 2 0 246.38 9.7 -1 2 0 249.48 9.5 -1 2 0 246.28 10 -1 2 0 239.38 9.9 0 -2 0 3461.25 101.49 0 -2 0 3508.95 102.19 0 -2 0 3482.75 102.29 0 -2 0 3449.95 101.79 0 2 0 3476.45 102.09 0 2 0 3492.75 102.29 0 2 0 3356.76 101.09 0 2 0 3496.15 101.59 -1 -2 0 1702.43 52.19 -1 -2 0 1706.53 51.89 -1 -2 0 1651.93 51.49 1 2 0 1668.33 49.5 1 2 0 1649.83 51.39 1 2 0 1655.23 51.99 1 2 0 1667.33 51.89 -2 -2 0 3325.67 99.99 -2 -2 0 3317.27 100.29 -2 -2 0 3199.08 99.19 2 2 0 3353.06 100.09 2 2 0 3373.16 99.59 2 2 0 3176.78 99.79 -3 -2 0 -3.5 3.5 -3 -2 0 8.5 4.8 -3 -2 0 6.5 4.1 3 2 0 7.3 4.5 3 2 0 3.3 3.8 3 2 0 0.9 3.4 -4 -2 0 2301.97 75.49 -4 -2 0 2357.26 74.89 -4 -2 0 2328.37 78.29 -4 -2 0 2408.56 79.29 4 2 0 2204.18 74.89 4 2 0 2416.66 75.19 4 2 0 2436.26 75.49 -5 -2 0 441.56 20.5 -5 -2 0 417.26 19.8 -5 -2 0 404.16 20 -5 -2 0 433.36 20.4 5 2 0 437.06 20.3 5 2 0 433.46 20.2 5 2 0 405.36 19.5 -6 -2 0 917.41 35.3 -6 -2 0 940.41 35.4 -6 -2 0 847.12 34.2 -6 -2 0 952.7 36 6 2 0 961.5 35 6 2 0 915.71 35 6 2 0 906.01 35 -7 -2 0 1075.19 40.5 -7 -2 0 1111.29 40.3 -7 -2 0 1003.5 38.9 -7 -2 0 1112.79 40.8 7 2 0 1155.78 40.3 7 2 0 1098.19 40.7 7 2 0 1038.7 39.5 -8 -2 0 184.48 13.7 -8 -2 0 178.78 14.2 -8 -2 0 196.78 13.9 -8 -2 0 189.38 13.4 8 2 0 188.18 13.8 8 2 0 173.58 13.8 8 2 0 193.98 13.3 -9 -2 0 357.96 18.2 -9 -2 0 379.16 19.2 -9 -2 0 365.66 19.2 9 2 0 341.07 18.3 9 2 0 334.67 26.5 9 2 0 348.87 17.2 9 2 0 365.86 19 -10 -2 0 1.9 5.7 -10 -2 0 1.1 4.9 -10 -2 0 12.6 6.2 10 2 0 19.3 6.8 10 2 0 19.6 7.4 10 2 0 15.2 4.8 -11 -2 0 67.79 9.4 -11 -2 0 105.79 11.4 11 2 0 82.59 10 11 2 0 92.59 9 -12 -2 0 2.9 5.2 -12 -2 0 -1.1 4.9 12 2 0 -2.3 4.1 12 2 0 4.7 5 -13 -2 0 21.5 7.7 -13 -2 0 26.9 6.9 14 -3 0 -9.4 7.6 -14 3 0 -2.8 4.4 -14 3 0 5.8 5.4 13 -3 0 64.89 9.6 13 -3 0 60.99 8.7 -13 3 0 85.49 9.8 -13 3 0 59.89 8.3 12 -3 0 11.1 6 12 -3 0 16.4 5.3 12 -3 0 15 6.7 -12 3 0 10.7 5.6 -12 3 0 14.8 5.8 11 -3 0 364.36 17.8 11 -3 0 350.46 18.7 11 -3 0 302.87 17.6 11 -3 0 274.47 19.6 -11 3 0 340.27 20.2 -11 3 0 318.97 17.9 -11 3 0 304.17 17 -11 3 0 329.17 17 10 -3 0 172.38 13.5 10 -3 0 179.08 15.5 10 -3 0 166.68 13.2 10 -3 0 167.58 11.7 10 -3 0 194.38 12.9 -10 3 0 165.08 12.1 -10 3 0 165.78 13.3 -10 3 0 161.28 12.2 9 -3 0 669.33 26.6 9 -3 0 627.64 25.4 9 -3 0 651.03 27.3 9 -3 0 626.24 27.2 9 -3 0 623.74 27.3 -9 3 0 622.94 27 -9 3 0 588.34 25.5 -9 3 0 656.83 27.2 -9 3 0 648.04 26.1 8 -3 0 567.94 26 8 -3 0 598.04 24 8 -3 0 593.34 25.7 8 -3 0 558.04 25.6 8 -3 0 606.24 25.3 -8 3 0 592.14 25.4 -8 3 0 620.84 24.5 -8 3 0 636.54 26.2 -8 3 0 618.14 25 7 -3 0 117.19 10.3 7 -3 0 112.39 11.5 7 -3 0 103.49 8.8 7 -3 0 101.09 9.3 7 -3 0 98.89 10 -7 3 0 112.49 9.8 -7 3 0 131.09 11.3 -7 3 0 114.69 9 -7 3 0 115.79 10.1 6 -3 0 2054.09 65.49 6 -3 0 2032.2 66.09 6 -3 0 1962.4 63.39 6 -3 0 2076.59 64.89 6 -3 0 1968.3 69.49 -6 3 0 1934.91 63.99 -6 3 0 2017.1 64.19 -6 3 0 2045.4 65.69 -6 3 0 2007.7 68.09 5 -3 0 42.4 7 5 -3 0 58.99 9.1 5 -3 0 38.9 5 5 -3 0 40.6 6.7 -5 3 0 39.4 5.7 -5 3 0 37.3 6.5 -5 3 0 51.89 6.8 -5 3 0 43.2 7.2 4 -3 0 4543.95 129.69 4 -3 0 4295.07 127.59 4 -3 0 4204.48 130.29 4 -3 0 4386.76 130.29 4 -3 0 4234.58 131.19 -4 3 0 4385.76 130.39 -4 3 0 4244.08 129.09 -4 3 0 4205.68 129.89 -4 3 0 4414.36 128.29 3 -3 0 610.54 22.2 3 -3 0 629.74 23.7 3 -3 0 609.04 22.7 3 -3 0 619.44 20.1 3 -3 0 617.94 22.9 -3 3 0 621.74 22.1 -3 3 0 621.64 22.8 -3 3 0 649.93 23 -3 3 0 615.44 20.4 2 -3 0 7088.09 207.08 2 -3 0 7034.3 207.38 2 -3 0 7129.69 207.88 -2 3 0 6842.22 206.78 -2 3 0 7105.29 207.68 -2 3 0 7197.88 207.38 -2 3 0 7174.58 208.28 1 -3 0 2072.99 63.49 1 -3 0 2095.89 63.99 1 -3 0 2071.39 63.09 1 -3 0 2087.09 63.49 -1 3 0 2112.99 63.49 -1 3 0 2115.99 63.49 -1 3 0 2050.39 63.89 -1 3 0 2062.99 63.29 0 -3 0 5602.14 166.18 0 -3 0 5540.15 164.58 0 -3 0 5662.33 166.58 0 -3 0 5709.03 165.28 0 3 0 5631.44 164.88 0 3 0 5640.14 165.38 0 3 0 5788.92 166.28 0 3 0 5709.43 166.48 -1 -3 0 682.03 25.2 -1 -3 0 722.23 24.9 -1 -3 0 702.93 24.6 -1 -3 0 711.13 22.3 1 3 0 726.53 24.8 1 3 0 706.13 25.1 1 3 0 712.13 22.4 1 3 0 704.13 24.9 -2 -3 0 185.48 11 -2 -3 0 190.28 10.9 -2 -3 0 174.58 10 2 3 0 201.08 10.5 2 3 0 178.18 10.5 2 3 0 190.88 10.8 2 3 0 186.58 7.8 -3 -3 0 1158.18 40.9 -3 -3 0 1164.78 40.2 -3 -3 0 1233.78 41.7 3 3 0 1191.28 41 3 3 0 1160.68 37.1 3 3 0 1157.58 40.9 3 3 0 1192.08 40.5 -4 -3 0 38.7 7.4 -4 -3 0 30.9 6.3 -4 -3 0 33.7 7.2 4 3 0 42.2 7.4 4 3 0 33 7 4 3 0 33 6.7 -5 -3 0 565.64 24.4 -5 -3 0 662.13 26.3 -5 -3 0 611.04 26.2 -5 -3 0 590.64 25.5 5 3 0 553.34 24.9 5 3 0 616.14 25.3 5 3 0 558.54 25.2 -6 -3 0 -3.1 4.5 -6 -3 0 0.5 4.3 -6 -3 0 -3.3 5 -6 -3 0 -1.5 5.1 6 3 0 0 5.5 6 3 0 -1.7 4.8 6 3 0 -1.4 4.6 -7 -3 0 290.07 17.3 -7 -3 0 332.67 18.2 -7 -3 0 328.97 18 -7 -3 0 274.97 16.4 7 3 0 304.77 17 7 3 0 322.27 17.3 7 3 0 326.57 17.3 -8 -3 0 10.5 6.2 -8 -3 0 -2.6 5 -8 -3 0 8.5 5.8 -8 -3 0 -0.9 4.8 8 3 0 4.8 5.8 8 3 0 9.2 5 8 3 0 9.3 6.1 -9 -3 0 24.5 6.6 -9 -3 0 40.8 8.1 -9 -3 0 27.1 7.5 -9 -3 0 33.5 13.7 9 3 0 41.1 8 9 3 0 36.1 7.1 9 3 0 34.9 6.1 -10 -3 0 3.3 5.5 -10 -3 0 0.5 5.1 10 3 0 5.1 5.3 10 3 0 2.5 4 -11 -3 0 8.3 5.4 -11 -3 0 4.5 6 11 3 0 4.4 4 11 3 0 -2.7 4.8 -12 -3 0 -3.7 4.6 -12 -3 0 -3.7 4.2 12 3 0 10.8 4.8 12 3 0 5.1 5.7 -13 -3 0 6.7 5.1 -13 -3 0 3.9 4.7 13 3 0 6.5 4.9 -14 4 0 14.8 6 -14 4 0 9.5 5.1 13 -4 0 5.1 5.2 13 -4 0 13.7 6.4 -13 4 0 13.1 5.8 -13 4 0 4 5.4 12 -4 0 63.19 9.3 12 -4 0 44.4 8.2 12 -4 0 53.79 8.4 -12 4 0 60.29 8.6 -12 4 0 92.79 9.7 11 -4 0 39.9 6.6 11 -4 0 38.9 8.2 11 -4 0 42.6 11.2 11 -4 0 39 8 11 -4 0 43.8 8.5 -11 4 0 33.8 7.3 -11 4 0 41.8 8.9 -11 4 0 27 7.3 10 -4 0 94.59 11.2 10 -4 0 78.79 8.7 10 -4 0 78.49 10.4 10 -4 0 88.99 10 -10 4 0 77.29 8.8 -10 4 0 120.49 11.5 -10 4 0 85.89 9.5 -10 4 0 82.29 11 9 -4 0 -2.3 4.9 9 -4 0 0.5 5.5 9 -4 0 -6.8 5.2 9 -4 0 -1.1 4.1 9 -4 0 1.7 5.2 -9 4 0 -1.2 4.6 -9 4 0 -0.4 5.4 -9 4 0 -8.5 4.4 -9 4 0 -0.9 4.8 8 -4 0 83.59 10.4 8 -4 0 117.19 10.7 8 -4 0 119.19 10.6 8 -4 0 108.29 9.7 8 -4 0 116.39 10.8 -8 4 0 108.69 11.1 -8 4 0 112.09 10.2 -8 4 0 108.89 10 -8 4 0 112.29 9.7 7 -4 0 43.9 6.3 7 -4 0 37.9 7.7 7 -4 0 45.3 7.2 7 -4 0 39.9 6.6 7 -4 0 30.5 6.6 -7 4 0 34.4 6.3 -7 4 0 44.8 7.2 -7 4 0 31.2 6.6 -7 4 0 34.9 7.4 6 -4 0 -0.7 4.5 6 -4 0 2.6 4.5 6 -4 0 -2.4 3.1 6 -4 0 -3.3 4.3 -6 4 0 -1.3 3.9 -6 4 0 3.9 3.6 -6 4 0 -2.7 4 -6 4 0 -4.9 4 5 -4 0 8.7 4.6 5 -4 0 1.4 4 5 -4 0 -2.8 4.7 5 -4 0 -1.8 2.4 5 -4 0 4.9 4.3 -5 4 0 0 3.8 -5 4 0 3.7 3.7 -5 4 0 0.6 3.1 -5 4 0 3.4 3.7 4 -4 0 201.88 11.3 4 -4 0 204.58 10.8 4 -4 0 213.68 12.4 4 -4 0 202.88 11.8 4 -4 0 201.78 8.5 -4 4 0 202.68 10.8 -4 4 0 202.68 9.1 -4 4 0 212.28 11.7 -4 4 0 196.78 11.4 3 -4 0 19.5 4.6 3 -4 0 20.8 4.6 3 -4 0 23.4 4.7 3 -4 0 21.6 4.9 -3 4 0 28.6 5.1 -3 4 0 18.6 4.5 -3 4 0 29.8 4.8 -3 4 0 21.1 5.4 -3 4 0 26.7 2.8 2 -4 0 710.13 24.8 2 -4 0 666.73 24.6 2 -4 0 701.03 24.7 2 -4 0 730.23 25.6 -2 4 0 664.03 24.2 -2 4 0 677.03 21.2 -2 4 0 679.73 25.2 -2 4 0 739.03 24.9 -2 4 0 738.63 25.7 1 -4 0 9.7 3.2 1 -4 0 16.1 4.4 1 -4 0 24.3 3.8 1 -4 0 7.3 3.4 -1 4 0 8.4 3.2 -1 4 0 15.8 3.9 -1 4 0 11.7 3.5 -1 4 0 16.7 2.5 -1 4 0 15.8 3.7 0 -4 0 184.78 9.9 0 -4 0 179.68 9.4 0 -4 0 173.08 7.9 0 4 0 184.18 9.5 0 4 0 195.98 8.5 0 4 0 188.18 9.7 0 4 0 185.18 8.8 -1 -4 0 11.1 2.2 -1 -4 0 8 3.4 -1 -4 0 8.5 4.5 -1 -4 0 4 3.2 1 4 0 1 3.1 1 4 0 11.4 4.1 1 4 0 7.4 2.1 1 4 0 6.7 3.4 -2 -4 0 207.28 12.4 -2 -4 0 194.58 11.4 -2 -4 0 195.78 11.4 2 4 0 186.88 11.3 2 4 0 218.78 11.3 2 4 0 190.18 11.6 2 4 0 206.98 8.4 -3 -4 0 210.68 12.8 -3 -4 0 180.88 11.2 3 4 0 197.48 8.6 3 4 0 173.38 11.6 3 4 0 181.28 12 -4 -4 0 577.74 24.3 -4 -4 0 622.74 26.1 -4 -4 0 611.04 25.4 4 4 0 634.24 25.2 4 4 0 623.94 21.4 4 4 0 591.54 25.5 -5 -4 0 173.98 12 -5 -4 0 194.68 13.7 -5 -4 0 201.18 13.3 5 4 0 191.48 13.1 5 4 0 192.38 12.7 5 4 0 187.58 12.5 5 4 0 190.58 9.7 -6 -4 0 751.72 29.7 -6 -4 0 713.03 29.9 -6 -4 0 721.33 29.5 -6 -4 0 677.73 28.2 6 4 0 675.43 28.6 6 4 0 703.53 29.4 6 4 0 725.63 29 -7 -4 0 181.38 13.1 -7 -4 0 173.58 13.5 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349.67 17.9 4 5 0 349.67 17.8 4 5 0 390.56 18.1 4 5 0 372.46 13.9 -5 -5 0 1729.93 59.09 -5 -5 0 1667.83 57.29 -5 -5 0 1709.63 58.29 5 5 0 1772.12 57.99 5 5 0 1695.63 57.99 5 5 0 1736.63 58.09 5 5 0 1739.03 53.39 -6 -5 0 -1.4 5.4 -6 -5 0 -3.3 5.2 6 5 0 12.9 5.7 6 5 0 0.9 2.8 6 5 0 7.5 5.7 6 5 0 0.6 5 -7 -5 0 692.93 29.2 -7 -5 0 738.93 30.7 -7 -5 0 704.13 29.6 7 5 0 740.63 29.3 7 5 0 694.43 25.2 7 5 0 685.93 29.2 7 5 0 707.93 29.3 -8 -5 0 33.7 6.7 -8 -5 0 27.2 7.4 -8 -5 0 23.3 6.8 -8 -5 0 40.6 7.9 8 5 0 36.3 8.4 8 5 0 39.1 5.3 8 5 0 30.4 7.1 8 5 0 31.9 7.3 -9 -5 0 81.89 10.8 -9 -5 0 84.39 10.2 9 5 0 104.19 11.2 9 5 0 82.19 7.4 9 5 0 80.89 6.9 -10 -5 0 14.3 5.9 -10 -5 0 19.2 6.4 10 5 0 12.5 4.1 10 5 0 14.1 3.7 10 5 0 24.4 6.7 -11 -5 0 8.4 5.9 -11 -5 0 23.2 6.5 11 5 0 24 5 11 5 0 13.9 3.8 11 5 0 22.2 6.4 -12 -5 0 19.6 5.7 -12 -5 0 25.8 6.7 12 5 0 5 3.4 12 5 0 9.8 4.9 14 -6 0 5.7 6 14 -6 0 5.9 4.9 -14 6 0 5 5.8 -14 6 0 13 4.9 13 -6 0 23.3 6.5 13 -6 0 17.7 5.9 13 -6 0 12.1 4.8 -13 6 0 8.7 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33.2 -4 7 0 904.61 32.2 -4 7 0 891.81 27.3 -4 7 0 896.81 31.8 3 -7 0 189.38 11.3 3 -7 0 184.38 12.1 3 -7 0 172.18 10.6 3 -7 0 187.98 12.7 -3 7 0 179.18 12.1 -3 7 0 180.38 6.9 -3 7 0 180.48 11.8 -3 7 0 175.18 10.5 -3 7 0 167.18 6.4 2 -7 0 1106.59 38.9 2 -7 0 1092.69 37.7 2 -7 0 1160.78 39.6 2 -7 0 1150.68 40.1 -2 7 0 1217.28 41.6 -2 7 0 1134.79 38.6 -2 7 0 1186.28 39.5 -2 7 0 1101.59 35.5 1 -7 0 170.18 11.2 1 -7 0 179.98 9.3 1 -7 0 176.78 12.5 1 -7 0 163.88 12 -1 7 0 186.68 8.8 -1 7 0 151.58 10.3 -1 7 0 169.58 10.3 0 -7 0 1026.5 36 0 -7 0 978.3 31.7 0 -7 0 999 35.3 0 -7 0 965.8 34.7 0 7 0 961.7 34.4 0 7 0 979.7 32.8 0 7 0 993.3 34.3 0 7 0 946.41 33.2 -1 -7 0 16.4 4.7 -1 -7 0 5.3 5.1 -1 -7 0 11.2 2.8 1 7 0 10.9 4.6 1 7 0 11.8 3.4 1 7 0 10.7 4.3 1 7 0 6.3 4.4 -2 -7 0 1507.55 50.79 -2 -7 0 1466.95 49.3 -2 -7 0 1502.95 49.1 2 7 0 1483.15 49.3 2 7 0 1399.36 49.3 2 7 0 1467.35 45.6 -3 -7 0 116.19 10.3 -3 -7 0 110.19 9.5 -3 -7 0 119.09 11.5 3 7 0 122.49 10 3 7 0 111.59 10.1 3 7 0 127.79 10.7 3 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0 44.1 6.8 -11 8 0 44.3 6 10 -8 0 146.69 13.5 10 -8 0 133.69 11.3 10 -8 0 126.89 11.5 10 -8 0 113.19 10.7 -10 8 0 138.59 8.9 -10 8 0 125.19 10.8 -10 8 0 129.49 10.5 9 -8 0 29.9 4.1 9 -8 0 21.7 6.9 9 -8 0 20.2 6.5 9 -8 0 22.1 6.4 -9 8 0 20.9 6.2 -9 8 0 18.4 6 -9 8 0 32 6.2 8 -8 0 293.67 16.3 8 -8 0 289.17 11.6 8 -8 0 301.07 16.1 8 -8 0 317.67 15.6 8 -8 0 309.37 16.7 -8 8 0 323.67 16.2 -8 8 0 302.37 14.9 -8 8 0 295.37 12.6 7 -8 0 7 4.9 7 -8 0 -5.2 4.4 7 -8 0 1 4.2 7 -8 0 9.7 4.7 -7 8 0 -2.2 3.5 -7 8 0 1.8 2.5 -7 8 0 -1.2 4.9 -7 8 0 -0.8 4.5 6 -8 0 1043.5 36.7 6 -8 0 993.6 36.3 6 -8 0 977 36 6 -8 0 1047.3 35.7 -6 8 0 974.3 34.6 -6 8 0 938.81 30.5 -6 8 0 982.8 35.3 -6 8 0 971.7 36.1 5 -8 0 69.19 8.1 5 -8 0 83.69 9.8 5 -8 0 81.49 8.8 5 -8 0 76.39 8.4 -5 8 0 82.19 10.2 -5 8 0 71.19 8 -5 8 0 81.49 8.1 -5 8 0 71.19 3.5 4 -8 0 1074.79 37.8 4 -8 0 1075.79 38.1 4 -8 0 1172.88 38.7 4 -8 0 1088.59 38.9 -4 8 0 1082.59 37.8 -4 8 0 1058.19 38.7 3 -8 0 430.96 19 3 -8 0 401.56 18.1 3 -8 0 432.86 19.6 3 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528.35 23.8 -8 5 2 587.34 24.9 7 -5 -2 4 5.2 7 -5 -2 6.1 4.8 7 -5 -2 10.1 4.1 7 -5 -2 4.8 5 7 -5 -2 11.5 5.3 -7 5 2 10.9 5 -7 5 2 6.6 5.2 -7 5 2 9.6 4.5 -7 5 2 9.4 5 6 -5 -2 595.54 22.1 6 -5 -2 640.74 25.6 6 -5 -2 615.94 25.9 6 -5 -2 662.73 25.2 6 -5 -2 606.24 25.3 -6 5 2 631.34 24.6 -6 5 2 603.84 25 -6 5 2 590.54 26.3 -6 5 2 610.44 22.6 -6 5 2 660.83 25.7 5 -5 -2 110.89 9.6 5 -5 -2 102.09 8.7 5 -5 -2 151.38 12.2 5 -5 -2 117.49 10.8 5 -5 -2 101.49 6.6 -5 5 2 114.19 10.1 -5 5 2 113.19 7.2 -5 5 2 116.29 10.5 -5 5 2 105.59 8.7 4 -5 -2 1451.65 47.8 4 -5 -2 1455.25 48.4 4 -5 -2 1461.95 48.1 4 -5 -2 1400.36 48 -4 5 2 1470.55 49.3 -4 5 2 1435.06 47.8 -4 5 2 1450.85 48.4 -4 5 2 1465.65 44.8 -4 5 2 1363.16 47.3 3 -5 -2 1343.57 45.3 3 -5 -2 1354.86 45.1 3 -5 -2 1293.67 45 3 -5 -2 1425.26 48 -3 5 2 1352.16 45.8 -3 5 2 1349.16 44.9 -3 5 2 1287.47 44.5 -3 5 2 1391.26 45.9 -3 5 2 1362.56 41.8 2 -5 -2 2152.58 68.69 2 -5 -2 2333.77 72.29 2 -5 -2 2163.58 68.49 2 -5 -2 2134.09 69.09 -2 5 2 2265.37 69.39 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1012.1 36.5 5 5 2 992.5 33.6 -6 -5 -2 379.46 19.4 -6 -5 -2 369.06 19.7 -6 -5 -2 334.67 18.5 6 5 2 386.96 19.7 6 5 2 363.96 15.9 6 5 2 346.57 18.5 6 5 2 413.16 20.1 -7 -5 -2 268.37 16.2 -7 -5 -2 260.87 15.9 -7 -5 -2 211.58 13.9 -7 -5 -2 259.97 15.7 7 5 2 245.78 15.3 7 5 2 236.68 17.4 7 5 2 248.18 12.7 -8 -5 -2 329.87 18.8 -8 -5 -2 351.26 18.7 8 5 2 378.46 19.3 8 5 2 333.37 18.9 8 5 2 355.26 18.6 8 5 2 318.37 15.1 -9 -5 -2 13.4 6.4 -9 -5 -2 15.9 6.3 9 5 2 18.5 6.5 9 5 2 12.8 4.4 -10 -5 -2 93.69 11 -10 -5 -2 111.59 11.9 10 5 2 86.49 7.5 10 5 2 87.79 10.1 -11 -5 -2 10.1 8.9 -11 -5 -2 13 6.5 11 5 2 2.7 4.5 11 5 2 0.2 3.1 11 5 2 5.7 6 14 -6 -2 38.6 7.8 14 -6 -2 33.1 6.8 -14 6 2 34.3 6.6 -14 6 2 27.5 6.7 13 -6 -2 -5.6 4.6 13 -6 -2 -8.8 4.7 -13 6 2 2.6 4.3 -13 6 2 5.5 5.7 12 -6 -2 80.89 9.4 12 -6 -2 88.89 9.8 12 -6 -2 95.89 11.2 -12 6 2 68.59 8 -12 6 2 82.39 10 11 -6 -2 70.29 9.3 11 -6 -2 73.29 10 11 -6 -2 87.99 8.5 -11 6 2 73.69 8.6 -11 6 2 67.59 9.4 -11 6 2 70.99 8.7 10 -6 -2 188.58 11 10 -6 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38.5 -5 6 2 1092.59 38.2 4 -6 -2 320.57 15.6 4 -6 -2 356.96 16.5 4 -6 -2 312.07 15.8 4 -6 -2 324.97 15.9 -4 6 2 310.97 12.3 -4 6 2 275.57 17.3 -4 6 2 307.17 15.3 -4 6 2 313.97 16.5 -4 6 2 346.87 16.5 3 -6 -2 2007.5 66.39 3 -6 -2 2055.39 65.79 3 -6 -2 2100.49 65.99 3 -6 -2 2085.09 65.69 -3 6 2 1988.3 65.49 -3 6 2 2071.89 62.09 -3 6 2 2036.4 65.69 -3 6 2 2071.79 66.69 -3 6 2 2146.19 66.39 2 -6 -2 943.91 33.3 2 -6 -2 951.6 33.4 2 -6 -2 949.21 33.5 2 -6 -2 909.81 32.2 -2 6 2 918.01 33.3 -2 6 2 943.61 33.3 -2 6 2 912.01 32.7 -2 6 2 896.01 32.8 1 -6 -2 761.92 28.5 1 -6 -2 789.02 28.3 1 -6 -2 761.02 28.1 1 -6 -2 758.52 26.7 -1 6 2 768.92 27.5 -1 6 2 694.83 25.6 -1 6 2 749.82 28.3 -1 6 2 719.53 27.7 0 -6 -2 1689.33 55.19 0 -6 -2 1629.54 52.89 0 -6 -2 1711.03 56.09 0 6 2 1695.03 53.89 0 6 2 1659.13 53.79 0 6 2 1810.92 55.89 0 6 2 1654.03 55.29 -1 -6 -2 37.6 4.7 -1 -6 -2 29.7 6.6 -1 -6 -2 38.7 7.1 1 6 2 43.8 5.5 1 6 2 50.89 6.8 1 6 2 19.2 5.6 -2 -6 -2 389.36 15.4 -2 -6 -2 388.46 19 -2 -6 -2 404.96 18.3 2 6 2 395.26 18 2 6 2 400.46 18.8 2 6 2 401.26 15.9 2 6 2 367.46 18.1 -3 -6 -2 10.9 6.5 -3 -6 -2 11 5.3 3 6 2 8.1 5.2 3 6 2 3.2 5.4 3 6 2 12.2 3.8 3 6 2 7.8 5.1 -4 -6 -2 144.49 11.4 -4 -6 -2 142.69 12.2 4 6 2 152.88 11.5 4 6 2 129.69 8.4 4 6 2 119.89 11.4 4 6 2 136.99 10.9 -5 -6 -2 7.5 4.5 -5 -6 -2 0.3 5.2 -5 -6 -2 2.1 5.3 5 6 2 -2.2 4.5 5 6 2 -2.3 4.8 5 6 2 1.5 4.5 -6 -6 -2 88.49 11.6 -6 -6 -2 87.19 9.6 -6 -6 -2 90.19 10.7 6 6 2 70.39 7.1 6 6 2 72.69 9.5 6 6 2 72.09 9.8 6 6 2 78.79 10.2 -7 -6 -2 0.9 6.2 -7 -6 -2 10.9 5.8 -7 -6 -2 7.6 5.8 -7 -6 -2 6.9 5.7 7 6 2 11.2 7 7 6 2 5.2 3.3 7 6 2 6.9 5 -8 -6 -2 6.2 6.1 -8 -6 -2 5.4 5.4 8 6 2 -0.2 3 8 6 2 -1.2 5.3 -9 -6 -2 4.1 5.9 -9 -6 -2 6.5 5.7 9 6 2 2.4 2.9 9 6 2 5 5.3 -10 -6 -2 -6.3 5.3 -10 -6 -2 5.5 5.6 10 6 2 2.9 5.4 10 6 2 -3.8 2.9 -11 -6 -2 0.3 5 -11 -6 -2 -3.9 5.1 11 6 2 -5.6 3.1 14 -7 -2 -4.5 4.5 14 -7 -2 -0.9 4.5 -14 7 2 -4.1 3.3 -14 7 2 7.7 6 13 -7 -2 -7.1 3.7 13 -7 -2 3.6 4.7 13 -7 -2 -0.8 5.3 -13 7 2 13.3 5.8 -13 7 2 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542.95 20.2 -6 7 -4 533.05 19.4 6 -7 4 572.14 24.3 6 -7 4 570.34 21.6 6 -7 4 528.45 22 6 -7 4 548.95 17.3 6 -7 4 566.04 23.4 -7 7 -4 45.5 5.4 -7 7 -4 49.9 8.2 -7 7 -4 51.09 6.4 7 -7 4 38.9 6.6 7 -7 4 57.29 8.1 7 -7 4 47.3 6.4 7 -7 4 35.6 7.2 7 -7 4 52.09 4.4 -8 7 -4 232.28 14.7 -8 7 -4 255.77 13.2 -8 7 -4 252.27 12.2 8 -7 4 233.68 14 8 -7 4 284.77 13.8 8 -7 4 262.47 10.9 8 -7 4 264.27 14.9 8 -7 4 247.18 15.9 -9 7 -4 9 4.3 -9 7 -4 6.6 5 -9 7 -4 5.5 5.5 9 -7 4 4.7 5.2 9 -7 4 8.8 4.9 9 -7 4 3.7 4.9 9 -7 4 5.9 3.2 9 -7 4 13.9 5.2 -10 7 -4 81.89 8.4 -10 7 -4 86.89 10.5 -10 7 -4 80.59 7.8 10 -7 4 78.99 6.6 10 -7 4 90.09 10.4 10 -7 4 60.39 8.8 -11 7 -4 12.8 4.7 -11 7 -4 5.6 4.5 11 -7 4 7.1 4.8 11 -7 4 7.3 5.5 11 -7 4 5.9 3.7 -12 7 -4 17.1 5.3 12 -7 4 14.3 4.4 12 -7 4 16.1 5.9 12 -7 4 7 5.1 -13 7 -4 6.2 5.2 -13 7 -4 13.9 5 13 -7 4 10.1 5.6 13 -7 4 8 6.1 13 -7 4 -0.3 3.6 -14 7 -4 14.5 5.1 14 -7 4 18.2 6.1 14 -7 4 1.7 5 -11 -6 4 35.6 7.1 -11 -6 4 24.1 6.8 10 6 -4 22.5 5.3 10 6 -4 21.3 3.6 -10 -6 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1119.39 35 1 -6 5 349.07 13.4 1 -6 5 344.27 13.8 1 -6 5 351.46 13.9 1 -6 5 343.37 17 1 -6 5 352.76 13.1 2 -6 5 486.25 16 2 -6 5 482.05 17.4 2 -6 5 480.55 17.5 2 -6 5 513.95 20.9 -3 6 -5 1681.83 59.19 3 -6 5 1647.34 53.79 3 -6 5 1609.74 50.79 3 -6 5 1649.73 50.49 3 -6 5 1597.84 48.1 -4 6 -5 422.56 19.1 4 -6 5 428.06 14.3 4 -6 5 462.95 19.4 4 -6 5 433.96 17.2 4 -6 5 439.06 16.7 -5 6 -5 901.41 33 -5 6 -5 891.01 27.2 5 -6 5 899.11 32.4 5 -6 5 890.91 28.6 5 -6 5 972 33.3 5 -6 5 892.11 31.7 -6 6 -5 -3.7 2.6 -6 6 -5 0.5 2.4 -6 6 -5 -2.2 4.6 6 -6 5 0 4.4 6 -6 5 0.2 2.2 6 -6 5 -1.2 4.1 6 -6 5 -0.9 3.7 -7 6 -5 808.82 27.4 -7 6 -5 807.92 31.1 -7 6 -5 802.52 28.3 7 -6 5 886.91 30 7 -6 5 826.32 31 7 -6 5 801.02 30.8 7 -6 5 840.12 27.9 -8 6 -5 93.39 7.5 -8 6 -5 105.69 10.6 8 -6 5 87.19 7 8 -6 5 92.29 9.7 8 -6 5 92.89 10.2 8 -6 5 93.79 8.9 -9 6 -5 438.06 18.8 -9 6 -5 392.46 17.2 -9 6 -5 438.76 20.6 9 -6 5 474.05 20.6 9 -6 5 438.46 20.7 9 -6 5 457.95 19 9 -6 5 440.86 19.8 -10 6 -5 80.09 7.6 -10 6 -5 95.59 8.9 10 -6 5 73.89 10 10 -6 5 86.69 7.6 10 -6 5 96.49 9.6 10 -6 5 104.99 13.5 -11 6 -5 48 6.5 -11 6 -5 50.99 6.9 11 -6 5 53.79 7.8 11 -6 5 56.09 8.4 11 -6 5 50.49 6.4 -12 6 -5 38.7 8.8 -12 6 -5 23.7 5.8 12 -6 5 29.3 5.6 12 -6 5 28.3 6.1 12 -6 5 25.4 6.7 -13 6 -5 25.1 6.5 -13 6 -5 20 5.2 13 -6 5 7 4.4 13 -6 5 21.6 6 13 -6 5 24.3 6.4 -14 6 -5 15.7 5.1 14 -6 5 32 11.4 14 -6 5 19.6 6.7 11 5 -5 4.4 4.8 11 5 -5 7.9 3.4 -11 -5 5 12.1 6.8 -11 -5 5 14 7.8 10 5 -5 89.19 7.8 10 5 -5 108.89 12.7 10 5 -5 149.09 10.4 -10 -5 5 103.19 10 -10 -5 5 106.09 10.2 9 5 -5 2.2 2.5 9 5 -5 2.7 4.8 -9 -5 5 5.4 5.4 -9 -5 5 -5.8 3.8 8 5 -5 298.87 12.4 8 5 -5 307.67 17.3 8 5 -5 349.27 16.5 8 5 -5 324.17 16.3 -8 -5 5 352.06 18.3 -8 -5 5 293.27 16.5 -8 -5 5 331.57 17.4 7 5 -5 98.29 5.9 7 5 -5 121.29 9.8 7 5 -5 102.19 9.9 -7 -5 5 123.69 11 -7 -5 5 130.79 11.4 -7 -5 5 136.79 14.8 -7 -5 5 112.89 9.4 6 5 -5 191.18 7.6 6 5 -5 190.18 13 6 5 -5 169.88 11.3 6 5 -5 190.98 11.5 -6 -5 5 188.18 12 -6 -5 5 220.08 14.1 -6 -5 5 190.68 13.2 5 5 -5 264.67 13 5 5 -5 239.08 12.9 5 5 -5 234.08 14.1 -5 -5 5 239.98 14.4 -5 -5 5 280.07 15.5 4 5 -5 171.88 9.5 4 5 -5 163.18 9.8 4 5 -5 179.88 11.7 -4 -5 5 178.68 12.7 -4 -5 5 165.38 11.6 -4 -5 5 185.58 12.4 3 5 -5 1571.54 48.7 3 5 -5 1575.34 51.99 3 5 -5 1549.05 49.2 -3 -5 5 1713.93 52.89 -3 -5 5 1578.34 52.19 -3 -5 5 1498.45 50.49 2 5 -5 152.88 6.3 2 5 -5 150.38 6.4 2 5 -5 164.98 9.8 -2 -5 5 142.09 9.6 -2 -5 5 156.28 9.1 -2 -5 5 170.08 11.9 1 5 -5 2148.09 66.59 -1 -5 5 2155.48 65.69 -1 -5 5 2230.58 67.19 -1 -5 5 2102.29 63.09 -1 -5 5 2171.88 62.89 -1 -5 5 2177.98 66.99 0 5 -5 74.79 5.5 0 -5 5 67.59 5.9 0 -5 5 70.19 5 0 -5 5 79.39 5.9 1 -5 5 1915.51 63.89 1 -5 5 2053.39 59.89 1 -5 5 1964.8 59.19 1 -5 5 1991.6 59.49 2 -5 5 436.66 14.9 2 -5 5 455.15 20.9 2 -5 5 442.86 15.4 2 -5 5 449.36 15.4 -3 5 -5 73.79 8.3 3 -5 5 53.79 5.1 3 -5 5 57.59 7 3 -5 5 64.09 4.9 -4 5 -5 376.86 17.1 4 -5 5 393.96 14.7 4 -5 5 355.86 13.5 4 -5 5 366.46 16.8 4 -5 5 366.06 15.3 -5 5 -5 47.2 4.2 -5 5 -5 42.2 3.7 5 -5 5 41 5.6 5 -5 5 45.5 6.8 5 -5 5 43 4.8 5 -5 5 53.39 6.8 -6 5 -5 416.46 19.2 -6 5 -5 424.06 15.9 -6 5 -5 411.46 16.7 6 -5 5 475.05 18.3 6 -5 5 428.66 17.1 6 -5 5 439.06 19.4 6 -5 5 470.45 19.6 -7 5 -5 4.5 4.8 -7 5 -5 9.6 3.8 -7 5 -5 10 4.5 7 -5 5 10.2 4.2 7 -5 5 5.8 4.9 7 -5 5 8.3 4.7 7 -5 5 9 5 -8 5 -5 160.08 11.7 -8 5 -5 169.48 10.9 -8 5 -5 135.39 9.2 8 -5 5 169.78 11.9 8 -5 5 186.38 11.7 8 -5 5 160.78 12.3 8 -5 5 165.18 10.2 -9 5 -5 19 5.7 -9 5 -5 24 5.3 -9 5 -5 20.7 6.6 9 -5 5 31.7 5.5 9 -5 5 16.4 6.1 9 -5 5 10.3 5.8 9 -5 5 24.1 6.4 -10 5 -5 8.8 4.4 -10 5 -5 23.2 6.7 -10 5 -5 9.3 5.4 10 -5 5 14.2 4.9 10 -5 5 17.3 6 10 -5 5 10.3 5.5 -11 5 -5 -2.5 4.1 -11 5 -5 1 4.5 -11 5 -5 -0.9 5.1 11 -5 5 2.3 5.2 11 -5 5 -3.6 5 11 -5 5 3.8 3.9 -12 5 -5 6.6 4.7 12 -5 5 2.5 5.2 12 -5 5 4.2 4.6 12 -5 5 6 4.5 -13 5 -5 13.8 5.2 13 -5 5 0.9 5.1 13 -5 5 2.4 5.5 -14 5 -5 4.5 4.6 14 -5 5 -2.6 4.9 14 -5 5 0.7 9.1 12 4 -5 9.6 4.2 -12 -4 5 4.7 5.7 -12 -4 5 8.3 5.2 11 4 -5 4.9 3.4 11 4 -5 1.1 4.7 -11 -4 5 0.8 6.1 -11 -4 5 5 5 10 4 -5 48.7 7.5 10 4 -5 33.9 7.3 10 4 -5 31.9 4.8 -10 -4 5 31.6 7.3 -10 -4 5 31.4 7.4 9 4 -5 3.2 4.9 9 4 -5 1 3.1 9 4 -5 -2.8 4.7 -9 -4 5 7.9 5.3 -9 -4 5 3.7 5 8 4 -5 16.7 5.9 8 4 -5 17.4 5.9 8 4 -5 17.1 4 -8 -4 5 12.6 5.3 -8 -4 5 1.3 5.3 -8 -4 5 18.1 9.7 -8 -4 5 27.2 7 7 4 -5 15.6 5.1 7 4 -5 -4 2.4 7 4 -5 2.9 5.2 7 4 -5 1.4 4.6 -7 -4 5 11 5.8 -7 -4 5 2.8 4.8 -7 -4 5 6.1 4.6 -7 -4 5 4.7 5.8 6 4 -5 11.6 5.8 6 4 -5 8.6 2.7 6 4 -5 11.4 5.1 6 4 -5 12.7 4.8 -6 -4 5 17.1 6.7 -6 -4 5 10.2 5.8 -6 -4 5 20 5.7 -6 -4 5 11.1 5.3 5 4 -5 20.8 5.6 5 4 -5 15.8 4.9 5 4 -5 22.9 3.1 -5 -4 5 24.9 5.7 -5 -4 5 19.7 5.7 -5 -4 5 28.5 6.9 4 4 -5 8 4.6 4 4 -5 9.1 2.1 4 4 -5 3.3 3.6 4 4 -5 9.2 3.8 -4 -4 5 9.5 5.1 -4 -4 5 1.7 4.4 3 4 -5 103.19 9.4 3 4 -5 75.49 5.9 3 4 -5 87.19 6 -3 -4 5 69.49 8 -3 -4 5 81.39 8.5 -3 -4 5 72.79 7.1 2 4 -5 140.69 9.3 2 4 -5 137.09 6.9 2 4 -5 139.39 5.5 -2 -4 5 125.89 7.9 -2 -4 5 138.59 9.1 -2 -4 5 134.89 5 -2 -4 5 128.69 9.2 1 4 -5 130.89 8.1 -1 -4 5 124.79 6.6 -1 -4 5 128.29 5.4 -1 -4 5 121.39 8 -1 -4 5 135.09 7.6 0 4 -5 1458.95 44.9 0 -4 5 1444.26 43.4 0 -4 5 1408.86 42.9 0 -4 5 1453.15 44 0 -4 5 1426.96 45 1 -4 5 34.4 3.9 1 -4 5 22.5 5.2 -2 4 -5 1835.92 56.69 2 -4 5 1837.72 53.99 2 -4 5 1798.82 56.69 2 -4 5 1670.63 55.09 2 -4 5 1794.52 52.79 -3 4 -5 7.4 4 3 -4 5 6.7 4 3 -4 5 10.1 2.7 3 -4 5 10.2 2.9 -4 4 -5 1478.45 48.8 4 -4 5 1462.05 48 4 -4 5 1523.55 46.8 4 -4 5 1477.15 46.8 4 -4 5 1545.65 49.2 -5 4 -5 580.84 19.9 -5 4 -5 571.04 23.1 -5 4 -5 621.14 20.8 5 -4 5 631.54 23.5 5 -4 5 610.04 22.1 5 -4 5 589.94 23.3 5 -4 5 581.04 21.6 -6 4 -5 412.76 20.7 -6 4 -5 431.66 17 -6 4 -5 389.66 15.7 6 -4 5 414.06 17.7 6 -4 5 403.06 18.9 6 -4 5 432.36 18.6 6 -4 5 407.86 17.3 -7 4 -5 752.22 29.8 -7 4 -5 809.42 27.7 -7 4 -5 791.02 28.9 7 -4 5 792.22 29 7 -4 5 847.62 30.4 7 -4 5 824.72 29.7 7 -4 5 758.22 30.7 -8 4 -5 9.7 5.2 -8 4 -5 7.8 4.8 8 -4 5 3.8 5 8 -4 5 -0.4 5.2 8 -4 5 8.5 5.4 8 -4 5 10.2 4.4 -9 4 -5 259.37 15.2 -9 4 -5 287.97 14.8 -9 4 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34.7 6.5 7 3 -5 38.4 7.2 7 3 -5 43.6 5.5 7 3 -5 44 7.3 -7 -3 5 39.1 7.9 -7 -3 5 31 6.9 -7 -3 5 33.8 7.5 -7 -3 5 36.5 6.8 6 3 -5 1127.49 40.2 6 3 -5 1092.89 37.3 6 3 -5 1052.99 38.2 6 3 -5 1044 34.6 -6 -3 5 1043.5 38.5 -6 -3 5 1030 39.4 -6 -3 5 973.4 37.1 -6 -3 5 1024 38.1 5 3 -5 270.57 14.6 5 3 -5 273.37 13.5 5 3 -5 261.27 14.4 5 3 -5 257.97 11.3 -5 -3 5 231.78 15.4 -5 -3 5 275.17 14.7 -5 -3 5 272.37 15 4 3 -5 3130.39 93.89 4 3 -5 3129.89 95.99 4 3 -5 3280.77 96.29 -4 -3 5 3120.49 97.29 -4 -3 5 3200.78 98.19 -4 -3 5 3143.89 100.39 3 3 -5 1930.61 60.09 3 3 -5 2002.6 62.89 3 3 -5 1983.5 58.89 3 3 -5 2000.4 60.19 -3 -3 5 1981.9 62.39 -3 -3 5 1903.81 63.79 -3 -3 5 1980.6 58.99 2 3 -5 3667.53 109.89 2 3 -5 3735.23 113.09 2 3 -5 3690.43 108.89 -2 -3 5 3802.52 109.79 -2 -3 5 3788.02 112.19 -2 -3 5 3743.63 111.59 -2 -3 5 3862.01 113.39 1 3 -5 3791.72 113.39 -1 -3 5 3789.52 110.99 -1 -3 5 3795.42 113.39 -1 -3 5 3800.62 111.19 -1 -3 5 3806.32 111.39 0 3 -5 664.03 23 0 -3 5 679.63 23.1 0 -3 5 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5.3 -12 -3 7 15.9 6.9 -12 -3 7 16.5 6 11 3 -7 0.9 3.4 11 3 -7 -4 4.3 -11 -3 7 -3.7 5.2 -11 -3 7 1.1 4.6 10 3 -7 114.59 9.9 10 3 -7 102.49 8.3 10 3 -7 102.89 9.8 -10 -3 7 124.99 11.6 -10 -3 7 94.69 10.6 9 3 -7 21 6 9 3 -7 14.9 5.2 9 3 -7 21.8 4.7 -9 -3 7 14.9 6 -9 -3 7 20 7 -9 -3 7 10 5.7 8 3 -7 112.99 8.4 8 3 -7 122.79 9.8 8 3 -7 144.69 10.4 -8 -3 7 141.59 12.1 -8 -3 7 109.89 11.9 7 3 -7 104.89 9.1 7 3 -7 136.49 11 7 3 -7 112.69 7.9 7 3 -7 133.09 10.1 -7 -3 7 117.89 10.3 -7 -3 7 134.79 12.2 -7 -3 7 119.39 10.4 -7 -3 7 149.39 11 6 3 -7 176.28 10.4 6 3 -7 191.68 11 6 3 -7 172.78 9.4 6 3 -7 183.48 12.5 -6 -3 7 167.68 11.8 -6 -3 7 188.08 11.9 -6 -3 7 171.78 12.6 -6 -3 7 170.38 11.9 5 3 -7 613.24 22.1 5 3 -7 562.44 24.1 5 3 -7 613.04 21.1 5 3 -7 603.44 21.7 -5 -3 7 594.44 20.9 -5 -3 7 562.14 23.9 -5 -3 7 564.94 24.5 -5 -3 7 605.64 24.1 -5 -3 7 574.04 25.4 4 3 -7 11.1 3.3 4 3 -7 12.7 3.2 4 3 -7 14.4 3.2 4 3 -7 16.7 5.1 -4 -3 7 19.3 5.6 -4 -3 7 17.9 4.9 -4 -3 7 13.4 3.2 -4 -3 7 13.2 4.5 3 3 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7.9 7 -7 9 69.49 7.6 7 -7 9 60.39 5.7 -8 7 -9 11 5.5 8 -7 9 13.1 3.5 8 -7 9 3.6 4.7 8 -7 9 10.7 4.3 8 -7 9 3.1 4.4 -9 7 -9 14.2 5.4 9 -7 9 6.1 4.2 9 -7 9 3.5 3.1 9 -7 9 1.5 4.1 9 -7 9 3.8 4.4 -10 7 -9 -1.8 4.9 10 -7 9 -3.4 3 10 -7 9 -1 3.7 10 -7 9 -3.4 6.8 10 -7 9 6.6 6.7 11 -7 9 10.3 5.2 11 -7 9 14.8 5.2 11 -7 9 9.1 4 12 -7 9 11.7 5 12 -7 9 9.5 4.3 12 -7 9 -1.4 4.2 13 -7 9 -3.8 4 13 -7 9 5.1 4.5 10 6 -9 18.1 5.2 10 6 -9 3.7 3.4 -10 -6 9 11.9 5.8 -10 -6 9 9.3 5 9 6 -9 3.3 3.4 9 6 -9 -2.5 4.1 -9 -6 9 -0.3 4.4 -9 -6 9 3.8 5.1 8 6 -9 3.2 3.2 -8 -6 9 -0.3 4 -8 -6 9 8.2 5.1 7 6 -9 7.2 3.2 7 6 -9 -2.2 2.4 -7 -6 9 6.5 4.9 -7 -6 9 -1.5 4.8 6 6 -9 32.8 2.9 6 6 -9 30.7 2.8 -6 -6 9 31.3 6.6 -6 -6 9 31.2 5.6 5 6 -9 31.5 6.7 -5 -6 9 27.3 6.2 -5 -6 9 26.3 6 -5 -6 9 26.7 5.3 4 6 -9 26.1 5.6 -4 -6 9 36.1 6.4 -4 -6 9 35.5 5.3 -4 -6 9 25.1 6 3 6 -9 57.99 7.2 -3 -6 9 56.99 6.2 -3 -6 9 59.89 7.2 -3 -6 9 62.79 7.8 2 6 -9 60.69 6.9 -2 -6 9 43 5.8 -2 -6 9 40.7 4.9 -2 -6 9 34.4 6 -2 -6 9 47.7 3.4 -1 -6 9 150.48 7.1 -1 -6 9 139.69 7.2 -1 -6 9 165.28 9.9 -1 -6 9 137.39 8 0 -6 9 5.8 3.5 0 -6 9 8.6 4.7 0 -6 9 1.6 1.8 0 -6 9 4 2.7 0 -6 9 2.1 2.3 1 -6 9 140.99 8.2 1 -6 9 129.59 8.1 1 -6 9 147.09 10.3 1 -6 9 120.19 5 2 -6 9 235.78 8.4 2 -6 9 261.77 12.5 2 -6 9 255.67 13.4 2 -6 9 255.37 11.2 3 -6 9 2.6 2.9 3 -6 9 2.6 1.9 3 -6 9 5.3 4.4 3 -6 9 9.7 2.4 4 -6 9 286.07 11.1 4 -6 9 281.47 11.8 4 -6 9 297.27 14.4 -5 6 -9 11.2 4.6 5 -6 9 0.9 3.1 5 -6 9 9.2 3.2 5 -6 9 2.2 4 5 -6 9 10.3 3.3 -6 6 -9 172.98 11.5 6 -6 9 192.08 9.8 6 -6 9 176.08 9.6 6 -6 9 176.18 10.7 6 -6 9 206.98 11.7 -7 6 -9 3.6 4.4 7 -6 9 2.5 4.3 7 -6 9 2.3 3.6 7 -6 9 -0.3 3.1 7 -6 9 2 3.9 -8 6 -9 111.49 10 8 -6 9 147.79 10.2 8 -6 9 125.49 9.5 8 -6 9 104.19 9.3 8 -6 9 129.19 8.8 -9 6 -9 13.5 5.5 9 -6 9 22.7 5.9 9 -6 9 27.4 6 9 -6 9 24.2 4.8 9 -6 9 21.2 5.4 -10 6 -9 36.7 3.6 -10 6 -9 56.09 11.1 -10 6 -9 39.1 3.4 10 -6 9 33.5 7.6 10 -6 9 25.2 6.4 10 -6 9 26.5 5.1 -11 6 -9 39.9 4.3 -11 6 -9 46.1 5 11 -6 9 47.9 6.2 11 -6 9 49.5 7.3 11 -6 9 40.7 6.6 -12 6 -9 9.2 3.6 12 -6 9 3.4 5 12 -6 9 6.9 4.2 12 -6 9 10.8 4.2 -13 6 -9 -0.5 3.6 -13 6 -9 9.5 3.9 13 -6 9 3.9 4.6 13 -6 9 8.2 5.6 11 5 -9 22.1 5.5 -11 -5 9 13.3 5.8 -11 -5 9 24.6 6.4 10 5 -9 1.6 4.7 10 5 -9 2.6 3.7 10 5 -9 -2.3 1.7 -10 -5 9 0.3 4.7 -10 -5 9 -3.1 4.7 9 5 -9 34.7 3.8 9 5 -9 32.6 5.9 9 5 -9 37.9 5.2 -9 -5 9 43.7 7.2 -9 -5 9 39.3 7.5 8 5 -9 45 4 8 5 -9 45.4 5.8 8 5 -9 46.6 5.3 -8 -5 9 43.9 6.9 -8 -5 9 58.39 8.1 -8 -5 9 53.89 7.9 7 5 -9 174.48 12.1 7 5 -9 166.68 9 7 5 -9 196.68 11.6 7 5 -9 168.38 7.4 -7 -5 9 179.18 12.7 -7 -5 9 162.68 11.4 -7 -5 9 165.98 12.3 -7 -5 9 203.78 16 6 5 -9 213.58 8.9 6 5 -9 219.28 9 6 5 -9 198.78 14.7 6 5 -9 195.48 8.3 -6 -5 9 243.38 13.8 -6 -5 9 211.78 14.5 -6 -5 9 209.78 12.1 -6 -5 9 193.18 13.1 5 5 -9 321.97 16.5 5 5 -9 304.37 11.5 -5 -5 9 343.67 16.8 -5 -5 9 321.47 15.3 -5 -5 9 346.17 16.3 4 5 -9 540.85 21.8 -4 -5 9 503.65 21.8 -4 -5 9 542.35 21.5 -4 -5 9 505.05 17.2 3 5 -9 67.59 7.5 -3 -5 9 64.49 7.9 -3 -5 9 66.69 4.5 2 5 -9 833.42 30.1 -2 -5 9 887.41 30.6 -2 -5 9 851.61 28.5 -2 -5 9 815.22 27.8 -2 -5 9 849.32 27.1 -1 -5 9 22.7 3.7 -1 -5 9 20.6 4.8 -1 -5 9 23.8 3.3 -1 -5 9 23.2 3.2 0 -5 9 1049.7 33.6 0 -5 9 1018.2 34.4 0 -5 9 1002.2 35.4 1 -5 9 186.78 10.1 1 -5 9 185.88 10.1 1 -5 9 169.78 10.8 2 -5 9 1317.87 42.3 2 -5 9 1287.17 43.6 2 -5 9 1356.86 43.7 3 -5 9 648.24 24.1 3 -5 9 663.13 20.2 3 -5 9 635.94 20.5 -4 5 -9 290.27 13.8 4 -5 9 298.77 11.3 4 -5 9 283.27 12 4 -5 9 279.07 13.6 -5 5 -9 465.75 19.2 5 -5 9 448.06 18.2 5 -5 9 461.85 18.9 5 -5 9 450.45 18 5 -5 9 475.95 17.3 -6 5 -9 50.29 6.7 6 -5 9 47.1 6.5 6 -5 9 51.79 6.4 6 -5 9 66.69 6.6 6 -5 9 55.19 7.1 -7 5 -9 129.99 9.8 7 -5 9 151.78 10.3 7 -5 9 151.78 9.7 7 -5 9 146.29 9.4 7 -5 9 158.18 10.8 -8 5 -9 12.5 4.7 8 -5 9 9.5 4.5 8 -5 9 4.7 4.6 8 -5 9 4.1 4.3 8 -5 9 1.1 3.4 -9 5 -9 195.18 12.4 -9 5 -9 178.78 7.7 -9 5 -9 192.08 8.2 9 -5 9 189.98 12 9 -5 9 190.08 11 9 -5 9 184.68 12.5 9 -5 9 178.68 11.9 -10 5 -9 1.5 4.9 -10 5 -9 3.7 3.1 -10 5 -9 -2.6 4.3 10 -5 9 7.9 4 10 -5 9 -0.1 4.9 10 -5 9 0.8 4.4 -11 5 -9 39.6 5.1 -11 5 -9 44.4 5.5 -11 5 -9 34.1 8.9 11 -5 9 51.69 7.1 11 -5 9 52.89 8.1 11 -5 9 54.39 7.7 -12 5 -9 5.6 3.9 -12 5 -9 -0.4 3.5 12 -5 9 4.9 5.4 12 -5 9 3 3.9 -13 5 -9 2.9 4 -13 5 -9 4.5 4.7 13 -5 9 3 4.3 11 4 -9 11.2 6.9 11 4 -9 5.6 3.5 11 4 -9 14 5.6 -11 -4 9 0.8 4.4 -11 -4 9 10.8 5.7 10 4 -9 61.49 5.9 10 4 -9 66.59 7.4 10 4 -9 59.19 7.1 -10 -4 9 71.39 9.2 -10 -4 9 67.49 9.6 9 4 -9 8 4.3 9 4 -9 4 4.2 9 4 -9 5.1 4.3 -9 -4 9 2.3 5 -9 -4 9 3.1 5.2 8 4 -9 207.48 11.1 8 4 -9 198.48 10.8 8 4 -9 164.88 9.3 -8 -4 9 222.18 15 -8 -4 9 217.18 13.7 7 4 -9 2.3 2.7 7 4 -9 7.3 5.6 7 4 -9 4.1 3.6 -7 -4 9 -3.4 4.8 -7 -4 9 2.7 5.4 -7 -4 9 4.8 4.8 6 4 -9 287.87 15.9 6 4 -9 296.67 11.9 6 4 -9 281.77 11.7 6 4 -9 278.97 11.8 -6 -4 9 280.87 16.7 -6 -4 9 289.27 15.6 -6 -4 9 272.27 14.5 -6 -4 9 292.27 15 5 4 -9 58.29 5.2 5 4 -9 51.79 3.5 5 4 -9 49 3.4 5 4 -9 44.7 7.3 -5 -4 9 57.29 7.2 -5 -4 9 48.8 4.9 -5 -4 9 60.59 8.2 -5 -4 9 59.59 8.6 -5 -4 9 58.79 7.6 4 4 -9 214.68 12.4 4 4 -9 192.98 9.1 -4 -4 9 214.08 12.6 -4 -4 9 190.48 11 -4 -4 9 194.48 9.1 -4 -4 9 203.08 11.3 3 4 -9 159.48 10.2 3 4 -9 140.39 7.5 -3 -4 9 135.59 9.7 -3 -4 9 127.69 7.2 -3 -4 9 125.09 8.2 -3 -4 9 129.89 8.4 2 4 -9 5.4 3.9 -2 -4 9 7.1 4.1 -2 -4 9 10.9 3.2 -2 -4 9 11.2 3.2 -1 -4 9 115.39 7.2 -1 -4 9 103.09 5.1 -1 -4 9 92.09 5 -1 -4 9 114.39 8.4 0 -4 9 67.99 6.5 0 -4 9 88.79 7.3 1 -4 9 215.68 11.1 1 -4 9 208.58 12.8 2 -4 9 94.79 7.4 2 -4 9 95.39 7.6 2 -4 9 107.69 8.6 3 -4 9 113.29 7.8 3 -4 9 116.89 9.7 3 -4 9 99.99 5.3 3 -4 9 112.79 5.3 -4 4 -9 5.3 3.6 4 -4 9 7.9 3.1 4 -4 9 19 6.9 4 -4 9 9.6 3.1 -5 4 -9 -0.2 3.5 5 -4 9 0.4 3.4 5 -4 9 6.1 3.8 5 -4 9 2.8 3.1 5 -4 9 4.1 3.7 -6 4 -9 5.2 4.7 6 -4 9 10.3 4.1 6 -4 9 6.2 3.8 6 -4 9 4.3 3.8 6 -4 9 8.3 4.7 -7 4 -9 -0.6 4.1 7 -4 9 6.2 4.7 7 -4 9 2.7 4 7 -4 9 -3.3 3.8 7 -4 9 -1.9 4.3 -8 4 -9 16.1 5.4 -8 4 -9 9.6 2.7 -8 4 -9 12.6 3 8 -4 9 12.9 4.8 8 -4 9 8.8 4.3 8 -4 9 12.4 5.4 8 -4 9 17 5.4 -9 4 -9 59.09 5.6 -9 4 -9 72.99 8.9 -9 4 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45.1 7.3 6 3 -9 51.89 5.5 -6 -3 9 55.09 8 -6 -3 9 73.99 10.1 -6 -3 9 55.39 7.5 -6 -3 9 62.79 8.4 5 3 -9 203.38 8.7 5 3 -9 193.68 9.9 5 3 -9 199.68 8.4 5 3 -9 168.38 11.7 -5 -3 9 175.58 11.1 -5 -3 9 202.28 9.9 -5 -3 9 190.68 11.6 -5 -3 9 173.18 12.7 -5 -3 9 200.28 12.4 4 3 -9 145.49 10.3 4 3 -9 136.19 8.1 -4 -3 9 145.69 8.1 -4 -3 9 144.09 10.4 -4 -3 9 123.09 8.8 -4 -3 9 133.79 9.3 -4 -3 9 131.59 11.2 3 3 -9 258.77 13.8 3 3 -9 276.57 12.1 -3 -3 9 286.87 12.3 -3 -3 9 244.58 13.5 -3 -3 9 253.87 11.6 -3 -3 9 261.07 12.1 2 3 -9 262.47 12.1 2 3 -9 269.97 13.6 -2 -3 9 259.87 11.1 -2 -3 9 264.07 11 -2 -3 9 264.87 11.9 -2 -3 9 273.47 13.7 1 3 -9 119.89 8.3 -1 -3 9 134.79 9.1 -1 -3 9 133.79 8.2 -1 -3 9 118.49 5.9 -1 -3 9 122.99 5.7 0 -3 9 1949.6 60.59 0 -3 9 1903.21 60.79 1 -3 9 91.99 6.8 1 -3 9 87.59 7.8 1 -3 9 96.09 8.1 2 -3 9 1610.84 49.2 2 -3 9 1688.63 54.19 2 -3 9 1641.04 51.19 2 -3 9 1678.53 48.9 -3 3 -9 50.49 5.2 3 -3 9 43.2 4.3 3 -3 9 42 7.2 3 -3 9 46.7 5.1 3 -3 9 45.9 4.4 -4 3 -9 1039.7 34.1 4 -3 9 976.7 33.9 4 -3 9 1095.19 34.3 4 -3 9 1035.2 34 -5 3 -9 144.79 8.7 5 -3 9 147.09 9.3 5 -3 9 137.79 9.8 5 -3 9 145.69 9 -6 3 -9 251.37 8.5 -6 3 -9 251.67 12.4 6 -3 9 258.57 13.5 6 -3 9 245.78 12.5 6 -3 9 261.37 13.6 6 -3 9 264.57 15.4 -7 3 -9 314.97 12.2 -7 3 -9 295.77 11.8 -7 3 -9 302.57 14.5 7 -3 9 314.77 15.5 7 -3 9 274.87 15.4 7 -3 9 313.17 14.8 7 -3 9 329.97 15.8 -8 3 -9 0.6 4.1 -8 3 -9 5.7 3.1 -8 3 -9 0.9 3.3 8 -3 9 1.1 3.9 8 -3 9 -4.9 4.5 8 -3 9 3.7 5 8 -3 9 6.6 4.6 -9 3 -9 217.38 13 -9 3 -9 248.48 12.1 -9 3 -9 250.97 15.4 9 -3 9 251.17 14.1 9 -3 9 258.77 13.7 9 -3 9 209.78 14.2 -10 3 -9 1.4 3.6 -10 3 -9 1.8 4.4 -10 3 -9 5 4.5 10 -3 9 6.9 5.7 10 -3 9 2.6 4.3 -11 3 -9 98.89 8.6 -11 3 -9 110.29 9 -11 3 -9 102.99 10 11 -3 9 108.79 9.8 11 -3 9 97.39 9.4 -12 3 -9 6.1 4.3 12 -3 9 9.1 4.9 12 -3 9 5.1 4.8 -13 3 -9 19.4 5.3 13 -3 9 17.6 7.5 12 2 -9 16.2 4.9 12 2 -9 15.1 5.3 -12 -2 9 13.9 5.6 -12 -2 9 10.1 8.9 11 2 -9 18.9 6 11 2 -9 32.3 5.5 11 2 -9 30.3 6.7 -11 -2 9 23.3 6.4 -11 -2 9 14.9 5.6 10 2 -9 52.09 7.5 10 2 -9 65.69 7 10 2 -9 48.7 7.1 -10 -2 9 48.7 8.4 -10 -2 9 49.3 8.2 9 2 -9 90.09 8.5 9 2 -9 81.29 8 9 2 -9 80.89 8.5 -9 -2 9 64.09 8.3 -9 -2 9 98.79 10.6 -9 -2 9 91.19 10.4 8 2 -9 463.55 18.7 8 2 -9 420.46 20.3 8 2 -9 410.46 18 8 2 -9 430.56 18.1 -8 -2 9 380.26 20.5 -8 -2 9 435.96 20.3 -8 -2 9 433.96 21.1 -8 -2 9 425.06 20.2 7 2 -9 35.1 6.1 7 2 -9 23.5 4.8 7 2 -9 37.6 8.4 -7 -2 9 26 6.8 -7 -2 9 35.2 7.1 -7 -2 9 24.6 5.2 -7 -2 9 49.1 7.8 -7 -2 9 25.5 6.2 6 2 -9 771.62 26.9 6 2 -9 703.23 25.8 6 2 -9 754.82 29.1 6 2 -9 787.52 27.2 -6 -2 9 787.32 29.4 -6 -2 9 733.43 28.4 -6 -2 9 754.22 30 -6 -2 9 713.33 26.5 -6 -2 9 722.03 28.1 5 2 -9 -0.9 2.6 5 2 -9 6.6 3.5 5 2 -9 -2 4 5 2 -9 2.1 3 -5 -2 9 9.1 4.7 -5 -2 9 2.6 3.2 -5 -2 9 -1.5 4.4 -5 -2 9 -6.1 3.6 -5 -2 9 -2.7 4.2 4 2 -9 697.93 27.3 4 2 -9 695.73 22.6 4 2 -9 705.03 25.7 4 2 -9 680.23 22.8 -4 -2 9 730.03 26.2 -4 -2 9 795.72 30.7 -4 -2 9 712.33 27.4 -4 -2 9 745.23 26.4 -4 -2 9 728.53 25.7 3 2 -9 196.78 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52.09 7.1 7 -2 -9 51.09 7.6 7 -2 -9 50.89 7.2 7 -2 -9 49.4 7.8 7 -2 -9 39.1 7.7 -7 2 9 49.99 7.4 -7 2 9 36.4 7.1 -7 2 9 44.2 7.7 -7 2 9 55.19 8.3 -7 2 9 49.9 7.5 6 -2 -9 25.7 7 6 -2 -9 35.8 6.5 6 -2 -9 24 5.5 6 -2 -9 40.5 6.8 6 -2 -9 42.4 7 -6 2 9 23.7 6 -6 2 9 39.6 6.7 -6 2 9 43.2 7.6 -6 2 9 41.3 6.9 -6 2 9 38.7 6.6 5 -2 -9 552.74 23.7 5 -2 -9 558.04 22 5 -2 -9 567.24 23.8 -5 2 9 570.04 23.1 -5 2 9 564.34 23.1 -5 2 9 539.55 21.9 -5 2 9 578.94 23.4 -5 2 9 544.05 22.7 4 -2 -9 576.74 22.8 4 -2 -9 570.74 21.3 4 -2 -9 539.55 22.9 4 -2 -9 531.35 21.2 -4 2 9 540.95 22.3 -4 2 9 513.85 21.7 -4 2 9 542.85 22.5 -4 2 9 573.14 23.1 -4 2 9 516.45 20.5 3 -2 -9 79.59 9.1 3 -2 -9 68.59 6.7 3 -2 -9 59.79 6.7 3 -2 -9 85.09 8 -3 2 9 57.49 7.8 -3 2 9 61.59 5.8 -3 2 9 61.89 7.7 -3 2 9 73.09 7.9 -3 2 9 63.69 7.3 2 -2 -9 1959.3 60.89 2 -2 -9 1900.41 63.09 2 -2 -9 1913.81 60.19 2 -2 -9 1886.21 60.79 -2 2 9 1994.3 61.99 -2 2 9 1966.3 63.39 -2 2 9 1989 62.39 -2 2 9 1959.1 58.79 -2 2 9 1973 62.69 1 -2 -9 55.29 7.5 1 -2 -9 37.2 5.4 1 -2 -9 42.2 4 1 -2 -9 62.89 6.4 -1 2 9 31.4 3 -1 2 9 29.8 5.6 -1 2 9 36.5 6.6 -1 2 9 29.7 5.9 0 -2 -9 2053.09 68.29 0 -2 -9 2139.39 65.89 0 -2 -9 2130.49 66.29 0 2 9 2186.78 68.89 0 2 9 2155.38 67.29 0 2 9 2107.09 66.99 -1 -2 -9 28 5.2 -1 -2 -9 35.9 6.8 -1 -2 -9 22.7 5.2 1 2 9 23.9 5.2 1 2 9 32.5 6.7 1 2 9 28.1 5.3 -2 -2 -9 1278.57 38.5 -2 -2 -9 1302.87 43.5 -2 -2 -9 1289.87 45.1 -2 -2 -9 1348.86 45.1 2 2 9 1344.77 45.6 2 2 9 1313.97 44.3 -3 -2 -9 411.26 15 -3 -2 -9 437.56 18.2 3 2 9 433.06 19.1 3 2 9 432.56 19.2 3 2 9 449.56 20.1 -4 -2 -9 424.66 18.2 -4 -2 -9 406.06 15.7 -4 -2 -9 402.66 18.2 4 2 9 430.26 19.7 4 2 9 396.56 19.1 4 2 9 435.06 19.8 4 2 9 386.26 18.6 -5 -2 -9 636.54 25.3 -5 -2 -9 633.04 23.4 -5 -2 -9 669.13 25.5 5 2 9 652.13 26.4 5 2 9 623.04 26.4 5 2 9 643.64 26.4 5 2 9 614.94 25.9 -6 -2 -9 59.59 8 -6 -2 -9 59.59 7.7 -6 -2 -9 64.19 7.2 6 2 9 63.99 8.9 6 2 9 54.89 8.3 6 2 9 62.59 8.9 6 2 9 65.39 9.1 -7 -2 -9 389.16 17.4 -7 -2 -9 393.66 18.7 -7 -2 -9 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3.4 4.8 -2 0 20 3.5 3.9 -2 0 20 0.3 3.9 -1 0 20 74.69 9.1 -1 0 20 80.59 10.6 -1 0 20 86.99 8.3 -1 0 20 69.69 8.9 0 0 20 40.2 6.6 0 0 20 36.5 6.9 0 0 20 43.1 7.5 0 0 20 39.2 6.5 1 0 20 55.79 6.4 1 0 20 58.19 7.7 1 0 20 49.3 8 2 0 20 51.79 6.3 2 0 20 59.79 8 2 0 20 57.09 7.8 2 0 20 53.19 6.4 3 0 20 22.5 5 4 0 20 22.7 5 4 0 20 35.5 6.7 5 0 20 6.4 5.1 5 0 20 7.1 4.4 -6 1 20 9.4 4.6 -5 1 20 12 2.6 -5 1 20 11 5.3 -5 1 20 14 5 -5 1 20 10.5 5.1 -4 1 20 40.8 6.9 -4 1 20 32.3 6.3 -4 1 20 17.2 4.9 -3 1 20 9.2 8.6 -3 1 20 9.5 4.8 -3 1 20 -1 4.1 -2 1 20 43 6.1 -2 1 20 42.5 7.1 -2 1 20 39.8 6.9 -1 1 20 5.8 3.7 -1 1 20 0.7 4.6 -1 1 20 3.7 4.2 0 1 20 41.1 7.4 0 1 20 39 7.3 0 1 20 32.9 5.5 1 1 20 -1.9 4.9 1 1 20 1.8 3.8 1 1 20 2.2 4.7 2 1 20 21.6 8.1 2 1 20 26.1 5.2 3 1 20 4.2 4.1 3 1 20 -0.1 4.5 4 1 20 2.3 4.2 4 1 20 -0.7 5.1 -5 2 20 -7.1 3.9 -5 2 20 6.8 5.4 -5 2 20 -2.5 4.7 -5 2 20 3.8 1.9 -4 2 20 -3.2 4.4 -4 2 20 7.2 4.7 -4 2 20 1.8 4.1 -3 2 20 11 5.4 -3 2 20 16.3 4.9 -3 2 20 13.5 7.4 -2 2 20 1.4 4.1 -2 2 20 3.7 4.8 -1 2 20 10.2 5.7 -1 2 20 25 5.4 -1 2 20 12.2 5.2 0 2 20 -2 4 0 2 20 -0.9 4.2 1 2 20 22.6 9.2 1 2 20 28.3 5.4 2 2 20 4.3 4.3 2 2 20 -3.7 3.8 3 2 20 7.7 4.7 3 2 20 6.9 5.1 -5 3 20 41.8 6.9 -5 3 20 37.3 6.4 -5 3 20 46.1 7.8 -4 3 20 5.9 5.1 -4 3 20 5 5.2 -4 3 20 12.7 5.1 -3 3 20 11.9 5.3 -3 3 20 19.3 5.7 -2 3 20 60.09 8.1 -2 3 20 50.89 7.4 -1 3 20 7.5 5.2 -1 3 20 8.3 5 0 3 20 69.69 9 0 3 20 60.99 8.5 0 3 20 64.79 8.1 1 3 20 -3.9 4.4 1 3 20 1.6 4.5 2 3 20 39.5 6.5 2 3 20 38 7 -4 4 20 14.9 5.5 -4 4 20 6.9 5.4 -4 4 20 10 5 -3 4 20 -8 4.2 -3 4 20 3.2 4.4 -3 4 20 4.3 4.5 2 -4 -20 -2.7 1.4 -2 4 20 6.8 5.1 -2 4 20 -0.8 4.4 -2 4 20 2.2 3.9 -1 4 20 4 4.5 -1 4 20 -4.2 4.1 -1 4 20 -6.7 4.3 0 -4 -20 -2.2 1.9 0 4 20 -2.6 4.5 0 4 20 -7.8 3.6 0 4 20 -0.7 4.4 -1 -4 -20 -5.6 1.9 -1 -4 -20 -6 2.5 1 4 20 1.3 4.1 1 4 20 5.1 4.7 0 -5 21 -0.1 3.5 0 -5 21 -4.2 2.5 0 -5 21 -2.6 4 1 -5 21 1.8 4 1 -5 21 4.7 4.2 1 -5 21 2.1 1.5 1 -5 21 -1 2.4 2 -5 21 -2.4 2.4 -2 -4 21 5.8 4.1 -2 -4 21 8.3 3.4 -2 -4 21 10.5 2.6 -2 -4 21 10.9 8.5 -1 -4 21 -3.7 4.5 -1 -4 21 3.4 2 -1 -4 21 5.1 2.9 -1 -4 21 1.5 1.8 -1 -4 21 8.9 3.3 -1 -4 21 1.7 3.7 0 -4 21 21.5 5.7 0 -4 21 14.9 4.6 0 -4 21 15.5 3.5 0 -4 21 18.4 3.6 1 -4 21 10.9 4.8 1 -4 21 3.8 3.2 1 -4 21 10.9 5.1 1 -4 21 10.4 3.2 2 -4 21 14.9 3.4 2 -4 21 20.5 5.4 2 -4 21 15.4 5 2 -4 21 16.5 3.4 3 -4 21 29 6.3 3 -4 21 28.3 4.4 3 -4 21 25.3 6.2 3 -4 21 20.7 3.8 -3 -3 21 25.4 7.5 -2 -3 21 4.9 3.4 -2 -3 21 10 3.6 -2 -3 21 0 4.6 -2 -3 21 5.2 1.8 -2 -3 21 0.2 3.7 -1 -3 21 31.3 6.6 -1 -3 21 27.3 4.5 -1 -3 21 26.4 5.3 -1 -3 21 23.6 4.2 0 -3 21 5.3 3.8 0 -3 21 -1.8 2.9 0 -3 21 -3 4.4 0 -3 21 -4.9 2.9 1 -3 21 27.8 6.3 1 -3 21 27.4 6.1 1 -3 21 25.9 4.2 1 -3 21 29.7 4.5 2 -3 21 16.4 5.1 2 -3 21 12 5.3 2 -3 21 4.3 3.3 2 -3 21 11.2 3.4 3 -3 21 24.4 4.1 3 -3 21 15.7 5.5 3 -3 21 41.1 4.7 -3 -2 21 5.8 4.2 -3 -2 21 1.2 1.7 -3 -2 21 -2.3 1.5 -3 -2 21 10.4 3.8 -3 -2 21 -4.8 3.8 -2 -2 21 4.8 3.9 -2 -2 21 1.9 5.2 -2 -2 21 1.7 4.6 -1 -2 21 3.5 3.8 -1 -2 21 8.1 3.8 -1 -2 21 8.2 8.1 -1 -2 21 1.9 3.2 0 -2 21 6.1 5.3 0 -2 21 4.5 3.8 0 -2 21 4.9 4.4 0 -2 21 6.8 3.4 1 -2 21 1.7 4.4 1 -2 21 -2 3.3 1 -2 21 2.2 5 1 -2 21 8.6 3.4 2 -2 21 17 4.2 2 -2 21 11.1 5.4 2 -2 21 10.5 5.6 2 -2 21 6.2 3.2 3 -2 21 3.5 5 3 -2 21 3.9 3.6 3 -2 21 3.8 5.3 -4 -1 21 47 5.8 -3 -1 21 7.8 3.6 -3 -1 21 7.7 4.5 -3 -1 21 13.5 5.2 -3 -1 21 13.8 4.8 -2 -1 21 27.8 6.4 -2 -1 21 35.3 5.5 -2 -1 21 20.4 5.2 -1 -1 21 45.5 7 -1 -1 21 50.49 6.6 -1 -1 21 52.19 6.8 0 -1 21 9.8 4.9 0 -1 21 12.1 4.8 0 -1 21 13.8 4.2 1 -1 21 71.39 8.5 1 -1 21 66.89 6.5 1 -1 21 65.99 9.2 2 -1 21 -3.6 3.1 2 -1 21 1.4 7.8 2 -1 21 -0.6 4.9 2 -1 21 -3.7 4.3 3 -1 21 39.2 6.9 3 -1 21 46.8 5.7 3 -1 21 48.9 7.7 -4 0 21 -3.1 5.9 -4 0 21 -0.9 3.8 -4 0 21 0.6 3.7 -3 0 21 15.9 5.4 -3 0 21 10.8 3.9 -3 0 21 15.6 5.2 -2 0 21 4.7 5.1 -2 0 21 3.2 3.7 -2 0 21 -0.5 4.2 -1 0 21 6 3.7 -1 0 21 11.2 5.5 -1 0 21 13.8 5.1 0 0 21 6.1 3.6 0 0 21 13.6 5.9 0 0 21 16.7 5.6 1 0 21 -6.3 4.6 1 0 21 3 3.3 2 0 21 20.9 6 2 0 21 16.7 4.2 2 0 21 22.4 6.2 3 0 21 2.9 4.4 3 0 21 3.1 3.5 -3 1 21 2.2 4.7 -3 1 21 2 3.8 -2 1 21 20.2 4.9 -2 1 21 32.7 6.3 -1 1 21 5 4.2 -1 1 21 9.7 5.2 0 1 21 16.4 4.9 0 1 21 15.3 5.6 0 1 21 7.4 5.1 1 1 21 10 5.6 1 1 21 -3.5 4.8 1 1 21 6.6 4.1 2 1 21 0.4 4.2 2 1 21 -2.1 3.8 2 1 21 2.9 4.3 -3 2 21 24.2 6.2 -3 2 21 21.9 5.7 -3 2 21 33.9 6.8 -2 2 21 -1.8 4 -2 2 21 -7.7 3.9 -2 2 21 1.5 4.9 -1 2 21 65.09 8.1 -1 2 21 44.1 6.4 -1 2 21 43.2 7.3 0 2 21 7.4 4.3 0 2 21 4.8 4.9 0 2 21 7.2 4.4 1 2 21 33.1 5.7 1 2 21 31.1 6.5 1 2 21 33.2 6.3 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag P1 Au1 Cl1 173.10(4) . . ? P2 Au2 Cl2 176.15(6) . . ? C1 P1 Au1 115.04(12) . . ? C20 P1 Au1 115.02(13) . . ? C20 P1 C1 104.51(17) . . ? C26 P1 Au1 106.27(13) . . ? C26 P1 C1 106.30(18) . . ? C26 P1 C20 109.35(18) . . ? C19 P2 Au2 114.24(12) . . ? C32 P2 Au2 111.30(13) . . ? C32 P2 C19 106.26(17) . . ? C38 P2 Au2 112.90(14) . . ? C38 P2 C19 104.46(16) . . ? C38 P2 C32 107.10(18) . . ? C2 C1 P1 122.5(3) . . ? C6 C1 P1 119.1(3) . . ? C6 C1 C2 118.4(4) . . ? H2 C2 C1 119.6(3) . . ? C3 C2 C1 120.9(4) . . ? C3 C2 H2 119.6(3) . . ? H3 C3 C2 119.9(3) . . ? C4 C3 C2 120.2(4) . . ? C4 C3 H3 119.9(3) . . ? H4 C4 C3 120.0(3) . . ? C5 C4 C3 120.1(4) . . ? C5 C4 H4 120.0(3) . . ? H5 C5 C4 120.0(3) . . ? C6 C5 C4 119.9(4) . . ? C6 C5 H5 120.0(2) . . ? C5 C6 C1 120.5(4) . . ? N1 C6 C1 120.1(3) . . ? N1 C6 C5 119.4(4) . . ? C7 N1 C6 122.9(3) . . ? H1 N1 C6 117(3) . . ? H1 N1 C7 118(3) . . ? O1 C7 N1 123.6(4) . . ? C8 C7 N1 115.6(3) . . ? C8 C7 O1 120.8(4) . . ? C9 C8 C7 118.4(4) . . ? N2 C8 C7 118.3(3) . . ? N2 C8 C9 123.1(4) . . ? H9 C9 C8 120.8(2) . . ? C10 C9 C8 118.4(4) . . ? C10 C9 H9 120.8(3) . . ? H10 C10 C9 120.2(3) . . ? C11 C10 C9 119.5(4) . . ? C11 C10 H10 120.2(3) . . ? H11 C11 C10 120.7(3) . . ? C12 C11 C10 118.6(4) . . ? C12 C11 H11 120.7(2) . . ? N2 C12 C11 123.5(3) . . ? C13 C12 C11 118.8(3) . . ? C13 C12 N2 117.7(3) . . ? C12 N2 C8 116.8(3) . . ? O2 C13 C12 121.1(3) . . ? N3 C13 C12 114.6(3) . . ? N3 C13 O2 124.2(4) . . ? C14 N3 C13 124.4(3) . . ? H3a N3 C13 117(3) . . ? H3a N3 C14 119(3) . . ? C15 C14 N3 120.9(3) . . ? C19 C14 N3 118.9(3) . . ? C19 C14 C15 120.2(3) . . ? H15 C15 C14 119.6(2) . . ? C16 C15 C14 120.7(4) . . ? C16 C15 H15 119.6(2) . . ? H16 C16 C15 120.1(2) . . ? C17 C16 C15 119.8(4) . . ? C17 C16 H16 120.1(2) . . ? H17 C17 C16 119.9(2) . . ? C18 C17 C16 120.3(4) . . ? C18 C17 H17 119.9(2) . . ? H18 C18 C17 119.7(2) . . ? C19 C18 C17 120.7(4) . . ? C19 C18 H18 119.7(2) . . ? C14 C19 P2 120.1(3) . . ? C18 C19 P2 121.5(3) . . ? C18 C19 C14 118.3(3) . . ? C21 C20 P1 119.7(3) . . ? C25 C20 P1 121.0(3) . . ? C25 C20 C21 119.3(4) . . ? H21 C21 C20 119.4(2) . . ? C22 C21 C20 121.2(4) . . ? C22 C21 H21 119.4(3) . . ? H22 C22 C21 120.1(3) . . ? C23 C22 C21 119.7(5) . . ? C23 C22 H22 120.1(3) . . ? H23 C23 C22 120.1(3) . . ? C24 C23 C22 119.8(5) . . ? C24 C23 H23 120.1(3) . . ? H24 C24 C23 119.7(3) . . ? C25 C24 C23 120.6(5) . . ? C25 C24 H24 119.7(3) . . ? C24 C25 C20 119.2(5) . . ? H25 C25 C20 120.4(3) . . ? H25 C25 C24 120.4(3) . . ? C27 C26 P1 124.6(4) . . ? C31 C26 P1 118.1(3) . . ? C31 C26 C27 117.1(4) . . ? H27 C27 C26 119.9(3) . . ? C28 C27 C26 120.2(5) . . ? C28 C27 H27 119.9(3) . . ? H28 C28 C27 119.4(3) . . ? C29 C28 C27 121.3(5) . . ? C29 C28 H28 119.4(3) . . ? H29 C29 C28 119.9(3) . . ? C30 C29 C28 120.2(5) . . ? C30 C29 H29 119.9(3) . . ? H30 C30 C29 120.6(3) . . ? C31 C30 C29 118.7(5) . . ? C31 C30 H30 120.6(3) . . ? C30 C31 C26 122.5(5) . . ? H31 C31 C26 118.8(3) . . ? H31 C31 C30 118.8(3) . . ? C33 C32 P2 122.0(3) . . ? C37 C32 P2 119.1(3) . . ? C37 C32 C33 118.9(4) . . ? H33 C33 C32 119.6(2) . . ? C34 C33 C32 120.8(4) . . ? C34 C33 H33 119.6(3) . . ? H34 C34 C33 119.6(3) . . ? C35 C34 C33 120.8(5) . . ? C35 C34 H34 119.6(3) . . ? H35 C35 C34 120.3(3) . . ? C36 C35 C34 119.4(5) . . ? C36 C35 H35 120.3(3) . . ? H36 C36 C35 119.7(3) . . ? C37 C36 C35 120.7(5) . . ? C37 C36 H36 119.7(3) . . ? C36 C37 C32 119.4(5) . . ? H37 C37 C32 120.3(3) . . ? H37 C37 C36 120.3(3) . . ? C39 C38 P2 122.4(3) . . ? C43 C38 P2 118.5(3) . . ? C43 C38 C39 119.0(4) . . ? H39 C39 C38 119.9(3) . . ? C40 C39 C38 120.3(5) . . ? C40 C39 H39 119.9(3) . . ? H40 C40 C39 119.8(3) . . ? C41 C40 C39 120.4(5) . . ? C41 C40 H40 119.8(3) . . ? H41 C41 C40 119.7(3) . . ? C42 C41 C40 120.6(5) . . ? C42 C41 H41 119.7(3) . . ? H42 C42 C41 120.2(3) . . ? C43 C42 C41 119.5(5) . . ? C43 C42 H42 120.2(3) . . ? C42 C43 C38 120.2(5) . . ? H43 C43 C38 119.9(3) . . ? H43 C43 C42 119.9(3) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Au1 Cl1 2.2718(11) . ? Au1 P1 2.2307(10) . ? Au2 Cl2 2.2644(13) . ? Au2 P2 2.2266(11) . ? P1 C1 1.817(4) . ? P1 C20 1.821(4) . ? P1 C26 1.808(4) . ? P2 C19 1.824(3) . ? P2 C32 1.815(4) . ? P2 C38 1.814(4) . ? C1 C2 1.388(5) . ? C1 C6 1.400(5) . ? C2 H2 0.9300 . ? C2 C3 1.386(6) . ? C3 H3 0.9300 . ? C3 C4 1.373(6) . ? C4 H4 0.9300 . ? C4 C5 1.382(6) . ? C5 H5 0.9300 . ? C5 C6 1.390(5) . ? C6 N1 1.418(5) . ? N1 C7 1.345(5) . ? N1 H1 0.80(4) . ? C7 O1 1.216(4) . ? C7 C8 1.497(5) . ? C8 C9 1.377(5) . ? C8 N2 1.349(4) . ? C9 H9 0.9300 . ? C9 C10 1.375(6) . ? C10 H10 0.9300 . ? C10 C11 1.366(6) . ? C11 H11 0.9300 . ? C11 C12 1.377(5) . ? C12 N2 1.336(4) . ? C12 C13 1.497(5) . ? C13 O2 1.212(4) . ? C13 N3 1.348(5) . ? N3 C14 1.419(4) . ? N3 H3a 0.79(4) . ? C14 C15 1.373(5) . ? C14 C19 1.393(5) . ? C15 H15 0.9300 . ? C15 C16 1.377(5) . ? C16 H16 0.9300 . ? C16 C17 1.367(5) . ? C17 H17 0.9300 . ? C17 C18 1.375(5) . ? C18 H18 0.9300 . ? C18 C19 1.396(5) . ? C20 C21 1.372(5) . ? C20 C25 1.371(5) . ? C21 H21 0.9300 . ? C21 C22 1.377(5) . ? C22 H22 0.9300 . ? C22 C23 1.364(7) . ? C23 H23 0.9300 . ? C23 C24 1.365(7) . ? C24 H24 0.9300 . ? C24 C25 1.400(6) . ? C25 H25 0.9300 . ? C26 C27 1.350(6) . ? C26 C31 1.380(6) . ? C27 H27 0.9300 . ? C27 C28 1.398(7) . ? C28 H28 0.9300 . ? C28 C29 1.319(7) . ? C29 H29 0.9300 . ? C29 C30 1.363(7) . ? C30 H30 0.9300 . ? C30 C31 1.367(6) . ? C31 H31 0.9300 . ? C32 C33 1.379(5) . ? C32 C37 1.381(5) . ? C33 H33 0.9300 . ? C33 C34 1.371(6) . ? C34 H34 0.9300 . ? C34 C35 1.359(6) . ? C35 H35 0.9300 . ? C35 C36 1.369(7) . ? C36 H36 0.9300 . ? C36 C37 1.395(6) . ? C37 H37 0.9300 . ? C38 C39 1.372(5) . ? C38 C43 1.393(6) . ? C39 H39 0.9300 . ? C39 C40 1.378(6) . ? C40 H40 0.9300 . ? C40 C41 1.361(7) . ? C41 H41 0.9300 . ? C41 C42 1.367(7) . ? C42 H42 0.9300 . ? C42 C43 1.386(6) . ? C43 H43 0.9300 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A C16 H16 O2 0.9300 2.408(5) 3.277(5) 155.65(12) 2_656 C21 H21 Au1 0.9300 2.969(4) 3.542(4) 121.32(8) . C33 H33 Cl1 0.9300 2.839(4) 3.519(4) 130.89(9) 2_666 C36 H36 O1 0.9300 2.455(6) 3.385(6) 178.94(16) 2_665 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Au1 P1 C1 C2 121.3(3) . . . . ? Au1 P1 C1 C6 -60.2(2) . . . . ? Au1 P1 C20 C21 -0.3(2) . . . . ? Au1 P1 C20 C25 177.8(3) . . . . ? Au1 P1 C26 C27 128.7(4) . . . . ? Au1 P1 C26 C31 -47.5(3) . . . . ? Au2 P2 C19 C14 53.23(19) . . . . ? Au2 P2 C19 C18 -123.2(2) . . . . ? Au2 P2 C32 C33 -146.6(2) . . . . ? Au2 P2 C32 C37 32.3(2) . . . . ? Au2 P2 C38 C39 -158.1(3) . . . . ? Au2 P2 C38 C43 24.6(2) . . . . ? P1 C1 C2 C3 176.8(4) . . . . ? P1 C1 C6 C5 -179.1(3) . . . . ? P1 C1 C6 N1 -1.3(3) . . . . ? P1 C20 C21 C22 176.0(3) . . . . ? P1 C20 C25 C24 -177.5(4) . . . . ? P1 C26 C27 C28 -177.0(5) . . . . ? P1 C26 C31 C30 178.3(4) . . . . ? P2 C19 C14 N3 4.6(3) . . . . ? P2 C19 C14 C15 -174.1(3) . . . . ? P2 C19 C18 C17 173.9(3) . . . . ? P2 C32 C33 C34 179.7(3) . . . . ? P2 C32 C37 C36 178.9(3) . . . . ? P2 C38 C39 C40 -177.1(4) . . . . ? P2 C38 C43 C42 177.5(4) . . . . ? C1 P1 C20 C21 -127.5(3) . . . . ? C1 P1 C20 C25 50.7(3) . . . . ? C1 P1 C26 C27 -108.3(4) . . . . ? C1 P1 C26 C31 75.5(3) . . . . ? C1 C2 C3 C4 2.4(5) . . . . ? C1 C6 C5 C4 2.3(5) . . . . ? C1 C6 N1 C7 -121.5(4) . . . . ? C2 C1 P1 C20 -111.6(4) . . . . ? C2 C1 P1 C26 4.0(4) . . . . ? C2 C1 C6 C5 -0.6(4) . . . . ? C2 C1 C6 N1 177.2(4) . . . . ? C2 C3 C4 C5 -0.6(6) . . . . ? C3 C2 C1 C6 -1.7(5) . . . . ? C3 C4 C5 C6 -1.7(6) . . . . ? C4 C5 C6 N1 -175.5(4) . . . . ? C5 C6 N1 C7 56.3(4) . . . . ? C6 C1 P1 C20 66.9(3) . . . . ? C6 C1 P1 C26 -177.5(3) . . . . ? C6 N1 C7 O1 -11.5(4) . . . . ? C6 N1 C7 C8 164.5(4) . . . . ? N1 C7 C8 C9 -160.9(4) . . . . ? N1 C7 C8 N2 15.7(4) . . . . ? C7 C8 C9 C10 174.2(4) . . . . ? C7 C8 N2 C12 -175.7(3) . . . . ? O1 C7 C8 C9 15.2(5) . . . . ? O1 C7 C8 N2 -168.2(4) . . . . ? C8 C9 C10 C11 1.8(5) . . . . ? C8 N2 C12 C11 1.1(4) . . . . ? C8 N2 C12 C13 -177.5(3) . . . . ? C9 C8 N2 C12 0.7(5) . . . . ? C9 C10 C11 C12 -0.1(6) . . . . ? C10 C9 C8 N2 -2.2(5) . . . . ? C10 C11 C12 N2 -1.5(5) . . . . ? C10 C11 C12 C13 177.1(4) . . . . ? C11 C12 C13 O2 10.8(4) . . . . ? C11 C12 C13 N3 -167.4(4) . . . . ? C12 C13 N3 C14 172.2(3) . . . . ? N2 C12 C13 O2 -170.5(3) . . . . ? N2 C12 C13 N3 11.2(4) . . . . ? C13 N3 C14 C15 54.7(4) . . . . ? C13 N3 C14 C19 -124.0(4) . . . . ? O2 C13 N3 C14 -6.0(5) . . . . ? N3 C14 C15 C16 -179.2(3) . . . . ? N3 C14 C19 C18 -178.9(3) . . . . ? C14 C15 C16 C17 -1.4(4) . . . . ? C14 C19 P2 C32 -69.9(3) . . . . ? C14 C19 P2 C38 177.1(3) . . . . ? C14 C19 C18 C17 -2.6(4) . . . . ? C15 C14 C19 C18 2.4(4) . . . . ? C15 C16 C17 C18 1.3(4) . . . . ? C16 C15 C14 C19 -0.5(4) . . . . ? C16 C17 C18 C19 0.7(5) . . . . ? C18 C19 P2 C32 113.7(3) . . . . ? C18 C19 P2 C38 0.6(3) . . . . ? C19 P2 C32 C33 -21.7(2) . . . . ? C19 P2 C32 C37 157.2(3) . . . . ? C19 P2 C38 C39 77.2(3) . . . . ? C19 P2 C38 C43 -100.1(3) . . . . ? C20 P1 C26 C27 4.0(4) . . . . ? C20 P1 C26 C31 -172.2(3) . . . . ? C20 C21 C22 C23 1.3(5) . . . . ? C20 C25 C24 C23 1.7(5) . . . . ? C21 C20 P1 C26 119.1(3) . . . . ? C21 C20 C25 C24 0.7(5) . . . . ? C21 C22 C23 C24 1.1(5) . . . . ? C22 C21 C20 C25 -2.2(5) . . . . ? C22 C23 C24 C25 -2.6(6) . . . . ? C25 C20 P1 C26 -62.7(4) . . . . ? C26 C27 C28 C29 -0.1(7) . . . . ? C26 C31 C30 C29 -2.0(6) . . . . ? C27 C26 C31 C30 1.9(6) . . . . ? C27 C28 C29 C30 0.0(9) . . . . ? C28 C27 C26 C31 -0.9(7) . . . . ? C28 C29 C30 C31 1.0(7) . . . . ? C32 P2 C38 C39 -35.3(3) . . . . ? C32 P2 C38 C43 147.4(3) . . . . ? C32 C33 C34 C35 0.7(5) . . . . ? C32 C37 C36 C35 2.2(5) . . . . ? C33 C32 P2 C38 89.6(3) . . . . ? C33 C32 C37 C36 -2.2(4) . . . . ? C33 C34 C35 C36 -0.7(5) . . . . ? C34 C33 C32 C37 0.8(5) . . . . ? C34 C35 C36 C37 -0.7(6) . . . . ? C37 C32 P2 C38 -91.6(3) . . . . ? C38 C39 C40 C41 -0.4(5) . . . . ? C38 C43 C42 C41 -0.1(5) . . . . ? C39 C38 C43 C42 0.1(5) . . . . ? C39 C40 C41 C42 0.4(6) . . . . ? C40 C39 C38 C43 0.2(5) . . . . ? C40 C41 C42 C43 -0.1(6) . . . . ? loop_ _atom_site_anharm_gc_c_label _atom_site_anharm_gc_c_111 _atom_site_anharm_gc_c_112 _atom_site_anharm_gc_c_113 _atom_site_anharm_gc_c_122 _atom_site_anharm_gc_c_123 _atom_site_anharm_gc_c_133 _atom_site_anharm_gc_c_222 _atom_site_anharm_gc_c_223 _atom_site_anharm_gc_c_233 _atom_site_anharm_gc_c_333 Au1 0.00000010(11) -0.00000013(6) -0.00000021(4) -0.00000011(6) -0.00000012(2) -0.00000001(2) -0.00000035(10) -0.00000013(3) -0.00000012(2) -0.00000017(3) Au2 0.00000039(11) 0.00000053(6) -0.00000011(4) 0.00000079(6) -0.00000031(2) -0.00000002(2) -0.00000183(12) 0.00000083(4) -0.00000019(2) -0.00000004(3) loop_ _atom_site_anharm_gc_d_label _atom_site_anharm_gc_d_1111 _atom_site_anharm_gc_d_1112 _atom_site_anharm_gc_d_1113 _atom_site_anharm_gc_d_1122 _atom_site_anharm_gc_d_1123 _atom_site_anharm_gc_d_1133 _atom_site_anharm_gc_d_1222 _atom_site_anharm_gc_d_1223 _atom_site_anharm_gc_d_1233 _atom_site_anharm_gc_d_1333 _atom_site_anharm_gc_d_2222 _atom_site_anharm_gc_d_2223 _atom_site_anharm_gc_d_2233 _atom_site_anharm_gc_d_2333 _atom_site_anharm_gc_d_3333 Au1 0.000000437(14) 0.000000122(7) 0.000000017(4) 0.000000159(5) 0.000000011(2) 0.0000000630(18) 0.000000102(6) 0.0000000142(19) 0.0000000154(12) 0.0000000078(16) 0.000000379(12) 0.000000024(4) 0.0000000574(17) 0.0000000071(16) 0.000000088(3) Au2 0.000000274(14) 0.000000071(7) 0.000000014(4) 0.000000103(5) 0.000000009(2) 0.0000000346(17) 0.000000063(7) 0.000000012(2) 0.0000000056(12) 0.0000000030(15) 0.000000291(14) 0.000000015(4) 0.0000000388(18) 0.0000000051(15) 0.000000045(2)