#------------------------------------------------------------------------------ #$Date: 2026-04-24 05:57:51 +0100 (Fri, 24 Apr 2026) $ #$Revision: 305615 $ #$URL: svn://www.crystallography.net/cod/cif/7/06/43/7064386.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7064386 loop_ _publ_author_name 'Caltagirone, Claudia' 'Lippolis, Vito' 'Olmos, Maria Elena' 'Coconubo, Laura' 'Moreno, Sonia' 'Picci, Giacomo' 'Monge, Miguel' 'L\'opez-de-Luzuriaga, Jos\'e Maria' _publ_section_title ; Structural and computational evidence of rare synergic N(amide)H•••Au(I) and N(amidate)•••Au(I) secondary bonding interactions ; _journal_name_full 'New Journal of Chemistry' _journal_paper_doi 10.1039/D6NJ00558F _journal_year 2026 _chemical_formula_moiety 'C43 H33 Au Cl N3 O2 P2' _chemical_formula_sum 'C43 H33 Au Cl N3 O2 P2' _chemical_formula_weight 918.127 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _symmetry_Int_Tables_number 14 _atom_sites_solution_primary iterative _audit_creation_date 2026-03-13 _audit_creation_method ; Olex2 1.5 (compiled 2025.07.13 svn.rb7424aed for OlexSys, GUI svn.r7314) ; _audit_update_record ; 2026-03-19 deposited with the CCDC. 2026-04-21 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 99.363(1) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 13.6230(5) _cell_length_b 13.1182(5) _cell_length_c 25.113(1) _cell_measurement_reflns_used 10327 _cell_measurement_temperature 298.00 _cell_measurement_theta_max 27.9 _cell_measurement_theta_min 2.4 _cell_volume 4428.1(3) _computing_cell_refinement 'SAINT V8.40A (?, 2016)' _computing_data_collection 'Collect (Bruker AXS BV, 1997-2004)' _computing_data_reduction 'SAINT V8.40A (?, 2016)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine 1.5 (Bourhis et al., 2015)' _computing_structure_solution 'olex2.solve 1.5 (Bourhis et al., 2015)' _diffrn_ambient_temperature 298.00 _diffrn_measured_fraction_theta_full 0.9985 _diffrn_measured_fraction_theta_max 0.9969 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0629 _diffrn_reflns_av_unetI/netI 0.0333 _diffrn_reflns_Laue_measured_fraction_full 0.9985 _diffrn_reflns_Laue_measured_fraction_max 0.9969 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 33 _diffrn_reflns_limit_l_min -33 _diffrn_reflns_number 101847 _diffrn_reflns_point_group_measured_fraction_full 0.9985 _diffrn_reflns_point_group_measured_fraction_max 0.9969 _diffrn_reflns_theta_full 25.2417 _diffrn_reflns_theta_max 27.94 _diffrn_reflns_theta_min 2.41 _exptl_absorpt_coefficient_mu 3.502 _exptl_absorpt_correction_T_max 0.823 _exptl_absorpt_correction_T_min 0.689 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0704 before and 0.0574 after correction. The Ratio of minimum to maximum transmission is 0.3537. The \l/2 correction factor is Not present. ; _exptl_crystal_colour yellow _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.377 _exptl_crystal_description prism _exptl_crystal_F_000 1812.852 _exptl_crystal_size_max 0.104 _exptl_crystal_size_mid 0.095 _exptl_crystal_size_min 0.064 _refine_diff_density_max 0.7531 _refine_diff_density_min -1.3528 _refine_diff_density_rms 0.1232 _refine_ls_d_res_high 0.7585 _refine_ls_d_res_low 8.4662 _refine_ls_goodness_of_fit_ref 0.9975 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_constraints 67 _refine_ls_number_parameters 488 _refine_ls_number_reflns 10570 _refine_ls_number_restraints 103 _refine_ls_restrained_S_all 0.9925 _refine_ls_R_factor_all 0.0581 _refine_ls_R_factor_gt 0.0395 _refine_ls_shift/su_max -0.0002 _refine_ls_shift/su_mean 0.0000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0496P)^2^+2.9398P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0919 _refine_ls_wR_factor_ref 0.1000 _reflns_Friedel_coverage 0.0 _reflns_limit_h_max 17 _reflns_limit_h_min -17 _reflns_limit_k_max 17 _reflns_limit_k_min 0 _reflns_limit_l_max 33 _reflns_limit_l_min 0 _reflns_number_gt 7880 _reflns_number_total 10570 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL 1_a.res in P2(1)/c CELL 0.71073 13.623 13.1182 25.113 90 99.363 90 ZERR 4 0.0005 0.0005 0.001 0 0.001 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Au Cl N O P UNIT 172 132 4 4 12 8 8 DELU $C $N $O HTAB C5 O2_$1 HTAB N1 Cl1 HTAB N3 Cl1 HTAB C18 Cl1_$2 HTAB N1 Au HTAB N3 Au EADP C34 C35 L.S. 20 PLAN 16 SIZE 0.064 0.095 0.104 TEMP 24.85 CONF ABIN MORE -1 FMAP 2 ACTA BOND $H LIST 4 MERG 2 OMIT -2 0 4 OMIT -1 1 1 OMIT -1 1 4 OMIT 0 1 2 OMIT 0 3 1 OMIT 1 1 0 OMIT 2 2 0 OMIT 2 3 2 WGHT 0.049577 2.939799 FVAR 0.215341 REM REM REM > REM REM Au 3 0.287940 0.379785 0.318576 11.00000 0.05819 0.05655 = 0.05764 -0.00432 0.00641 0.00933 Cl1 4 0.441227 0.505102 0.324694 11.00000 0.06449 0.06741 = 0.07115 0.00944 0.01478 -0.00762 P1 7 0.156929 0.493866 0.312724 11.00000 0.04845 0.04598 = 0.05210 -0.00012 0.00879 0.00299 P2 7 0.364114 0.221273 0.326153 11.00000 0.04583 0.04785 = 0.04860 -0.00377 0.00583 0.00280 C1 1 0.186742 0.626794 0.329432 11.00000 0.05626 0.04702 = 0.05430 0.00137 0.01172 0.00192 C2 1 0.150038 0.706042 0.294433 11.00000 0.07171 0.05265 = 0.06486 -0.00148 0.00082 0.00810 AFIX 43 H2 2 0.111017 0.690914 0.261447 11.00000 -1.20000 AFIX 0 C3 1 0.171150 0.806346 0.308366 11.00000 0.07966 0.05105 = 0.08685 0.00583 -0.00211 0.00173 AFIX 43 H3 2 0.145571 0.858411 0.285030 11.00000 -1.20000 AFIX 0 C4 1 0.229932 0.829425 0.356686 11.00000 0.08670 0.04807 = 0.08590 -0.01179 0.00505 -0.00266 AFIX 43 H4 2 0.244016 0.897127 0.365920 11.00000 -1.20000 AFIX 0 C5 1 0.268244 0.752476 0.391647 11.00000 0.06235 0.05570 = 0.06617 -0.00535 0.00646 -0.00145 AFIX 43 H5 2 0.307347 0.768461 0.424486 11.00000 -1.20000 AFIX 0 C6 1 0.248397 0.652212 0.377750 11.00000 0.05270 0.04642 = 0.05452 -0.00048 0.01016 0.00706 N1 5 0.291744 0.573138 0.412573 11.00000 0.05791 0.05318 = 0.04929 -0.00102 0.00447 0.01006 AFIX 43 H1 2 0.329151 0.529559 0.399948 11.00000 -1.20000 AFIX 0 C7 1 0.277830 0.562445 0.463827 11.00000 0.05904 0.05541 = 0.05249 -0.00407 0.01163 0.00230 O1 6 0.220158 0.613646 0.485162 11.00000 0.08547 0.07781 = 0.06545 0.00042 0.02382 0.02289 C8 1 0.338787 0.479001 0.494477 11.00000 0.05779 0.05598 = 0.04588 -0.00232 0.00621 -0.00648 C9 1 0.332650 0.460979 0.547915 11.00000 0.07882 0.07802 = 0.04959 0.00075 0.01875 0.00560 AFIX 43 H9 2 0.289651 0.499022 0.565258 11.00000 -1.20000 AFIX 0 C10 1 0.391058 0.385859 0.575305 11.00000 0.08836 0.09431 = 0.04935 0.00888 0.01399 0.00416 AFIX 43 H10 2 0.389818 0.373832 0.611685 11.00000 -1.20000 AFIX 0 C11 1 0.451202 0.329061 0.547734 11.00000 0.07277 0.07113 = 0.05260 0.00884 0.00565 0.00556 AFIX 43 H11 2 0.489665 0.276295 0.564834 11.00000 -1.20000 AFIX 0 C12 1 0.453582 0.351572 0.494346 11.00000 0.05527 0.05822 = 0.04495 0.00032 0.00300 -0.00241 N2 5 0.398723 0.425485 0.467442 11.00000 0.05171 0.05073 = 0.04189 -0.00300 0.00339 -0.00287 C13 1 0.518700 0.289409 0.463977 11.00000 0.04910 0.05610 = 0.04849 -0.00005 -0.00077 -0.00278 O2 6 0.569620 0.219938 0.484738 11.00000 0.08312 0.07289 = 0.06058 0.01076 0.00299 0.02076 N3 5 0.512199 0.317072 0.411263 11.00000 0.05336 0.05108 = 0.04923 -0.00352 0.00125 0.00627 AFIX 43 H3a 2 0.477675 0.370203 0.400406 11.00000 -1.20000 AFIX 0 C14 1 0.558889 0.263589 0.373226 11.00000 0.04943 0.04830 = 0.05436 0.00099 0.00897 0.00053 C15 1 0.661532 0.257171 0.379133 11.00000 0.05409 0.06216 = 0.07514 -0.00777 0.00146 0.00213 AFIX 43 H15 2 0.701151 0.284410 0.409449 11.00000 -1.20000 AFIX 0 C16 1 0.704135 0.210134 0.339721 11.00000 0.04280 0.07647 = 0.10153 -0.00395 0.01327 0.00627 AFIX 43 H16 2 0.773031 0.204930 0.343757 11.00000 -1.20000 AFIX 0 C17 1 0.646591 0.170598 0.294382 11.00000 0.06386 0.07272 = 0.07580 -0.00795 0.02702 0.00848 AFIX 43 H17 2 0.676650 0.141127 0.267445 11.00000 -1.20000 AFIX 0 C18 1 0.544629 0.174629 0.288866 11.00000 0.05832 0.05872 = 0.05532 -0.00384 0.00928 0.00558 AFIX 43 H18 2 0.505791 0.147329 0.258311 11.00000 -1.20000 AFIX 0 C19 1 0.499444 0.219293 0.328733 11.00000 0.04864 0.04480 = 0.05383 0.00185 0.00860 0.00542 C20 1 0.069931 0.455221 0.356620 11.00000 0.05029 0.05933 = 0.05797 0.00676 0.00767 0.00021 C21 1 0.039068 0.353596 0.354245 11.00000 0.06564 0.05818 = 0.10240 0.00805 0.02207 -0.00173 AFIX 43 H21 2 0.061551 0.308736 0.330200 11.00000 -1.20000 AFIX 0 C22 1 -0.025084 0.320109 0.387843 11.00000 0.07272 0.07791 = 0.12888 0.03698 0.03446 0.00027 AFIX 43 H22 2 -0.046217 0.252605 0.386221 11.00000 -1.20000 AFIX 0 C23 1 -0.057906 0.386410 0.423784 11.00000 0.06506 0.12793 = 0.07745 0.04556 0.01806 0.00186 AFIX 43 H23 2 -0.099374 0.363105 0.447154 11.00000 -1.20000 AFIX 0 C24 1 -0.029797 0.485088 0.425000 11.00000 0.06665 0.12383 = 0.05384 -0.00037 0.01192 0.00227 AFIX 43 H24 2 -0.053577 0.529577 0.448773 11.00000 -1.20000 AFIX 0 C25 1 0.033307 0.521296 0.391815 11.00000 0.05978 0.07982 = 0.05819 -0.00345 0.01122 -0.00246 AFIX 43 H25 2 0.051333 0.589737 0.392966 11.00000 -1.20000 AFIX 0 C26 1 0.083555 0.502798 0.245578 11.00000 0.05579 0.05025 = 0.05687 -0.00308 0.01006 -0.00325 C27 1 0.127670 0.483855 0.201421 11.00000 0.06943 0.07353 = 0.06342 -0.00525 0.00876 0.01266 AFIX 43 H27 2 0.192894 0.460321 0.205936 11.00000 -1.20000 AFIX 0 C28 1 0.075677 0.499564 0.150193 11.00000 0.10194 0.09534 = 0.05438 -0.00042 0.01800 0.00672 AFIX 43 H28 2 0.106371 0.486362 0.120438 11.00000 -1.20000 AFIX 0 C29 1 -0.019094 0.533808 0.142536 11.00000 0.08849 0.07883 = 0.06438 0.00957 -0.00826 -0.00165 AFIX 43 H29 2 -0.053050 0.544736 0.107782 11.00000 -1.20000 AFIX 0 C30 1 -0.064682 0.552258 0.186039 11.00000 0.05874 0.08530 = 0.07675 0.00605 -0.00425 -0.00649 AFIX 43 H30 2 -0.129927 0.575820 0.180902 11.00000 -1.20000 AFIX 0 C31 1 -0.014295 0.536079 0.237856 11.00000 0.05586 0.07112 = 0.06575 0.00060 0.00585 0.00181 AFIX 43 H31 2 -0.046062 0.547524 0.267403 11.00000 -1.20000 AFIX 0 C32 1 0.346466 0.150974 0.386058 11.00000 0.05971 0.05707 = 0.04720 -0.00719 0.00625 -0.01103 C33 1 0.407868 0.068804 0.404914 11.00000 0.07842 0.05981 = 0.05816 -0.00122 0.00029 -0.00898 AFIX 43 H33 2 0.461512 0.052842 0.387797 11.00000 -1.20000 AFIX 0 C34 1 0.390731 0.011139 0.448147 11.00000 0.12349 0.10349 = 0.06743 0.01751 -0.00315 -0.04147 AFIX 43 H34 2 0.431553 -0.044086 0.459614 11.00000 -1.20000 AFIX 0 C35 1 0.313798 0.035357 0.473996 11.00000 0.12349 0.10349 = 0.06743 0.01751 -0.00315 -0.04147 AFIX 43 H35 2 0.302241 -0.003787 0.503226 11.00000 -1.20000 AFIX 0 C36 1 0.253028 0.116255 0.457817 11.00000 0.09994 0.15822 = 0.07012 -0.01336 0.03863 -0.04025 AFIX 43 H36 2 0.201451 0.132387 0.476466 11.00000 -1.20000 AFIX 0 C37 1 0.268359 0.176096 0.412430 11.00000 0.07138 0.10925 = 0.06409 -0.01280 0.01421 -0.00915 AFIX 43 H37 2 0.226764 0.230703 0.400879 11.00000 -1.20000 AFIX 0 C38 1 0.314377 0.139268 0.269861 11.00000 0.05030 0.05788 = 0.04956 0.00049 0.00374 -0.00477 C39 1 0.251066 0.179237 0.225690 11.00000 0.07246 0.06692 = 0.05348 0.00365 0.00559 -0.00213 AFIX 43 H39 2 0.233182 0.247696 0.225088 11.00000 -1.20000 AFIX 0 C40 1 0.214923 0.116419 0.182683 11.00000 0.08749 0.10270 = 0.05283 0.00235 -0.00803 -0.02468 AFIX 43 H40 2 0.172677 0.143296 0.153206 11.00000 -1.20000 AFIX 0 C41 1 0.240099 0.015967 0.182748 11.00000 0.07538 0.08891 = 0.05974 -0.02455 0.01597 -0.02888 AFIX 43 H41 2 0.214732 -0.025184 0.153584 11.00000 -1.20000 AFIX 0 C42 1 0.302267 -0.024209 0.225396 11.00000 0.09396 0.07128 = 0.07339 -0.02180 0.00785 -0.00980 AFIX 43 H42 2 0.320174 -0.092593 0.225093 11.00000 -1.20000 AFIX 0 C43 1 0.338903 0.036105 0.269138 11.00000 0.07202 0.06495 = 0.06898 -0.01190 -0.00464 0.00610 AFIX 43 H43 2 0.380387 0.007678 0.298448 11.00000 -1.20000 AFIX 0 HKLF 4 END Q1 1 0.288889 0.3 0.322222 11 0.05 0.75 Q2 1 0.355556 0.388889 0.3 11 0.05 0.67 Q4 1 0.311111 0.466667 0.3 11 0.05 0.63 Q5 1 0.111111 0.5 0.277778 11 0.05 0.61 Q6 1 0.288889 0.911111 0.322222 11 0.05 0.61 Q7 1 0.222222 0.344444 0.344444 11 0.05 0.58 Q8 1 -0.155556 0.522222 0.188889 11 0.05 0.57 Q9 1 0.6 0.211111 0.288889 11 0.05 0.54 Q10 1 0.377778 0.488889 0.344444 11 0.05 0.53 Q11 1 -0.222222 0.588889 0.155556 11 0.05 0.53 Q13 1 0.466667 0.477778 0.3 11 0.05 0.49 Q14 1 0.4 0.566667 0.322222 11 0.05 0.49 Q12 1 0.222222 0.544444 0.311111 11 0.05 0.5 Q15 1 0.466667 0.333333 0.4 11 0.05 0.49 Q3 1 0.2 0.411111 0.322222 11 0.05 0.67 Q16 1 0.311111 0.177778 0.355556 11 0.05 0.48 REM The information below was added by Olex2. REM REM R1 = 0.0395 for 7880 Fo > 4sig(Fo) and 0.0581 for all 10570 data REM 488 parameters refined using 103 restraints REM Highest difference peak 0.7531, deepest hole -1.3528 REM Mean Shift 0.0000, Max Shift -0.0002. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0581 REM R1_gt = 0.0395 REM wR_ref = 0.1000 REM GOOF = 0.9975 REM Shift_max = -0.0002 REM Shift_mean = 0.0000 REM Reflections_all = 10570 REM Reflections_gt = 7880 REM Parameters = 488 REM Hole = -1.3528 REM Peak = 0.7531 REM Flack = n/a ; _cod_data_source_file d6nj00558f2.cif _cod_data_source_block bsm140lc156a _cod_original_formula_sum 'C43 H33 Au1 Cl1 N3 O2 P2' _cod_database_code 7064386 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All N(H) groups 2. Rigid bond restraints C1, C2, C3, C4, C5, C6, C7, C8, C9, C10, C11, C12, C13, C14, C15, C16, C17, C18, C19, C20, C21, C22, C23, C24, C25, C26, C27, C28, C29, C30, C31, C32, C33, C34, C35, C36, C37, C38, C39, C40, C41, C42, C43, N1, N2, N3, O1, O2 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01 3. Uiso/Uaniso restraints and constraints Uanis(C34) = Uanis(C35) 4.a Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3), C4(H4), C5(H5), N1(H1), C9(H9), C10(H10), C11(H11), N3(H3a), C15(H15), C16(H16), C17(H17), C18(H18), C21(H21), C22(H22), C23(H23), C24(H24), C25(H25), C27(H27), C28(H28), C29(H29), C30(H30), C31(H31), C33(H33), C34(H34), C35(H35), C36(H36), C37(H37), C39(H39), C40(H40), C41(H41), C42(H42), C43(H43) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_fab_file ; -17 0 2 -1.9690 -0.1101 -17 0 4 -0.2275 -1.1757 -17 0 6 -1.2378 -0.3607 -17 0 8 0.4700 0.2029 -17 0 10 -1.1224 -0.3074 -17 0 12 -0.4586 -0.1919 -17 0 14 3.2990 0.7160 -17 1 1 2.0505 -0.5263 -17 1 2 0.1455 -0.2369 -17 1 3 1.8944 0.5040 -17 1 4 -0.0264 -0.0005 -17 1 5 -2.1877 0.0926 -17 1 6 1.8924 0.3931 -17 1 7 -1.2363 0.0999 -17 1 8 2.6475 0.0748 -17 1 9 -0.2425 -0.0438 -17 1 10 1.0419 -0.0551 -17 1 11 1.5348 0.0948 -17 1 12 3.5562 0.5196 -17 1 13 0.7267 0.3086 -17 1 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7 -0.3617 -0.4372 15 8 0 0.0692 0.1080 15 8 1 0.2748 0.1324 15 8 2 0.7724 -0.1178 15 8 3 1.0140 -0.1694 15 8 4 -0.1392 0.2936 15 8 5 -0.1921 0.2661 15 9 0 -0.1714 0.5671 15 9 1 -0.6264 -0.0452 16 0 0 -1.1303 0.7605 16 0 2 1.3112 0.0871 16 0 4 1.6305 -0.0574 16 0 6 1.7809 0.1720 16 0 8 1.0442 0.0549 16 0 10 -0.0876 -0.8079 16 1 0 -0.3729 -0.7074 16 1 1 2.6367 0.4829 16 1 2 1.3837 0.0283 16 1 3 0.5779 0.1211 16 1 4 -0.4145 0.0797 16 1 5 -1.2458 -0.0252 16 1 6 2.1416 0.1836 16 1 7 -1.5082 -0.3142 16 1 8 0.6870 0.1654 16 1 9 -0.3113 -0.4183 16 2 0 -3.2408 -0.2993 16 2 1 -0.5026 0.5343 16 2 2 -5.8788 -0.2060 16 2 3 0.3731 0.0078 16 2 4 -2.0138 -0.0122 16 2 5 -0.8078 0.2051 16 2 6 0.3637 0.1043 16 2 7 -0.9678 0.0934 16 2 8 -0.8505 0.3320 16 2 9 3.1330 -0.6153 16 3 0 -1.9651 -0.0171 16 3 1 2.1603 -0.1161 16 3 2 -1.9125 0.0538 16 3 3 2.7535 0.0427 16 3 4 1.0607 -0.3231 16 3 5 -1.2692 0.1783 16 3 6 2.4343 -0.1569 16 3 7 1.4039 -0.2367 16 3 8 -0.0897 0.2906 16 4 0 -1.0934 -0.0499 16 4 1 1.8746 -0.1076 16 4 2 0.2403 -0.3239 16 4 3 0.3623 0.1168 16 4 4 2.6664 -0.5420 16 4 5 -1.8418 0.1569 16 4 6 1.9613 -0.3898 16 4 7 -0.6410 -0.4147 16 5 0 1.4571 -0.3032 16 5 1 0.9906 0.1118 16 5 2 0.5911 -0.3771 16 5 3 -1.8716 0.1304 16 5 4 0.1522 0.0857 16 5 5 -2.1978 -0.0378 16 5 6 -0.5086 0.0178 16 6 0 0.7211 -0.2653 16 6 1 -1.9268 -0.3267 16 6 2 0.1068 0.2685 16 6 3 -0.4235 -0.3335 16 6 4 1.9078 0.2919 16 7 0 0.7289 0.6805 16 7 1 0.1161 0.4047 17 0 0 2.6104 -0.2693 17 0 2 3.5165 0.5994 17 0 4 0.8374 0.1484 17 1 0 0.7946 0.4031 17 1 1 -0.7691 -0.1008 17 1 2 -2.6253 0.0721 17 1 3 -0.8738 -0.2295 17 1 4 0.5716 0.3256 17 1 5 0.0772 -0.2488 17 2 0 -4.0939 -0.4231 17 2 1 0.1487 -0.5637 17 2 2 -2.1257 0.3769 17 2 3 -0.6414 0.5046 17 2 4 0.3609 0.3393 17 3 0 -1.5701 0.1994 17 3 1 2.0225 0.1123 17 3 2 0.8726 0.0726 17 3 3 -2.0643 -0.3243 17 4 0 -0.5206 -0.1134 17 4 1 1.9793 0.2058 17 4 2 2.9046 -1.1464 0 0 0 0.0 0.0 ; _iucr_refine_fcf_details ; data_bsm140lc156a_CCDC1 _computing_structure_refinement 'olex2.refine 1.5 (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,y+1/2,-z+1/2 3 -x,-y,-z 4 x,-y-1/2,z-1/2 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_Int_Tables_number 14 _cell_length_a 13.6230(5) _cell_length_b 13.1182(5) _cell_length_c 25.113(1) _cell_angle_alpha 90 _cell_angle_beta 99.363(1) _cell_angle_gamma 90 _cell_volume 4428.1(3) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status -17 0 2 4.434 87.067 94.515 66.647 o -17 0 4 373.083 481.702 129.253 32.847 o -17 0 6 1269.660 1402.080 190.550 13.550 o -17 0 8 390.687 508.924 185.455 16.664 o -17 0 10 39.901 43.697 133.700 33.431 o -17 0 12 1033.820 1004.960 165.467 18.254 o -17 0 14 264.962 37.883 123.676 37.753 o -17 1 1 546.676 522.471 82.005 66.709 o -17 1 2 237.097 207.565 68.561 109.507 o -17 1 3 224.465 355.586 86.338 71.479 o -17 1 4 258.971 388.313 91.710 63.193 o -17 1 5 12.298 -23.024 100.043 59.983 o -17 1 6 22.478 110.235 89.734 73.292 o -17 1 7 286.400 347.331 104.238 50.156 o -17 1 8 338.604 372.215 119.635 38.474 o -17 1 9 464.329 402.367 107.474 45.116 o -17 1 10 439.120 207.671 91.678 61.465 o -17 1 11 281.819 354.526 96.478 57.655 o -17 1 12 190.751 245.812 122.013 38.554 o -17 1 13 110.805 212.979 90.606 69.276 o -17 1 14 50.191 186.337 145.980 27.844 o -17 1 15 294.388 194.084 98.074 57.026 o -17 2 1 90.751 96.046 78.907 92.309 o -17 2 2 32.102 -84.212 84.212 84.100 o -17 2 3 169.463 112.193 67.883 117.866 o -17 2 4 88.604 135.580 79.760 89.889 o -17 2 5 1002.250 1021.320 126.049 28.182 o -17 2 6 23.931 182.121 113.339 45.990 o -17 2 7 743.546 838.862 189.768 15.133 o -17 2 8 36.675 105.032 159.547 23.472 o -17 2 9 3.112 9.798 115.477 45.076 o -17 2 10 4.901 -47.961 80.247 93.314 o -17 2 11 481.564 429.974 99.640 50.899 o -17 2 12 6.456 -80.933 80.933 91.698 o -17 2 13 635.566 714.417 112.749 38.247 o -17 2 14 0.564 37.958 79.228 95.285 o -17 3 1 343.957 487.307 81.228 74.052 o -17 3 2 779.528 852.877 121.710 32.069 o -17 3 3 342.831 235.637 112.053 43.958 o -17 3 4 114.660 152.665 87.091 75.234 o -17 3 5 104.216 176.852 114.232 44.687 o -17 3 6 65.338 -85.156 85.156 81.496 o -17 3 7 59.227 32.991 94.934 65.648 o -17 3 8 341.155 192.608 90.833 64.591 o -17 3 9 345.993 580.434 243.684 9.854 o -17 3 10 520.169 449.079 174.770 18.454 o -17 3 11 276.610 213.901 102.908 52.319 o -17 3 12 43.149 56.507 86.566 78.777 o -17 3 13 1.019 -10.299 89.486 75.134 o -17 4 1 16.706 -66.621 66.621 134.587 o -17 4 2 22.830 -22.987 81.872 89.177 o -17 4 3 28.945 28.663 85.155 82.009 o -17 4 4 537.148 472.006 93.181 55.461 o -17 4 5 14.856 -80.754 80.754 91.869 o -17 4 6 662.970 342.004 87.504 59.873 o -17 4 7 48.730 123.212 89.608 72.865 o -17 4 8 248.820 200.084 90.847 66.351 o -17 4 9 4.656 90.982 82.729 86.651 o -17 4 10 46.621 119.468 85.546 79.826 o -17 4 11 6.207 73.311 81.257 89.971 o -17 4 12 530.100 661.689 114.507 38.555 o -17 5 1 240.962 269.933 80.190 82.195 o -17 5 2 221.504 264.444 95.020 61.043 o -17 5 3 976.417 1065.470 112.973 33.050 o -17 5 4 7.737 115.472 76.377 100.864 o -17 5 5 305.433 340.401 93.224 60.973 o -17 5 6 34.996 114.458 76.578 99.400 o -17 5 7 15.461 -85.996 85.996 81.041 o -17 5 8 136.854 103.246 107.771 50.054 o -17 5 9 213.532 64.755 89.011 71.042 o -16 0 2 1470.420 1397.120 173.516 15.236 o -16 0 4 673.569 745.349 151.444 22.986 o -16 0 6 126.665 69.007 225.350 11.771 o -16 0 8 1013.390 1424.430 205.942 12.270 o -16 0 10 2137.950 2196.700 326.703 4.833 o -16 0 12 213.787 123.420 121.218 39.291 o -16 0 14 300.371 223.223 69.889 102.395 o -16 0 16 1228.610 1157.710 124.122 26.726 o -16 0 18 714.548 697.816 124.644 31.916 o -16 1 1 5.434 -55.504 61.158 160.436 o -16 1 2 12.570 41.304 63.522 146.731 o -16 1 3 149.545 92.320 69.208 115.395 o -16 1 4 577.960 602.202 94.125 52.667 o -16 1 5 1081.760 1127.920 104.643 35.123 o -16 1 6 603.695 664.059 126.033 32.225 o -16 1 7 370.429 570.988 148.918 25.146 o -16 1 8 234.451 65.759 100.632 56.092 o -16 1 9 0.167 15.203 73.918 109.834 o -16 1 10 72.990 116.687 83.918 82.231 o -16 1 11 526.113 665.214 105.250 44.361 o -16 1 12 449.152 515.232 118.947 37.427 o -16 1 13 700.857 687.118 83.965 58.492 o -16 1 14 683.386 466.977 107.489 42.175 o -16 1 15 223.265 385.970 74.943 90.886 o -16 1 16 66.910 106.305 68.506 121.721 o -16 1 17 38.711 164.790 78.946 92.785 o -16 1 18 275.354 276.409 101.526 53.233 o -16 1 19 325.386 373.219 99.613 53.672 o -16 2 1 1321.860 1292.630 118.514 27.189 o -16 2 2 20.124 92.617 63.741 143.356 o -16 2 3 1490.460 1334.350 109.909 28.129 o -16 2 4 19.068 -45.354 108.940 50.547 o -16 2 5 1.276 -76.549 76.549 102.658 o -16 2 6 0.486 -75.522 75.522 105.496 o -16 2 7 1021.220 911.518 112.496 33.558 o -16 2 8 3.311 30.429 93.524 68.515 o -16 2 9 1068.050 1222.840 130.394 25.745 o -16 2 10 20.519 68.088 81.655 88.790 o -16 2 11 265.117 303.505 91.152 64.602 o -16 2 12 0.482 -46.741 46.741 275.334 o -16 2 13 119.652 51.884 88.125 74.531 o -16 2 14 12.217 -32.785 67.369 131.895 o -16 2 15 920.504 945.147 104.077 38.375 o -16 2 16 5.448 1.480 74.162 109.176 o -16 2 17 497.906 444.159 87.449 62.527 o -16 2 18 2.089 -74.637 74.637 107.950 o -16 2 19 19.164 35.873 101.144 58.402 o -16 3 1 40.167 -16.942 60.605 160.333 o -16 3 2 74.678 83.814 68.793 120.944 o -16 3 3 242.480 339.888 97.555 57.254 o -16 3 4 796.009 535.650 90.518 52.263 o -16 3 5 653.858 679.510 93.829 50.872 o -16 3 6 661.178 646.318 101.137 45.535 o -16 3 7 107.233 120.894 92.132 68.017 o -16 3 8 36.320 -92.223 93.392 68.428 o -16 3 9 115.127 132.751 89.331 71.885 o -16 3 10 231.016 294.304 93.698 62.191 o -16 3 11 238.020 129.923 100.539 55.711 o -16 3 12 764.013 557.567 129.483 30.094 o -16 3 13 155.942 114.994 88.403 72.653 o -16 3 14 236.627 265.811 83.033 77.473 o -16 3 15 2.333 -73.520 73.520 111.243 o -16 3 16 16.722 -75.921 75.921 103.811 o -16 3 17 45.951 -38.439 76.493 101.251 o -16 3 18 192.142 206.978 84.699 76.674 o -16 4 1 0.884 -41.646 50.854 232.544 o -16 4 2 1197.590 1205.700 77.190 46.193 o -16 4 3 48.498 52.578 65.178 136.745 o -16 4 4 172.200 223.119 82.284 81.162 o -16 4 5 123.118 214.965 72.054 105.546 o -16 4 6 434.139 447.523 95.652 55.152 o -16 4 7 8.744 22.512 117.033 43.811 o -16 4 8 1071.590 1123.120 126.618 27.174 o -16 4 9 105.597 126.979 87.624 74.846 o -16 4 10 590.635 354.751 83.130 66.423 o -16 4 11 61.091 -3.721 102.065 57.090 o -16 4 12 2.152 -65.112 73.387 111.654 o -16 4 13 76.025 106.509 70.535 114.699 o -16 4 14 391.396 351.615 91.661 61.005 o -16 4 15 9.921 -74.999 74.999 106.618 o -16 4 16 583.927 354.327 100.456 49.264 o -16 4 17 201.937 211.886 103.960 52.264 o -16 5 1 292.361 372.201 105.443 48.903 o -16 5 2 153.292 140.685 84.913 78.124 o -16 5 3 83.317 128.208 63.025 140.451 o -16 5 4 428.161 447.405 92.750 58.177 o -16 5 5 737.279 847.113 95.403 46.837 o -16 5 6 116.876 196.031 62.925 135.811 o -16 5 7 635.973 565.990 119.775 35.255 o -16 5 8 0.584 -52.595 84.534 84.201 o -16 5 9 15.336 -56.358 56.358 187.676 o -16 5 10 231.865 189.767 83.789 77.376 o -16 5 11 176.180 97.695 69.258 113.696 o -16 5 12 271.362 226.337 78.981 84.130 o -16 5 13 769.594 644.144 97.042 46.802 o -16 5 14 129.205 157.332 86.081 76.520 o -16 5 15 85.586 32.810 86.419 78.365 o -16 5 16 36.234 64.324 90.645 72.022 o -16 6 1 1108.960 982.632 91.454 42.091 o -16 6 2 25.985 28.450 64.862 140.359 o -16 6 3 601.252 656.900 79.618 66.093 o -16 6 4 142.341 144.872 80.264 87.046 o -16 6 5 53.070 92.424 68.421 123.149 o -16 6 6 39.243 55.525 71.700 114.040 o -16 6 7 256.275 452.946 79.052 80.779 o -16 6 8 14.609 20.748 56.643 184.711 o -16 6 9 1065.190 1158.120 107.682 33.864 o -16 6 10 100.540 128.519 77.433 94.793 o -16 6 11 349.039 345.514 86.908 67.823 o -16 6 12 67.299 95.764 137.886 31.258 o -16 6 13 1.459 -69.014 81.549 90.453 o -16 6 14 1.765 -10.647 80.294 93.292 o -16 7 1 12.333 8.073 67.188 132.361 o -16 7 2 15.426 174.801 192.132 16.209 o -16 7 3 156.063 73.773 68.963 116.296 o -16 7 4 447.240 237.145 79.817 76.864 o -16 7 5 218.248 233.130 75.900 92.025 o -16 7 6 493.914 509.431 82.169 68.145 o -16 7 7 240.929 297.223 88.393 68.836 o -16 7 8 65.686 17.919 61.498 152.961 o -16 7 9 6.330 52.204 63.337 147.633 o -16 7 10 57.749 82.853 91.631 69.965 o -16 7 11 122.453 264.488 77.071 92.443 o -15 0 2 21.220 -74.589 92.208 70.432 o -15 0 4 3538.660 3562.350 701.819 1.127 o -15 0 6 3817.210 4157.890 277.363 4.759 o -15 0 8 763.477 972.525 380.507 4.041 o -15 0 10 635.254 428.682 146.985 25.014 o -15 0 12 3744.120 3485.240 131.609 9.872 o -15 0 14 1589.040 1446.600 118.078 24.750 o -15 0 16 67.827 153.769 96.435 62.647 o -15 0 18 1445.220 1269.330 146.036 19.975 o -15 0 20 1665.790 1783.140 170.265 14.626 o -15 0 22 143.523 13.024 71.929 109.568 o -15 1 1 1629.060 1640.500 117.226 23.980 o -15 1 2 2108.320 2568.320 198.639 10.256 o -15 1 3 1766.800 1874.570 111.021 23.496 o -15 1 4 102.655 198.095 72.540 105.546 o -15 1 5 36.653 61.205 62.293 149.806 o -15 1 6 508.097 423.425 97.112 52.755 o -15 1 7 579.867 594.505 90.464 56.017 o -15 1 8 1665.520 1970.700 182.708 13.011 o -15 1 9 1155.630 1162.930 145.876 21.508 o -15 1 10 841.311 929.103 155.406 21.062 o -15 1 11 690.010 693.037 68.111 76.719 o -15 1 12 23.480 112.764 74.158 106.270 o -15 1 13 29.637 68.921 52.571 207.959 o -15 1 14 813.029 957.835 77.911 57.724 o -15 1 15 749.652 913.664 75.226 62.599 o -15 1 16 1484.570 1528.490 96.235 31.355 o -15 1 17 940.263 1197.000 99.247 38.946 o -15 1 18 199.199 185.262 68.734 111.663 o -15 1 19 226.492 257.622 85.408 74.033 o -15 1 20 199.859 371.646 94.611 60.975 o -15 1 21 81.891 123.549 97.657 61.152 o -15 1 22 252.493 203.352 82.491 78.812 o -15 2 1 2.213 -14.507 69.709 123.732 o -15 2 2 35.891 61.735 59.773 162.277 o -15 2 3 1647.630 1673.140 107.376 26.007 o -15 2 4 3.404 36.361 59.583 167.495 o -15 2 5 2097.070 2046.770 138.223 16.783 o -15 2 6 8.482 45.357 77.914 98.129 o -15 2 7 287.005 261.034 86.012 71.585 o -15 2 8 23.427 -59.485 110.594 49.016 o -15 2 9 205.156 321.142 91.809 64.767 o -15 2 10 81.672 91.721 50.737 211.754 o -15 2 11 1279.040 1319.850 104.421 31.992 o -15 2 12 20.909 -2.104 78.490 97.031 o -15 2 13 1116.060 1054.970 106.835 34.221 o -15 2 14 71.454 26.819 60.024 159.332 o -15 2 15 92.210 -52.549 58.194 168.262 o -15 2 16 77.950 -16.964 67.548 127.440 o -15 2 17 490.282 484.468 130.463 31.603 o -15 2 18 14.088 13.501 68.576 126.856 o -15 2 19 864.502 813.978 93.766 46.115 o -15 2 20 73.658 133.424 98.840 59.786 o -15 2 21 272.949 199.198 108.696 47.398 o -15 2 22 75.051 92.392 182.552 17.922 o -15 3 1 366.672 391.862 54.002 137.883 o -15 3 2 502.922 604.229 83.385 65.139 o -15 3 3 28.836 75.978 65.906 134.345 o -15 3 4 37.028 96.217 103.808 54.955 o -15 3 5 290.295 257.994 77.111 86.466 o -15 3 6 223.244 374.920 102.490 52.360 o -15 3 7 861.288 820.367 155.550 21.150 o -15 3 8 789.305 623.338 106.139 40.807 o -15 3 9 225.296 134.072 62.430 131.865 o -15 3 10 319.300 257.634 76.215 87.137 o -15 3 11 149.361 155.252 71.026 108.513 o -15 3 12 17.267 -60.730 60.730 161.676 o -15 3 13 134.791 71.844 72.973 105.738 o -15 3 14 141.986 36.762 47.279 233.461 o -15 3 15 211.531 25.851 70.180 111.031 o -15 3 16 483.715 338.042 68.656 93.182 o -15 3 17 10.082 -20.305 63.443 148.782 o -15 3 18 43.563 -79.124 79.124 94.799 o -15 3 19 65.229 -91.083 91.083 71.399 o -15 3 20 8.919 -89.775 89.775 74.507 o -15 3 21 83.853 -0.679 74.843 104.234 o -15 4 1 16.610 2.131 50.008 237.320 o -15 4 2 654.442 560.938 87.926 57.215 o -15 4 3 3.751 -14.487 57.703 180.340 o -15 4 4 827.638 799.632 76.549 60.719 o -15 4 5 167.493 150.198 55.199 167.788 o -15 4 6 391.678 446.441 66.155 100.390 o -15 4 7 280.418 338.045 84.654 72.788 o -15 4 8 189.195 124.069 51.723 185.935 o -15 4 9 33.884 -69.239 69.239 123.784 o -15 4 10 922.474 833.716 83.431 52.126 o -15 4 11 196.031 170.118 56.145 158.809 o -15 4 12 677.206 463.073 65.071 86.999 o -15 4 13 219.565 254.546 80.588 82.374 o -15 4 14 21.940 -49.799 64.834 141.703 o -15 4 15 98.159 126.230 71.902 109.132 o -15 4 16 95.374 -10.645 59.805 159.479 o -15 4 17 3.707 -15.795 68.058 129.722 o -15 4 18 509.329 342.024 79.466 73.805 o -15 4 19 36.242 55.715 77.948 96.970 o -15 4 20 115.964 65.239 76.275 98.123 o -15 5 1 698.678 724.337 76.956 65.196 o -15 5 2 240.139 169.074 59.341 140.845 o -15 5 3 241.885 187.329 61.791 130.860 o -15 5 4 0.435 -45.441 63.692 148.319 o -15 5 5 6.411 28.998 74.839 106.658 o -15 5 6 376.869 427.123 76.666 81.153 o -15 5 7 1030.960 1137.070 94.769 40.360 o -15 5 8 679.875 785.926 90.519 52.087 o -15 5 9 890.635 967.796 78.270 55.293 o -15 5 10 180.484 167.033 58.069 151.756 o -15 5 11 94.225 52.466 71.017 113.647 o -15 5 12 8.906 -31.668 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106.197 o -14 5 1 559.107 532.556 69.279 84.034 o -14 5 2 498.631 551.937 69.951 85.160 o -14 5 3 1532.920 1585.050 96.499 30.430 o -14 5 4 228.622 246.215 66.975 113.331 o -14 5 5 1243.130 1444.350 89.981 37.223 o -14 5 6 139.744 118.637 51.181 197.122 o -14 5 7 31.510 90.374 48.864 236.516 o -14 5 8 47.675 102.029 68.158 124.094 o -14 5 9 470.318 470.358 69.442 89.174 o -14 5 10 648.954 632.043 85.193 59.196 o -14 5 11 1237.490 1098.500 93.300 38.346 o -14 5 12 752.992 571.301 81.124 61.439 o -14 5 13 191.508 249.424 50.941 181.047 o -14 5 14 14.262 37.333 120.871 41.007 o -14 5 15 37.785 -30.606 54.336 198.741 o -14 5 16 133.359 97.431 61.245 145.220 o -14 5 17 576.033 676.753 79.785 66.342 o -14 5 18 375.765 372.297 82.414 73.050 o -14 5 19 822.498 727.475 86.681 52.903 o -14 5 20 84.828 23.366 93.868 66.788 o -14 5 21 77.743 -33.568 78.111 96.129 o -14 5 22 10.505 -27.854 62.014 155.648 o -14 6 1 2844.410 2983.580 123.699 13.573 o -14 6 2 21.632 109.969 59.863 160.900 o -14 6 3 616.524 623.379 73.434 73.814 o -14 6 4 87.079 79.766 48.406 230.611 o -14 6 5 451.605 441.941 65.008 99.664 o -14 6 6 114.827 154.640 63.351 135.838 o -14 6 7 3343.420 3233.900 108.413 12.446 o -14 6 8 9.599 106.961 55.954 184.666 o -14 6 9 1706.750 1914.690 99.271 26.361 o -14 6 10 28.870 47.771 54.569 195.123 o -14 6 11 13.492 43.748 58.379 172.991 o -14 6 12 41.384 17.190 60.415 160.453 o -14 6 13 1346.860 1514.800 87.179 36.338 o -14 6 14 62.941 84.788 81.915 86.856 o -14 6 15 1659.350 1579.150 102.046 27.651 o -14 6 16 27.716 125.746 60.621 155.847 o -14 6 17 442.794 384.280 89.453 62.127 o -14 6 18 3.671 -65.039 65.039 142.025 o -14 6 19 180.191 181.339 82.656 80.854 o -14 6 20 67.843 123.597 107.611 50.774 o -14 6 21 871.367 898.111 108.713 36.896 o -14 7 1 10.236 26.446 59.202 169.454 o -14 7 2 262.317 203.656 46.715 197.911 o -14 7 3 710.663 776.987 87.988 53.657 o -14 7 4 1388.080 1586.890 125.877 23.768 o -14 7 5 1509.170 1733.760 83.016 33.970 o -14 7 6 758.748 759.297 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5 295.963 254.177 68.093 106.302 o -13 1 6 2560.180 2878.590 135.918 13.744 o -13 1 7 2295.680 2560.750 228.473 8.224 o -13 1 8 2666.740 2615.610 121.675 15.101 o -13 1 9 1305.010 1406.190 78.162 41.648 o -13 1 10 200.630 229.653 46.240 210.044 o -13 1 11 24.465 42.197 54.261 198.230 o -13 1 12 977.140 1099.820 81.421 49.452 o -13 1 13 691.267 688.670 77.288 65.594 o -13 1 14 2796.360 2834.310 118.091 14.467 o -13 1 15 602.844 732.687 68.153 79.493 o -13 1 16 1399.670 1366.410 85.998 37.110 o -13 1 17 142.064 176.514 47.715 216.002 o -13 1 18 68.377 199.511 47.623 228.962 o -13 1 19 6.013 -7.578 54.944 198.572 o -13 1 20 599.422 563.075 66.338 86.279 o -13 1 21 488.963 683.253 70.707 81.534 o -13 1 22 590.999 674.874 104.420 44.040 o -13 1 23 390.280 257.851 70.358 96.100 o -13 1 24 36.587 26.730 76.651 100.703 o -13 1 25 3.378 -57.806 68.652 127.506 o -13 1 26 51.738 152.894 122.671 39.289 o -13 2 1 1030.910 1054.850 81.157 48.953 o -13 2 2 68.370 86.960 51.378 209.496 o -13 2 3 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1288.400 111.349 31.105 o -13 3 2 2123.400 2194.310 98.990 21.931 o -13 3 3 137.003 154.154 54.757 173.533 o -13 3 4 13.311 -18.007 52.333 217.649 o -13 3 5 566.734 664.743 69.261 80.862 o -13 3 6 1284.470 1348.090 71.245 45.924 o -13 3 7 1147.170 1152.340 74.897 49.202 o -13 3 8 1909.210 1910.410 121.868 20.450 o -13 3 9 227.318 147.549 52.417 175.109 o -13 3 10 356.316 334.399 57.402 130.250 o -13 3 11 30.026 -5.934 41.678 334.910 o -13 3 12 76.068 78.056 53.059 196.968 o -13 3 13 766.529 928.569 84.628 53.594 o -13 3 14 781.547 693.879 72.193 68.273 o -13 3 15 378.828 358.868 61.556 115.205 o -13 3 16 1406.140 1363.340 90.108 35.457 o -13 3 17 153.567 237.643 66.218 120.367 o -13 3 18 30.544 -32.328 49.527 239.401 o -13 3 19 164.977 148.099 47.802 213.714 o -13 3 20 80.646 71.802 58.583 163.746 o -13 3 21 363.750 326.124 69.136 98.406 o -13 3 22 480.481 469.847 65.588 96.089 o -13 3 23 258.226 310.882 63.188 120.592 o -13 3 24 309.935 245.085 67.745 106.678 o -13 3 25 13.699 46.412 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14.247 o -12 5 12 849.048 848.552 73.530 62.212 o -12 5 13 711.872 860.762 75.654 64.107 o -12 5 14 224.499 233.902 62.658 127.430 o -12 5 15 232.420 342.981 55.154 150.010 o -12 5 16 321.952 379.995 52.779 147.670 o -12 5 17 1882.950 1943.820 85.318 27.634 o -12 5 18 843.101 984.914 85.267 50.843 o -12 5 19 1073.960 1204.340 82.246 45.875 o -12 5 20 103.391 14.395 52.232 203.428 o -12 5 21 80.108 77.619 57.997 166.604 o -12 5 22 130.360 64.442 65.737 128.898 o -12 5 23 377.681 426.989 70.899 91.639 o -12 5 24 410.953 451.876 85.471 66.892 o -12 5 25 694.024 653.171 84.052 58.984 o -12 6 1 1928.990 2016.560 77.465 28.411 o -12 6 2 384.111 463.115 53.112 135.493 o -12 6 3 520.925 458.730 58.614 109.002 o -12 6 4 1.390 9.530 49.569 243.723 o -12 6 5 3787.280 3643.090 139.217 9.296 o -12 6 6 370.775 424.655 56.516 127.818 o -12 6 7 3163.740 3108.510 112.863 12.998 o -12 6 8 471.720 481.791 67.143 93.165 o -12 6 9 626.128 566.733 72.420 75.882 o -12 6 10 157.696 168.910 43.164 250.569 o 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55.061 191.556 o -12 8 12 1322.380 1343.520 82.780 39.842 o -12 8 13 7.448 13.015 52.722 214.380 o -12 8 14 1178.120 1197.370 78.827 45.783 o -12 8 15 202.094 150.409 62.491 132.772 o -12 8 16 118.761 25.110 78.441 93.604 o -12 8 17 167.903 84.448 64.192 131.379 o -12 8 18 112.032 157.302 72.663 105.703 o -12 8 19 48.987 87.738 67.771 125.787 o -12 8 20 535.417 631.018 133.378 29.721 o -12 8 21 28.758 90.721 78.344 95.690 o -12 8 22 439.163 364.704 81.763 72.286 o -12 9 1 186.721 222.109 52.545 174.867 o -12 9 2 571.317 505.703 84.417 63.458 o -12 9 3 1050.410 1049.850 87.836 44.533 o -12 9 4 293.886 340.783 65.401 110.977 o -12 9 5 974.285 757.097 82.660 52.406 o -12 9 6 4.382 117.481 57.033 178.001 o -12 9 7 3.167 18.213 58.527 174.455 o -12 9 8 248.927 243.575 66.282 114.194 o -12 9 9 303.351 360.329 69.011 100.879 o -12 9 10 810.329 787.462 55.913 85.124 o -12 9 11 618.864 571.972 73.106 75.110 o -12 9 12 108.716 63.257 61.927 145.662 o -12 9 13 94.569 69.529 59.142 159.651 o -12 9 14 23.565 -62.464 62.464 152.412 o -12 9 15 79.875 84.903 60.852 152.003 o -12 9 16 338.259 392.225 65.146 107.401 o -12 9 17 494.512 503.828 79.387 71.866 o -12 9 18 189.500 211.056 75.370 94.712 o -12 9 19 344.661 342.571 90.386 63.537 o -12 9 20 76.336 115.638 72.223 109.444 o -12 10 1 699.187 664.216 60.800 87.475 o -12 10 2 63.658 43.566 51.394 213.653 o -12 10 3 205.244 112.672 56.698 158.284 o -12 10 4 78.124 60.208 57.290 171.597 o -12 10 5 523.467 575.965 97.400 51.016 o -12 10 6 20.963 -5.657 82.041 88.862 o -12 10 7 1203.240 1104.060 125.224 26.762 o -12 10 8 43.163 68.438 61.710 151.725 o -12 10 9 616.573 531.998 79.451 67.671 o -12 10 10 14.905 39.464 72.011 114.525 o -12 10 11 14.964 99.667 64.463 140.376 o -12 10 12 19.096 -51.714 51.714 221.885 o -12 10 13 679.393 487.540 66.338 84.275 o -12 10 14 64.879 99.117 61.530 149.533 o -12 10 15 519.071 602.008 80.244 68.534 o -12 10 16 63.263 68.953 66.236 131.134 o -12 10 17 84.455 104.533 70.222 115.297 o -12 10 18 1.174 -20.941 126.175 37.795 o -12 11 1 168.724 134.417 62.684 135.162 o -12 11 2 669.756 760.144 99.529 45.704 o -12 11 3 312.677 333.503 60.457 124.192 o -12 11 4 1112.590 998.899 87.036 44.337 o -12 11 5 276.959 391.205 70.588 97.811 o -12 11 6 230.326 297.423 63.239 122.841 o -12 11 7 93.844 120.460 65.125 131.710 o -12 11 8 138.416 47.444 67.151 123.935 o -12 11 9 194.527 177.898 68.382 113.131 o -12 11 10 1039.780 1183.400 97.971 38.323 o -12 11 11 401.556 516.315 82.288 70.470 o -12 11 12 586.145 805.080 91.816 52.625 o -12 11 13 4.916 79.028 79.781 93.241 o -12 11 14 1.832 19.500 60.906 161.236 o -12 11 15 104.431 128.008 84.219 80.736 o -12 11 16 226.927 136.843 66.868 116.956 o -12 12 1 135.759 80.247 70.708 111.899 o -12 12 2 55.945 40.988 68.823 122.999 o -12 12 3 116.038 52.352 72.454 108.425 o -12 12 4 452.059 396.462 80.529 73.200 o -12 12 5 3.249 24.127 68.050 129.110 o -12 12 6 1324.070 1323.370 113.376 28.584 o -12 12 7 143.633 248.323 70.891 106.917 o -12 12 8 450.383 542.887 79.321 72.719 o -12 12 9 245.988 241.463 73.570 95.855 o -12 12 10 3.773 134.706 71.215 115.364 o -12 12 11 1.866 -56.710 56.710 186.914 o -12 12 12 460.260 361.247 76.665 79.370 o -11 0 2 8710.390 8167.350 262.086 2.208 o -11 0 4 2241.360 2416.510 244.327 7.574 o -11 0 6 911.916 790.812 69.477 65.016 o -11 0 8 6505.780 6487.570 175.507 3.914 o -11 0 10 3459.260 3600.560 162.368 8.997 o -11 0 12 65.162 54.937 56.978 175.071 o -11 0 14 2024.400 2186.620 134.827 17.240 o -11 0 16 4189.000 3740.370 169.222 7.465 o -11 0 18 806.897 942.202 149.932 22.482 o -11 0 20 16.202 78.352 83.728 84.495 o -11 0 22 555.617 778.805 163.690 20.316 o -11 0 24 842.240 778.938 113.138 35.670 o -11 0 26 36.904 0.069 102.367 57.027 o -11 0 28 132.644 73.772 116.290 43.336 o -11 1 1 431.521 406.147 55.689 125.772 o -11 1 2 74.853 48.199 56.513 177.083 o -11 1 3 912.321 791.372 86.085 50.815 o -11 1 4 3934.480 3854.150 236.248 5.741 o -11 1 5 2171.220 2003.540 83.737 24.839 o -11 1 6 4952.910 4719.780 151.108 6.296 o -11 1 7 2154.120 2165.790 75.548 25.611 o -11 1 8 1016.080 880.784 65.555 63.553 o -11 1 9 29.741 6.092 40.223 357.511 o -11 1 10 7.043 -26.673 37.977 413.299 o -11 1 11 535.449 536.064 54.394 114.877 o -11 1 12 2131.190 2132.660 96.825 22.447 o -11 1 13 2587.730 2820.870 87.089 18.302 o -11 1 14 1768.760 1932.250 82.956 29.482 o -11 1 15 717.111 737.308 70.521 71.738 o -11 1 16 1191.310 1373.530 83.560 41.458 o -11 1 17 521.616 533.695 64.171 94.888 o -11 1 18 422.129 423.925 68.835 93.736 o -11 1 19 654.100 702.751 74.922 69.265 o -11 1 20 1073.230 1276.930 97.476 37.480 o -11 1 21 1088.340 972.400 83.492 47.145 o -11 1 22 169.854 211.058 70.476 107.667 o -11 1 23 10.260 -9.230 71.857 116.095 o -11 1 24 17.977 -19.006 70.503 120.209 o -11 1 25 98.371 92.903 69.577 116.906 o -11 1 26 226.643 229.435 124.602 36.871 o -11 1 27 254.242 302.699 95.129 60.035 o -11 1 28 200.856 346.933 89.555 67.567 o -11 1 29 117.619 138.022 74.764 100.408 o -11 2 1 4162.440 4274.720 122.417 8.514 o -11 2 2 116.143 35.743 51.691 203.709 o -11 2 3 12649.000 12342.400 210.352 1.286 o -11 2 4 615.984 543.183 55.459 106.030 o -11 2 5 1752.830 1690.010 80.982 31.638 o -11 2 6 55.335 65.147 35.655 414.457 o -11 2 7 1065.450 1044.120 57.579 65.559 o -11 2 8 261.384 257.641 42.144 222.300 o -11 2 9 8452.690 8217.440 131.880 2.807 o -11 2 10 928.856 1008.440 64.503 65.323 o -11 2 11 4830.480 5042.470 121.861 6.816 o -11 2 12 99.543 171.160 48.766 216.603 o -11 2 13 219.440 258.843 40.893 241.794 o -11 2 14 0.372 -1.529 39.375 387.972 o -11 2 15 1839.100 2022.220 105.486 23.519 o -11 2 16 23.592 70.805 50.039 229.401 o -11 2 17 4739.190 5047.160 177.492 5.822 o -11 2 18 154.066 207.774 58.379 150.964 o -11 2 19 1198.390 1050.280 88.153 41.810 o -11 2 20 3.968 -66.284 66.284 136.729 o -11 2 21 100.451 128.800 73.717 103.992 o -11 2 22 28.056 30.172 61.162 157.236 o -11 2 23 1777.760 1744.500 109.932 24.120 o -11 2 24 66.948 79.150 73.142 108.024 o -11 2 25 859.133 1073.870 95.714 42.905 o -11 2 26 0.876 67.079 95.120 66.012 o -11 2 27 364.241 308.034 90.332 63.555 o -11 2 28 6.514 150.255 80.770 89.939 o -11 3 1 3621.200 3466.700 107.021 11.298 o -11 3 2 796.791 689.258 68.080 72.549 o -11 3 3 47.035 10.231 37.958 389.262 o -11 3 4 934.499 936.112 58.708 72.121 o -11 3 5 3861.780 3590.250 87.923 11.191 o -11 3 6 3185.440 3292.710 94.495 13.708 o -11 3 7 3632.790 3470.780 96.624 11.723 o -11 3 8 4349.400 4282.050 87.263 9.070 o -11 3 9 450.871 491.320 52.500 129.383 o -11 3 10 21.207 -44.449 44.449 298.254 o -11 3 11 622.845 747.609 70.699 74.881 o -11 3 12 3085.980 2907.420 114.621 13.509 o -11 3 13 2601.460 2522.220 74.730 20.433 o -11 3 14 3712.810 3656.730 96.620 11.199 o -11 3 15 1564.500 1721.150 79.191 34.491 o -11 3 16 586.797 734.579 61.385 90.737 o -11 3 17 11.719 120.015 61.493 153.222 o -11 3 18 305.649 316.217 61.819 121.197 o -11 3 19 810.600 932.677 73.478 62.151 o -11 3 20 1057.340 1138.850 84.617 45.456 o -11 3 21 1721.690 1987.040 101.951 25.319 o -11 3 22 1327.280 1405.490 94.403 34.602 o -11 3 23 841.509 784.845 87.799 51.043 o -11 3 24 26.367 0.932 66.459 134.624 o -11 3 25 8.132 59.774 63.021 148.675 o -11 3 26 104.653 151.217 73.988 102.643 o -11 3 27 448.892 435.988 80.317 73.002 o -11 3 28 803.609 614.224 89.686 52.023 o -11 4 1 106.774 121.458 38.138 331.861 o -11 4 2 6682.010 6636.320 111.564 4.259 o -11 4 3 28.594 111.369 41.284 320.566 o -11 4 4 11928.700 11487.600 171.725 1.485 o -11 4 5 49.143 93.226 46.479 255.216 o -11 4 6 1022.390 1064.360 74.138 53.814 o -11 4 7 131.674 94.709 47.900 224.525 o -11 4 8 4521.110 4586.740 92.624 8.282 o -11 4 9 229.812 264.450 45.710 204.549 o -11 4 10 13313.800 13617.900 205.084 1.149 o -11 4 11 56.124 152.376 49.389 221.440 o -11 4 12 4031.760 4182.410 122.747 8.847 o -11 4 13 176.174 208.018 57.998 150.503 o -11 4 14 284.135 355.410 63.373 116.758 o -11 4 15 12.455 -47.638 47.638 262.339 o -11 4 16 2130.290 2501.840 99.228 20.779 o -11 4 17 3.226 54.980 48.799 246.376 o -11 4 18 2946.800 3019.190 118.093 13.562 o -11 4 19 77.863 233.764 58.779 155.182 o -11 4 20 1089.130 1017.330 89.275 43.325 o -11 4 21 16.758 177.686 58.981 162.740 o -11 4 22 368.635 397.793 67.292 100.429 o -11 4 23 6.545 2.766 66.998 133.603 o -11 4 24 1319.130 1362.830 93.025 35.512 o -11 4 25 0.600 -1.439 69.633 124.084 o -11 4 26 987.708 1131.620 145.209 22.483 o -11 4 27 1.093 -6.638 71.532 117.562 o -11 5 1 4028.420 3678.960 89.811 10.525 o -11 5 2 22.767 1.478 40.388 358.679 o -11 5 3 965.441 973.328 62.274 66.664 o -11 5 4 626.898 820.324 109.865 39.391 o -11 5 5 2848.370 2910.490 92.701 16.151 o -11 5 6 2266.520 2377.700 97.267 20.556 o -11 5 7 9047.090 8897.150 153.390 2.417 o -11 5 8 1529.690 1640.330 64.375 40.714 o -11 5 9 1286.560 1466.900 80.407 40.439 o -11 5 10 20.845 43.008 51.319 221.365 o -11 5 11 855.977 1037.020 82.077 52.357 o -11 5 12 2173.330 2124.710 74.818 25.744 o -11 5 13 4579.040 4394.380 106.698 8.043 o -11 5 14 799.380 917.678 68.496 67.718 o -11 5 15 1583.820 1697.050 98.273 28.812 o -11 5 16 667.986 598.145 69.307 77.949 o -11 5 17 188.624 82.667 90.869 68.654 o -11 5 18 70.052 136.065 62.862 141.831 o -11 5 19 636.253 800.183 78.832 63.894 o -11 5 20 321.231 307.432 65.828 109.209 o -11 5 21 1569.380 1555.220 92.383 31.423 o -11 5 22 442.348 497.251 71.918 85.386 o -11 5 23 239.382 220.528 63.279 124.775 o -11 5 24 45.924 155.198 65.659 131.687 o -11 5 25 20.732 41.252 77.256 99.449 o -11 5 26 120.798 51.272 78.459 93.068 o -11 5 27 322.850 349.287 75.446 86.746 o -11 6 1 7393.120 7075.930 131.783 3.554 o -11 6 2 1517.500 1558.640 79.928 36.139 o -11 6 3 4944.240 4971.150 114.333 6.844 o -11 6 4 117.582 173.190 48.617 214.219 o -11 6 5 1750.020 1666.370 85.179 30.692 o -11 6 6 192.059 151.352 58.783 148.283 o -11 6 7 1186.530 1301.480 85.477 41.235 o -11 6 8 0.541 -18.425 39.104 393.281 o -11 6 9 3569.540 3729.080 101.917 11.292 o -11 6 10 304.786 284.261 63.622 117.041 o -11 6 11 2550.980 2380.400 87.894 19.831 o -11 6 12 1573.810 1721.870 84.426 32.751 o -11 6 13 11.046 3.621 47.187 267.234 o -11 6 14 201.096 265.710 55.883 154.339 o -11 6 15 1084.600 1077.290 81.054 47.651 o -11 6 16 51.981 27.740 76.950 99.388 o -11 6 17 2069.690 2198.870 103.242 21.616 o -11 6 18 593.666 770.615 78.448 65.990 o -11 6 19 740.486 856.431 106.420 39.834 o -11 6 20 191.879 80.242 64.577 128.488 o -11 6 21 27.319 27.054 67.720 128.924 o -11 6 22 11.913 -60.508 60.508 163.321 o -11 6 23 990.720 682.796 82.797 52.768 o -11 6 24 89.176 81.819 77.176 96.603 o -11 6 25 438.445 318.839 78.862 77.338 o -11 6 26 113.256 155.357 70.655 111.317 o -11 7 1 151.906 133.118 41.368 274.595 o -11 7 2 188.419 206.599 45.129 222.778 o -11 7 3 1172.720 1106.460 73.210 50.165 o -11 7 4 1651.210 1814.660 89.055 29.946 o -11 7 5 2334.280 2366.200 100.199 19.765 o -11 7 6 2769.160 2811.060 92.499 16.821 o -11 7 7 198.853 284.396 53.858 162.819 o -11 7 8 878.193 989.377 52.818 79.822 o -11 7 9 662.508 630.230 51.421 107.384 o -11 7 10 4.069 18.680 46.452 275.514 o -11 7 11 838.613 911.398 70.494 64.460 o -11 7 12 2097.510 2108.440 129.144 17.854 o -11 7 13 542.043 444.672 65.070 94.469 o -11 7 14 1848.650 1764.380 98.738 25.887 o -11 7 15 28.407 61.380 55.989 184.920 o -11 7 16 552.826 609.394 68.207 84.332 o -11 7 17 782.252 887.339 120.350 32.480 o -11 7 18 328.197 392.728 81.213 75.945 o -11 7 19 435.770 658.912 87.250 61.711 o -11 7 20 1402.550 1261.310 102.085 31.804 o -11 7 21 46.792 11.671 64.183 142.416 o -11 7 22 739.475 606.568 88.953 54.002 o -11 7 23 40.066 154.150 152.566 25.586 o -11 7 24 45.531 137.960 121.667 40.009 o -11 7 25 176.700 312.627 87.279 71.716 o -11 8 1 80.081 9.084 44.792 276.050 o -11 8 2 3367.580 3275.160 97.452 12.894 o -11 8 3 586.158 582.330 52.756 112.624 o -11 8 4 739.335 837.992 66.180 74.154 o -11 8 5 310.175 285.788 52.586 155.204 o -11 8 6 404.650 428.648 80.675 73.931 o -11 8 7 345.164 544.720 58.829 118.285 o -11 8 8 1930.210 1810.590 66.536 32.067 o -11 8 9 89.353 87.043 47.915 233.657 o -11 8 10 1700.650 1740.850 89.850 29.597 o -11 8 11 227.736 202.617 55.033 158.712 o -11 8 12 60.577 31.050 51.700 212.769 o -11 8 13 297.433 383.761 77.525 83.230 o -11 8 14 573.831 741.735 77.931 67.621 o -11 8 15 200.449 153.909 61.434 136.716 o -11 8 16 1467.300 1339.350 94.983 33.069 o -11 8 17 124.671 74.350 61.971 143.755 o -11 8 18 582.186 545.964 85.773 61.209 o -11 8 19 304.814 341.003 86.062 70.098 o -11 8 20 7.117 108.929 76.923 99.603 o -11 8 21 320.805 535.957 153.002 24.128 o -11 8 22 261.213 225.892 97.332 58.090 o -11 8 23 3.896 -18.301 71.772 116.655 o -11 8 24 471.189 530.729 116.624 38.485 o -11 9 1 689.262 703.581 60.805 86.947 o -11 9 2 18.638 -24.404 45.173 289.667 o -11 9 3 224.293 158.538 54.959 161.942 o -11 9 4 878.225 1023.300 82.638 51.598 o -11 9 5 1751.200 1788.380 92.196 28.215 o -11 9 6 494.715 469.553 68.672 89.463 o -11 9 7 1138.750 980.846 87.713 43.653 o -11 9 8 4.023 -44.107 44.107 308.088 o -11 9 9 136.049 139.119 71.117 109.284 o -11 9 10 252.189 324.307 64.741 115.930 o -11 9 11 157.544 208.882 61.933 136.026 o -11 9 12 1217.530 1066.800 82.810 44.127 o -11 9 13 1087.530 985.311 81.780 48.096 o -11 9 14 448.166 571.859 97.308 52.347 o -11 9 15 566.230 554.143 77.838 70.897 o -11 9 16 1.127 -16.661 68.378 128.653 o -11 9 17 3.278 -18.921 67.025 133.769 o -11 9 18 244.764 220.531 72.997 97.661 o -11 9 19 290.885 261.769 85.992 71.510 o -11 9 20 535.107 420.953 104.116 46.620 o -11 9 21 368.341 287.528 89.637 64.537 o -11 9 22 81.994 35.468 84.169 82.542 o -11 10 1 1306.490 1324.130 71.219 45.718 o -11 10 2 86.241 68.192 48.126 234.369 o -11 10 3 1781.220 1758.880 95.439 27.285 o -11 10 4 59.640 74.112 69.180 120.708 o -11 10 5 382.240 402.258 72.531 88.815 o -11 10 6 45.386 134.983 74.882 103.003 o -11 10 7 174.985 220.214 69.256 110.544 o -11 10 8 3.839 50.831 61.243 157.993 o -11 10 9 1432.820 1410.570 89.331 35.062 o -11 10 10 8.385 -24.084 56.766 185.803 o -11 10 11 1981.380 1766.980 90.847 26.356 o -11 10 12 19.905 13.752 54.907 196.149 o -11 10 13 53.858 135.116 73.443 106.552 o -11 10 14 5.222 59.473 73.712 109.352 o -11 10 15 365.042 359.243 76.483 83.108 o -11 10 16 3.970 78.852 73.246 110.378 o -11 10 17 841.100 871.409 100.662 41.745 o -11 10 18 74.442 145.168 75.244 100.747 o -11 10 19 471.058 481.450 127.860 32.891 o -11 10 20 2.208 -57.660 81.060 91.527 o -11 11 1 171.739 239.091 57.840 150.111 o -11 11 2 125.780 133.947 59.359 152.668 o -11 11 3 20.789 29.998 55.739 189.343 o -11 11 4 316.657 386.800 62.361 116.340 o -11 11 5 785.000 855.488 78.624 59.203 o -11 11 6 1258.290 1382.390 147.933 20.156 o -11 11 7 459.005 643.014 76.284 75.090 o -11 11 8 978.855 888.353 68.663 61.941 o -11 11 9 164.885 230.688 62.566 132.279 o -11 11 10 37.993 130.913 61.235 151.812 o -11 11 11 230.509 150.082 58.172 147.326 o -11 11 12 1025.000 1105.510 87.672 44.585 o -11 11 13 369.635 229.811 85.719 70.354 o -11 11 14 731.327 696.774 80.852 60.625 o -11 11 15 235.088 358.996 77.307 86.260 o -11 11 16 55.166 44.923 75.591 102.472 o -11 11 17 4.918 0.722 74.197 109.109 o -11 11 18 35.721 85.373 76.302 100.594 o -11 12 1 5.943 22.927 54.073 203.425 o -11 12 2 1136.980 1196.480 80.101 45.918 o -11 12 3 73.483 53.924 55.245 184.604 o -11 12 4 580.681 658.444 68.390 81.713 o -11 12 5 74.929 84.704 60.971 151.881 o -11 12 6 37.744 69.934 65.949 133.805 o -11 12 7 19.224 38.736 61.498 155.936 o -11 12 8 768.026 901.805 117.040 33.980 o -11 12 9 200.271 329.019 97.181 58.402 o -11 12 10 1435.720 1444.320 104.945 29.603 o -11 12 11 85.741 91.807 69.722 117.125 o -11 12 12 320.054 182.367 80.077 81.291 o -11 12 13 4.951 107.360 72.227 112.793 o -11 12 14 62.085 29.424 74.698 104.902 o -11 12 15 94.068 194.453 76.340 96.402 o -11 13 1 738.837 716.197 83.422 57.735 o -11 13 2 16.193 14.483 67.593 130.389 o -11 13 3 1.616 -78.650 125.582 38.151 o -11 13 4 78.575 123.040 92.698 67.703 o -11 13 5 707.596 645.524 106.134 41.666 o -11 13 6 160.300 156.255 69.855 111.257 o -11 13 7 1228.940 1200.420 96.970 36.160 o -11 13 8 0.747 -65.687 65.687 139.426 o -11 13 9 266.735 311.273 76.571 87.397 o -11 13 10 64.088 185.500 64.455 134.069 o -11 13 11 108.853 272.378 88.663 71.584 o -10 0 2 4787.090 4260.390 223.216 5.204 o -10 0 4 9597.110 9433.380 363.681 1.567 o -10 0 6 6329.820 6180.110 193.183 3.941 o -10 0 8 390.396 530.023 80.531 73.043 o -10 0 10 7564.120 7488.050 160.214 3.209 o -10 0 12 19901.800 19090.000 451.134 0.498 o -10 0 14 6909.320 6995.220 202.347 3.350 o -10 0 16 978.325 1136.150 106.570 35.400 o -10 0 18 1435.770 1442.130 124.742 24.199 o -10 0 20 3795.600 4169.060 196.706 6.840 o -10 0 22 121.783 69.695 96.877 61.921 o -10 0 24 69.572 244.133 97.381 60.796 o -10 0 26 1034.210 882.753 162.471 19.004 o -10 0 28 367.373 180.145 118.154 39.893 o -10 0 30 18.808 -100.741 100.741 59.081 o -10 1 1 5350.260 5398.030 131.524 5.795 o -10 1 2 3544.050 3580.220 101.914 11.590 o -10 1 3 3391.480 3304.150 114.977 11.825 o -10 1 4 1117.500 1043.160 61.145 60.875 o -10 1 5 38.513 20.686 47.465 255.940 o -10 1 6 573.045 704.482 53.749 106.747 o -10 1 7 851.987 842.429 50.856 87.823 o -10 1 8 3788.850 3882.000 89.371 10.926 o -10 1 9 2267.210 2517.130 96.882 20.143 o -10 1 10 3030.540 3143.690 93.568 14.709 o -10 1 11 311.894 354.501 45.347 183.678 o -10 1 12 16.703 -38.083 38.083 405.701 o -10 1 13 3.058 -37.418 37.418 427.990 o -10 1 14 1260.080 1588.280 88.908 36.384 o -10 1 15 2759.370 2696.580 97.462 16.726 o -10 1 16 4742.360 4751.080 125.601 7.074 o -10 1 17 721.189 820.002 74.993 65.139 o -10 1 18 434.382 407.301 77.020 78.902 o -10 1 19 621.497 615.303 73.438 73.776 o -10 1 20 0.799 25.524 57.511 180.489 o -10 1 21 749.064 698.654 77.563 63.437 o -10 1 22 497.926 585.974 78.781 71.304 o -10 1 23 1337.130 1503.430 103.049 30.894 o -10 1 24 579.942 731.429 86.384 58.470 o -10 1 25 591.990 609.942 90.623 55.469 o -10 1 26 100.808 83.736 74.499 102.836 o -10 1 27 13.523 51.745 69.117 123.929 o -10 1 28 41.605 117.187 86.249 78.705 o -10 1 29 303.759 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2446.710 2976.780 107.959 16.586 o -10 3 19 222.368 216.155 60.041 137.655 o -10 3 20 142.663 197.999 69.791 111.274 o -10 3 21 23.318 42.994 57.539 176.960 o -10 3 22 409.386 547.356 76.008 78.919 o -10 3 23 848.630 955.620 87.146 49.670 o -10 3 24 1476.770 1497.790 130.186 22.521 o -10 3 25 643.796 626.140 104.080 43.901 o -10 3 26 414.893 325.005 74.328 85.721 o -10 3 27 9.002 -49.082 63.161 150.187 o -10 3 28 109.823 113.070 80.507 88.013 o -10 3 29 172.466 174.173 87.689 72.755 o -10 4 1 168.081 209.594 41.434 257.958 o -10 4 2 630.076 690.622 59.126 93.349 o -10 4 3 5.363 -39.707 39.707 379.157 o -10 4 4 6950.520 6939.070 132.210 3.845 o -10 4 5 160.753 359.999 52.758 168.190 o -10 4 6 15304.000 15242.400 201.071 0.913 o -10 4 7 281.645 333.669 48.591 173.942 o -10 4 8 4732.360 4352.610 105.944 7.825 o -10 4 9 53.334 80.156 42.824 296.963 o -10 4 10 119.828 111.899 46.380 237.925 o -10 4 11 428.476 285.912 40.091 195.145 o -10 4 12 7354.320 7315.630 116.641 3.589 o -10 4 13 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88.683 70.093 o -10 8 24 44.136 6.388 76.187 102.006 o -10 8 25 50.163 59.995 67.080 129.035 o -10 9 1 1470.950 1296.180 74.488 41.201 o -10 9 2 204.230 309.156 51.323 173.033 o -10 9 3 1526.930 1591.340 86.722 33.498 o -10 9 4 7.245 -52.843 52.843 214.415 o -10 9 5 46.937 26.746 49.508 233.870 o -10 9 6 362.638 394.182 53.444 140.102 o -10 9 7 612.676 648.940 65.823 84.419 o -10 9 8 986.127 1278.810 79.671 48.455 o -10 9 9 3156.130 3100.290 141.173 11.281 o -10 9 10 634.619 645.639 78.433 66.648 o -10 9 11 481.645 390.659 81.140 71.549 o -10 9 12 5.042 2.398 60.979 161.311 o -10 9 13 15.928 35.849 64.444 142.585 o -10 9 14 833.748 747.705 85.317 53.547 o -10 9 15 1223.320 1366.730 95.385 35.808 o -10 9 16 808.421 882.419 96.112 44.936 o -10 9 17 1562.880 1739.570 124.315 22.551 o -10 9 18 143.292 103.558 68.585 117.361 o -10 9 19 275.637 298.857 85.070 72.791 o -10 9 20 176.847 186.039 77.895 90.141 o -10 9 21 40.748 14.199 73.887 108.323 o -10 9 22 250.112 124.406 114.514 43.507 o 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102.138 o -10 11 1 607.725 564.389 67.531 83.937 o -10 11 2 1769.810 2015.180 98.802 25.466 o -10 11 3 519.996 644.396 68.882 83.932 o -10 11 4 707.221 815.254 84.865 56.009 o -10 11 5 118.342 86.818 57.003 167.400 o -10 11 6 34.492 25.522 41.745 327.469 o -10 11 7 198.044 251.381 67.228 114.224 o -10 11 8 1215.290 1085.820 78.223 46.502 o -10 11 9 1005.870 1065.200 81.263 49.310 o -10 11 10 1446.580 1542.020 87.101 34.777 o -10 11 11 381.118 444.089 66.969 99.234 o -10 11 12 67.249 7.697 56.910 177.855 o -10 11 13 23.670 130.522 61.455 151.981 o -10 11 14 259.578 258.089 66.917 111.350 o -10 11 15 401.459 371.815 74.584 84.871 o -10 11 16 494.166 621.926 85.401 62.823 o -10 11 17 533.143 480.418 85.350 63.658 o -10 11 18 284.131 170.861 77.326 87.819 o -10 11 19 24.578 11.326 70.440 119.832 o -10 11 20 8.160 154.030 73.183 108.813 o -10 12 1 92.241 138.965 54.749 180.019 o -10 12 2 32.972 164.721 63.156 142.295 o -10 12 3 15.659 101.011 55.374 188.019 o -10 12 4 1806.450 1893.020 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569.824 81.499 66.513 o -10 13 12 19.621 22.312 74.749 106.536 o -10 13 13 2.668 -5.045 74.359 108.736 o -10 13 14 56.259 55.915 111.906 47.401 o -10 14 1 47.706 24.943 70.500 118.182 o -10 14 2 111.028 177.623 73.838 102.218 o -10 14 3 139.028 118.945 70.607 111.087 o -10 14 4 12.553 -40.463 68.183 128.761 o -10 14 5 785.793 546.388 85.230 56.964 o -10 14 6 332.114 463.666 83.376 71.606 o -10 14 7 333.500 354.430 80.752 77.088 o -10 14 8 311.717 376.030 87.055 68.148 o -10 14 9 1.280 -81.945 187.612 17.096 o -9 0 2 9035.070 8726.540 374.551 1.659 o -9 0 4 255.285 184.744 47.729 194.667 o -9 0 6 285.279 160.319 63.326 123.516 o -9 0 8 22267.500 22706.100 372.103 0.418 o -9 0 10 6932.960 6664.790 156.225 3.770 o -9 0 12 75.164 -57.115 57.115 176.189 o -9 0 14 6930.100 6661.320 175.742 3.625 o -9 0 16 2097.290 2075.700 130.232 17.783 o -9 0 18 2642.600 3004.370 227.743 7.641 o -9 0 20 10.117 48.561 88.170 76.734 o -9 0 22 3275.860 3358.210 195.641 8.045 o -9 0 24 1672.940 1761.490 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60.730 o 8 4 7 123.569 146.488 50.249 203.794 o 8 4 8 7348.090 6728.650 138.406 3.636 o 8 4 9 150.164 158.745 48.703 209.003 o 8 4 10 11946.300 11993.900 173.050 1.444 o 8 4 11 54.741 97.917 36.477 389.365 o 8 4 12 1505.200 1675.560 85.100 33.751 o 8 4 13 160.526 124.802 36.744 326.836 o 8 4 14 664.268 682.420 48.880 110.134 o 8 4 15 209.349 223.957 58.779 143.370 o 8 4 16 2366.300 2403.040 70.977 23.204 o 8 4 17 20.890 38.053 35.081 459.152 o 8 4 18 2167.620 2017.720 91.501 23.489 o 8 4 19 26.947 75.522 45.298 275.641 o 8 4 20 281.516 285.032 54.740 149.556 o 8 4 21 11.500 14.694 55.389 193.800 o 8 4 22 677.840 842.383 135.086 27.705 o 8 4 23 10.176 200.015 84.407 81.835 o 8 4 24 1365.480 1365.410 187.346 13.773 o 8 4 25 68.019 119.321 106.761 51.586 o 8 5 0 12111.100 11648.100 155.741 1.465 o 8 5 1 2261.500 2585.090 80.885 22.039 o 8 5 2 1118.940 1248.270 60.313 58.017 o 8 5 3 1049.100 1190.040 57.328 63.605 o 8 5 4 1141.070 1196.770 56.993 60.406 o 8 5 5 1904.100 1844.330 86.082 27.765 o 8 5 6 5759.810 5941.450 96.683 5.485 o 8 5 7 4233.820 4126.650 79.074 9.720 o 8 5 8 3180.580 3057.620 86.627 14.692 o 8 5 9 1751.110 1673.030 66.052 35.932 o 8 5 10 3.280 -4.891 34.008 517.469 o 8 5 11 510.330 520.695 46.547 139.118 o 8 5 12 1043.700 1219.410 60.856 60.603 o 8 5 13 2052.920 1931.340 73.949 28.203 o 8 5 14 756.259 871.262 51.386 92.183 o 8 5 15 1663.110 1722.640 74.781 34.386 o 8 5 16 41.645 -20.484 39.376 368.308 o 8 5 17 585.867 527.176 51.048 118.958 o 8 5 18 179.806 220.185 36.477 302.336 o 8 5 19 389.803 368.691 73.266 87.812 o 8 5 20 464.067 419.901 58.045 116.032 o 8 5 21 1015.980 1004.080 82.573 48.884 o 8 5 22 374.019 453.532 63.653 107.017 o 8 5 23 333.968 303.149 62.315 118.180 o 8 5 24 9.928 78.581 68.855 124.334 o 8 5 25 7.174 103.966 71.221 115.903 o 8 6 0 92.529 119.024 38.022 340.211 o 8 6 1 4795.870 4485.060 93.324 7.854 o 8 6 2 224.966 224.061 38.980 261.201 o 8 6 3 6230.000 6204.750 106.561 4.823 o 8 6 4 635.219 593.883 51.441 110.987 o 8 6 5 4057.370 3841.530 91.852 10.167 o 8 6 6 1.001 -26.769 33.738 527.800 o 8 6 7 164.208 218.883 46.278 218.058 o 8 6 8 11.562 18.943 40.258 362.004 o 8 6 9 3744.960 3986.050 89.514 10.897 o 8 6 10 12.877 4.394 34.096 504.714 o 8 6 11 6441.050 6184.590 115.923 4.580 o 8 6 12 246.667 384.733 35.395 258.974 o 8 6 13 432.934 448.211 45.633 156.651 o 8 6 14 5.944 12.270 41.148 350.503 o 8 6 15 265.428 250.870 52.261 164.241 o 8 6 16 191.039 197.717 43.743 233.850 o 8 6 17 2509.060 2576.770 87.925 19.459 o 8 6 18 193.462 115.966 54.990 167.832 o 8 6 19 1248.620 1283.910 70.002 48.105 o 8 6 20 2.104 10.971 69.874 122.884 o 8 6 21 67.154 21.128 49.439 231.182 o 8 6 22 74.079 67.579 70.346 116.341 o 8 6 23 284.281 298.916 100.495 53.950 o 8 6 24 4.735 5.131 69.169 125.409 o 8 7 0 6151.670 6401.230 140.351 4.505 o 8 7 1 1053.670 1112.220 60.765 62.182 o 8 7 2 70.838 50.228 36.989 384.224 o 8 7 3 614.019 640.163 52.377 108.879 o 8 7 4 140.056 163.085 39.677 291.826 o 8 7 5 5656.710 5216.030 93.807 6.041 o 8 7 6 4160.950 3929.610 121.086 8.895 o 8 7 7 1632.700 1777.450 67.990 36.453 o 8 7 8 2510.650 2482.370 81.195 20.524 o 8 7 9 1302.160 1296.980 55.441 54.446 o 8 7 10 6.268 50.463 33.069 520.420 o 8 7 11 52.038 66.057 40.232 335.591 o 8 7 12 1205.710 1291.830 62.091 53.591 o 8 7 13 864.429 962.755 54.976 78.786 o 8 7 14 2541.770 2454.140 72.809 21.338 o 8 7 15 1638.880 1742.370 60.280 38.988 o 8 7 16 931.507 999.591 60.511 69.136 o 8 7 17 400.345 454.473 64.798 102.715 o 8 7 18 220.235 245.777 49.074 187.516 o 8 7 19 67.611 72.223 38.044 362.008 o 8 7 20 756.359 821.748 47.194 100.246 o 8 7 21 249.876 368.060 62.097 122.514 o 8 7 22 607.298 552.095 69.764 80.771 o 8 7 23 476.661 522.003 77.089 75.386 o 8 8 0 2252.290 2257.540 84.251 22.959 o 8 8 1 3924.600 3646.120 91.818 10.788 o 8 8 2 9301.130 9240.410 141.169 2.324 o 8 8 3 594.550 626.904 54.261 106.998 o 8 8 4 9300.550 9108.920 147.786 2.326 o 8 8 5 47.584 1.124 34.437 469.119 o 8 8 6 36.795 34.503 34.316 467.699 o 8 8 7 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2 2500.260 2552.750 112.841 16.850 o 11 4 3 146.823 242.795 39.958 273.434 o 11 4 4 8329.220 7913.480 123.829 2.946 o 11 4 5 471.837 628.500 45.063 141.722 o 11 4 6 6426.790 6090.780 110.306 4.674 o 11 4 7 173.876 270.512 52.645 172.847 o 11 4 8 189.523 205.426 52.578 175.430 o 11 4 9 16.572 -20.571 45.761 282.947 o 11 4 10 2060.020 2013.020 91.210 24.462 o 11 4 11 115.946 220.204 55.237 169.524 o 11 4 12 2880.490 2990.040 109.006 14.546 o 11 4 13 137.394 132.009 51.260 195.937 o 11 4 14 512.496 542.392 49.351 129.633 o 11 4 15 17.335 68.941 40.879 338.933 o 11 4 16 11.498 -24.578 48.913 249.171 o 11 4 17 60.921 28.994 56.138 182.063 o 11 4 18 830.635 1026.520 86.493 49.786 o 11 4 19 40.570 83.012 53.641 197.595 o 11 4 20 841.230 671.364 101.618 42.542 o 11 4 21 14.056 21.526 67.409 131.018 o 11 5 0 1873.100 1886.890 76.205 30.101 o 11 5 1 7945.840 7552.960 140.753 3.120 o 11 5 2 1993.730 2181.990 96.753 23.325 o 11 5 3 2960.630 2837.750 87.281 16.198 o 11 5 4 134.726 138.421 39.928 295.093 o 11 5 5 21.823 23.098 35.191 461.137 o 11 5 6 194.982 241.113 43.915 226.606 o 11 5 7 3386.380 3275.350 88.018 13.324 o 11 5 8 1618.550 1645.670 69.922 37.183 o 11 5 9 2636.650 2752.420 99.978 16.976 o 11 5 10 465.623 487.543 63.049 101.739 o 11 5 11 765.405 659.509 67.392 75.242 o 11 5 12 108.154 165.765 52.773 188.106 o 11 5 13 948.210 943.156 55.009 75.126 o 11 5 14 233.445 268.674 48.257 188.224 o 11 5 15 1487.400 1536.470 64.404 42.601 o 11 5 16 314.935 384.860 44.617 184.249 o 11 5 17 996.614 917.684 62.092 66.704 o 11 5 18 73.880 92.995 42.851 288.221 o 11 5 19 35.522 44.999 48.711 241.671 o 11 5 20 7.500 30.941 50.171 234.826 o 11 6 0 21.421 94.987 52.603 206.993 o 11 6 1 25.186 55.210 35.479 440.797 o 11 6 2 1477.490 1535.290 63.699 43.097 o 11 6 3 1690.600 1629.290 64.153 37.893 o 11 6 4 622.572 829.496 55.158 96.276 o 11 6 5 3307.430 3178.000 98.426 13.234 o 11 6 6 142.369 103.237 41.410 281.732 o 11 6 7 2062.330 2068.960 74.671 27.205 o 11 6 8 4.621 42.952 39.207 378.711 o 11 6 9 100.608 55.228 38.085 349.942 o 11 6 10 192.555 250.751 39.849 259.231 o 11 6 11 2151.340 2032.450 85.180 24.640 o 11 6 12 377.045 422.737 52.011 142.048 o 11 6 13 2462.030 2524.760 108.594 17.574 o 11 6 14 48.683 82.485 40.941 323.326 o 11 6 15 262.167 213.363 45.757 202.951 o 11 6 16 9.260 -39.835 39.835 374.931 o 11 6 17 224.436 243.114 45.673 207.884 o 11 6 18 165.259 185.093 112.080 45.800 o 11 6 19 1161.530 1200.650 102.313 34.763 o 11 7 0 4765.840 4801.550 120.318 7.111 o 11 7 1 434.156 610.187 51.019 129.455 o 11 7 2 2685.510 2678.440 88.643 17.996 o 11 7 3 1265.590 1449.520 72.863 44.455 o 11 7 4 32.598 44.405 36.258 422.212 o 11 7 5 989.122 866.390 48.625 81.747 o 11 7 6 550.117 629.469 50.743 118.304 o 11 7 7 156.414 212.762 42.985 246.822 o 11 7 8 2394.140 2394.040 100.578 19.263 o 11 7 9 764.910 951.162 77.694 59.300 o 11 7 10 1501.210 1645.630 81.471 35.209 o 11 7 11 553.558 559.652 60.327 99.780 o 11 7 12 4.483 58.556 53.345 206.587 o 11 7 13 1.851 7.564 43.304 319.036 o 11 7 14 661.073 587.994 79.694 65.275 o 11 7 15 212.935 257.176 51.247 175.810 o 11 7 16 1034.010 978.468 77.010 52.556 o 11 7 17 227.327 273.989 73.955 95.096 o 11 7 18 173.927 200.936 85.889 75.254 o 11 8 0 981.454 1114.820 69.218 57.899 o 11 8 1 113.697 146.597 49.622 209.902 o 11 8 2 132.983 56.596 41.166 295.118 o 11 8 3 323.027 457.916 72.745 89.735 o 11 8 4 2701.390 2447.350 83.561 19.102 o 11 8 5 227.952 161.155 48.214 198.400 o 11 8 6 1297.820 1338.600 69.159 46.777 o 11 8 7 13.061 -14.352 36.798 436.128 o 11 8 8 169.024 147.796 50.717 193.330 o 11 8 9 26.508 24.277 42.156 324.506 o 11 8 10 369.220 336.269 50.391 153.998 o 11 8 11 56.865 17.322 47.477 252.092 o 11 8 12 1491.200 1420.680 60.508 45.349 o 11 8 13 29.695 70.117 35.917 423.345 o 11 8 14 953.163 816.310 54.544 78.488 o 11 8 15 5.232 119.369 104.155 54.808 o 11 8 16 0.449 -16.810 56.946 185.526 o 11 8 17 2.980 24.689 57.945 177.629 o 11 9 0 496.880 568.856 60.279 103.196 o 11 9 1 1022.820 1084.190 68.269 57.850 o 11 9 2 843.568 944.160 65.270 68.939 o 11 9 3 669.031 756.692 58.620 89.990 o 11 9 4 13.570 13.714 44.837 293.439 o 11 9 5 187.514 108.548 45.302 232.353 o 11 9 6 4.903 5.500 38.157 409.098 o 11 9 7 289.351 283.247 45.390 193.641 o 11 9 8 302.500 241.241 39.736 231.127 o 11 9 9 611.521 591.411 56.356 102.817 o 11 9 10 225.730 145.301 60.980 136.755 o 11 9 11 34.643 3.817 67.257 130.925 o 11 9 12 33.480 29.108 84.452 83.250 o 11 9 13 50.440 35.571 61.239 154.741 o 11 9 14 61.518 77.428 110.263 48.668 o 11 9 15 283.715 195.720 67.453 110.285 o 11 9 16 122.477 127.345 67.026 122.939 o 11 10 0 0.087 -41.161 64.909 142.830 o 11 10 1 17.973 -40.618 47.439 263.248 o 11 10 2 19.855 22.323 50.904 226.836 o 11 10 3 1229.210 1172.970 92.884 38.120 o 11 10 4 16.325 -17.823 51.719 222.298 o 11 10 5 780.373 658.835 57.128 88.708 o 11 10 6 2.228 -42.168 51.227 228.943 o 11 10 7 544.220 457.060 60.652 102.953 o 11 10 8 3.872 -50.543 50.543 234.876 o 11 10 9 72.732 138.219 57.330 167.787 o 11 10 10 102.778 71.241 63.269 140.110 o 11 10 11 453.564 228.077 70.339 93.857 o 11 10 12 51.100 157.354 69.433 118.145 o 11 10 13 468.887 519.906 99.464 50.564 o 11 10 14 14.421 -25.117 62.466 153.108 o 11 11 0 1037.170 1087.350 75.315 52.328 o 11 11 1 889.451 754.182 66.180 69.860 o 11 11 2 1655.120 1513.510 85.344 32.769 o 11 11 3 149.002 246.630 42.784 246.114 o 11 11 4 18.636 -20.900 57.495 180.040 o 11 11 5 2.170 -16.863 59.019 172.561 o 11 11 6 152.544 150.918 62.890 134.969 o 11 11 7 60.843 41.461 101.271 57.738 o 11 11 8 1407.920 1303.590 106.046 30.216 o 11 11 9 309.458 435.249 76.596 83.544 o 11 11 10 284.797 297.553 78.217 83.898 o 11 11 11 43.524 69.906 67.585 127.278 o 11 12 0 241.746 200.429 78.026 87.395 o 11 12 1 9.176 14.856 47.844 259.189 o 11 12 2 71.741 98.759 40.873 312.778 o 11 12 3 70.968 114.839 74.072 104.548 o 11 12 4 1150.740 1262.310 137.207 23.338 o 11 12 5 163.746 194.089 95.743 61.709 o 11 12 6 988.471 989.933 134.963 25.580 o 11 12 7 54.138 77.601 95.966 64.013 o 11 12 8 70.271 82.711 107.657 50.903 o 11 13 0 99.952 145.515 82.432 83.978 o 11 13 1 1007.700 1056.620 96.106 40.596 o 11 13 2 174.081 214.971 78.236 89.033 o 11 13 3 572.573 691.991 85.013 60.488 o 11 13 4 174.768 231.652 76.081 93.302 o 12 0 0 5208.330 5140.190 199.235 4.972 o 12 0 2 4922.420 4927.490 115.539 6.884 o 12 0 4 44.733 52.724 49.051 235.923 o 12 0 6 3407.620 3393.560 116.488 11.565 o 12 0 8 6394.150 5914.170 195.193 3.960 o 12 0 10 2823.690 2859.330 169.036 10.619 o 12 0 12 262.181 295.786 56.355 144.548 o 12 0 14 2205.620 2397.650 113.055 18.739 o 12 0 16 2136.830 1982.300 174.513 12.730 o 12 0 18 70.621 88.217 58.244 165.711 o 12 0 20 223.442 206.354 90.372 67.438 o 12 1 0 508.388 502.428 59.770 105.737 o 12 1 1 131.194 99.926 42.708 271.714 o 12 1 2 1158.100 1268.930 65.659 53.095 o 12 1 3 1907.420 1989.660 60.712 32.398 o 12 1 4 4848.480 4730.910 92.208 7.571 o 12 1 5 1460.230 1666.930 63.200 42.271 o 12 1 6 1985.610 1887.630 73.133 29.408 o 12 1 7 739.375 681.980 43.718 113.470 o 12 1 8 38.692 94.542 32.465 489.050 o 12 1 9 115.242 106.095 38.173 331.036 o 12 1 10 1177.940 1185.360 53.606 61.607 o 12 1 11 1297.470 1521.880 62.768 47.753 o 12 1 12 1737.170 1822.260 69.934 33.919 o 12 1 13 790.344 720.147 58.948 83.872 o 12 1 14 367.651 350.223 59.670 121.674 o 12 1 15 22.660 37.383 33.993 485.925 o 12 1 16 183.980 146.443 41.705 259.887 o 12 1 17 580.640 590.342 54.786 108.317 o 12 1 18 610.152 553.122 59.590 97.890 o 12 1 19 880.177 747.338 62.307 74.694 o 12 1 20 208.406 258.138 84.419 76.057 o 12 2 0 117.903 103.242 45.284 249.269 o 12 2 1 5030.220 4950.960 111.575 6.785 o 12 2 2 231.340 307.129 46.021 198.344 o 12 2 3 928.186 976.286 58.681 71.553 o 12 2 4 11.482 12.342 29.573 661.660 o 12 2 5 264.230 256.005 36.594 264.420 o 12 2 6 24.252 7.979 43.650 306.801 o 12 2 7 1822.060 1893.980 74.770 31.031 o 12 2 8 56.399 135.908 48.578 229.660 o 12 2 9 1428.530 1688.990 79.492 36.656 o 12 2 10 5.934 82.898 43.315 305.243 o 12 2 11 135.262 159.203 62.113 138.997 o 12 2 12 24.700 73.743 45.214 277.445 o 12 2 13 726.364 788.438 68.253 73.155 o 12 2 14 1.186 29.793 33.191 530.962 o 12 2 15 1361.950 1329.170 59.985 49.917 o 12 2 16 69.526 26.848 56.712 177.717 o 12 2 17 531.711 564.464 49.510 126.161 o 12 2 18 4.195 -24.665 45.057 295.240 o 12 2 19 23.965 14.258 50.739 228.258 o 12 2 20 71.366 60.956 52.856 200.288 o 12 3 0 14.804 9.969 47.440 262.821 o 12 3 1 47.277 46.917 43.846 291.201 o 12 3 2 994.901 1064.100 66.738 60.219 o 12 3 3 815.657 813.617 71.230 66.117 o 12 3 4 2184.160 2336.440 78.504 24.063 o 12 3 5 2224.980 2205.770 69.173 25.713 o 12 3 6 308.032 284.933 34.030 265.973 o 12 3 7 88.398 111.444 52.921 193.767 o 12 3 8 594.163 602.558 58.311 99.784 o 12 3 9 329.067 242.460 51.112 161.930 o 12 3 10 645.050 630.345 57.769 96.654 o 12 3 11 1914.620 2066.750 101.161 23.596 o 12 3 12 828.038 888.731 67.726 68.007 o 12 3 13 925.050 974.031 72.831 58.712 o 12 3 14 125.776 269.123 87.206 73.487 o 12 3 15 26.070 -13.365 44.423 297.149 o 12 3 16 16.999 16.260 37.652 410.057 o 12 3 17 90.586 93.277 39.373 327.115 o 12 3 18 601.416 635.357 73.150 74.527 o 12 3 19 182.942 203.675 61.866 134.508 o 12 4 0 6771.590 7083.020 187.902 3.505 o 12 4 1 26.649 40.951 46.706 264.389 o 12 4 2 2967.100 2860.540 97.446 15.338 o 12 4 3 284.646 237.613 45.202 199.821 o 12 4 4 176.887 116.048 36.657 322.782 o 12 4 5 200.613 152.755 38.218 288.321 o 12 4 6 2450.950 2389.490 104.349 18.487 o 12 4 7 387.248 473.213 69.224 93.451 o 12 4 8 2539.880 2451.920 100.699 18.230 o 12 4 9 233.555 287.634 54.339 156.398 o 12 4 10 1387.800 1439.870 115.780 26.880 o 12 4 11 32.290 64.060 49.989 228.869 o 12 4 12 108.768 97.371 56.341 171.452 o 12 4 13 59.548 92.831 70.240 116.772 o 12 4 14 575.934 550.358 67.727 85.406 o 12 4 15 13.179 37.837 40.230 357.689 o 12 4 16 1003.030 990.101 60.337 66.659 o 12 4 17 94.584 90.101 57.213 168.650 o 12 4 18 249.633 119.914 60.128 139.084 o 12 4 19 14.082 51.367 63.705 145.433 o 12 5 0 926.793 1100.830 78.751 52.419 o 12 5 1 228.881 296.565 95.628 59.944 o 12 5 2 1375.550 1259.780 85.429 38.523 o 12 5 3 2831.980 2769.480 85.699 17.179 o 12 5 4 2367.240 2408.190 79.387 22.097 o 12 5 5 4033.550 4011.090 95.463 9.900 o 12 5 6 686.768 820.153 56.053 91.101 o 12 5 7 330.293 386.841 62.433 115.201 o 12 5 8 51.072 53.871 35.740 418.829 o 12 5 9 282.253 252.071 57.413 140.654 o 12 5 10 60.435 101.551 57.812 168.394 o 12 5 11 2641.800 2438.300 111.147 16.622 o 12 5 12 489.650 657.020 67.565 87.221 o 12 5 13 717.162 751.646 67.983 74.584 o 12 5 14 246.815 248.301 44.468 210.806 o 12 5 15 27.198 -30.745 36.830 426.638 o 12 5 16 22.942 86.092 42.224 313.931 o 12 5 17 207.305 195.557 54.272 165.100 o 12 5 18 137.139 127.083 53.551 182.088 o 12 6 0 503.922 515.893 48.387 134.676 o 12 6 1 5210.950 4943.970 118.323 6.434 o 12 6 2 187.856 275.767 43.085 230.521 o 12 6 3 1611.090 1579.880 73.485 36.688 o 12 6 4 14.409 108.428 40.194 342.860 o 12 6 5 490.877 545.079 47.786 136.266 o 12 6 6 18.868 116.523 43.489 293.716 o 12 6 7 3242.630 2969.900 99.758 13.793 o 12 6 8 153.884 190.377 39.350 285.983 o 12 6 9 2065.330 2058.300 72.575 27.615 o 12 6 10 110.416 89.654 38.723 328.845 o 12 6 11 143.702 89.621 50.462 203.675 o 12 6 12 105.750 190.737 39.531 300.747 o 12 6 13 824.659 813.771 54.790 85.091 o 12 6 14 40.681 52.770 43.300 299.214 o 12 6 15 1359.540 1373.050 79.669 40.308 o 12 6 16 96.977 90.369 73.937 104.345 o 12 6 17 676.288 719.818 77.447 65.401 o 12 7 0 36.449 49.204 36.308 417.336 o 12 7 1 136.870 128.072 39.857 296.980 o 12 7 2 893.889 951.746 54.208 78.435 o 12 7 3 432.793 353.520 57.155 123.643 o 12 7 4 1873.790 1933.510 86.210 27.589 o 12 7 5 1249.960 1396.270 71.894 45.826 o 12 7 6 1116.520 1205.510 91.883 40.011 o 12 7 7 250.164 208.854 44.517 213.857 o 12 7 8 33.992 79.475 40.521 335.747 o 12 7 9 131.953 179.882 56.522 163.383 o 12 7 10 955.013 957.083 72.050 58.737 o 12 7 11 596.767 506.582 50.907 119.242 o 12 7 12 988.981 992.595 59.889 67.562 o 12 7 13 242.148 247.902 49.737 180.305 o 12 7 14 126.891 204.092 61.464 140.482 o 12 7 15 3.714 8.430 49.759 241.533 o 12 7 16 85.191 43.900 58.275 166.311 o 12 8 0 1909.060 1827.730 74.092 30.506 o 12 8 1 28.985 96.449 42.414 307.546 o 12 8 2 2107.600 2207.330 86.218 24.080 o 12 8 3 4.392 58.506 46.082 274.699 o 12 8 4 199.281 230.912 39.165 266.405 o 12 8 5 97.220 109.805 55.936 174.322 o 12 8 6 853.813 805.183 58.797 78.731 o 12 8 7 197.711 210.759 42.889 237.510 o 12 8 8 2029.570 1937.310 88.265 25.623 o 12 8 9 29.138 67.873 50.941 221.006 o 12 8 10 752.647 769.130 64.648 76.948 o 12 8 11 10.135 50.937 64.063 144.135 o 12 8 12 22.527 28.995 49.736 236.213 o 12 8 13 3.339 18.882 50.861 230.393 o 12 8 14 598.767 568.439 86.352 59.947 o 12 8 15 28.360 95.699 57.976 171.117 o 12 9 0 32.281 29.287 66.973 131.404 o 12 9 1 179.651 139.158 50.677 192.610 o 12 9 2 192.082 207.133 52.086 177.636 o 12 9 3 1009.460 1034.140 58.456 67.207 o 12 9 4 41.931 92.442 46.023 261.718 o 12 9 5 499.534 455.762 52.899 125.324 o 12 9 6 303.128 241.561 44.188 201.968 o 12 9 7 39.390 60.615 45.129 276.242 o 12 9 8 17.550 69.800 58.349 171.432 o 12 9 9 302.617 300.889 46.292 184.879 o 12 9 10 136.188 134.151 41.435 278.561 o 12 9 11 441.941 348.798 66.172 100.272 o 12 9 12 184.593 178.190 69.832 109.523 o 12 9 13 242.503 187.132 66.298 116.235 o 12 10 0 105.410 159.996 51.415 197.672 o 12 10 1 1462.500 1359.410 89.364 34.994 o 12 10 2 55.768 114.803 49.106 227.339 o 12 10 3 48.988 36.987 48.408 242.608 o 12 10 4 66.330 -44.713 44.713 281.998 o 12 10 5 19.769 53.844 41.565 330.385 o 12 10 6 105.767 57.167 38.984 333.810 o 12 10 7 898.677 850.146 92.962 45.762 o 12 10 8 50.353 -4.614 49.100 239.544 o 12 10 9 569.831 422.004 77.943 72.756 o 12 10 10 14.214 55.491 65.975 135.634 o 12 10 11 4.250 -28.117 61.583 158.336 o 12 11 0 69.377 248.700 67.447 121.093 o 12 11 1 1.125 20.398 52.257 218.586 o 12 11 2 519.901 553.493 61.730 99.223 o 12 11 3 48.736 166.717 53.082 194.404 o 12 11 4 634.389 547.566 75.358 71.989 o 12 11 5 197.323 99.929 94.242 63.797 o 12 11 6 235.733 182.732 73.553 97.568 o 12 11 7 202.368 284.006 94.125 62.272 o 12 11 8 32.342 13.646 70.562 118.994 o 12 12 0 951.504 960.784 124.069 29.443 o 12 12 1 161.086 193.222 88.531 71.513 o 12 12 2 1037.760 1204.080 99.309 37.581 o 12 12 3 0.445 -2.667 76.400 103.087 o 12 12 4 13.715 -94.904 94.904 66.616 o 12 12 5 64.067 134.434 101.954 56.397 o 13 0 0 4.953 -77.722 94.053 67.956 o 13 0 2 5561.520 5126.240 187.785 4.881 o 13 0 4 6563.580 6685.100 154.584 3.998 o 13 0 6 810.371 790.637 77.161 60.759 o 13 0 8 1089.760 1029.390 86.779 44.620 o 13 0 10 3157.920 3050.730 104.073 13.687 o 13 0 12 2208.170 2234.800 95.236 21.750 o 13 0 14 53.100 13.457 58.590 169.331 o 13 0 16 732.283 727.781 102.631 43.004 o 13 0 18 1574.020 1337.840 105.941 28.501 o 13 1 0 3018.610 3181.370 128.105 12.369 o 13 1 1 2815.570 2765.040 105.401 15.595 o 13 1 2 1991.550 2067.490 87.099 25.594 o 13 1 3 16.817 21.537 41.307 341.707 o 13 1 4 169.054 192.123 35.838 319.979 o 13 1 5 951.310 1025.320 53.529 74.520 o 13 1 6 2139.700 2174.080 68.136 26.938 o 13 1 7 2080.540 2174.900 85.783 24.532 o 13 1 8 2078.020 2087.040 67.836 28.169 o 13 1 9 872.725 851.869 50.813 86.348 o 13 1 10 381.751 334.309 38.671 207.490 o 13 1 11 124.881 215.219 42.044 263.672 o 13 1 12 229.762 223.523 36.983 278.030 o 13 1 13 946.970 958.362 50.288 79.754 o 13 1 14 1251.860 1344.690 57.410 54.160 o 13 1 15 591.778 533.535 46.599 129.161 o 13 1 16 454.721 464.938 56.170 119.936 o 13 1 17 41.217 -21.124 57.156 179.669 o 13 1 18 0.877 13.108 47.901 260.617 o 13 2 0 423.859 378.523 61.674 111.116 o 13 2 1 674.416 690.531 93.346 50.794 o 13 2 2 255.373 290.936 47.580 186.610 o 13 2 3 3480.560 3439.680 94.429 12.370 o 13 2 4 18.937 38.471 39.294 371.392 o 13 2 5 1825.800 1782.970 63.577 34.520 o 13 2 6 81.845 124.771 33.258 426.353 o 13 2 7 22.776 -31.070 31.080 595.161 o 13 2 8 89.406 89.639 32.298 453.886 o 13 2 9 501.713 567.938 54.205 116.802 o 13 2 10 91.013 77.720 43.950 272.978 o 13 2 11 1661.160 1657.660 79.178 33.579 o 13 2 12 7.980 104.674 46.191 266.784 o 13 2 13 525.508 494.614 46.605 138.693 o 13 2 14 17.097 18.977 43.517 309.149 o 13 2 15 9.657 18.458 48.397 252.890 o 13 2 16 19.380 21.099 43.848 303.588 o 13 2 17 743.054 675.330 87.541 54.425 o 13 2 18 47.270 102.723 46.550 253.837 o 13 3 0 888.473 892.354 70.491 63.144 o 13 3 1 848.003 919.172 104.595 39.153 o 13 3 2 778.939 855.163 59.787 79.928 o 13 3 3 1282.880 1408.770 79.211 41.552 o 13 3 4 297.967 284.272 52.631 156.551 o 13 3 5 35.437 18.238 36.219 429.462 o 13 3 6 1817.050 1814.190 67.606 33.404 o 13 3 7 622.114 583.336 55.530 103.999 o 13 3 8 692.960 678.516 68.519 76.354 o 13 3 9 767.968 905.264 81.644 56.320 o 13 3 10 265.086 262.782 52.381 162.979 o 13 3 11 57.880 110.860 70.994 114.059 o 13 3 12 129.910 203.491 51.820 188.182 o 13 3 13 184.408 197.077 56.437 157.245 o 13 3 14 296.689 270.452 68.416 105.007 o 13 3 15 296.483 228.449 60.391 129.802 o 13 3 16 481.468 430.892 54.272 124.291 o 13 3 17 42.931 -10.000 48.065 251.122 o 13 4 0 34.252 20.558 84.864 82.537 o 13 4 1 6.473 -44.899 44.899 296.655 o 13 4 2 296.757 360.187 55.935 139.573 o 13 4 3 448.000 556.649 65.303 96.069 o 13 4 4 2198.240 2072.750 80.420 24.831 o 13 4 5 88.779 161.103 32.992 414.553 o 13 4 6 920.331 1080.640 51.209 77.000 o 13 4 7 18.630 -4.517 45.344 287.538 o 13 4 8 92.507 134.928 51.279 202.560 o 13 4 9 29.546 45.943 47.977 249.946 o 13 4 10 832.058 885.207 75.870 60.005 o 13 4 11 144.482 142.417 52.773 184.686 o 13 4 12 1004.120 976.782 73.092 56.238 o 13 4 13 4.788 11.098 66.009 137.472 o 13 4 14 261.433 184.415 58.975 139.701 o 13 4 15 22.335 76.741 61.938 151.997 o 13 4 16 25.615 45.256 63.270 146.772 o 13 4 17 28.368 17.246 66.075 135.544 o 13 5 0 1625.870 1649.940 85.225 32.306 o 13 5 1 918.240 876.017 84.963 50.631 o 13 5 2 831.393 779.080 72.745 64.618 o 13 5 3 541.307 669.336 64.775 89.146 o 13 5 4 11.168 31.832 42.017 330.778 o 13 5 5 171.900 132.666 39.365 289.537 o 13 5 6 460.269 439.896 62.858 103.944 o 13 5 7 815.931 766.810 55.210 86.342 o 13 5 8 543.131 632.743 65.773 88.272 o 13 5 9 743.359 732.367 68.951 72.737 o 13 5 10 148.252 171.787 55.927 165.028 o 13 5 11 8.591 45.243 50.535 230.041 o 13 5 12 56.999 168.957 56.563 172.018 o 13 5 13 216.616 220.089 73.456 97.814 o 13 5 14 190.028 172.669 59.447 144.697 o 13 5 15 543.438 390.796 84.662 65.328 o 13 5 16 224.620 212.664 63.105 126.682 o 13 6 0 51.954 52.452 52.865 203.678 o 13 6 1 290.866 332.366 59.919 127.654 o 13 6 2 33.401 60.627 52.570 208.027 o 13 6 3 3217.390 3243.390 129.505 11.610 o 13 6 4 73.969 132.028 56.231 174.048 o 13 6 5 2704.550 2685.330 115.740 15.344 o 13 6 6 93.059 202.181 43.710 258.035 o 13 6 7 105.413 136.727 39.146 315.746 o 13 6 8 19.852 34.246 36.499 427.985 o 13 6 9 1185.890 1149.880 78.155 46.485 o 13 6 10 138.515 120.133 39.653 300.202 o 13 6 11 2006.310 2006.390 110.687 21.459 o 13 6 12 24.047 127.674 41.670 313.914 o 13 6 13 746.985 708.736 81.443 59.487 o 13 6 14 30.891 46.193 60.552 159.394 o 13 6 15 43.164 62.396 59.294 164.087 o 13 7 0 1674.910 1794.260 123.516 21.865 o 13 7 1 1028.300 1205.500 85.480 44.878 o 13 7 2 1084.090 1096.890 77.296 49.795 o 13 7 3 390.904 416.947 46.996 159.384 o 13 7 4 3.193 51.785 40.313 357.564 o 13 7 5 334.733 420.462 55.821 133.483 o 13 7 6 963.275 1031.070 67.011 61.549 o 13 7 7 1242.740 1291.090 69.874 48.229 o 13 7 8 1012.590 1200.970 76.380 50.838 o 13 7 9 513.240 521.956 49.023 131.529 o 13 7 10 41.426 62.368 39.295 355.631 o 13 7 11 40.018 67.322 60.456 158.147 o 13 7 12 137.475 85.892 51.334 198.983 o 13 7 13 489.689 496.217 71.400 84.303 o 13 7 14 494.213 482.054 90.666 58.702 o 13 8 0 17.098 56.523 61.596 154.894 o 13 8 1 5.310 18.658 50.693 231.577 o 13 8 2 1135.960 993.621 77.415 49.714 o 13 8 3 73.079 119.706 44.005 271.534 o 13 8 4 2515.250 2367.520 94.844 19.294 o 13 8 5 39.337 55.269 69.390 121.548 o 13 8 6 597.281 619.785 53.381 108.896 o 13 8 7 41.046 50.156 42.247 313.574 o 13 8 8 313.706 314.842 50.094 163.747 o 13 8 9 73.408 119.409 50.993 208.922 o 13 8 10 1077.600 1152.770 91.463 41.232 o 13 8 11 46.999 59.889 58.667 167.210 o 13 8 12 630.211 662.495 93.458 51.752 o 13 9 0 446.830 399.923 51.736 136.734 o 13 9 1 402.838 345.544 49.870 151.316 o 13 9 2 104.036 139.148 45.954 242.180 o 13 9 3 2.707 20.853 42.129 334.181 o 13 9 4 17.165 51.263 42.515 317.840 o 13 9 5 612.185 641.393 55.373 102.958 o 13 9 6 167.946 160.842 48.314 208.349 o 13 9 7 1053.860 1065.920 84.930 46.032 o 13 9 8 437.242 428.435 75.036 81.646 o 13 9 9 178.492 159.778 69.915 110.070 o 13 9 10 96.726 137.152 75.007 100.636 o 13 10 0 198.244 203.279 65.374 121.337 o 13 10 1 104.321 113.574 50.224 209.938 o 13 10 2 489.942 440.585 53.248 125.943 o 13 10 3 540.053 481.316 71.411 82.490 o 13 10 4 54.169 112.840 72.778 108.888 o 13 10 5 630.563 537.390 81.806 64.446 o 13 10 6 0.182 -3.259 52.270 220.234 o 13 10 7 8.249 -33.087 52.820 214.451 o 13 10 8 144.197 211.583 80.280 85.933 o 13 11 0 740.541 803.439 120.694 33.010 o 13 11 1 81.747 248.003 88.105 73.284 o 13 11 2 163.871 118.352 61.443 141.043 o 13 11 3 129.810 114.290 97.404 60.836 o 13 11 4 73.050 36.357 63.707 141.718 o 14 0 0 4829.460 5318.910 207.421 5.059 o 14 0 2 776.850 873.773 96.949 44.954 o 14 0 4 1571.050 1425.010 83.845 34.985 o 14 0 6 4970.790 4784.630 160.877 6.046 o 14 0 8 2350.790 2236.240 108.060 19.032 o 14 0 10 5.926 23.043 56.413 187.068 o 14 0 12 1532.790 1626.350 111.011 26.241 o 14 0 14 1754.040 1569.050 141.311 18.816 o 14 0 16 381.143 487.485 90.887 60.716 o 14 1 0 128.450 165.948 57.794 158.230 o 14 1 1 1166.950 1291.960 79.615 44.637 o 14 1 2 1962.460 2273.390 154.106 14.928 o 14 1 3 1697.400 1730.200 90.935 29.407 o 14 1 4 2051.940 2246.230 96.381 22.689 o 14 1 5 525.323 594.296 41.243 148.525 o 14 1 6 87.430 122.100 34.271 404.008 o 14 1 7 39.519 48.828 35.214 439.341 o 14 1 8 535.137 597.076 44.098 138.737 o 14 1 9 1506.940 1434.010 57.648 45.993 o 14 1 10 1078.060 1168.770 54.954 64.730 o 14 1 11 798.162 747.377 55.390 87.665 o 14 1 12 385.621 448.508 43.513 172.190 o 14 1 13 8.285 -26.867 37.170 430.500 o 14 1 14 4.756 -2.474 45.708 286.768 o 14 1 15 105.756 125.035 52.618 192.307 o 14 1 16 312.455 243.078 57.303 138.665 o 14 2 0 9.959 -58.902 58.902 172.479 o 14 2 1 1225.370 1398.260 82.953 40.943 o 14 2 2 25.047 135.134 56.763 176.329 o 14 2 3 26.149 31.416 52.252 213.842 o 14 2 4 87.828 124.459 44.478 261.995 o 14 2 5 921.155 904.904 63.239 68.759 o 14 2 6 0.795 16.252 35.432 472.749 o 14 2 7 1553.280 1573.700 57.606 43.336 o 14 2 8 6.549 25.862 33.765 510.563 o 14 2 9 553.728 586.963 40.838 146.346 o 14 2 10 19.744 42.137 50.636 227.455 o 14 2 11 157.907 128.087 47.077 222.470 o 14 2 12 2.769 -16.904 44.251 306.480 o 14 2 13 673.113 579.268 65.263 84.067 o 14 2 14 14.421 -22.258 53.221 210.345 o 14 2 15 561.385 443.296 70.204 84.369 o 14 3 0 4.550 -15.884 57.270 182.984 o 14 3 1 22.726 83.534 49.831 230.212 o 14 3 2 914.196 987.871 67.123 63.809 o 14 3 3 251.735 228.655 53.583 161.129 o 14 3 4 1158.110 1212.330 66.213 53.531 o 14 3 5 606.322 787.942 66.593 80.368 o 14 3 6 27.360 64.535 45.634 273.142 o 14 3 7 389.488 388.055 41.442 186.143 o 14 3 8 63.142 -14.943 57.233 176.807 o 14 3 9 84.531 73.914 44.872 265.374 o 14 3 10 583.101 551.979 62.293 94.469 o 14 3 11 652.172 512.401 60.614 94.686 o 14 3 12 316.499 302.781 70.686 97.812 o 14 3 13 173.740 223.616 58.137 149.382 o 14 3 14 148.334 216.975 57.533 154.888 o 14 3 15 76.386 103.615 57.265 169.592 o 14 4 0 1011.570 1175.990 81.239 48.030 o 14 4 1 115.328 194.198 53.497 180.855 o 14 4 2 675.903 772.330 62.921 82.747 o 14 4 3 65.615 44.737 45.613 266.112 o 14 4 4 16.104 10.572 40.919 350.529 o 14 4 5 533.333 415.493 49.020 135.076 o 14 4 6 558.754 470.343 41.681 151.135 o 14 4 7 173.589 188.086 35.315 325.309 o 14 4 8 1456.600 1508.270 82.601 36.485 o 14 4 9 20.688 39.677 55.649 189.364 o 14 4 10 384.353 380.934 54.314 135.616 o 14 4 11 117.433 174.700 53.989 179.001 o 14 4 12 40.151 -15.779 59.291 167.358 o 14 4 13 88.151 304.779 183.166 17.656 o 14 4 14 347.173 245.537 110.906 44.703 o 14 5 0 0.238 -51.854 51.854 223.775 o 14 5 1 472.426 421.583 95.771 54.604 o 14 5 2 177.561 217.665 60.777 138.513 o 14 5 3 1190.270 1291.960 118.047 28.364 o 14 5 4 586.976 437.813 56.090 110.728 o 14 5 5 561.080 519.505 52.579 117.787 o 14 5 6 142.701 185.834 47.145 219.232 o 14 5 7 33.767 72.577 42.217 312.639 o 14 5 8 41.604 46.069 43.201 301.261 o 14 5 9 534.080 458.201 62.985 98.671 o 14 5 10 255.416 332.324 57.917 137.560 o 14 5 11 676.839 687.072 81.840 61.190 o 14 5 12 242.256 312.266 78.766 84.071 o 14 5 13 177.306 161.742 91.003 67.920 o 14 6 0 131.269 310.790 64.097 126.428 o 14 6 1 2168.150 1925.140 129.585 17.892 o 14 6 2 32.706 75.162 49.058 236.012 o 14 6 3 21.233 -35.416 44.976 291.431 o 14 6 4 3.748 -15.746 47.871 261.768 o 14 6 5 769.605 750.669 71.751 68.200 o 14 6 6 76.333 82.974 55.871 178.703 o 14 6 7 1850.590 1651.760 70.912 33.250 o 14 6 8 6.346 12.089 38.316 403.204 o 14 6 9 511.278 462.951 47.875 138.335 o 14 6 10 2.483 26.265 64.020 145.735 o 14 6 11 152.223 132.709 65.644 125.643 o 14 6 12 16.649 152.884 73.743 106.893 o 14 7 0 302.506 285.202 62.140 121.573 o 14 7 1 269.374 356.697 75.227 89.082 o 14 7 2 1043.530 919.414 71.826 56.916 o 14 7 3 915.837 871.815 66.312 66.552 o 14 7 4 704.380 755.707 67.043 76.224 o 14 7 5 520.445 547.436 57.037 109.447 o 14 7 6 67.684 56.104 48.797 233.370 o 14 7 7 69.493 119.867 53.432 192.454 o 14 7 8 228.301 224.424 57.643 146.186 o 14 7 9 452.854 527.289 69.610 88.362 o 14 7 10 961.795 854.519 67.295 64.304 o 14 7 11 358.529 208.235 69.451 100.907 o 14 8 0 1364.550 1231.940 93.978 35.404 o 14 8 1 16.673 -15.505 56.837 184.405 o 14 8 2 164.130 124.776 55.381 168.712 o 14 8 3 6.463 -18.043 49.510 244.241 o 14 8 4 266.896 237.248 59.727 134.175 o 14 8 5 37.654 113.108 55.499 183.787 o 14 8 6 1385.320 1447.640 89.623 35.347 o 14 8 7 15.268 50.480 54.274 198.817 o 14 8 8 576.977 537.734 64.731 90.779 o 14 8 9 0.545 -6.115 55.607 194.558 o 14 9 0 7.400 -1.224 66.764 134.571 o 14 9 1 446.543 253.086 74.301 85.940 o 14 9 2 224.470 195.779 63.306 126.616 o 14 9 3 792.034 691.626 75.651 64.245 o 14 9 4 244.233 241.404 62.168 127.349 o 14 9 5 294.952 297.192 63.649 117.186 o 14 9 6 24.739 39.619 56.901 180.874 o 14 9 7 48.320 34.566 60.153 160.410 o 14 10 0 128.683 228.345 72.121 104.808 o 14 10 1 637.652 526.472 98.753 48.516 o 14 10 2 15.561 -52.585 52.585 215.243 o 14 10 3 3.357 23.025 73.937 109.496 o 15 0 0 806.055 1143.360 115.199 33.351 o 15 0 2 3641.270 3926.650 169.640 8.124 o 15 0 4 907.661 752.124 90.319 48.246 o 15 0 6 44.254 113.721 72.651 109.666 o 15 0 8 889.601 1034.360 85.964 48.892 o 15 0 10 1201.780 1170.210 106.375 32.875 o 15 0 12 82.154 188.062 90.072 70.865 o 15 1 0 577.841 602.811 72.892 76.361 o 15 1 1 337.666 363.082 66.283 105.477 o 15 1 2 50.113 68.043 53.345 199.382 o 15 1 3 254.355 267.508 54.337 155.197 o 15 1 4 1035.950 1048.180 53.749 69.937 o 15 1 5 511.043 652.087 82.629 65.176 o 15 1 6 941.103 994.514 63.749 65.822 o 15 1 7 1302.910 1372.190 57.971 51.967 o 15 1 8 244.527 208.643 40.312 246.469 o 15 1 9 176.755 254.658 39.324 268.259 o 15 1 10 46.613 35.565 57.647 174.237 o 15 1 11 246.101 163.806 49.209 189.130 o 15 1 12 415.456 352.829 52.533 139.877 o 15 1 13 503.358 550.921 63.437 96.857 o 15 2 0 16.188 -54.080 54.080 203.538 o 15 2 1 713.732 879.734 73.447 66.066 o 15 2 2 29.875 93.317 53.840 196.976 o 15 2 3 2316.190 2322.770 94.045 20.845 o 15 2 4 1.653 -16.324 46.008 283.875 o 15 2 5 515.769 530.868 60.752 102.198 o 15 2 6 98.989 87.018 40.951 304.175 o 15 2 7 70.360 122.279 41.357 302.869 o 15 2 8 11.811 80.932 33.593 487.709 o 15 2 9 1292.410 1339.060 57.446 53.022 o 15 2 10 46.895 26.815 55.392 188.625 o 15 2 11 670.712 800.079 69.812 73.170 o 15 2 12 39.135 78.754 55.431 186.133 o 15 3 0 1028.690 1136.530 86.184 45.101 o 15 3 1 364.678 429.522 61.370 114.224 o 15 3 2 407.323 411.050 52.311 138.414 o 15 3 3 449.971 422.383 56.013 122.548 o 15 3 4 169.970 259.686 56.340 155.906 o 15 3 5 56.349 104.592 43.606 282.893 o 15 3 6 828.637 835.497 79.063 57.917 o 15 3 7 303.250 298.928 46.644 183.098 o 15 3 8 569.601 497.219 43.093 143.564 o 15 3 9 280.422 376.626 61.734 121.091 o 15 3 10 6.974 -65.899 65.899 138.139 o 15 3 11 5.825 -4.569 60.132 165.910 o 15 3 12 174.101 128.957 58.327 153.060 o 15 4 0 15.447 -14.610 50.762 230.812 o 15 4 1 243.650 168.038 54.308 162.261 o 15 4 2 874.242 879.462 63.804 70.534 o 15 4 3 71.674 81.959 49.803 221.654 o 15 4 4 680.756 794.824 67.412 75.916 o 15 4 5 6.055 -2.026 48.461 254.955 o 15 4 6 137.268 117.852 55.543 171.378 o 15 4 7 70.145 96.252 39.359 335.040 o 15 4 8 118.860 142.389 50.821 200.955 o 15 4 9 17.478 7.065 49.578 240.756 o 15 4 10 806.667 729.724 77.233 61.658 o 15 4 11 1.831 3.693 79.269 95.662 o 15 5 0 465.378 364.360 68.664 93.419 o 15 5 1 342.076 239.570 55.883 141.231 o 15 5 2 13.803 -21.821 58.718 173.174 o 15 5 3 118.498 139.950 52.768 188.493 o 15 5 4 94.652 34.396 48.007 237.160 o 15 5 5 685.431 589.438 60.045 91.518 o 15 5 6 334.786 301.123 50.563 159.833 o 15 5 7 332.931 258.769 56.150 140.203 o 15 5 8 372.848 329.062 63.489 111.454 o 15 5 9 8.691 -53.095 85.831 81.499 o 15 5 10 25.327 7.971 61.504 156.673 o 15 6 0 41.964 96.745 58.853 164.894 o 15 6 1 1239.740 1496.940 88.506 37.500 o 15 6 2 65.719 124.800 82.487 85.082 o 15 6 3 1451.530 1389.120 106.345 29.290 o 15 6 4 9.374 -25.205 48.539 253.437 o 15 6 5 92.958 128.975 120.228 40.688 o 15 6 6 29.195 3.411 52.107 216.729 o 15 6 7 133.194 122.943 56.835 164.736 o 15 6 8 15.268 14.125 55.842 190.283 o 15 6 9 632.667 657.426 80.970 63.683 o 15 7 0 723.140 647.409 75.328 67.443 o 15 7 1 64.756 62.048 56.801 175.755 o 15 7 2 0.538 -1.832 59.675 168.941 o 15 7 3 37.151 48.785 55.752 186.141 o 15 7 4 552.456 430.171 67.301 90.128 o 15 7 5 260.447 271.816 61.916 125.846 o 15 7 6 521.410 525.529 74.492 77.576 o 15 7 7 243.318 281.405 63.064 123.048 o 15 8 0 306.101 330.560 91.927 62.575 o 15 8 1 6.638 56.109 63.458 146.914 o 15 8 2 986.641 1053.500 91.493 43.486 o 15 8 3 10.601 30.470 65.193 139.905 o 15 8 4 600.360 550.840 75.595 72.780 o 15 8 5 7.072 30.953 82.117 88.657 o 15 9 0 389.998 459.000 87.461 64.830 o 15 9 1 274.503 145.246 90.329 67.081 o 16 0 0 1019.430 1183.920 124.161 28.108 o 16 0 2 32.727 33.408 85.596 81.037 o 16 0 4 837.632 852.346 96.018 44.773 o 16 0 6 568.309 493.672 99.461 49.264 o 16 0 8 261.559 241.549 65.851 114.731 o 16 1 0 179.102 189.726 64.259 126.745 o 16 1 1 626.812 799.850 84.142 58.748 o 16 1 2 844.995 1006.140 86.448 49.733 o 16 1 3 467.219 397.692 60.455 110.526 o 16 1 4 85.458 153.893 53.321 188.636 o 16 1 5 276.646 384.661 56.247 139.206 o 16 1 6 101.883 148.570 66.041 126.947 o 16 1 7 56.063 -1.366 55.843 186.216 o 16 1 8 238.619 133.142 51.102 181.741 o 16 1 9 450.365 413.339 52.637 132.849 o 16 2 0 161.899 159.343 57.009 158.901 o 16 2 1 663.032 627.924 81.944 62.219 o 16 2 2 13.820 35.426 52.261 215.385 o 16 2 3 160.086 124.076 61.945 139.099 o 16 2 4 96.071 133.006 40.720 300.058 o 16 2 5 1021.040 1193.350 77.097 50.263 o 16 2 6 0.420 37.667 54.629 199.111 o 16 2 7 894.929 869.914 69.155 64.566 o 16 2 8 24.841 -18.033 50.252 233.740 o 16 2 9 37.257 191.053 64.286 136.394 o 16 3 0 65.313 34.023 62.352 148.351 o 16 3 1 306.054 269.142 71.034 98.309 o 16 3 2 865.448 766.037 76.606 60.072 o 16 3 3 312.519 445.346 64.390 109.262 o 16 3 4 584.068 630.800 90.374 55.650 o 16 3 5 49.187 33.294 50.859 221.219 o 16 3 6 30.816 107.674 53.785 196.245 o 16 3 7 137.795 192.293 77.828 91.521 o 16 3 8 394.441 428.205 70.887 90.877 o 16 4 0 623.671 562.660 85.759 60.042 o 16 4 1 50.172 8.970 60.640 158.888 o 16 4 2 0.759 -57.795 57.795 180.085 o 16 4 3 7.290 44.276 68.804 125.567 o 16 4 4 459.511 431.457 93.058 57.417 o 16 4 5 29.498 26.118 53.039 207.620 o 16 4 6 1300.220 1133.460 75.035 45.951 o 16 4 7 17.132 -52.846 52.846 212.903 o 16 5 0 33.545 123.470 78.321 95.059 o 16 5 1 875.181 927.266 77.607 56.748 o 16 5 2 633.506 500.219 75.729 72.336 o 16 5 3 494.687 519.118 64.827 95.490 o 16 5 4 330.201 305.832 65.547 109.453 o 16 5 5 3.509 24.357 57.062 183.077 o 16 5 6 0.601 -50.444 50.444 236.394 o 16 6 0 0.136 -6.970 60.307 165.457 o 16 6 1 112.232 73.607 65.726 129.803 o 16 6 2 84.477 110.815 59.139 158.663 o 16 6 3 133.550 97.873 56.306 168.839 o 16 6 4 25.612 -25.983 69.178 124.428 o 16 7 0 513.086 531.848 96.198 52.587 o 16 7 1 106.903 115.613 69.318 116.686 o 17 0 0 493.538 344.583 103.438 48.188 o 17 0 2 577.488 482.673 105.759 44.505 o 17 0 4 96.930 112.352 113.296 45.724 o 17 1 0 158.506 205.187 66.397 120.488 o 17 1 1 185.213 177.380 77.312 91.237 o 17 1 2 89.436 8.794 63.329 143.147 o 17 1 3 37.178 91.907 125.127 38.023 o 17 1 4 268.039 209.421 65.842 115.343 o 17 1 5 215.669 204.758 82.603 79.634 o 17 2 0 44.611 90.058 67.642 126.432 o 17 2 1 1086.300 1088.350 101.280 36.791 o 17 2 2 32.109 62.419 71.175 115.857 o 17 2 3 744.342 730.018 81.435 59.290 o 17 2 4 45.663 139.558 77.473 96.397 o 17 3 0 262.394 257.750 74.779 92.216 o 17 3 1 43.009 46.231 66.190 133.275 o 17 3 2 12.635 -74.025 74.025 109.326 o 17 3 3 53.205 1.107 74.503 106.340 o 17 4 0 918.360 1087.530 97.571 40.881 o 17 4 1 11.245 91.917 68.881 123.821 o 17 4 2 913.454 880.493 136.116 25.959 o ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,y+1/2,-z+1/2 3 -x,-y,-z 4 x,-y-1/2,z-1/2 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp Au Au 0.28794(3) 0.37978(3) 0.318576(16) 0.0578(2) Uani 1.000000 . . Cl1 Cl 0.44123(9) 0.50510(10) 0.32469(5) 0.0673(3) Uani 1.000000 . . P1 P 0.15693(8) 0.49387(8) 0.31272(5) 0.0488(3) Uani 1.000000 . . P2 P 0.36411(8) 0.22127(8) 0.32615(4) 0.0476(2) Uani 1.000000 . . C1 C 0.1867(3) 0.6268(3) 0.32943(17) 0.0522(9) Uani 1.000000 . U C2 C 0.1500(4) 0.7060(3) 0.2944(2) 0.0642(12) Uani 1.000000 . U H2 H 0.1110(4) 0.6909(3) 0.2614(2) 0.0771(14) Uiso 1.000000 R . C3 C 0.1711(4) 0.8063(4) 0.3084(2) 0.0743(14) Uani 1.000000 . U H3 H 0.1456(4) 0.8584(4) 0.2850(2) 0.0891(17) Uiso 1.000000 R . C4 C 0.2299(4) 0.8294(4) 0.3567(2) 0.0746(14) Uani 1.000000 . U H4 H 0.2440(4) 0.8971(4) 0.3659(2) 0.0895(17) Uiso 1.000000 R . C5 C 0.2682(3) 0.7525(4) 0.3916(2) 0.0619(11) Uani 1.000000 . U H5 H 0.3073(3) 0.7685(4) 0.4245(2) 0.0742(13) Uiso 1.000000 R . C6 C 0.2484(3) 0.6522(3) 0.37775(17) 0.0511(9) Uani 1.000000 . U N1 N 0.2917(3) 0.5731(3) 0.41257(14) 0.0539(8) Uani 1.000000 . U H1 H 0.3292(3) 0.5296(3) 0.39995(14) 0.0647(10) Uiso 1.000000 R . C7 C 0.2778(3) 0.5624(3) 0.46383(18) 0.0554(10) Uani 1.000000 . U O1 O 0.2202(3) 0.6136(3) 0.48516(14) 0.0750(10) Uani 1.000000 . U C8 C 0.3388(3) 0.4790(3) 0.49448(17) 0.0535(10) Uani 1.000000 . U C9 C 0.3327(4) 0.4610(4) 0.54791(18) 0.0679(12) Uani 1.000000 . U H9 H 0.2897(4) 0.4990(4) 0.56526(18) 0.0815(15) Uiso 1.000000 R . C10 C 0.3911(4) 0.3859(4) 0.5753(2) 0.0770(15) Uani 1.000000 . U H10 H 0.3898(4) 0.3738(4) 0.6117(2) 0.0924(17) Uiso 1.000000 R . C11 C 0.4512(4) 0.3291(4) 0.54773(19) 0.0660(12) Uani 1.000000 . U H11 H 0.4897(4) 0.2763(4) 0.56483(19) 0.0792(14) Uiso 1.000000 R . C12 C 0.4536(3) 0.3516(3) 0.49435(17) 0.0534(10) Uani 1.000000 . U N2 N 0.3987(2) 0.4255(3) 0.46744(13) 0.0486(8) Uani 1.000000 . U C13 C 0.5187(3) 0.2894(3) 0.46398(17) 0.0522(9) Uani 1.000000 . U O2 O 0.5696(3) 0.2199(3) 0.48474(13) 0.0732(9) Uani 1.000000 . U N3 N 0.5122(3) 0.3171(3) 0.41126(14) 0.0520(8) Uani 1.000000 . U H3a H 0.4777(3) 0.3702(3) 0.40041(14) 0.0624(10) Uiso 1.000000 R . C14 C 0.5589(3) 0.2636(3) 0.37323(17) 0.0506(9) Uani 1.000000 . U C15 C 0.6615(3) 0.2572(4) 0.3791(2) 0.0648(12) Uani 1.000000 . U H15 H 0.7012(3) 0.2844(4) 0.4094(2) 0.0778(14) Uiso 1.000000 R . C16 C 0.7041(3) 0.2101(4) 0.3397(2) 0.0734(14) Uani 1.000000 . U H16 H 0.7730(3) 0.2049(4) 0.3438(2) 0.0881(16) Uiso 1.000000 R . C17 C 0.6466(4) 0.1706(4) 0.2944(2) 0.0691(13) Uani 1.000000 . U H17 H 0.6767(4) 0.1411(4) 0.2674(2) 0.0829(15) Uiso 1.000000 R . C18 C 0.5446(3) 0.1746(3) 0.28887(18) 0.0575(10) Uani 1.000000 . U H18 H 0.5058(3) 0.1473(3) 0.25831(18) 0.0689(13) Uiso 1.000000 R . C19 C 0.4994(3) 0.2193(3) 0.32873(17) 0.0491(9) Uani 1.000000 . U C20 C 0.0699(3) 0.4552(4) 0.35662(18) 0.0560(10) Uani 1.000000 . U C21 C 0.0391(4) 0.3536(4) 0.3542(3) 0.0745(14) Uani 1.000000 . U H21 H 0.0616(4) 0.3087(4) 0.3302(3) 0.0894(17) Uiso 1.000000 R . C22 C -0.0251(4) 0.3201(5) 0.3878(3) 0.0912(18) Uani 1.000000 . U H22 H -0.0462(4) 0.2526(5) 0.3862(3) 0.109(2) Uiso 1.000000 R . C23 C -0.0579(4) 0.3864(6) 0.4238(3) 0.0894(17) Uani 1.000000 . U H23 H -0.0994(4) 0.3631(6) 0.4472(3) 0.107(2) Uiso 1.000000 R . C24 C -0.0298(4) 0.4851(5) 0.4250(2) 0.0812(15) Uani 1.000000 . U H24 H -0.0536(4) 0.5296(5) 0.4488(2) 0.0974(18) Uiso 1.000000 R . C25 C 0.0333(4) 0.5213(4) 0.39182(19) 0.0658(12) Uani 1.000000 . U H25 H 0.0513(4) 0.5897(4) 0.39297(19) 0.0789(14) Uiso 1.000000 R . C26 C 0.0836(3) 0.5028(3) 0.24558(18) 0.0542(10) Uani 1.000000 . U C27 C 0.1277(4) 0.4839(4) 0.2014(2) 0.0690(13) Uani 1.000000 . U H27 H 0.1929(4) 0.4603(4) 0.2059(2) 0.0828(15) Uiso 1.000000 R . C28 C 0.0757(5) 0.4996(5) 0.1502(2) 0.0833(16) Uani 1.000000 . U H28 H 0.1064(5) 0.4864(5) 0.1204(2) 0.1000(19) Uiso 1.000000 R . C29 C -0.0191(5) 0.5338(4) 0.1425(2) 0.0795(15) Uani 1.000000 . U H29 H -0.0531(5) 0.5447(4) 0.1078(2) 0.0954(18) Uiso 1.000000 R . C30 C -0.0647(4) 0.5523(4) 0.1860(2) 0.0753(14) Uani 1.000000 . U H30 H -0.1299(4) 0.5758(4) 0.1809(2) 0.0904(17) Uiso 1.000000 R . C31 C -0.0143(3) 0.5361(4) 0.2379(2) 0.0647(12) Uani 1.000000 . U H31 H -0.0461(3) 0.5475(4) 0.2674(2) 0.0776(14) Uiso 1.000000 R . C32 C 0.3465(3) 0.1510(3) 0.38606(17) 0.0549(10) Uani 1.000000 . U C33 C 0.4079(4) 0.0688(4) 0.4049(2) 0.0667(12) Uani 1.000000 . U H33 H 0.4615(4) 0.0528(4) 0.3878(2) 0.0800(15) Uiso 1.000000 R . C34 C 0.3907(6) 0.0111(5) 0.4481(2) 0.1002(17) Uani 1.000000 . U H34 H 0.4316(6) -0.0441(5) 0.4596(2) 0.120(2) Uiso 1.000000 R . C35 C 0.3138(6) 0.0354(6) 0.4740(3) 0.1002(17) Uani 1.000000 . U H35 H 0.3022(6) -0.0038(6) 0.5032(3) 0.120(2) Uiso 1.000000 R . C36 C 0.2530(6) 0.1163(6) 0.4578(3) 0.107(2) Uani 1.000000 . U H36 H 0.2015(6) 0.1324(6) 0.4765(3) 0.128(3) Uiso 1.000000 R . C37 C 0.2684(4) 0.1761(5) 0.4124(2) 0.0812(15) Uani 1.000000 . U H37 H 0.2268(4) 0.2307(5) 0.4009(2) 0.0975(19) Uiso 1.000000 R . C38 C 0.3144(3) 0.1393(3) 0.26986(17) 0.0531(10) Uani 1.000000 . U C39 C 0.2511(4) 0.1792(4) 0.22569(18) 0.0648(12) Uani 1.000000 . U H39 H 0.2332(4) 0.2477(4) 0.22509(18) 0.0778(14) Uiso 1.000000 R . C40 C 0.2149(4) 0.1164(5) 0.1827(2) 0.0832(16) Uani 1.000000 . U H40 H 0.1727(4) 0.1433(5) 0.1532(2) 0.100(2) Uiso 1.000000 R . C41 C 0.2401(4) 0.0160(5) 0.1827(2) 0.0741(14) Uani 1.000000 . U H41 H 0.2147(4) -0.0252(5) 0.1536(2) 0.0889(17) Uiso 1.000000 R . C42 C 0.3023(4) -0.0242(4) 0.2254(2) 0.0802(15) Uani 1.000000 . U H42 H 0.3202(4) -0.0926(4) 0.2251(2) 0.0962(18) Uiso 1.000000 R . C43 C 0.3389(4) 0.0361(4) 0.2691(2) 0.0704(13) Uani 1.000000 . U H43 H 0.3804(4) 0.0077(4) 0.2984(2) 0.0845(16) Uiso 1.000000 R . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Au 0.0582(4) 0.0566(3) 0.0576(4) 0.0093(2) 0.0064(2) -0.0043(2) Cl1 0.0645(7) 0.0674(7) 0.0712(7) -0.0076(5) 0.0148(6) 0.0094(6) P1 0.0484(6) 0.0460(6) 0.0521(6) 0.0030(4) 0.0088(5) -0.0001(5) P2 0.0458(5) 0.0479(6) 0.0486(6) 0.0028(4) 0.0058(4) -0.0038(5) C1 0.056(2) 0.047(2) 0.054(2) 0.0019(18) 0.0117(18) 0.0014(18) C2 0.072(3) 0.053(2) 0.065(3) 0.008(2) 0.001(2) -0.001(2) C3 0.080(3) 0.051(3) 0.087(4) 0.002(2) -0.002(3) 0.006(2) C4 0.087(4) 0.048(3) 0.086(4) -0.003(2) 0.005(3) -0.012(2) C5 0.062(3) 0.056(2) 0.066(3) -0.001(2) 0.006(2) -0.005(2) C6 0.053(2) 0.046(2) 0.055(2) 0.0071(17) 0.0102(18) -0.0005(18) N1 0.058(2) 0.053(2) 0.0493(19) 0.0101(16) 0.0045(16) -0.0010(16) C7 0.059(3) 0.055(3) 0.052(2) 0.0023(19) 0.012(2) -0.0041(19) O1 0.085(2) 0.078(2) 0.065(2) 0.0229(18) 0.0238(18) 0.0004(17) C8 0.058(2) 0.056(2) 0.046(2) -0.0065(18) 0.0062(18) -0.0023(18) C9 0.079(3) 0.078(3) 0.050(2) 0.006(2) 0.019(2) 0.001(2) C10 0.088(4) 0.094(4) 0.049(3) 0.004(3) 0.014(2) 0.009(3) C11 0.073(3) 0.071(3) 0.053(2) 0.006(2) 0.006(2) 0.009(2) C12 0.055(2) 0.058(2) 0.045(2) -0.0024(18) 0.0030(18) 0.0003(18) N2 0.0517(19) 0.0507(19) 0.0419(18) -0.0029(15) 0.0034(14) -0.0030(15) C13 0.049(2) 0.056(2) 0.048(2) -0.0028(18) -0.0008(17) -0.0000(19) O2 0.083(2) 0.073(2) 0.061(2) 0.0208(18) 0.0030(17) 0.0108(17) N3 0.0534(19) 0.051(2) 0.0492(19) 0.0063(15) 0.0012(15) -0.0035(15) C14 0.049(2) 0.048(2) 0.054(2) 0.0005(17) 0.0090(18) 0.0010(18) C15 0.054(2) 0.062(3) 0.075(3) 0.002(2) 0.001(2) -0.008(2) C16 0.043(2) 0.076(3) 0.102(4) 0.006(2) 0.013(2) -0.004(3) C17 0.064(3) 0.073(3) 0.076(3) 0.008(2) 0.027(2) -0.008(3) C18 0.058(2) 0.059(3) 0.055(3) 0.006(2) 0.009(2) -0.004(2) C19 0.049(2) 0.045(2) 0.054(2) 0.0054(17) 0.0086(17) 0.0019(17) C20 0.050(2) 0.059(3) 0.058(3) 0.0002(19) 0.0077(19) 0.007(2) C21 0.066(3) 0.058(3) 0.102(4) -0.002(2) 0.022(3) 0.008(3) C22 0.073(4) 0.078(4) 0.129(5) 0.000(3) 0.034(3) 0.037(3) C23 0.065(3) 0.128(5) 0.077(4) 0.002(3) 0.018(3) 0.046(3) C24 0.067(3) 0.124(4) 0.054(3) 0.002(3) 0.012(2) -0.000(3) C25 0.060(3) 0.080(3) 0.058(3) -0.002(2) 0.011(2) -0.003(2) C26 0.056(2) 0.050(2) 0.057(2) -0.0033(19) 0.0101(19) -0.0031(19) C27 0.069(3) 0.074(3) 0.063(3) 0.013(2) 0.009(2) -0.005(2) C28 0.102(4) 0.095(4) 0.054(3) 0.007(3) 0.018(3) -0.000(3) C29 0.088(4) 0.079(4) 0.064(3) -0.002(3) -0.008(3) 0.010(3) C30 0.059(3) 0.085(4) 0.077(3) -0.006(3) -0.004(2) 0.006(3) C31 0.056(2) 0.071(3) 0.066(3) 0.002(2) 0.006(2) 0.001(2) C32 0.060(2) 0.057(2) 0.047(2) -0.0110(19) 0.0062(18) -0.0072(18) C33 0.078(3) 0.060(3) 0.058(3) -0.009(2) 0.000(2) -0.001(2) C34 0.123(4) 0.103(3) 0.067(3) -0.041(3) -0.003(2) 0.018(2) C35 0.123(4) 0.103(3) 0.067(3) -0.041(3) -0.003(2) 0.018(2) C36 0.100(5) 0.158(7) 0.070(4) -0.040(5) 0.039(3) -0.013(4) C37 0.071(3) 0.109(5) 0.064(3) -0.009(3) 0.014(3) -0.013(3) C38 0.050(2) 0.058(2) 0.050(2) -0.0048(18) 0.0037(17) 0.0005(19) C39 0.072(3) 0.067(3) 0.053(3) -0.002(2) 0.006(2) 0.004(2) C40 0.087(4) 0.103(4) 0.053(3) -0.025(3) -0.008(3) 0.002(3) C41 0.075(3) 0.089(4) 0.060(3) -0.029(3) 0.016(2) -0.025(3) C42 0.094(4) 0.071(3) 0.073(3) -0.010(3) 0.008(3) -0.022(3) C43 0.072(3) 0.065(3) 0.069(3) 0.006(2) -0.005(2) -0.012(2) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source Au -1.91220 8.83481 16.88190 18.59130 25.55820 5.86000 0.46110 8.62160 1.48260 36.39560 12.06580 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' C 0.00313 0.00162 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.21560 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' Cl 0.14908 0.15974 11.46040 7.19640 6.25560 1.64550 0.01040 1.16620 18.51940 47.77840 -9.55740 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.00304 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' N 0.00612 0.00332 12.21260 3.13220 2.01250 1.16630 0.00570 9.89330 28.99750 0.58260 -11.52900 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' O 0.01085 0.00610 3.04850 2.28680 1.54630 0.86700 13.27710 5.70110 0.32390 32.90890 0.25080 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' P 0.10265 0.09519 6.43450 4.17910 1.78000 1.49080 1.90670 27.15700 0.52600 68.16450 1.11490 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u -2 0 0 1183.78 36.8 2 0 0 1229.08 36.9 -2 0 0 1178.88 33.7 -2 0 0 1173.28 33.6 -2 0 0 1205.58 33.6 3 0 0 4792.72 134.69 -3 0 0 4706.53 130.09 -3 0 0 4858.41 134.89 -3 0 0 4696.13 130.19 -3 0 0 4681.43 130.09 -4 0 0 1843.52 53.89 -4 0 0 1891.11 53.99 -4 0 0 1907.21 53.59 4 0 0 1828.82 59.09 -4 0 0 1960.5 59.89 -5 0 0 3619.74 100.49 -5 0 0 3566.44 101.39 5 0 0 3535.55 107.59 -5 0 0 3622.64 101.49 -5 0 0 3724.33 108.29 6 0 0 32.4 8.2 -6 0 0 19.1 4.5 -6 0 0 24.1 4.2 -6 0 0 18 4.5 -6 0 0 24.3 8.6 -7 0 0 1041.3 31.5 -7 0 0 1024.8 40.9 -7 0 0 1031.4 33.6 -7 0 0 1037.1 33.8 -8 0 0 334.67 13 -8 0 0 340.07 15.6 -8 0 0 368.76 22.6 -8 0 0 353.86 15.7 -9 0 0 606.34 30.4 -9 0 0 581.74 19.6 -9 0 0 648.54 23.8 -9 0 0 589.94 23.1 -10 0 0 18.7 8.5 -10 0 0 38.2 7.1 -10 0 0 26.1 6.7 -10 0 0 24.3 3.8 -11 0 0 164.18 18.6 -11 0 0 140.09 11.9 -11 0 0 155.08 11.6 -12 0 0 229.48 15 -12 0 0 234.08 14.2 -12 0 0 261.57 20.8 -13 0 0 -12.2 5 -13 0 0 -1.4 8.3 -13 0 0 4.1 5.3 -14 0 0 249.88 15.3 -14 0 0 267.77 21.7 -14 0 0 263.57 21.3 -14 0 0 221.28 14.9 -15 0 0 51.79 9.6 -15 0 0 53.59 13.1 -15 0 0 49.3 8.9 -15 0 0 61.09 13.2 -16 0 0 34.2 12.1 -16 0 0 57.79 10.4 -16 0 0 69.19 14.4 -16 0 0 52.89 9.5 -17 0 0 19 9.5 -17 0 0 14.7 6.6 -17 0 0 14.7 10.3 -1 1 0 217.58 12.1 2 -1 0 2296.67 66.19 2 -1 0 2256.67 64.09 2 -1 0 2177.18 63.89 -2 -1 0 2218.18 62.19 -2 -1 0 2229.48 64.29 2 -1 0 2267.17 62.89 -2 1 0 2241.38 66.09 -2 1 0 2298.97 64.39 -2 1 0 2267.97 62.69 -2 1 0 2304.87 64.49 2 1 0 2276.87 64.49 -3 -1 0 584.84 17.7 3 -1 0 631.44 19.8 -3 -1 0 595.44 17.9 3 -1 0 621.64 23.3 -3 -1 0 579.74 20 3 -1 0 565.94 19.4 -3 1 0 576.84 18 3 1 0 598.14 20.4 -3 1 0 623.84 23.3 -3 1 0 610.94 20.4 -3 1 0 585.04 20.2 -4 -1 0 2243.98 63.49 4 -1 0 2313.67 70.39 -4 -1 0 2256.87 63.39 4 -1 0 2295.47 64.49 -4 -1 0 2254.67 65.49 4 -1 0 2288.47 64.49 -4 -1 0 2262.87 69.79 -4 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343.27 14.1 0 2 0 329.47 13.7 0 2 0 336.17 13.6 0 2 0 341.17 13.5 0 2 0 324.97 12 1 -2 0 1099.19 34.7 -1 -2 0 1110.19 34.7 1 -2 0 1110.49 33.9 -1 -2 0 1046.8 33.2 -1 -2 0 1048.9 31.8 1 -2 0 1051.19 34 1 -2 0 1106.79 33.8 -1 -2 0 1102.29 33.5 1 -2 0 1114.59 34.5 -1 2 0 1095.49 33.7 -1 2 0 1132.79 34.5 -1 2 0 1106.09 34.8 -1 2 0 1112.69 34 1 2 0 1115.49 34.7 1 2 0 1069.99 32 1 2 0 978.8 32.8 1 2 0 1119.79 33.2 -1 2 0 1093.69 34.4 2 -2 0 131.59 7.8 2 -2 0 124.49 8.8 -2 -2 0 119.39 8.7 -2 -2 0 126.59 7 -2 -2 0 122.69 7.6 -2 -2 0 123.09 7.1 2 -2 0 116.99 9.2 2 -2 0 125.29 8.4 2 2 0 118.19 8.7 -2 2 0 114.29 8.4 -2 2 0 124.29 7.4 -2 2 0 122.79 8.6 -2 2 0 108.49 9 2 2 0 112.79 6.2 2 2 0 120.39 6.6 -2 2 0 134.59 9.4 -3 -2 0 693.73 24.5 3 -2 0 665.43 23.8 3 -2 0 715.43 26.4 -3 -2 0 659.13 21.9 3 -2 0 682.23 22.3 -3 -2 0 669.03 21.6 3 -2 0 686.03 24 -3 2 0 655.33 24.2 -3 2 0 694.83 22.1 3 2 0 669.93 24.5 -3 2 0 709.53 24.8 -3 2 0 694.63 26.4 4 -2 0 383.26 16.1 4 -2 0 370.36 15.8 4 -2 0 371.56 14.3 -4 -2 0 394.76 16.8 -4 -2 0 396.06 14.1 4 -2 0 383.26 19.2 -4 -2 0 381.96 13.7 -4 2 0 369.26 19.1 -4 2 0 400.36 14 4 2 0 404.86 17.1 -4 2 0 382.56 16.9 -4 2 0 404.76 17.1 -5 -2 0 40.4 4.5 5 -2 0 36 8.5 5 -2 0 23.3 5.2 5 -2 0 20.3 5.1 -5 -2 0 33.5 6.4 -5 2 0 32.6 4.2 5 2 0 44.7 7.1 -5 2 0 32.2 6.9 -5 2 0 34.5 6.6 -5 2 0 65.09 10.8 6 -2 0 10.4 5.9 -6 -2 0 6.6 7.3 6 -2 0 13.6 4.3 -6 -2 0 20 6 -6 -2 0 8.1 4.1 -6 -2 0 12 3.8 6 -2 0 16.5 4.5 -6 2 0 12.4 3.2 -6 2 0 7.2 7.5 6 2 0 11.7 5.6 -6 2 0 17.7 5.9 -6 2 0 16 5.9 7 -2 0 244.98 10.7 -7 -2 0 230.18 11.9 -7 -2 0 234.28 11.3 7 -2 0 244.88 17.9 7 -2 0 242.38 10.7 -7 -2 0 258.07 13.7 -7 2 0 245.18 18.4 -7 2 0 246.78 9.3 -7 2 0 258.67 14.6 7 2 0 223.78 14.2 -7 2 0 268.97 14.6 -8 -2 0 199.68 20.2 8 -2 0 175.78 15.6 -8 -2 0 130.79 9.8 -8 -2 0 143.79 10.7 -8 -2 0 135.69 9.3 -8 2 0 157.38 12.5 -8 2 0 147.99 11.6 -8 2 0 154.28 16 -9 -2 0 9.3 8.6 9 -2 0 15.2 8.2 -9 -2 0 -0.3 4.9 -9 -2 0 6.1 4.6 -9 -2 0 3.8 4.3 -9 2 0 0.2 7.7 -9 2 0 -5.5 5 -9 2 0 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4.2 0 -3 0 3.7 3.9 0 3 0 1.5 3.9 0 3 0 2.7 3 0 3 0 0.5 4.2 0 3 0 5.8 4.5 0 3 0 1.7 4.2 1 -3 0 4720.23 133.49 1 -3 0 4751.22 132.69 1 -3 0 4753.22 133.99 -1 -3 0 4719.03 134.59 -1 -3 0 4648.73 132.89 -1 -3 0 4781.32 134.39 -1 -3 0 4450.95 132.79 1 -3 0 4893.31 134.29 -1 -3 0 4464.65 130.19 1 -3 0 4729.43 134.39 -1 3 0 4758.62 133.39 -1 3 0 4811.62 132.79 -1 3 0 4878.81 134.89 1 3 0 4539.25 130.49 1 3 0 4537.75 132.59 -1 3 0 4772.52 134.19 -1 3 0 4807.52 134.19 1 3 0 4749.32 134.39 1 3 0 4747.12 132.79 -2 -3 0 3041.6 90.19 2 -3 0 3196.78 91.19 2 -3 0 3176.68 92.49 -2 -3 0 3080.09 88.89 -2 -3 0 3017.2 90.39 2 -3 0 3182.08 92.19 -2 -3 0 3206.98 92.69 2 -3 0 3248.58 93.29 -2 3 0 3035.8 93.19 -2 3 0 3086.59 92.29 2 3 0 3129.89 89.79 2 3 0 3107.39 89.59 2 3 0 3229.48 92.79 -2 3 0 3239.88 92.79 -2 3 0 3187.28 90.79 -2 3 0 3135.99 92.39 2 3 0 3215.38 89.39 3 -3 0 240.28 12.6 3 -3 0 242.58 14.1 -3 -3 0 242.28 12.1 -3 -3 0 245.08 14.2 -3 -3 0 233.08 11.6 3 -3 0 261.27 15 -3 -3 0 236.68 12 3 -3 0 229.68 13 -3 3 0 263.87 15.2 -3 3 0 241.08 12 3 3 0 241.88 10.3 -3 3 0 277.37 15.6 -3 3 0 246.08 14.1 -3 3 0 251.77 13.9 3 3 0 242.28 14.1 3 3 0 227.38 10.4 -4 -3 0 472.45 20.1 -4 -3 0 488.25 21 4 -3 0 471.05 18.5 -4 -3 0 467.45 17.7 4 -3 0 463.85 20.2 4 -3 0 460.15 19.8 4 -3 0 474.85 22.3 -4 -3 0 486.55 18.3 -4 3 0 474.25 22.6 -4 3 0 496.55 21.6 -4 3 0 487.55 23.1 -4 3 0 480.45 18 -4 3 0 472.75 20.8 4 3 0 462.25 20.9 -5 -3 0 117.69 10.9 5 -3 0 96.59 8.3 -5 -3 0 111.49 8 5 -3 0 112.19 10.1 5 -3 0 104.29 9.4 5 -3 0 136.79 13 -5 -3 0 111.09 8.4 -5 3 0 107.89 12.8 -5 3 0 95.89 10.2 5 3 0 104.39 10.4 -5 3 0 108.79 11.2 -5 3 0 103.09 7.8 -5 3 0 130.59 14.6 6 -3 0 1336.57 43.1 -6 -3 0 1277.67 41.1 -6 -3 0 1291.17 40.7 -6 -3 0 1367.36 44.4 6 -3 0 1345.97 48.3 6 -3 0 1321.17 42.8 6 3 0 1347.77 45.1 -6 3 0 1295.57 39.8 -6 3 0 1393.56 45.7 -6 3 0 1289.97 48.2 -6 3 0 1328.67 45 7 -3 0 121.39 9.9 -7 -3 0 115.29 8.8 -7 -3 0 112.99 11 -7 -3 0 122.49 8.7 7 -3 0 133.59 14.2 7 -3 0 112.49 9.2 -7 3 0 124.99 11.6 -7 3 0 113.99 7.2 -7 3 0 108.79 13.9 -7 3 0 121.19 12 7 3 0 106.29 10.8 8 -3 0 606.74 22 -8 -3 0 625.94 30.1 -8 -3 0 615.94 24.7 -8 -3 0 584.74 22.4 8 -3 0 629.94 22 -8 -3 0 620.24 22.3 8 -3 0 597.54 29.9 -8 3 0 597.04 29.8 -8 3 0 682.23 27 -8 3 0 547.15 26.9 8 3 0 573.24 25.2 -8 3 0 606.34 19.3 -9 -3 0 143.49 10.2 -9 -3 0 136.69 9.9 -9 -3 0 178.78 17.7 9 -3 0 173.98 16.4 -9 -3 0 152.58 12.1 9 -3 0 141.39 8.1 9 -3 0 144.69 7.9 -9 3 0 162.28 18.7 -9 3 0 155.68 22.7 -9 3 0 162.58 13.1 -9 3 0 162.48 17.1 -10 -3 0 47.7 8.1 -10 -3 0 38.5 11.2 -10 -3 0 42.4 6.6 -10 -3 0 37.6 6 10 -3 0 39.9 12 -10 3 0 37.8 8.4 -10 3 0 16.6 9.5 -10 3 0 37.6 9.1 -10 3 0 39.2 10.8 -11 -3 0 125.59 10 -11 -3 0 125.09 11 11 -3 0 186.18 30.2 -11 -3 0 104.09 9.6 -11 -3 0 133.29 16 -11 3 0 152.88 18.3 -11 3 0 120.79 13.5 -11 3 0 135.29 14.4 -11 3 0 153.78 18 -12 -3 0 -2.1 5.1 -12 -3 0 1.7 4.8 -12 -3 0 -2.1 7.9 -12 -3 0 8.2 5.2 -12 3 0 -3.8 9.3 -12 3 0 -1.3 6.8 -12 3 0 -0.4 6.4 -12 3 0 -0.1 8.4 -13 -3 0 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235.68 13.5 1 4 0 218.88 10.7 1 4 0 215.08 13.9 -1 4 0 213.88 12.1 1 4 0 205.48 12.3 -1 4 0 216.98 13.4 -1 4 0 218.68 13.5 1 4 0 238.28 14.9 -2 -4 0 4668.73 133.49 -2 -4 0 4550.54 131.39 -2 -4 0 4554.54 131.19 -2 -4 0 4214.58 127.79 2 -4 0 4488.65 133.19 2 -4 0 4734.63 132.19 -2 -4 0 4704.93 133.99 2 -4 0 4678.53 133.29 2 -4 0 4631.84 132.89 2 4 0 4544.15 133.29 -2 4 0 4777.62 134.39 -2 4 0 4735.43 133.59 -2 4 0 4626.74 132.29 -2 4 0 4626.74 131.59 2 4 0 4262.17 129.99 -2 4 0 4611.14 133.19 2 4 0 4624.74 128.59 2 4 0 4553.84 130.19 -3 -4 0 579.74 22.8 3 -4 0 567.04 24.2 -3 -4 0 586.24 22.8 3 -4 0 604.54 25.2 3 -4 0 610.04 26 -3 -4 0 580.34 21.4 -3 -4 0 591.34 25.5 3 -4 0 603.84 23.9 -3 4 0 629.64 25.8 3 4 0 573.04 25.2 3 4 0 588.24 21.7 -3 4 0 582.54 26.4 -3 4 0 623.04 23.2 3 4 0 567.54 21.4 -3 4 0 580.54 25 -3 4 0 599.34 25.6 -4 -4 0 1353.56 46 4 -4 0 1312.87 47.1 -4 -4 0 1253.27 42.6 -4 -4 0 1306.47 42.9 -4 -4 0 1382.86 42.9 4 -4 0 1373.86 43.7 4 -4 0 1297.27 45.3 4 -4 0 1336.97 44.9 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661.63 26.7 0 -4 3 705.93 27 0 -4 3 763.42 28.5 0 -4 -3 739.83 29 0 4 3 716.33 27.5 0 4 -3 765.22 28.5 0 4 -3 752.82 28.7 0 4 3 692.53 27.1 0 4 3 712.93 28.4 0 4 3 723.53 28 0 4 3 659.43 22.8 0 4 -3 752.72 27.9 0 4 -3 729.63 29 0 4 -3 761.32 29 -1 -4 -3 29.9 8 1 -4 3 29.4 7.9 -1 -4 -3 17.9 5.2 -1 -4 -3 20 6.5 1 -4 3 17.3 6.1 1 -4 3 19.7 7.3 1 -4 3 14.8 5.5 1 -4 3 17.9 6.5 -1 -4 -3 12 5.3 1 4 3 8.7 4.8 1 4 3 19.8 6.1 -1 4 -3 21.4 6.6 1 4 3 20.1 5.7 -1 4 -3 13.3 5.8 -1 4 -3 8.9 6 -1 4 -3 17.1 6.5 1 4 3 18.5 6 -1 4 -3 17.7 6.7 2 -4 3 18.9 6 2 -4 3 27.4 7.1 -2 -4 -3 17.2 5.6 -2 -4 -3 35.9 9 -2 -4 -3 14.4 4.8 2 -4 3 24.2 6.6 -2 -4 -3 24.8 6.1 2 -4 3 19 6.7 2 -4 3 22.5 6.6 -2 4 -3 26.1 7.3 2 4 3 34.2 8.7 2 4 3 25 5.2 -2 4 -3 30.5 7.4 -2 4 -3 21.5 7.4 2 4 3 29.6 5.6 -2 4 -3 29.9 7.1 -2 4 -3 15.1 6.2 -3 -4 -3 115.79 9.4 -3 -4 -3 138.59 13.4 3 -4 3 145.49 12 3 -4 3 136.89 12.5 3 -4 3 162.38 11.8 3 -4 3 162.18 12.7 -3 -4 -3 117.99 7 3 -4 3 135.19 12.7 -3 -4 -3 109.49 9.6 3 4 3 145.09 15 3 4 3 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3 247.78 37.7 12 -5 -3 239.18 13.6 -12 -5 3 221.88 15 -12 -5 3 205.38 14.6 -12 -5 3 229.88 15.2 -12 5 3 193.98 20.2 12 5 -3 187.88 14.7 -12 5 3 241.08 21.4 -12 5 3 250.17 18.7 -11 -5 3 49.2 9 -11 -5 3 47.8 9 11 -5 -3 45.6 8 11 -5 -3 40.4 8.1 -11 -5 3 46.7 11.7 -11 -5 3 58.29 9.4 -11 -5 3 38 10.8 -11 5 3 36 9.8 -11 5 3 42.8 11.9 -11 5 3 37.7 11.9 11 5 -3 40.8 8.9 10 -5 -3 420.26 27 -10 -5 3 401.36 22.8 -10 -5 3 395.26 20.8 10 -5 -3 420.66 20.4 -10 -5 3 413.86 24.4 -10 -5 3 435.36 21.8 -10 5 3 396.86 24.2 -10 5 3 501.75 25.6 10 5 -3 438.66 22.2 -10 5 3 455.95 27.6 9 -5 -3 154.48 23.3 -9 -5 3 131.59 12.1 -9 -5 3 112.19 12.5 -9 -5 3 127.49 14 -9 -5 3 135.29 16.3 9 -5 -3 130.49 11.7 -9 5 3 165.18 17.3 -9 5 3 125.99 17.3 -9 5 3 126.69 15.7 9 5 -3 137.69 13.3 -8 -5 3 33.7 9 8 -5 -3 56.39 12.4 -8 -5 3 66.39 18.2 8 -5 -3 51.79 7 -8 -5 3 51.69 8.8 8 -5 -3 51.49 8.8 -8 -5 3 55.39 10.1 8 -5 -3 45.1 15 8 5 -3 42.7 9.9 -8 5 3 45.3 6.5 -8 5 3 43.3 11.8 -8 5 3 77.39 12.3 -8 5 3 77.79 12.6 -7 -5 3 131.29 12.2 7 -5 -3 150.88 13.4 7 -5 -3 145.39 15.6 -7 -5 3 168.68 19.5 -7 -5 3 132.59 13 7 -5 -3 138.49 10.8 -7 -5 3 141.89 13.8 7 5 -3 137.39 13.4 -7 5 3 150.28 16.3 7 5 -3 134.39 8.4 -7 5 3 146.89 13.8 7 5 -3 132.29 7.9 -7 5 3 113.39 9.6 -7 5 3 132.49 16 -6 -5 3 38.3 8.4 6 -5 -3 27.1 6.8 -6 -5 3 18.4 6.6 6 -5 -3 22.4 10 -6 -5 3 27.7 8.8 6 -5 -3 26.7 8 -6 -5 3 23.7 7.5 6 -5 -3 29.4 7.5 6 5 -3 21.6 8.2 6 5 -3 25.6 5.9 -6 5 3 25.5 5.7 -6 5 3 25.1 8.9 -6 5 3 23.5 8.9 6 5 -3 21.7 4.9 -6 5 3 40.4 10.9 -5 -5 3 1999 64.69 -5 -5 3 1997.2 64.89 -5 -5 3 1984.5 64.99 5 -5 -3 2002.9 68.19 5 -5 -3 2050.59 67.39 5 -5 -3 1951 65.69 -5 -5 3 2064.89 66.49 5 -5 -3 2100.39 63.39 -5 5 3 2062.49 62.69 -5 5 3 2109.19 71.09 5 5 -3 1998.1 62.09 -5 5 3 2023.5 67.39 5 5 -3 2007.1 62.59 5 5 -3 2008.5 67.29 -5 5 3 2162.28 69.59 4 -5 -3 155.98 16.2 -4 -5 3 124.79 12.3 4 -5 -3 118.49 12.1 -4 -5 3 118.89 10.9 -4 -5 3 127.09 11.7 -4 -5 3 129.19 14.4 4 -5 -3 117.99 13.7 4 -5 -3 123.99 11.9 4 5 -3 121.39 11.5 -4 5 3 139.29 14.2 -4 5 3 132.79 11.2 -4 5 3 122.29 14.4 4 5 -3 130.49 10.8 -4 5 3 117.79 13.2 4 5 -3 117.79 12.6 3 -5 -3 1272.77 42.9 -3 -5 3 1251.47 44.9 -3 -5 3 1109.59 42.6 -3 -5 3 1209.78 41.4 -3 -5 3 1212.38 43.1 3 -5 -3 1253.87 45.1 -3 5 3 1283.87 42.9 -3 5 3 1108.49 43.5 3 5 -3 1288.67 43 -3 5 3 1212.48 42 3 5 -3 1240.68 42.3 -3 5 3 1231.38 48.1 -3 5 3 1253.57 45.4 3 5 -3 1220.88 41.8 3 5 -3 1205.68 44.4 -2 -5 3 610.14 25.7 -2 -5 3 560.34 25.1 2 -5 -3 557.94 26.2 -2 -5 3 598.34 26.8 2 -5 -3 579.84 25.4 -2 -5 3 572.64 26.7 -2 -5 3 553.54 23.2 2 -5 -3 605.64 25.7 2 -5 -3 554.74 25.1 -2 5 3 616.24 27 2 5 -3 595.04 25.5 -2 5 3 576.74 23.3 -2 5 3 591.54 26.4 -2 5 3 594.24 24.9 2 5 -3 530.55 23.9 -2 5 3 524.95 25.2 2 5 -3 551.64 25.9 2 5 -3 578.34 24 -1 -5 3 54.79 7.9 1 -5 -3 37.6 7.7 1 -5 -3 103.59 12.8 -1 -5 3 54.69 8.8 -1 -5 3 39.5 8.1 1 -5 -3 44.5 8 -1 -5 3 52.39 9.7 1 -5 -3 63.39 10.6 -1 -5 3 41.4 8.4 -1 5 3 69.39 10.7 -1 5 3 69.49 10.4 -1 5 3 71.69 10.4 1 5 -3 70.19 10.3 1 5 -3 70.39 9.4 1 5 -3 64.99 10 -1 5 3 59.89 7.3 -1 5 3 69.89 10.1 1 5 -3 75.69 10.1 0 -5 3 1285.27 45.2 0 -5 3 1255.07 45.3 0 -5 -3 1234.58 43.4 0 -5 3 1278.97 44.8 0 -5 -3 1318.27 44.7 0 -5 3 1293.87 43.1 0 -5 3 1206.18 43.9 0 -5 -3 1324.17 45.7 0 -5 -3 1166.78 43.5 0 5 3 1249.77 44.7 0 5 -3 1301.57 44.6 0 5 -3 1339.57 43.8 0 5 3 1285.47 43.7 0 5 -3 1296.67 44.9 0 5 -3 1249.57 44.6 0 5 3 1290.97 45.1 0 5 3 1228.38 38.4 0 5 -3 1229.18 45.3 0 5 3 1306.37 44 -1 -5 -3 89.89 10.3 1 -5 3 117.69 13.5 -1 -5 -3 100.89 12.4 1 -5 3 98.69 10.2 -1 -5 -3 108.99 10.2 -1 -5 -3 110.29 12.1 1 -5 3 149.39 15.5 1 -5 3 88.99 10.5 1 -5 3 101.69 12.3 1 5 3 98.19 10.4 -1 5 -3 118.69 13.8 -1 5 -3 114.99 12.1 -1 5 -3 110.49 13.5 1 5 3 117.59 12.3 -1 5 -3 106.09 10.5 1 5 3 91.29 5.6 -1 5 -3 110.39 11.5 1 5 3 102.49 11 1 5 3 95.09 11.8 -2 -5 -3 1166.28 40.8 -2 -5 -3 1221.28 44.5 -2 -5 -3 1260.07 43.2 2 -5 3 1245.88 44.1 2 -5 3 1208.98 43.5 2 -5 3 1231.98 43.5 2 -5 3 1251.77 42.9 2 -5 3 1239.78 43.3 -2 -5 -3 1192.68 41.2 2 5 3 1147.49 46.1 2 5 3 1081.79 39 -2 5 -3 1232.88 43.5 2 5 3 1237.38 40.3 -2 5 -3 1200.78 42.7 -2 5 -3 1176.48 43.5 -2 5 -3 1196.68 43.6 -2 5 -3 1242.38 44.5 3 -5 3 149.99 14 -3 -5 -3 154.18 11.1 3 -5 3 168.38 13.7 -3 -5 -3 142.29 12.7 -3 -5 -3 181.98 15.5 -3 -5 -3 136.69 11.2 -3 -5 -3 144.89 6.8 3 -5 3 175.88 12.9 3 -5 3 169.68 15.9 3 5 3 157.68 9.5 3 5 3 180.98 15 -3 5 -3 163.58 14.5 -3 5 -3 175.28 14.3 -3 5 -3 169.38 13.1 -3 5 -3 148.69 14.5 3 5 3 153.18 10 4 -5 3 878.81 34.7 4 -5 3 821.62 32.6 4 -5 3 853.51 32.6 -4 -5 -3 777.12 33.7 -4 -5 -3 752.92 28.8 -4 -5 -3 790.92 26.1 4 -5 3 820.52 31.8 4 -5 3 875.41 34.2 -4 -5 -3 800.32 29.3 -4 5 -3 814.12 34.2 -4 5 -3 830.82 39.3 -4 5 -3 856.01 33.8 -4 5 -3 840.52 32.9 4 5 3 782.82 33.9 -4 5 -3 790.32 31.1 5 -5 3 1005.6 37.3 -5 -5 -3 979.2 33 5 -5 3 1038.4 39.8 -5 -5 -3 970.7 33.5 -5 -5 -3 997.1 43.7 5 -5 3 1039.2 37.3 -5 -5 -3 1003.9 33.6 5 -5 3 1010.6 36.4 -5 5 -3 1000.4 40.3 -5 5 -3 939.71 35.4 5 5 3 971.9 39.2 -5 5 -3 1017.8 40.9 -5 5 -3 1067.09 39.6 -5 5 -3 983.3 38 6 -5 3 23.6 8.1 -6 -5 -3 32.1 5.9 6 -5 3 27.8 7.8 -6 -5 -3 29.6 6.3 6 -5 3 19.3 6.7 -6 -5 -3 30.2 8.9 -6 -5 -3 34.7 6.9 6 -5 3 24.5 7.4 -6 5 -3 18.3 9.6 -6 5 -3 22.7 7.6 6 5 3 32.1 9 -6 5 -3 35.9 7.4 -6 5 -3 17.2 8.5 -6 5 -3 36.4 9.6 7 -5 3 35.5 7 -7 -5 -3 51.19 11.1 -7 -5 -3 37.1 6.1 -7 -5 -3 34.7 6.4 7 -5 3 36.4 7.8 7 -5 3 29.6 10.7 -7 5 -3 27.7 7.7 -7 5 -3 30 9.6 7 5 3 53.39 11 -7 5 -3 43.3 7.9 -7 5 -3 31.7 10.6 -7 5 -3 42.3 10.1 -8 -5 -3 51.99 7.2 8 -5 3 68.09 8.4 8 -5 3 49.9 8.1 -8 -5 -3 57.19 11.5 -8 -5 -3 43.5 6.7 8 -5 3 49.99 10.7 -8 5 -3 53.99 9.8 -8 5 -3 55.99 10.7 -8 5 -3 68.39 13.2 8 5 3 66.59 11.9 -8 5 -3 59.69 13.6 -8 5 -3 50.19 7.7 9 -5 3 385.06 23.8 9 -5 3 367.06 16.1 9 -5 3 342.47 15.6 -9 -5 -3 353.46 15.6 -9 -5 -3 346.17 15.5 -9 -5 -3 348.57 20.8 -9 5 -3 346.87 16.1 -9 5 -3 376.56 24.7 -9 5 -3 370.06 21.6 -9 5 -3 402.56 24.2 -9 5 -3 359.36 20.6 10 -5 3 169.28 8.2 10 -5 3 203.88 28.6 -10 -5 -3 184.28 15.9 -10 -5 -3 202.98 17.7 -10 -5 -3 156.48 10.3 10 -5 3 156.88 7.9 -10 -5 -3 188.28 10.8 -10 5 -3 165.28 15.8 -10 5 -3 209.18 16.5 -10 5 -3 200.58 18.9 -10 5 -3 181.68 10.5 -10 5 -3 208.38 22.8 -11 -5 -3 141.29 16.4 -11 -5 -3 118.29 9.1 -11 -5 -3 132.39 13.7 11 -5 3 154.88 29.2 -11 -5 -3 124.09 9.4 -11 5 -3 137.19 8.8 -11 5 -3 128.89 14.7 -11 5 -3 145.19 20.7 -11 5 -3 136.09 17.6 -11 5 -3 139.49 15.2 -12 -5 -3 127.69 9.7 -12 -5 -3 140.69 13.5 -12 -5 -3 116.49 9.6 -12 -5 -3 139.69 13.9 -12 -5 -3 124.29 16 -12 5 -3 144.19 21.2 -12 5 -3 124.79 17 -12 5 -3 141.29 15.3 -12 5 -3 123.39 7.6 -13 -5 -3 34.7 10.9 -13 -5 -3 19.1 7.8 -13 -5 -3 21.8 7.2 -13 -5 -3 43.5 6.7 -13 -5 -3 26.1 6 -13 5 -3 41.2 12.2 -13 5 -3 21.1 8.4 -13 5 -3 29.8 10.6 -14 -5 -3 51.19 10.3 -14 -5 -3 72.49 10.4 -14 -5 -3 65.69 13.7 -14 -5 -3 62.19 7.5 -14 -5 -3 43.3 7.2 -14 5 -3 33.2 10.6 -14 5 -3 32.3 16.3 -14 5 -3 86.09 12.7 -14 5 -3 72.79 15.1 -15 -5 -3 3.8 8.2 -15 -5 -3 9.4 6.7 -15 -5 -3 11.8 5.2 -15 -5 -3 5.5 4.5 -15 -5 -3 5.9 7.3 -15 5 -3 1.5 8.8 -15 5 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3 268.57 19.2 -11 6 3 228.58 21.2 -11 6 3 209.58 19.7 11 6 -3 224.78 17.6 -11 6 3 199.88 28.1 10 -6 -3 44.2 11.3 10 -6 -3 72.29 11.7 10 -6 -3 71.69 9.6 -10 -6 3 76.09 10.8 -10 -6 3 84.09 12.4 -10 -6 3 68.79 11.9 -10 -6 3 65.79 10.2 -10 6 3 59.99 11.9 -10 6 3 48.5 13.1 -10 6 3 58.39 12.9 -10 6 3 55.49 13.2 10 6 -3 46.8 10 9 -6 -3 121.29 10.1 9 -6 -3 121.59 11.7 -9 -6 3 113.09 13.1 -9 -6 3 119.09 13.3 9 -6 -3 138.99 15.2 9 -6 -3 140.99 21.3 -9 -6 3 112.09 14 -9 -6 3 139.69 14.9 -9 6 3 143.09 18.3 -9 6 3 146.49 17.9 9 6 -3 125.29 15.1 -9 6 3 110.79 8.5 -9 6 3 158.88 18 -9 6 3 125.69 15.4 -8 -6 3 616.64 27.2 -8 -6 3 549.85 27.1 8 -6 -3 607.84 26.6 8 -6 -3 554.94 22.8 -8 -6 3 582.54 27.9 8 -6 -3 596.74 30 -8 -6 3 566.14 25.6 8 -6 -3 587.14 27.9 8 6 -3 542.95 26.8 -8 6 3 492.55 27.4 -8 6 3 592.04 30.4 -8 6 3 562.74 30.5 -8 6 3 571.74 22.2 -8 6 3 600.24 29.1 7 -6 -3 13.4 7.6 -7 -6 3 7.4 6.5 7 -6 -3 6 8.7 7 -6 -3 13.3 6.5 -7 -6 3 3.1 6.8 -7 -6 3 -3 6.2 7 -6 -3 18.7 7.7 -7 -6 3 5.1 10.7 7 6 -3 14.1 7.9 -7 6 3 21.5 8.5 -7 6 3 2.5 4.5 7 6 -3 13.7 4.6 -7 6 3 15 9.7 -7 6 3 14.5 8.8 -7 6 3 16.1 9.4 -6 -6 3 473.75 22.6 6 -6 -3 463.15 23.1 -6 -6 3 488.55 22.7 -6 -6 3 461.45 23.9 -6 -6 3 420.26 21.7 6 -6 -3 476.15 21.7 6 -6 -3 469.15 25.2 6 -6 -3 465.35 25.5 -6 6 3 472.65 26.7 -6 6 3 451.25 20.3 6 6 -3 469.45 24 -6 6 3 469.25 25.4 -6 6 3 444.56 24.4 6 6 -3 447.76 19.2 6 6 -3 454.25 19.8 -6 6 3 446.06 25 5 -6 -3 26.9 7.9 -5 -6 3 24.5 7.8 -5 -6 3 29.1 8.1 -5 -6 3 25.1 9.1 5 -6 -3 15.4 8.2 5 -6 -3 25.1 8 -5 -6 3 24.4 7 5 -6 -3 24.9 8.7 -5 6 3 43.2 10.2 -5 6 3 29.5 7.7 5 6 -3 31.3 7 -5 6 3 35.7 9.2 -5 6 3 30.9 10.4 5 6 -3 30.8 7.2 5 6 -3 29.8 9 -5 6 3 28.8 8.3 5 6 -3 27 8.9 4 -6 -3 1018.1 40.4 -4 -6 3 1117.79 40.9 4 -6 -3 1180.98 43.3 4 -6 -3 1095.29 40.3 -4 -6 3 1109.09 44.4 4 -6 -3 1114.19 43 -4 -6 3 1083.49 40.5 -4 -6 3 1114.89 38.8 -4 6 3 1120.09 41.2 -4 6 3 1103.59 42.4 4 6 -3 1060.29 39.3 -4 6 3 1098.39 39.3 4 6 -3 1090.49 42 -4 6 3 1208.28 44.5 4 6 -3 1093.69 40 4 6 -3 1024.4 38.2 -4 6 3 1026.3 41.8 3 -6 -3 343.57 19.8 3 -6 -3 367.66 20.7 3 -6 -3 340.17 20 -3 -6 3 348.47 17.3 -3 -6 3 355.96 21 3 -6 -3 326.17 24.2 -3 -6 3 345.77 19.5 -3 -6 3 355.66 33.6 -3 -6 3 374.16 20.7 -3 6 3 347.17 18.9 -3 6 3 379.76 22.8 3 6 -3 319.27 20.6 3 6 -3 362.76 18.8 -3 6 3 331.17 18.9 -3 6 3 335.07 20.2 3 6 -3 340.27 18.9 3 6 -3 364.16 18.5 2 -6 -3 855.21 33 2 -6 -3 824.62 34.5 2 -6 -3 807.42 32.9 -2 -6 3 760.92 33.7 -2 -6 3 740.03 32.1 -2 -6 3 773.02 29.6 -2 -6 3 762.42 32.2 -2 -6 3 764.12 33.1 2 -6 -3 769.62 32.5 2 6 -3 769.52 31.9 2 6 -3 773.12 33.2 -2 6 3 797.22 33.3 -2 6 3 811.42 34.2 -2 6 3 778.72 32.7 -2 6 3 797.92 32.8 -2 6 3 811.42 30.1 2 6 -3 796.52 34.5 2 6 -3 815.52 30.6 1 -6 -3 1595.44 54.19 -1 -6 3 1628.04 55.89 1 -6 -3 1630.04 55.09 -1 -6 3 1565.84 54.39 -1 -6 3 1556.04 54.29 1 -6 -3 1560.34 54.99 1 -6 -3 1626.34 55.19 -1 -6 3 1593.64 55.49 -1 -6 3 1607.24 51.79 -1 6 3 1528.15 49.4 -1 6 3 1580.24 55.19 -1 6 3 1602.94 54.69 1 6 -3 1585.74 52.19 1 6 -3 1635.84 54.69 -1 6 3 1631.14 59.49 1 6 -3 1555.34 57.49 -1 6 3 1481.15 53.89 1 6 -3 1538.55 54.59 0 -6 -3 312.47 20.8 0 -6 3 335.67 19.9 0 -6 3 358.06 21.8 0 -6 3 352.56 20.5 0 -6 -3 357.06 20.2 0 -6 3 325.97 17.5 0 -6 -3 340.47 20.9 0 -6 3 334.17 19.3 0 6 -3 351.66 20.3 0 6 3 310.77 14 0 6 -3 348.37 18.7 0 6 3 343.37 20.4 0 6 3 389.46 20 0 6 -3 319.87 19.7 0 6 3 322.57 18.3 0 6 -3 329.77 19.1 0 6 -3 307.57 20.1 0 6 3 347.07 19.9 -1 -6 -3 1523.85 51.89 -1 -6 -3 1611.14 54.49 1 -6 3 1487.85 52.59 1 -6 3 1456.05 51.99 1 -6 3 1522.45 53.59 -1 -6 -3 1506.55 51.69 1 -6 3 1550.24 53.39 1 -6 3 1541.35 51.19 -1 6 -3 1508.55 52.39 -1 6 -3 1562.64 51.69 1 6 3 1506.45 52.99 1 6 3 1511.05 53.39 1 6 3 1511.75 50.69 1 6 3 1501.35 50.49 -1 6 -3 1477.15 52.79 1 6 3 1463.35 44.4 -1 6 -3 1522.25 53.99 -1 6 -3 1484.25 52.09 -2 -6 -3 556.04 33.4 -2 -6 -3 643.14 26.6 2 -6 3 660.03 29.3 2 -6 3 665.73 29.2 -2 -6 -3 585.04 26.7 2 -6 3 665.03 28.3 2 -6 3 625.64 28.9 -2 6 -3 656.83 28.8 2 6 3 592.64 25.4 2 6 3 626.04 19.9 -2 6 -3 640.34 28.6 -2 6 -3 702.23 30.8 2 6 3 662.33 29.7 2 6 3 612.24 25.4 -2 6 -3 695.73 28.9 3 -6 3 800.62 32.8 -3 -6 -3 708.23 28.7 -3 -6 -3 725.63 29.3 3 -6 3 725.93 31.6 -3 -6 -3 684.73 22 3 -6 3 763.92 31.8 3 -6 3 725.83 30.6 -3 -6 -3 783.72 31.7 -3 -6 -3 781.22 33.8 3 -6 3 756.92 31.9 -3 6 -3 798.72 32.9 -3 6 -3 781.12 33.2 3 6 3 702.53 26.7 3 6 3 762.62 27.5 -3 6 -3 742.53 33.8 3 6 3 752.72 32.8 -3 6 -3 735.03 31.4 -3 6 -3 743.03 33.9 4 -6 3 374.96 21.5 4 -6 3 445.86 23.3 4 -6 3 417.96 25.5 -4 -6 -3 409.06 22.1 4 -6 3 409.66 22.2 4 -6 3 421.86 21.1 -4 -6 -3 363.56 14.1 -4 -6 -3 405.16 24 -4 -6 -3 436.56 20.2 -4 -6 -3 403.46 19.4 -4 6 -3 434.16 24.2 4 6 3 401.96 15.8 4 6 3 397.66 22.9 -4 6 -3 421.36 23.7 -4 6 -3 416.66 31.3 -4 6 -3 412.76 22.1 4 6 3 393.56 15.5 -4 6 -3 390.96 22.6 -5 -6 -3 203.18 12.8 -5 -6 -3 201.08 13.3 5 -6 3 180.08 15.5 5 -6 3 212.48 26.8 -5 -6 -3 205.08 17.6 5 -6 3 183.68 15.7 5 -6 3 196.48 14.5 -5 -6 -3 174.88 9.9 -5 6 -3 187.18 17.4 5 6 3 199.78 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133.89 12.7 10 -3 -4 173.78 11.7 -10 -3 4 156.48 13.2 -10 -3 4 181.28 18.1 -10 -3 4 142.79 11.5 -10 -3 4 133.69 16.5 10 -3 -4 151.08 12.1 -10 3 4 164.78 15.6 10 3 -4 120.59 11.3 -10 3 4 166.68 19.2 -9 -3 4 334.97 17.3 -9 -3 4 376.66 23.2 -9 -3 4 335.57 18.4 9 -3 -4 369.76 17.9 -9 -3 4 372.56 24.1 9 -3 -4 396.86 19.2 9 -3 -4 336.57 23.4 -9 3 4 381.36 24.2 9 3 -4 368.96 17.9 -9 3 4 373.96 21.1 -9 3 4 403.96 21.8 8 -3 -4 149.88 15.8 8 -3 -4 127.19 11 -8 -3 4 142.19 12 8 -3 -4 156.28 13.2 -8 -3 4 135.79 11.5 -8 -3 4 133.99 11.5 -8 -3 4 145.09 14.7 -8 3 4 181.68 20 -8 3 4 163.28 14.6 8 3 -4 122.09 11.4 -8 3 4 139.09 13.1 -7 -3 4 1129.99 39.9 7 -3 -4 1128.39 40.4 7 -3 -4 1216.18 41.9 -7 -3 4 1193.58 44.9 -7 -3 4 1145.79 39.3 7 -3 -4 1211.48 45.4 -7 -3 4 1146.39 40.8 -7 3 4 1171.68 42.9 -7 3 4 1162.58 42.5 7 3 -4 1164.48 36.5 7 3 -4 1079.19 35.4 7 3 -4 1113.69 39.4 -7 3 4 1185.38 45.7 -6 -3 4 -5.7 5.9 6 -3 -4 -5.1 5.7 -6 -3 4 0 5.2 -6 -3 4 6.8 5.5 -6 -3 4 3.8 5.5 6 -3 -4 -2.3 5.8 6 -3 -4 -3 3 6 -3 -4 8.4 5.3 6 3 -4 -1.1 4.9 -6 3 4 -12.9 8.1 -6 3 4 3.2 6.4 6 3 -4 2.7 4 6 3 -4 -5.5 4.4 -5 -3 4 1087.79 41.1 -5 -3 4 1145.39 39 5 -3 -4 1100.59 39.6 5 -3 -4 1133.59 40.9 -5 -3 4 1133.99 39.5 -5 -3 4 1128.89 38.9 5 -3 -4 1122.79 35.1 5 3 -4 1146.39 37.8 5 3 -4 1058.19 36.7 -5 3 4 1181.98 42.8 5 3 -4 1130.19 38.9 -5 3 4 1132.19 41.1 -5 3 4 1127.89 41.2 4 -3 -4 1853.31 62.29 4 -3 -4 1957 57.49 -4 -3 4 1955.8 62.09 4 -3 -4 1948.41 62.29 -4 -3 4 1879.51 60.29 -4 -3 4 1855.41 60.49 -4 -3 4 1960.2 60.49 -4 3 4 1959.1 62.39 -4 3 4 1901.41 57.39 4 3 -4 1884.21 59.49 -4 3 4 1954.5 62.09 4 3 -4 1925.41 62.89 4 3 -4 1874.41 58.89 -4 3 4 1982.2 63.19 4 3 -4 1949.8 60.49 3 -3 -4 368.56 16 -3 -3 4 330.17 16.7 3 -3 -4 345.67 17.8 -3 -3 4 330.07 17.5 3 -3 -4 358.36 18.8 -3 -3 4 338.27 17.7 -3 -3 4 332.27 17.1 3 -3 -4 329.47 17.2 -3 3 4 351.46 18.3 3 3 -4 356.16 17.4 3 3 -4 323.27 18 -3 3 4 323.07 15.1 -3 3 4 336.87 17.9 3 3 -4 340.07 16.4 -3 3 4 326.67 18 3 3 -4 363.66 17.3 -2 -3 4 1523.05 51.09 2 -3 -4 1608.24 51.09 -2 -3 4 1588.94 51.09 2 -3 -4 1598.24 52.19 -2 -3 4 1599.14 51.09 -2 -3 4 1592.54 51.69 2 -3 -4 1618.64 51.49 2 -3 -4 1649.33 50.49 -2 3 4 1607.24 50.19 2 3 -4 1634.14 50.89 -2 3 4 1503.05 51.59 2 3 -4 1603.84 51.29 -2 3 4 1564.34 51.59 2 3 -4 1555.14 51.29 -2 3 4 1624.24 51.39 2 3 -4 1672.83 51.79 -1 -3 4 104.99 9.9 1 -3 -4 105.19 10.1 -1 -3 4 94.59 9 1 -3 -4 118.89 10.7 1 -3 -4 105.09 9.2 -1 -3 4 92.49 9.4 -1 -3 4 86.19 9.3 -1 -3 4 90.49 9.9 1 -3 -4 96.69 10.2 1 3 -4 93.79 10.1 -1 3 4 102.59 9.2 1 3 -4 115.39 11.6 -1 3 4 82.69 8.9 -1 3 4 92.69 9.5 1 3 -4 111.49 9.6 -1 3 4 93.59 9.3 1 3 -4 108.69 9.9 0 -3 -4 785.22 27.4 0 -3 -4 725.13 25.9 0 -3 4 715.13 26.7 0 -3 4 729.43 27 0 -3 -4 754.32 28.1 0 -3 4 738.83 27.3 0 -3 -4 659.63 24.9 0 -3 4 742.83 27 0 -3 4 745.93 28 0 3 4 697.13 25.6 0 3 -4 689.23 26.9 0 3 -4 707.23 26.9 0 3 4 671.13 26 0 3 -4 706.73 26.9 0 3 4 680.73 25.4 0 3 -4 705.43 27.1 0 3 4 722.03 27.5 0 3 -4 697.03 27.2 1 -3 4 848.62 29.4 -1 -3 -4 795.62 27.4 1 -3 4 770.42 29.9 1 -3 4 792.52 29.5 1 -3 4 805.42 28.8 -1 -3 -4 800.52 27.1 -1 -3 -4 820.42 30.6 -1 -3 -4 785.72 27.8 1 -3 4 775.22 28.6 -1 3 -4 776.92 29.2 -1 3 -4 736.83 29.2 -1 3 -4 768.32 28.8 -1 3 -4 783.32 29.4 1 3 4 754.12 26.2 1 3 4 781.12 27.6 1 3 4 820.42 30.4 1 3 4 811.52 27.1 -1 3 -4 781.32 28.8 -2 -3 -4 1843.52 59.69 -2 -3 -4 2000.1 63.19 -2 -3 -4 1865.31 54.69 2 -3 4 2014 60.79 -2 -3 -4 1919.11 57.99 2 -3 4 2082.19 62.59 -2 -3 -4 1958.7 58.59 2 -3 4 2013.1 62.89 2 -3 4 2083.79 61.19 2 -3 4 2028.7 61.59 -2 3 -4 2054.19 63.39 -2 3 -4 1953.2 61.49 -2 3 -4 2050.99 61.89 -2 3 -4 2031 61.39 2 3 4 1936.61 55.89 2 3 4 1856.81 55.59 2 3 4 1989.4 63.19 -2 3 -4 1947.21 61.39 3 -3 4 647.44 24.1 -3 -3 -4 604.04 20.8 3 -3 4 632.54 27.1 -3 -3 -4 600.94 20.8 -3 -3 -4 665.93 27.2 3 -3 4 642.04 25.9 3 -3 4 646.24 25.9 -3 -3 -4 606.54 21.3 3 -3 4 658.93 24.5 -3 3 -4 656.03 25.4 -3 3 -4 678.43 26.5 -3 3 -4 667.23 27.7 3 3 4 597.64 26.8 -3 3 -4 688.23 25.5 -3 3 -4 665.03 25.5 4 -3 4 176.08 14.3 4 -3 4 199.68 13.9 4 -3 4 167.68 10.6 -4 -3 -4 161.28 7.3 -4 -3 -4 159.78 7.5 -4 -3 -4 175.48 14 -4 -3 -4 173.58 9.9 4 -3 4 184.28 11.2 4 3 4 164.28 13.9 -4 3 -4 191.68 12.3 -4 3 -4 187.98 13.9 -4 3 -4 177.38 14.8 -4 3 -4 193.38 12.8 -4 3 -4 164.18 12 5 -3 4 1778.02 54.39 -5 -3 -4 1752.52 59.09 5 -3 4 1833.22 59.89 5 -3 4 1828.32 54.29 -5 -3 -4 1769.72 55.49 -5 3 -4 1889.41 62.29 -5 3 -4 1780.22 56.59 -5 3 -4 1819.62 59.99 -5 3 -4 1795.72 57.19 -5 3 -4 1823.22 57.09 -6 -3 -4 54.89 8 6 -3 4 42.3 5.4 -6 -3 -4 47.7 9.2 6 -3 4 37.6 5.4 6 -3 4 57.29 10.5 -6 3 -4 36.8 8.8 -6 3 -4 44.3 8.1 -6 3 -4 51.09 7.8 -6 3 -4 54.19 8.7 -6 3 -4 44.8 10.3 -7 -3 -4 1012 39.5 -7 -3 -4 978.5 36.3 -7 -3 -4 998.6 37.6 7 -3 4 1033.7 40 -7 3 -4 1045 36.1 -7 3 -4 1051.69 36.6 -7 3 -4 984.6 34.4 -7 3 -4 1011.7 41.9 -7 3 -4 1005.3 40.1 -8 -3 -4 122.69 12.8 -8 -3 -4 136.59 14.4 -8 -3 -4 102.99 12.6 8 -3 4 100.59 13.9 -8 3 -4 106.79 10.6 -8 3 -4 108.39 11.1 -8 3 -4 136.19 16.9 -8 3 -4 103.89 9.1 -8 3 -4 154.18 17 9 -3 4 160.58 16.4 -9 -3 -4 173.78 16.6 -9 -3 -4 164.98 13.7 -9 -3 -4 139.89 14 -9 3 -4 145.59 10.3 -9 3 -4 141.89 12.7 -9 3 -4 149.29 16.1 -9 3 -4 155.38 12 -9 3 -4 183.68 17.7 -10 -3 -4 178.78 8.7 10 -3 4 203.48 18.4 -10 -3 -4 188.78 8.4 -10 -3 -4 192.48 16.1 -10 -3 -4 210.78 18.3 -10 3 -4 202.08 19.7 -10 3 -4 196.48 10.9 -10 3 -4 234.48 18.7 -10 3 -4 204.68 14.3 -11 -3 -4 11.6 8 11 -3 4 24 11.1 -11 -3 -4 19.4 7.4 -11 -3 -4 25.3 9.3 -11 -3 -4 13.5 3.5 -11 3 -4 14.2 4.5 -11 3 -4 26 7.2 -11 3 -4 17.4 6.7 -11 3 -4 11.7 9.2 -11 3 -4 15.5 9.4 -12 -3 -4 105.79 11.3 12 -3 4 140.99 25 -12 -3 -4 91.99 12.9 -12 -3 -4 99.29 7.4 -12 -3 -4 107.69 15.3 -12 3 -4 109.29 7.6 -12 3 -4 109.29 15.4 -12 3 -4 144.69 12 -12 3 -4 108.09 12.3 -12 3 -4 98.89 7.2 -13 -3 -4 15 5.9 -13 -3 -4 13.8 4.3 -13 -3 -4 19.6 8.6 -13 -3 -4 15.1 9.3 -13 3 -4 16.1 7.6 -13 3 -4 14.2 6.4 -13 3 -4 -1.3 7.4 -14 -3 -4 59.49 7 -14 -3 -4 61.19 8.7 -14 -3 -4 46.9 10.9 -14 -3 -4 51.79 6.6 -14 -3 -4 59.19 12.8 -14 3 -4 54.49 9.6 -14 3 -4 69.09 12.9 -14 3 -4 58.19 12.6 -14 3 -4 46.9 9.2 -15 -3 -4 3.8 4.4 -15 -3 -4 16.1 7.2 -15 -3 -4 18.6 8.8 -15 -3 -4 24.8 9.7 -15 3 -4 13.3 7.3 -15 3 -4 13.4 12.7 -15 3 -4 8.8 8.5 -15 3 -4 6.4 8.7 -16 -3 -4 14.4 9.6 -16 -3 -4 27.5 5.8 -16 -3 -4 41.5 7.3 -16 -3 -4 17.1 8.6 -16 3 -4 7.6 9.1 -16 3 -4 26.1 9.9 -16 3 -4 45 11.8 -16 3 -4 36.4 8.3 -17 -4 4 25.4 7.6 -17 -4 4 17.6 12.9 -17 4 4 28.2 10.7 -17 4 4 26.6 9.1 -17 4 4 8.6 10.3 -16 -4 4 28.2 7.8 -16 -4 4 15 13.8 -16 -4 4 -0.1 8.9 -16 4 4 0.7 9.9 -16 4 4 3.4 9.8 -16 4 4 8.7 6.9 -15 -4 4 54.49 11.4 -15 -4 4 40 5.9 -15 -4 4 36.1 15.6 -15 -4 4 19.5 7.4 -15 4 4 34.1 11.4 -15 4 4 26.7 11.1 -15 4 4 38.3 14.5 -14 -4 4 1.4 6.9 -14 -4 4 9.2 6.3 -14 -4 4 20.8 8.9 -14 -4 4 6.2 4.9 -14 4 4 18.8 11 -14 4 4 4 7.2 -13 -4 4 112.19 12.5 -13 -4 4 101.39 10.2 -13 -4 4 144.89 29 -13 -4 4 116.59 17.1 -13 -4 4 101.39 12.5 -13 4 4 117.89 16.4 -13 4 4 95.19 15.4 -13 4 4 110.19 14.4 -12 -4 4 20 10.2 -12 -4 4 -7.4 5.2 -12 -4 4 6.7 5.3 12 -4 -4 11.2 4.6 -12 -4 4 3.5 9.1 12 -4 -4 5.7 5.1 -12 -4 4 1.8 5.8 -12 4 4 3.8 7.8 -12 4 4 7.7 10.3 11 -4 -4 490.75 26.7 -11 -4 4 555.34 24.3 -11 -4 4 551.74 23.1 11 -4 -4 534.25 22.7 11 -4 -4 481.05 29.6 -11 -4 4 537.35 30.4 -11 -4 4 524.25 28.7 -11 -4 4 552.64 24.6 -11 4 4 525.75 27.1 -11 4 4 545.95 30.5 -11 4 4 527.55 27.4 10 -4 -4 331.27 18.2 -10 -4 4 301.57 22.7 -10 -4 4 306.87 18.1 10 -4 -4 323.17 23.7 -10 -4 4 311.57 17.4 -10 -4 4 279.77 20.7 10 -4 -4 318.27 18.5 -10 -4 4 327.47 22.5 -10 4 4 320.17 23 -10 4 4 338.07 21.4 -10 4 4 372.86 21.3 -9 -4 4 164.38 13.6 -9 -4 4 159.88 13.4 9 -4 -4 183.28 17.6 -9 -4 4 171.18 16.4 9 -4 -4 161.78 12.5 -9 -4 4 161.28 13.4 9 -4 -4 163.78 14.4 -9 4 4 167.58 15.7 -9 4 4 162.38 17.4 9 4 -4 123.49 13.9 -9 4 4 169.48 15.3 8 -4 -4 837.32 36.8 -8 -4 4 821.32 34.9 8 -4 -4 756.22 24.7 -8 -4 4 832.42 31.5 -8 -4 4 817.92 31.4 8 -4 -4 822.22 32.9 8 -4 -4 843.82 31.8 -8 4 4 815.02 34.2 -8 4 4 758.42 33.2 8 4 -4 809.82 31.7 -8 4 4 805.02 36.6 7 -4 -4 58.59 10.9 7 -4 -4 46.6 6.1 7 -4 -4 38.9 9.7 -7 -4 4 42.2 8.4 -7 -4 4 48 9.9 -7 -4 4 60.69 9.8 -7 -4 4 41.5 8.8 -7 4 4 46.4 9.6 -7 4 4 59.69 13.1 7 4 -4 51.29 9.4 7 4 -4 58.59 6.7 7 4 -4 57.19 7 -7 4 4 47.7 10.9 6 -4 -4 1748.72 57.49 -6 -4 4 1698.63 55.69 -6 -4 4 1688.53 54.99 6 -4 -4 1638.24 58.79 -6 -4 4 1694.63 55.39 6 -4 -4 1712.83 51.19 -6 -4 4 1703.93 58.69 6 -4 -4 1629.24 55.99 -6 4 4 1691.33 57.69 -6 4 4 1697.53 59.59 6 4 -4 1721.33 55.89 -6 4 4 1630.24 50.79 6 4 -4 1626.44 51.69 -5 -4 4 452.75 21.1 -5 -4 4 453.55 22.1 5 -4 -4 455.05 23.7 -5 -4 4 446.76 22.4 5 -4 -4 455.75 18.8 -5 -4 4 442.36 21.3 5 -4 -4 435.46 23 5 4 -4 466.55 19.6 -5 4 4 452.05 23.3 -5 4 4 449.06 24.5 5 4 -4 470.75 22.1 -5 4 4 441.46 18.5 5 4 -4 467.15 20.3 -5 4 4 470.25 23.1 4 -4 -4 2252.47 72.59 4 -4 -4 2336.17 72.39 -4 -4 4 2241.28 70.49 -4 -4 4 2252.37 70.19 4 -4 -4 2233.88 67.59 -4 -4 4 2202.08 69.59 -4 -4 4 2218.78 70.29 4 -4 -4 2196.58 70.49 4 4 -4 2186.38 68.09 -4 4 4 2235.58 75.99 4 4 -4 2242.38 70.39 4 4 -4 2144.49 68.59 -4 4 4 2290.57 71.89 -4 4 4 2186.58 67.19 4 4 -4 2242.88 71.39 -4 4 4 2229.08 72.49 3 -4 -4 3819.22 107.79 -3 -4 4 3693.83 108.49 -3 -4 4 3758.12 109.89 -3 -4 4 3769.32 109.29 3 -4 -4 3592.04 109.49 3 -4 -4 3689.53 110.09 3 -4 -4 3999.9 111.69 -3 -4 4 3483.55 108.79 -3 4 4 3503.15 109.89 3 4 -4 3551.84 107.69 -3 4 4 3383.96 109.39 3 4 -4 3706.03 109.69 3 4 -4 3651.53 108.59 3 4 -4 3786.82 109.49 -3 4 4 3789.82 107.59 -3 4 4 3761.02 110.59 -2 -4 4 0.6 4.3 -2 -4 4 11.1 5.7 2 -4 -4 4.8 6.3 -2 -4 4 15 6.8 -2 -4 4 1.9 5.5 2 -4 -4 4.9 4.6 2 -4 -4 14.8 6.3 2 -4 -4 7 5.4 -2 4 4 2.9 5.9 2 4 -4 4.7 5.4 -2 4 4 4.1 5.6 -2 4 4 13.8 6.5 -2 4 4 7.7 5.3 2 4 -4 14.2 6.1 2 4 -4 -1.8 5.1 2 4 -4 4.2 5.2 1 -4 -4 1649.73 53.89 -1 -4 4 1723.43 54.09 -1 -4 4 1712.43 55.29 1 -4 -4 1704.43 54.59 -1 -4 4 1738.43 55.89 -1 -4 4 1690.43 55.39 -1 -4 4 1781.72 55.49 1 -4 -4 1764.22 55.79 1 -4 -4 1740.53 55.39 -1 4 4 1667.53 54.89 -1 4 4 1641.94 54.39 1 4 -4 1660.73 54.29 -1 4 4 1684.33 54.59 1 4 -4 1572.94 54.39 1 4 -4 1689.63 55.39 -1 4 4 1712.63 54.99 1 4 -4 1576.84 53.99 0 -4 -4 20.1 7.2 0 -4 -4 6.8 5.8 0 -4 4 22.6 6.5 0 -4 4 15.2 6 0 -4 4 12.2 6.6 0 -4 -4 22 5.9 0 -4 4 32.4 8.7 0 -4 -4 6.4 5.2 0 -4 4 19.8 6.1 0 4 -4 24.7 6.8 0 4 -4 33.1 7.6 0 4 4 22.4 6.9 0 4 -4 13.6 6.2 0 4 -4 18 6.3 0 4 4 18.8 6 0 4 -4 32 7 0 4 4 13.5 5.4 0 4 4 17.3 6.3 -1 -4 -4 1083.59 36.9 -1 -4 -4 1101.39 39.4 1 -4 4 1088.79 38.9 1 -4 4 1091.69 38.2 -1 -4 -4 1043.9 36 1 -4 4 1092.59 38 -1 -4 -4 1047.7 36.4 1 -4 4 1080.39 37.9 1 -4 4 1101.69 38.2 -1 4 -4 998.2 37.7 1 4 4 1082.79 36 1 4 4 991.2 35 -1 4 -4 1028.8 38.1 -1 4 -4 1072.19 38.2 -1 4 -4 1081.69 38.3 -1 4 -4 1063.29 37.9 1 4 4 1032.5 36.9 1 4 4 1100.39 39.1 2 -4 4 750.42 30.3 -2 -4 -4 755.32 28.5 2 -4 4 773.32 29.4 -2 -4 -4 763.62 31.1 2 -4 4 796.32 30.7 2 -4 4 734.53 28.7 -2 -4 -4 724.03 27.3 -2 -4 -4 733.33 26.7 2 -4 4 775.72 30 2 4 4 723.63 25.2 -2 4 -4 784.12 29.8 -2 4 -4 730.63 30.4 -2 4 -4 761.22 30.2 2 4 4 758.12 31 -2 4 -4 765.62 30 2 4 4 747.63 25.9 -2 4 -4 778.72 29.7 3 -4 4 1122.19 41.3 3 -4 4 1130.29 39.1 -3 -4 -4 1124.19 36.4 -3 -4 -4 1063.39 35.8 3 -4 4 1172.88 39 3 -4 4 1125.69 40.3 -3 -4 -4 1098.79 32.8 -3 -4 -4 1072.09 32.4 3 -4 4 1104.79 40.4 -3 -4 -4 1118.49 41.5 -3 4 -4 1106.59 39.2 -3 4 -4 1122.49 40.7 3 4 4 1155.28 41.7 -3 4 -4 1125.39 41.7 -3 4 -4 1153.68 40 -3 4 -4 1133.39 40.1 -4 -4 -4 1920.41 58.09 -4 -4 -4 1925.21 58.29 4 -4 4 1981.8 65.49 4 -4 4 2010.1 63.49 4 -4 4 1985.5 64.49 -4 -4 -4 1909.01 57.19 4 -4 4 2033.1 62.09 4 -4 4 2016.7 61.59 -4 -4 -4 1985.3 64.99 -4 4 -4 2010.2 64.99 -4 4 -4 2009.9 63.19 -4 4 -4 1935.31 61.99 -4 4 -4 1924.51 63.09 -4 4 -4 2021.5 66.39 4 4 4 1926.31 65.09 -5 -4 -4 87.89 7.1 5 -4 4 100.49 10.7 5 -4 4 108.39 9.7 -5 -4 -4 124.09 14 -5 -4 -4 83.59 7.3 5 -4 4 113.19 13.7 5 -4 4 142.99 14.2 -5 4 -4 107.29 12.5 -5 4 -4 135.89 15.1 -5 4 -4 112.99 11.2 5 4 4 140.19 18.5 -5 4 -4 123.09 10.5 -5 4 -4 137.69 15.8 6 -4 4 856.91 30.4 6 -4 4 920.61 36 6 -4 4 866.71 30.1 -6 -4 -4 830.52 27.1 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9.2 -16 -4 6 11.1 9.2 -16 -4 6 25.7 7.8 -16 4 6 22.6 8.5 -16 4 6 22.2 10.7 -15 -4 6 24.5 12.2 -15 -4 6 17.7 10.4 -15 -4 6 22 4.5 -15 -4 6 23.1 7.5 -15 4 6 27.5 9.4 -15 4 6 6.5 9.2 14 -4 -6 48.4 5.7 -14 -4 6 55.09 9.2 -14 -4 6 49.5 6.9 14 -4 -6 50.59 5.4 -14 -4 6 46.7 11.7 -14 4 6 62.19 13.9 -14 4 6 47.7 10.2 -13 -4 6 13.8 5.9 -13 -4 6 19.9 7.3 -13 -4 6 9.8 8.6 -13 -4 6 5.8 6.7 -13 4 6 3.2 8.7 -13 4 6 23.8 9.3 -13 4 6 12.7 10.8 13 4 -6 11.1 5.9 12 -4 -6 201.48 17.7 -12 -4 6 287.57 35.9 12 -4 -6 201.88 13.7 -12 -4 6 212.38 20.2 -12 -4 6 210.28 15.9 -12 -4 6 224.68 13.8 -12 -4 6 218.68 16.2 -12 4 6 220.98 17.7 11 -4 -6 55.49 8.8 -11 -4 6 41.4 10 -11 -4 6 39.4 11.7 11 -4 -6 60.09 16.7 11 -4 -6 54.39 12.4 -11 -4 6 51.49 9.1 -11 -4 6 43.4 9.4 -11 4 6 42.5 10.6 -11 4 6 35.1 15 -11 4 6 59.79 11.5 -10 -4 6 742.13 30.5 -10 -4 6 704.43 34.1 -10 -4 6 726.23 35.1 10 -4 -6 679.83 28.7 10 -4 -6 702.33 41.5 10 -4 -6 747.93 30.7 -10 -4 6 654.03 29.8 -10 -4 6 702.13 28.2 -10 4 6 683.63 32.3 10 4 -6 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96.99 10.7 -6 4 6 84.89 12.2 5 -4 -6 2000.2 66.99 -5 -4 6 2015.3 64.79 5 -4 -6 2033.1 66.99 -5 -4 6 1888.91 64.49 5 -4 -6 1941.41 65.29 5 -4 -6 2057.89 61.79 5 4 -6 2020 63.49 -5 4 6 1953.5 66.69 5 4 -6 1952.5 64.39 5 4 -6 2049.49 64.29 -5 4 6 2109.39 71.39 5 4 -6 2014.9 67.69 -4 -4 6 26.1 8.1 -4 -4 6 1.6 6.1 -4 -4 6 6.7 6.8 4 -4 -6 18 6.9 4 -4 -6 6.1 7 4 -4 -6 20.1 6.5 -4 -4 6 3.7 6.5 4 -4 -6 6.9 8.6 -4 4 6 5.8 6.8 4 4 -6 0.9 7 -4 4 6 -4.4 6.2 -4 4 6 9.2 6.8 4 4 -6 5 5.5 4 4 -6 13.3 7 4 4 -6 5 6.4 3 -4 -6 2982.5 88.69 -3 -4 6 2936.91 90.49 -3 -4 6 2976.2 90.19 -3 -4 6 2998.5 90.39 3 -4 -6 2859.01 89.39 -3 -4 6 2927.01 90.49 3 -4 -6 2950.8 90.79 3 -4 -6 3063.89 92.19 3 4 -6 2966.8 90.89 3 4 -6 2913.61 90.09 3 4 -6 2991.5 89.49 -3 4 6 2885.31 90.59 3 4 -6 2910.11 90.19 -3 4 6 2993.9 88.59 -3 4 6 2646.44 91.79 -3 4 6 2959.6 90.19 -2 -4 6 965.7 35.9 2 -4 -6 983.6 35.9 2 -4 -6 957.5 34.8 2 -4 -6 908.91 35.3 -2 -4 6 954.8 36.1 -2 -4 6 967.7 36.8 2 -4 -6 965.6 37.2 -2 -4 6 952.9 36.2 2 4 -6 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2088.49 65.99 -2 2 -7 2125.29 63.49 2 2 7 1974.5 60.39 -2 2 -7 2069.69 62.89 -2 2 -7 2011.6 61.29 -2 2 -7 2045.3 65.39 -3 -2 -7 347.57 15.8 3 -2 7 376.26 15.4 3 -2 7 338.77 19.5 3 -2 7 376.96 15 -3 -2 -7 347.07 13.3 -3 -2 -7 368.76 13.9 3 -2 7 365.76 16.4 -3 2 -7 361.36 16.5 -3 2 -7 373.26 19.3 -3 2 -7 354.66 17 3 2 7 355.26 15.8 -3 2 -7 369.86 16.6 -3 2 -7 371.66 20.3 4 -2 7 367.76 17.8 -4 -2 -7 382.16 16.6 4 -2 7 394.46 21.2 -4 -2 -7 360.16 17.1 4 -2 7 360.16 13.5 4 -2 7 362.86 13.4 -4 -2 -7 366.56 21 -4 2 -7 393.66 17.8 -4 2 -7 355.36 18.9 -4 2 -7 385.76 17.1 -4 2 -7 362.66 21 -4 2 -7 359.06 16.4 -5 -2 -7 1758.22 57.49 -5 -2 -7 1819.02 58.09 -5 -2 -7 1829.22 61.69 5 -2 7 1881.01 62.29 5 -2 7 1841.12 58.99 -5 2 -7 1816.52 59.69 -5 2 -7 1821.72 58.79 -5 2 -7 1909.51 56.99 -5 2 -7 1864.71 56.59 6 -2 7 21.7 7.5 -6 -2 -7 25 7.2 -6 -2 -7 37 8 -6 -2 -7 29.5 8.2 -6 2 -7 19.4 9.1 -6 2 -7 25.8 6.4 -6 2 -7 33.1 7.6 -6 2 -7 27.1 5.8 -6 2 -7 31.6 8.2 -7 -2 -7 1058.19 39.7 7 -2 7 1035.8 39.5 -7 -2 -7 1033.7 38.6 -7 -2 -7 1018.1 38.5 -7 2 -7 1051.09 39.3 -7 2 -7 1042 35.2 -7 2 -7 1088.29 42.6 -7 2 -7 1001.1 37.2 -7 2 -7 1035.6 35.1 -8 -2 -7 48.9 11.8 -8 -2 -7 50.59 10 8 -2 7 59.49 10.2 -8 2 -7 35.7 7 -8 2 -7 52.69 7.9 -8 2 -7 41.6 10.7 -8 2 -7 41.5 7.8 -8 2 -7 59.09 11.3 9 -2 7 431.46 23.7 -9 -2 -7 418.26 23.2 -9 -2 -7 438.66 23.4 -9 -2 -7 463.95 22.9 -9 2 -7 466.15 24.2 -9 2 -7 447.36 19.2 -9 2 -7 452.35 26.3 -9 2 -7 413.16 18.7 -9 2 -7 363.56 25.9 -10 -2 -7 160.18 14.3 -10 -2 -7 156.58 16.1 10 -2 7 179.88 16.3 -10 -2 -7 210.98 16.9 -10 2 -7 178.08 12.3 -10 2 -7 195.48 11.9 -10 2 -7 181.18 17.1 -10 2 -7 195.98 18.2 -11 -2 -7 75.19 12.9 -11 -2 -7 67.39 10.6 -11 -2 -7 45.3 11.1 -11 2 -7 64.89 8.9 -11 2 -7 62.29 12.2 -11 2 -7 70.79 9.8 -11 2 -7 56.89 12.1 -12 -2 -7 83.19 12.4 -12 -2 -7 87.09 5.7 -12 -2 -7 73.79 5.3 -12 -2 -7 99.59 12.1 -12 -2 -7 97.19 14.6 -12 2 -7 95.99 10.2 -12 2 -7 86.09 14.2 -12 2 -7 98.39 10.6 -12 2 -7 115.09 15.5 -13 -2 -7 0.2 6.5 -13 -2 -7 -2.8 3.2 -13 -2 -7 -1.5 7.1 -13 -2 -7 -0.8 5.8 -13 -2 -7 6.7 3.4 -13 2 -7 -4.3 7.6 -13 2 -7 3 5.2 -13 2 -7 5.8 7.6 -13 2 -7 -2.3 4.9 -13 2 -7 -8.7 4.2 -13 2 -7 -9.4 4.3 -14 -2 -7 77.89 6.5 -14 -2 -7 66.99 9.7 -14 -2 -7 75.19 6.5 -14 -2 -7 72.39 13.2 -14 -2 -7 81.89 13.3 -14 2 -7 74.29 7.9 -14 2 -7 56.19 13 -14 2 -7 60.09 9.3 -14 2 -7 69.59 7.4 -14 2 -7 53.09 11.4 -14 2 -7 86.09 9.4 -15 -2 -7 14.6 8.3 -15 -2 -7 2.7 6.9 -15 -2 -7 18.9 4.7 -15 -2 -7 -4.1 3.7 -15 -2 -7 3 5.3 -15 2 -7 2.8 8.2 -15 2 -7 2.6 6.8 -15 2 -7 0.3 3.1 -15 2 -7 8.1 3.7 -15 2 -7 -0.1 7.1 -15 2 -7 15.3 6.8 -16 -2 -7 40 6 -16 -2 -7 31.7 10.7 -16 -2 -7 39.2 10.1 -16 -2 -7 47.7 7.4 -16 2 -7 40.2 10.6 -16 2 -7 32.7 10.4 -16 2 -7 38.9 8.3 -17 -3 7 8.3 6.8 -17 -3 7 -1.3 8.5 -17 3 7 -10.8 7 -17 3 7 10.1 7.8 -16 -3 7 -7.2 8.2 -16 -3 7 11.8 6.7 -16 3 7 3.9 5.9 -16 3 7 14.5 9.6 -15 -3 7 19.9 10 -15 -3 7 48 9.7 -15 -3 7 11.3 11.1 -15 3 7 38 11.7 -15 3 7 55.29 11.2 -14 -3 7 -9.5 7.8 -14 -3 7 7.9 7.6 -14 -3 7 -2.7 6.1 -14 3 7 -7.1 7.6 -14 3 7 -0.3 7 -13 -3 7 51.99 9.8 13 -3 -7 48.3 7.1 -13 -3 7 44.8 11.6 13 -3 -7 59.19 8.1 -13 -3 7 65.39 11.9 -13 3 7 44.1 9.7 -13 3 7 58.99 12.2 -13 3 7 53.59 13.4 -12 -3 7 16.2 7.3 12 -3 -7 -4.5 5.9 -12 -3 7 16.1 7.8 12 -3 -7 13.4 6.7 -12 -3 7 -6.5 8.8 -12 -3 7 12 9.2 -12 -3 7 6.9 4.9 -12 3 7 0.2 7.6 12 3 -7 11.6 4.9 -12 3 7 6.5 7.9 -12 3 7 30.1 9.7 -11 -3 7 182.88 19.3 11 -3 -7 166.28 17.6 -11 -3 7 188.68 21 -11 -3 7 154.68 14.2 11 -3 -7 146.39 12.4 -11 -3 7 165.38 11.3 -11 -3 7 161.68 15.4 11 3 -7 147.49 11.1 -11 3 7 152.38 17.4 -11 3 7 168.58 16.8 -11 3 7 166.28 17.8 -10 -3 7 15.3 6.4 10 -3 -7 28.1 10.4 -10 -3 7 14.5 9.7 -10 -3 7 13.4 8.6 -10 -3 7 6.4 6.9 10 -3 -7 7.5 6 -10 -3 7 19.4 8.6 10 3 -7 19.5 6.3 10 3 -7 8.8 4.2 10 3 -7 25.4 5.9 -10 3 7 20.6 8.2 -10 3 7 11 9.5 -10 3 7 10.5 8.2 9 -3 -7 194.28 14.5 9 -3 -7 208.58 18.5 -9 -3 7 185.28 18.5 9 -3 -7 222.28 18.8 -9 -3 7 184.08 15.4 -9 -3 7 205.28 15.9 -9 -3 7 220.98 18.9 -9 -3 7 177.58 13.3 -9 3 7 187.48 18.7 -9 3 7 206.18 16.9 -9 3 7 200.98 16.6 9 3 -7 168.78 12.5 9 3 -7 212.08 12.2 9 3 -7 174.78 12.7 -8 -3 7 408.76 24.2 -8 -3 7 389.36 19.7 -8 -3 7 459.65 22.7 8 -3 -7 405.26 21.4 -8 -3 7 430.46 22.5 8 -3 -7 443.26 25.4 -8 3 7 386.16 22.8 8 3 -7 426.06 19.9 8 3 -7 425.56 20.1 8 3 -7 455.05 19.3 -8 3 7 419.76 25.2 -8 3 7 430.46 23.1 -7 -3 7 32.3 8.9 -7 -3 7 41.9 9.9 7 -3 -7 50.09 11.8 -7 -3 7 21.6 7.9 -7 -3 7 28.1 7.8 7 -3 -7 32.2 8.1 7 -3 -7 39.8 9.6 7 -3 -7 43.8 5.9 -7 3 7 35.5 10.7 7 3 -7 52.39 8.5 -7 3 7 24.2 8.4 7 3 -7 40.5 7.9 -7 3 7 28.8 9.4 7 3 -7 34.4 9.1 6 -3 -7 245.98 18 6 -3 -7 255.27 17.9 6 -3 -7 203.88 12.1 -6 -3 7 229.98 15.8 -6 -3 7 260.97 16.5 -6 -3 7 230.88 15.3 -6 -3 7 224.28 18 6 -3 -7 259.57 16.2 -6 3 7 263.07 19 6 3 -7 232.18 14.5 -6 3 7 251.37 19.1 -6 3 7 214.98 16.5 6 3 -7 227.48 15.1 -5 -3 7 45.1 10.8 5 -3 -7 41.8 10.1 -5 -3 7 44.8 13.4 5 -3 -7 48.8 7.4 -5 -3 7 30.4 7.7 5 -3 -7 24.2 8.1 5 -3 -7 37.1 8.5 -5 -3 7 35.1 8.3 5 3 -7 32.4 8.1 -5 3 7 33.4 9 5 3 -7 41.6 8.2 -5 3 7 26.6 9.2 5 3 -7 47.3 8 -5 3 7 27.1 9.1 5 3 -7 27.9 9.3 -4 -3 7 1621.64 52.99 -4 -3 7 1538.55 52.99 -4 -3 7 1465.55 51.59 4 -3 -7 1530.95 52.49 4 -3 -7 1571.74 50.19 4 -3 -7 1549.94 56.39 -4 -3 7 1599.14 54.29 4 -3 -7 1614.24 54.89 4 3 -7 1548.45 52.49 4 3 -7 1504.85 51.49 4 3 -7 1536.05 51.79 4 3 -7 1579.04 55.09 -4 3 7 1608.14 53.79 -4 3 7 1500.25 52.69 3 -3 -7 1264.97 45.3 3 -3 -7 1231.28 42 -3 -3 7 1198.58 43.5 -3 -3 7 1188.28 43 3 -3 -7 1191.28 42.9 -3 -3 7 1240.58 43.4 -3 -3 7 1223.18 43.9 3 -3 -7 1181.68 42 3 3 -7 1262.87 44.9 3 3 -7 1215.78 42.7 3 3 -7 1303.37 44.2 3 3 -7 1222.18 43 -3 3 7 1187.68 43.5 -3 3 7 1194.68 44.1 -3 3 7 1222.18 42.5 -2 -3 7 197.58 14.3 2 -3 -7 243.08 14.4 2 -3 -7 204.48 12.6 -2 -3 7 199.08 14.4 -2 -3 7 210.08 14.5 2 -3 -7 206.48 15.7 -2 -3 7 208.38 15.3 2 -3 -7 221.78 14.5 2 3 -7 205.28 14 -2 3 7 209.58 13.4 -2 3 7 195.38 13 -2 3 7 209.58 14.9 -2 3 7 207.38 14.2 2 3 -7 214.78 15.7 2 3 -7 201.88 14.5 2 3 -7 231.48 15.7 -1 -3 7 346.97 19.1 1 -3 -7 322.07 15.1 1 -3 -7 349.47 19 1 -3 -7 339.47 17 -1 -3 7 310.17 16.7 -1 -3 7 344.27 18.2 -1 -3 7 334.47 17.8 1 -3 -7 339.47 18.7 -1 -3 7 337.27 18.1 -1 3 7 311.17 16.8 -1 3 7 318.47 15.3 -1 3 7 352.46 15.9 -1 3 7 347.17 17.9 1 3 -7 341.07 18.7 1 3 -7 316.07 18.6 1 3 -7 315.17 18.1 1 3 -7 309.07 17 0 -3 -7 10.3 4.3 0 -3 7 10.8 6.2 0 -3 -7 10.3 5.2 0 -3 7 12.5 4.9 0 -3 -7 8.4 6.1 0 -3 7 9.3 6.2 0 -3 -7 13.3 6.2 0 -3 -7 8.1 4 0 -3 7 12.9 7 0 -3 7 -3.7 4.7 0 3 -7 1.3 5 0 3 -7 16.5 6.6 0 3 7 17.3 4.7 0 3 -7 6.8 5.8 0 3 7 13.9 4.5 0 3 -7 5.2 6.5 0 3 7 16.4 5.4 0 3 7 12.3 5.4 -1 -3 -7 1596.84 49.99 1 -3 7 1723.63 53.99 -1 -3 -7 1660.13 51.99 -1 -3 -7 1665.23 49.4 -1 -3 -7 1732.43 56.99 1 -3 7 1710.43 54.19 1 -3 7 1657.63 55.59 1 -3 7 1664.63 52.89 -1 -3 -7 1732.03 53.69 1 -3 7 1688.73 56.39 -1 3 -7 1643.34 52.79 1 3 7 1635.94 50.59 1 3 7 1634.74 49 1 3 7 1679.23 51.29 -1 3 -7 1654.03 54.19 -1 3 -7 1638.84 55.69 1 3 7 1646.94 50.49 -1 3 -7 1705.73 54.99 -1 3 -7 1694.33 56.29 -2 -3 -7 144.89 9.1 -2 -3 -7 137.39 10.3 -2 -3 -7 149.69 14.1 -2 -3 -7 136.79 8.1 2 -3 7 156.48 11.3 2 -3 7 135.69 10.7 -2 -3 -7 148.59 9.6 2 -3 7 130.49 10.3 2 -3 7 143.69 12.9 -2 3 -7 152.78 12.5 -2 3 -7 128.39 11.1 2 3 7 127.09 7.8 -2 3 -7 137.79 12.7 -2 3 -7 146.79 11.1 -2 3 -7 139.49 13.6 2 3 7 141.99 7 2 3 7 132.79 6.7 3 -3 7 501.15 21 -3 -3 -7 458.95 18 3 -3 7 545.65 28.6 3 -3 7 507.55 21.8 -3 -3 -7 517.45 18.7 -3 -3 -7 506.75 25.2 3 -3 7 489.45 20.4 3 3 7 508.25 18.3 -3 3 -7 507.75 23.8 -3 3 -7 472.45 22.2 -3 3 -7 518.75 22.2 -3 3 -7 551.24 25.8 -3 3 -7 483.95 21.6 -4 -3 -7 2007.8 56.79 -4 -3 -7 2004.1 65.79 4 -3 7 1930.41 58.89 4 -3 7 1931.61 59.19 4 -3 7 1953.1 62.39 4 -3 7 1933.61 65.69 -4 -3 -7 1903.51 56.19 -4 -3 -7 1927.71 58.89 -4 3 -7 1917.41 61.39 -4 3 -7 1980 63.69 -4 3 -7 1981 62.49 -4 3 -7 2004.2 62.09 -4 3 -7 2032.1 72.09 5 -3 7 286.97 17 5 -3 7 295.97 12.7 5 -3 7 282.87 13 5 -3 7 270.67 18.7 -5 -3 -7 298.67 19.5 -5 -3 -7 296.87 14.9 -5 3 -7 311.77 20.6 -5 3 -7 325.37 18.1 -5 3 -7 287.27 17.2 -5 3 -7 290.07 16 -5 3 -7 322.27 16.8 -6 -3 -7 109.99 11.9 6 -3 7 101.49 12.3 6 -3 7 98.29 13.9 -6 -3 -7 100.69 11 -6 3 -7 87.69 10.7 -6 3 -7 77.99 12.9 -6 3 -7 76.59 11 -6 3 -7 94.29 11.6 -6 3 -7 87.59 10.2 -7 -3 -7 -1.8 5.3 -7 -3 -7 -3.1 6.2 -7 -3 -7 -5.1 5.9 7 -3 7 -1.5 6.2 -7 3 -7 -3.8 4.2 -7 3 -7 5.5 5.6 -7 3 -7 -2.1 7.6 -7 3 -7 -7.3 5.3 -7 3 -7 -1.1 6.3 -8 -3 -7 135.79 13.8 8 -3 7 133.59 13.8 -8 -3 -7 136.19 14.4 -8 -3 -7 145.59 14.6 -8 3 -7 168.98 20.7 -8 3 -7 128.99 11.8 -8 3 -7 194.18 18.5 -8 3 -7 135.59 15 -9 -3 -7 139.49 15.8 -9 -3 -7 139.29 14.9 -9 -3 -7 142.09 14.1 9 -3 7 122.39 14.8 -9 3 -7 112.09 12 -9 3 -7 104.19 16.8 -9 3 -7 140.99 16.7 -9 3 -7 135.09 20.1 -9 3 -7 132.09 11.4 -10 -3 -7 91.09 13.4 10 -3 7 112.29 15.1 -10 -3 -7 86.19 12 -10 -3 -7 99.69 13.3 -10 3 -7 98.89 11.1 -10 3 -7 92.89 12.8 -10 3 -7 79.89 13.3 -10 3 -7 91.09 14.5 11 -3 7 165.78 19.1 -11 -3 -7 141.19 15.3 -11 -3 -7 144.09 16.6 -11 -3 -7 132.59 14.3 -11 3 -7 122.69 15.2 -11 3 -7 140.39 12.1 -11 3 -7 160.78 19.8 -11 3 -7 142.89 11.8 -12 -3 -7 13.3 7.5 12 -3 7 2.6 8.1 -12 -3 -7 9.2 6.1 -12 -3 -7 8.4 7.4 -12 3 -7 5.3 6.2 -12 3 -7 -7.2 5.4 -12 3 -7 8.1 7.5 -12 3 -7 5.3 10.1 -13 -3 -7 29.2 7.8 -13 -3 -7 37.7 9.7 -13 -3 -7 29.8 9.6 -13 3 -7 14.4 9.8 -13 3 -7 10.5 14.1 -13 3 -7 35.1 6.3 -13 3 -7 25.7 5.3 -13 3 -7 21.9 7.2 -13 3 -7 20.8 7.5 -14 -3 -7 17 3.9 -14 -3 -7 30.9 9.9 -14 -3 -7 13.6 6.3 -14 -3 -7 8.9 9.9 -14 3 -7 20.5 4.6 -14 3 -7 10.8 4 -14 3 -7 22.6 7.8 -14 3 -7 24.7 8.4 -14 3 -7 23.3 11.2 -14 3 -7 15.7 9.5 -15 -3 -7 16.4 8 -15 -3 -7 6.7 5.5 -15 -3 -7 15.1 4.3 -15 -3 -7 11.3 3.9 -15 -3 -7 16.5 8.2 -15 3 -7 10.8 6.8 -15 3 -7 29.2 10.7 -16 -3 -7 -2.8 6.9 -16 -3 -7 14.8 6.1 -16 -3 -7 3.1 4.1 -16 -3 -7 9.2 7.8 -16 3 -7 4.3 6.7 -16 3 -7 28.9 16.3 -16 3 -7 22.5 8.6 -17 -4 7 9.9 7.3 -17 -4 7 3.2 9.3 -17 4 7 8 9 -17 4 7 1.2 8.1 -16 -4 7 18.9 9.7 -16 -4 7 -6.3 7.1 -16 4 7 4 7.6 -16 4 7 -8.4 7.9 -15 -4 7 21.8 10.3 -15 -4 7 21.1 9.5 -15 -4 7 6.3 6.8 -15 4 7 22.9 9 -15 4 7 9.9 9.8 -14 -4 7 13.7 6.4 -14 -4 7 14.1 4.9 -14 -4 7 5.8 8.5 14 -4 -7 1.9 4.6 14 -4 -7 7 5.1 -14 4 7 1.7 8.3 -13 -4 7 8.3 8.1 -13 -4 7 6.9 7.7 13 -4 -7 4.7 5.6 -13 -4 7 -5.9 4.6 -13 -4 7 -1.6 5.7 -13 4 7 9 8.3 -13 4 7 -5.2 8.3 13 4 -7 -3.8 6.1 -12 -4 7 8.7 7 12 -4 -7 19 6.8 12 -4 -7 5.9 6.5 -12 -4 7 8 7 -12 -4 7 1.8 5.3 -12 -4 7 10.8 8.6 -12 4 7 12.8 8.4 12 4 -7 -2.3 7.8 -12 4 7 17.7 9.5 -12 4 7 8.3 10.4 -11 -4 7 16.7 6.9 -11 -4 7 -2.4 7.7 -11 -4 7 0.2 6.9 -11 -4 7 4.3 7.1 11 -4 -7 3.6 6.1 -11 -4 7 6.4 8.8 11 -4 -7 4.9 8 11 4 -7 0.4 6.1 -11 4 7 3.1 8.5 -11 4 7 8.8 7.9 -11 4 7 2.6 9.2 -10 -4 7 9.9 7.8 -10 -4 7 14.3 7.2 -10 -4 7 0 8.9 10 -4 -7 21.5 6.9 -10 -4 7 25.1 10.5 -10 -4 7 37.8 9.2 10 -4 -7 -0.5 7.7 -10 4 7 18 9.6 10 4 -7 7.4 5.9 -10 4 7 17.1 8.6 10 4 -7 14.7 3.9 10 4 -7 21.3 5.4 -10 4 7 9 9.1 -9 -4 7 1.1 8 -9 -4 7 5.8 6.7 -9 -4 7 8.6 7.1 -9 -4 7 1.1 6 9 -4 -7 10.3 7.3 9 -4 -7 7.2 8.3 9 -4 -7 5.4 6.4 9 4 -7 -5.3 5.8 -9 4 7 8.2 8.5 9 4 -7 1.3 4.2 -9 4 7 16.3 8.6 9 4 -7 13.4 5.8 -9 4 7 4.5 7.4 8 -4 -7 1.9 5.9 -8 -4 7 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-2 -2 11 453.75 22.6 2 -2 -11 398.96 22 -2 -2 11 394.26 22.5 -2 -2 11 420.96 22.3 2 2 -11 433.96 23.2 -2 2 11 405.96 21.2 2 2 -11 428.86 23.7 -2 2 11 382.46 17.7 2 2 -11 432.26 23.5 -2 2 11 385.66 20.9 2 2 -11 411.76 21.6 -1 -2 11 1337.77 48.7 1 -2 -11 1343.67 46.8 -1 -2 11 1384.96 47.7 -1 -2 11 1373.26 51.49 1 -2 -11 1329.97 47.1 1 -2 -11 1306.87 41.5 -1 2 11 1389.56 46.7 1 2 -11 1332.27 49 1 2 -11 1331.67 47.8 1 2 -11 1384.16 48.9 -1 2 11 1347.87 46.2 -1 2 11 1303.97 41.4 -1 2 11 1345.97 47 1 2 -11 1367.16 49.5 0 -2 11 71.89 8 0 -2 11 38.6 8.9 0 -2 -11 54.99 8.6 0 -2 11 70.69 10.4 0 -2 -11 73.19 9.9 0 -2 -11 74.69 11.6 0 -2 11 77.39 10.9 0 -2 -11 55.39 5.4 0 2 -11 67.19 11.3 0 2 11 58.19 5.3 0 2 11 73.09 9.8 0 2 11 74.69 9.4 0 2 -11 53.19 10.9 0 2 -11 94.99 12.7 0 2 11 79.69 9.8 -1 -2 -11 2015.2 63.69 1 -2 11 2012 63.19 1 -2 11 1988 59.39 -1 -2 -11 1993.9 62.49 -1 -2 -11 1933.21 62.09 1 -2 11 1924.41 65.49 1 -2 11 1969.2 62.79 1 2 11 1963.1 60.59 1 2 11 2007.6 60.59 -1 2 -11 2040.7 65.29 -1 2 -11 1937.31 63.79 -1 2 -11 1970.5 66.69 1 2 11 1981 62.09 -1 2 -11 2002.1 66.69 -2 -2 -11 342.37 16.8 2 -2 11 361.96 20.7 2 -2 11 389.26 18 2 -2 11 374.06 17.4 -2 -2 -11 402.46 18.9 -2 -2 -11 417.56 19.2 2 -2 11 361.66 15.7 -2 2 -11 346.97 15.6 -2 2 -11 376.56 21.6 2 2 11 350.46 14 -2 2 -11 346.37 22.4 -2 2 -11 372.76 20.2 -2 2 -11 324.27 18.1 2 2 11 384.66 17.8 2 2 11 360.86 14.2 3 -2 11 1132.39 42.6 -3 -2 -11 1176.58 38.3 3 -2 11 1168.68 37.2 -3 -2 -11 1139.79 39.4 -3 -2 -11 1072.49 32.6 3 -2 11 1111.69 36.5 -3 -2 -11 1031.4 32.4 -3 -2 -11 1091.39 36.9 3 -2 11 1150.48 36.6 -3 2 -11 1138.59 39.4 -3 2 -11 1058.49 36.1 -3 2 -11 1159.38 43.8 -3 2 -11 1090.89 42.9 3 2 11 1111.89 38.6 -3 2 -11 1189.28 40.5 -4 -2 -11 1216.58 41.3 4 -2 11 1188.28 35.6 4 -2 11 1153.88 38.6 4 -2 11 1161.28 35.7 -4 -2 -11 1129.49 37.2 -4 -2 -11 1139.69 35.8 4 -2 11 1171.48 44.4 -4 -2 -11 1228.38 38.5 -4 2 -11 1181.68 45.2 -4 2 -11 1184.98 40.8 4 2 11 1154.28 40.6 -4 2 -11 1123.09 44.1 -4 2 -11 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-14.9 6.6 1 2 -32 12.2 14.7 1 2 -32 21.9 11 0 -2 -32 14.2 9.4 0 -2 32 6.3 8.1 0 2 -32 4 13.8 0 2 32 -4.1 6.6 0 2 -32 21.3 11.1 -1 -2 -32 19 8.5 1 -2 32 1.6 6.5 -1 2 -32 2 10.1 6 -3 -32 2 9.8 -6 -3 32 -2.7 6 6 3 -32 2.6 10.4 -6 3 32 -3.2 4.9 -6 3 32 -2.7 7.9 -5 -3 32 5.8 5.9 5 -3 -32 24.3 12.3 -5 -3 32 28.7 10.1 5 3 -32 15.2 11.3 5 3 -32 3.4 11.5 -5 3 32 5 8.4 -4 -3 32 20.7 9.2 4 -3 -32 0.1 9.3 4 3 -32 -10.7 7.9 -4 3 32 8.7 8.5 4 3 -32 3.7 9.2 -3 -3 32 1.2 7.7 3 -3 -32 7.1 9.1 3 3 -32 8.6 9.6 3 3 -32 6.5 10.8 -3 3 32 -2.9 7.8 2 -3 -32 -5.4 11.4 -2 -3 32 3 7.7 2 -3 -32 3 8.1 2 3 -32 11.5 11.9 2 3 -32 -0.5 9.8 -2 3 32 -7.2 7.1 1 -3 -32 5.1 8.3 -1 -3 32 -2.7 7.6 1 3 -32 13 10 1 3 -32 1.8 9.8 -1 3 32 4.3 7.2 0 -3 -32 42.5 11.3 0 -3 32 10.1 7.9 0 3 32 5 7.3 0 3 -32 6.9 9.6 0 3 -32 2.5 10.3 4 -4 -32 57.99 14.1 4 -4 -32 26.5 11.1 -4 -4 32 42.2 11.4 -4 4 32 45.3 11.1 4 4 -32 51.99 13.5 4 4 -32 40.7 12.7 -3 -4 32 23.8 8.9 3 -4 -32 18.9 10.8 3 -4 -32 -17.3 8 3 4 -32 9.2 10 3 4 -32 12.7 11.3 -3 4 32 6 7.9 -2 -4 32 13.3 8 2 -4 -32 10.6 10.3 2 -4 -32 16.4 10.7 -2 4 32 -1.7 7.7 2 4 -32 -4.9 8.6 2 4 -32 20.7 11.4 -1 -4 32 11.6 8.5 -1 4 32 9.3 7.3 4 0 -33 -14.8 10.4 -4 0 33 -2.7 7.6 4 0 -33 10.7 9.5 3 0 -33 12.1 9.2 -3 0 33 16.1 8.7 -2 0 33 14 8.7 2 0 -33 -4.2 8 3 -1 -33 3.8 9.1 -3 -1 33 7.6 8.5 3 -1 -33 5.1 9.5 3 1 -33 7.9 9.4 -3 1 33 15.2 8.8 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag P1 Au Cl1 101.26(4) . . ? P2 Au Cl1 102.38(4) . . ? P2 Au P1 156.23(4) . . ? C1 P1 Au 117.57(15) . . ? C20 P1 Au 110.69(15) . . ? C20 P1 C1 105.7(2) . . ? C26 P1 Au 113.71(15) . . ? C26 P1 C1 102.70(19) . . ? C26 P1 C20 105.4(2) . . ? C19 P2 Au 116.72(14) . . ? C32 P2 Au 113.97(16) . . ? C32 P2 C19 103.4(2) . . ? C38 P2 Au 111.22(15) . . ? C38 P2 C19 105.3(2) . . ? C38 P2 C32 105.1(2) . . ? C2 C1 P1 121.5(3) . . ? C6 C1 P1 120.5(3) . . ? C6 C1 C2 118.0(4) . . ? H2 C2 C1 119.7(3) . . ? C3 C2 C1 120.7(5) . . ? C3 C2 H2 119.7(3) . . ? H3 C3 C2 120.0(3) . . ? C4 C3 C2 120.1(5) . . ? C4 C3 H3 120.0(3) . . ? H4 C4 C3 119.8(3) . . ? C5 C4 C3 120.3(5) . . ? C5 C4 H4 119.8(3) . . ? H5 C5 C4 120.1(3) . . ? C6 C5 C4 119.9(4) . . ? C6 C5 H5 120.1(3) . . ? C5 C6 C1 120.9(4) . . ? N1 C6 C1 119.4(4) . . ? N1 C6 C5 119.8(4) . . ? H1 N1 C6 118.0(2) . . ? C7 N1 C6 123.9(4) . . ? C7 N1 H1 118.0(2) . . ? O1 C7 N1 124.5(4) . . ? C8 C7 N1 114.5(4) . . ? C8 C7 O1 121.0(4) . . ? C9 C8 C7 120.4(4) . . ? N2 C8 C7 116.8(4) . . ? N2 C8 C9 122.8(4) . . ? H9 C9 C8 120.4(3) . . ? C10 C9 C8 119.1(5) . . ? C10 C9 H9 120.4(3) . . ? H10 C10 C9 120.7(3) . . ? C11 C10 C9 118.6(5) . . ? C11 C10 H10 120.7(3) . . ? H11 C11 C10 120.5(3) . . ? C12 C11 C10 118.9(5) . . ? C12 C11 H11 120.5(3) . . ? N2 C12 C11 123.1(4) . . ? C13 C12 C11 119.2(4) . . ? C13 C12 N2 117.7(4) . . ? C12 N2 C8 117.3(4) . . ? O2 C13 C12 122.3(4) . . ? N3 C13 C12 113.5(4) . . ? N3 C13 O2 124.2(4) . . ? H3a N3 C13 118.0(2) . . ? C14 N3 C13 123.9(4) . . ? C14 N3 H3a 118.0(2) . . ? C15 C14 N3 121.0(4) . . ? C19 C14 N3 118.7(4) . . ? C19 C14 C15 120.3(4) . . ? H15 C15 C14 120.4(3) . . ? C16 C15 C14 119.2(4) . . ? C16 C15 H15 120.4(3) . . ? H16 C16 C15 119.5(3) . . ? C17 C16 C15 121.1(4) . . ? C17 C16 H16 119.5(3) . . ? H17 C17 C16 120.0(3) . . ? C18 C17 C16 120.0(5) . . ? C18 C17 H17 120.0(3) . . ? H18 C18 C17 119.9(3) . . ? C19 C18 C17 120.2(4) . . ? C19 C18 H18 119.9(3) . . ? C14 C19 P2 118.1(3) . . ? C18 C19 P2 122.8(3) . . ? C18 C19 C14 119.1(4) . . ? C21 C20 P1 117.5(4) . . ? C25 C20 P1 123.4(4) . . ? C25 C20 C21 119.1(5) . . ? H21 C21 C20 120.2(3) . . ? C22 C21 C20 119.6(6) . . ? C22 C21 H21 120.2(4) . . ? H22 C22 C21 119.9(4) . . ? C23 C22 C21 120.3(6) . . ? C23 C22 H22 119.9(4) . . ? H23 C23 C22 120.0(4) . . ? C24 C23 C22 119.9(5) . . ? C24 C23 H23 120.0(4) . . ? H24 C24 C23 119.3(4) . . ? C25 C24 C23 121.4(6) . . ? C25 C24 H24 119.3(4) . . ? C24 C25 C20 119.7(5) . . ? H25 C25 C20 120.2(3) . . ? H25 C25 C24 120.2(4) . . ? C27 C26 P1 119.5(3) . . ? C31 C26 P1 121.4(4) . . ? C31 C26 C27 118.9(4) . . ? H27 C27 C26 119.9(3) . . ? C28 C27 C26 120.2(5) . . ? C28 C27 H27 119.9(3) . . ? H28 C28 C27 119.5(3) . . ? C29 C28 C27 121.1(5) . . ? C29 C28 H28 119.5(3) . . ? H29 C29 C28 120.2(3) . . ? C30 C29 C28 119.6(5) . . ? C30 C29 H29 120.2(3) . . ? H30 C30 C29 119.8(3) . . ? C31 C30 C29 120.3(5) . . ? C31 C30 H30 119.8(3) . . ? C30 C31 C26 119.9(5) . . ? H31 C31 C26 120.1(3) . . ? H31 C31 C30 120.1(3) . . ? C33 C32 P2 121.3(4) . . ? C37 C32 P2 119.5(4) . . ? C37 C32 C33 119.1(5) . . ? H33 C33 C32 119.2(3) . . ? C34 C33 C32 121.5(6) . . ? C34 C33 H33 119.2(4) . . ? H34 C34 C33 120.2(4) . . ? C35 C34 C33 119.5(7) . . ? C35 C34 H34 120.2(4) . . ? H35 C35 C34 119.4(4) . . ? C36 C35 C34 121.1(6) . . ? C36 C35 H35 119.4(4) . . ? H36 C36 C35 119.9(4) . . ? C37 C36 C35 120.3(7) . . ? C37 C36 H36 119.9(4) . . ? C36 C37 C32 118.4(6) . . ? H37 C37 C32 120.8(3) . . ? H37 C37 C36 120.8(4) . . ? C39 C38 P2 120.1(4) . . ? C43 C38 P2 121.6(3) . . ? C43 C38 C39 118.3(4) . . ? H39 C39 C38 120.2(3) . . ? C40 C39 C38 119.6(5) . . ? C40 C39 H39 120.2(3) . . ? H40 C40 C39 119.4(3) . . ? C41 C40 C39 121.2(5) . . ? C41 C40 H40 119.4(3) . . ? H41 C41 C40 120.0(3) . . ? C42 C41 C40 120.1(5) . . ? C42 C41 H41 120.0(3) . . ? H42 C42 C41 119.9(3) . . ? C43 C42 C41 120.2(5) . . ? C43 C42 H42 119.9(3) . . ? C42 C43 C38 120.7(5) . . ? H43 C43 C38 119.7(3) . . ? H43 C43 C42 119.7(3) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Au Cl1 2.6424(12) . ? Au P1 2.3154(11) . ? Au P2 2.3179(11) . ? P1 C1 1.824(4) . ? P1 C20 1.817(5) . ? P1 C26 1.819(5) . ? P2 C19 1.834(4) . ? P2 C32 1.814(5) . ? P2 C38 1.817(4) . ? C1 C2 1.400(6) . ? C1 C6 1.399(6) . ? C2 H2 0.9300 . ? C2 C3 1.380(7) . ? C3 H3 0.9300 . ? C3 C4 1.374(7) . ? C4 H4 0.9300 . ? C4 C5 1.383(7) . ? C5 H5 0.9300 . ? C5 C6 1.376(6) . ? C6 N1 1.422(5) . ? N1 H1 0.8600 . ? N1 C7 1.339(5) . ? C7 O1 1.222(5) . ? C7 C8 1.507(6) . ? C8 C9 1.379(6) . ? C8 N2 1.342(5) . ? C9 H9 0.9300 . ? C9 C10 1.378(7) . ? C10 H10 0.9300 . ? C10 C11 1.375(7) . ? C11 H11 0.9300 . ? C11 C12 1.378(6) . ? C12 N2 1.338(5) . ? C12 C13 1.501(6) . ? C13 O2 1.211(5) . ? C13 N3 1.362(5) . ? N3 H3a 0.8600 . ? N3 C14 1.417(5) . ? C14 C15 1.385(6) . ? C14 C19 1.396(6) . ? C15 H15 0.9300 . ? C15 C16 1.373(7) . ? C16 H16 0.9300 . ? C16 C17 1.375(7) . ? C17 H17 0.9300 . ? C17 C18 1.374(6) . ? C18 H18 0.9300 . ? C18 C19 1.387(6) . ? C20 C21 1.396(7) . ? C20 C25 1.387(7) . ? C21 H21 0.9300 . ? C21 C22 1.382(8) . ? C22 H22 0.9300 . ? C22 C23 1.379(9) . ? C23 H23 0.9300 . ? C23 C24 1.349(8) . ? C24 H24 0.9300 . ? C24 C25 1.376(7) . ? C25 H25 0.9300 . ? C26 C27 1.367(6) . ? C26 C31 1.386(6) . ? C27 H27 0.9300 . ? C27 C28 1.379(7) . ? C28 H28 0.9300 . ? C28 C29 1.351(8) . ? C29 H29 0.9300 . ? C29 C30 1.363(8) . ? C30 H30 0.9300 . ? C30 C31 1.385(7) . ? C31 H31 0.9300 . ? C32 C33 1.399(7) . ? C32 C37 1.382(7) . ? C33 H33 0.9300 . ? C33 C34 1.374(7) . ? C34 H34 0.9300 . ? C34 C35 1.357(10) . ? C35 H35 0.9300 . ? C35 C36 1.366(10) . ? C36 H36 0.9300 . ? C36 C37 1.427(9) . ? C37 H37 0.9300 . ? C38 C39 1.392(6) . ? C38 C43 1.395(6) . ? C39 H39 0.9300 . ? C39 C40 1.384(7) . ? C40 H40 0.9300 . ? C40 C41 1.362(8) . ? C41 H41 0.9300 . ? C41 C42 1.359(8) . ? C42 H42 0.9300 . ? C42 C43 1.380(7) . ? C43 H43 0.9300 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Au P1 C1 C2 128.5(3) . . . . ? Au P1 C1 C6 -50.7(2) . . . . ? Au P1 C20 C21 -48.1(3) . . . . ? Au P1 C20 C25 132.0(3) . . . . ? Au P1 C26 C27 -28.5(3) . . . . ? Au P1 C26 C31 156.5(3) . . . . ? Au P2 C19 C14 65.6(2) . . . . ? Au P2 C19 C18 -115.3(3) . . . . ? Au P2 C32 C33 -162.1(3) . . . . ? Au P2 C32 C37 20.6(3) . . . . ? Au P2 C38 C39 9.5(3) . . . . ? Au P2 C38 C43 -171.3(3) . . . . ? P1 C1 C2 C3 178.2(4) . . . . ? P1 C1 C6 C5 -177.5(4) . . . . ? P1 C1 C6 N1 3.1(4) . . . . ? P1 C20 C21 C22 178.4(4) . . . . ? P1 C20 C25 C24 -177.8(4) . . . . ? P1 C26 C27 C28 -173.9(4) . . . . ? P1 C26 C31 C30 173.2(4) . . . . ? P2 C19 C14 N3 -6.5(4) . . . . ? P2 C19 C14 C15 175.0(3) . . . . ? P2 C19 C18 C17 -176.5(4) . . . . ? P2 C32 C33 C34 -175.6(4) . . . . ? P2 C32 C37 C36 176.8(4) . . . . ? P2 C38 C39 C40 179.0(4) . . . . ? P2 C38 C43 C42 -178.4(4) . . . . ? C1 P1 C20 C21 -176.4(3) . . . . ? C1 P1 C20 C25 3.7(3) . . . . ? C1 P1 C26 C27 99.6(3) . . . . ? C1 P1 C26 C31 -75.4(3) . . . . ? C1 C2 C3 C4 0.9(6) . . . . ? C1 C6 C5 C4 -2.4(5) . . . . ? C1 C6 N1 C7 -121.4(4) . . . . ? C2 C1 P1 C20 -107.4(4) . . . . ? C2 C1 P1 C26 2.9(4) . . . . ? C2 C1 C6 C5 3.2(5) . . . . ? C2 C1 C6 N1 -176.2(4) . . . . ? C2 C3 C4 C5 -0.0(7) . . . . ? C3 C2 C1 C6 -2.5(6) . . . . ? C3 C4 C5 C6 0.7(7) . . . . ? C4 C5 C6 N1 177.0(5) . . . . ? C5 C6 N1 C7 59.3(5) . . . . ? C6 C1 P1 C20 73.3(4) . . . . ? C6 C1 P1 C26 -176.4(4) . . . . ? C6 N1 C7 O1 6.4(5) . . . . ? C6 N1 C7 C8 -174.5(4) . . . . ? N1 C7 C8 C9 179.0(4) . . . . ? N1 C7 C8 N2 -0.3(4) . . . . ? C7 C8 C9 C10 -178.4(5) . . . . ? C7 C8 N2 C12 179.7(4) . . . . ? O1 C7 C8 C9 -2.0(6) . . . . ? O1 C7 C8 N2 178.8(4) . . . . ? C8 C9 C10 C11 -2.1(6) . . . . ? C8 N2 C12 C11 -0.3(5) . . . . ? C8 N2 C12 C13 178.3(4) . . . . ? C9 C8 N2 C12 0.4(5) . . . . ? C9 C10 C11 C12 2.3(6) . . . . ? C10 C9 C8 N2 0.8(6) . . . . ? C10 C11 C12 N2 -1.1(6) . . . . ? C10 C11 C12 C13 -179.7(5) . . . . ? C11 C12 C13 O2 -0.1(5) . . . . ? C11 C12 C13 N3 178.1(4) . . . . ? C12 C13 N3 C14 -173.6(3) . . . . ? N2 C12 C13 O2 -178.8(4) . . . . ? N2 C12 C13 N3 -0.6(4) . . . . ? C13 N3 C14 C15 -64.0(5) . . . . ? C13 N3 C14 C19 117.6(4) . . . . ? O2 C13 N3 C14 4.5(6) . . . . ? N3 C14 C15 C16 -176.0(5) . . . . ? N3 C14 C19 C18 174.3(4) . . . . ? C14 C15 C16 C17 0.8(6) . . . . ? C14 C19 P2 C32 -60.4(4) . . . . ? C14 C19 P2 C38 -170.5(3) . . . . ? C14 C19 C18 C17 2.6(5) . . . . ? C15 C14 C19 C18 -4.1(5) . . . . ? C15 C16 C17 C18 -2.3(6) . . . . ? C16 C15 C14 C19 2.4(6) . . . . ? C16 C17 C18 C19 0.5(6) . . . . ? C18 C19 P2 C32 118.7(4) . . . . ? C18 C19 P2 C38 8.6(4) . . . . ? C19 P2 C32 C33 -34.4(3) . . . . ? C19 P2 C32 C37 148.3(3) . . . . ? C19 P2 C38 C39 -117.8(3) . . . . ? C19 P2 C38 C43 61.4(3) . . . . ? C20 P1 C26 C27 -150.0(3) . . . . ? C20 P1 C26 C31 35.1(3) . . . . ? C20 C21 C22 C23 -0.5(6) . . . . ? C20 C25 C24 C23 -0.7(6) . . . . ? C21 C20 P1 C26 75.3(4) . . . . ? C21 C20 C25 C24 2.2(5) . . . . ? C21 C22 C23 C24 2.1(7) . . . . ? C22 C21 C20 C25 -1.7(7) . . . . ? C22 C23 C24 C25 -1.5(7) . . . . ? C25 C20 P1 C26 -104.7(4) . . . . ? C26 C27 C28 C29 0.1(6) . . . . ? C26 C31 C30 C29 1.2(6) . . . . ? C27 C26 C31 C30 -1.8(5) . . . . ? C27 C28 C29 C30 -0.7(7) . . . . ? C28 C27 C26 C31 1.1(6) . . . . ? C28 C29 C30 C31 0.0(7) . . . . ? C32 P2 C38 C39 133.3(3) . . . . ? C32 P2 C38 C43 -47.5(3) . . . . ? C32 C33 C34 C35 -1.4(6) . . . . ? C32 C37 C36 C35 -0.9(6) . . . . ? C33 C32 P2 C38 75.8(4) . . . . ? C33 C32 C37 C36 -0.5(5) . . . . ? C33 C34 C35 C36 -0.1(7) . . . . ? C34 C33 C32 C37 1.6(6) . . . . ? C34 C35 C36 C37 1.2(7) . . . . ? C37 C32 P2 C38 -101.4(4) . . . . ? C38 C39 C40 C41 0.0(6) . . . . ? C38 C43 C42 C41 -1.2(6) . . . . ? C39 C38 C43 C42 0.8(6) . . . . ? C39 C40 C41 C42 -0.4(7) . . . . ? C40 C39 C38 C43 -0.3(6) . . . . ? C40 C41 C42 C43 1.0(6) . . . . ? loop_ _restr_U_rigid_atom_site_label_1 _restr_U_rigid_atom_site_label_2 _restr_U_rigid_target_weight_param _restr_U_rigid_U_parallel _restr_U_rigid_diff C1 C2 0.0100 0.0516 -0.0045 C1 C3 0.0100 0.0483 -0.0032 C1 C5 0.0100 0.0542 0.0003 C1 C6 0.0100 0.0567 0.0014 C1 N1 0.0100 0.0509 0.0083 C2 C3 0.0100 0.0555 -0.0007 C2 C4 0.0100 0.0565 0.0046 C2 C6 0.0100 0.0550 0.0044 C3 C4 0.0100 0.0739 0.0013 C3 C5 0.0100 0.0666 0.0040 C4 C5 0.0100 0.0690 0.0100 C4 C6 0.0100 0.0505 0.0088 C5 C6 0.0100 0.0513 0.0044 C5 N1 0.0100 0.0549 0.0070 C6 N1 0.0100 0.0474 0.0005 C6 C7 0.0100 0.0548 -0.0037 N1 C7 0.0100 0.0527 0.0009 N1 O1 0.0100 0.0531 -0.0006 N1 C8 0.0100 0.0503 -0.0021 C7 O1 0.0100 0.0506 -0.0012 C7 C8 0.0100 0.0585 -0.0016 C7 C9 0.0100 0.0585 -0.0022 C7 N2 0.0100 0.0541 -0.0001 O1 C8 0.0100 0.0608 -0.0050 C8 C9 0.0100 0.0475 0.0003 C8 C10 0.0100 0.0536 -0.0041 C8 C12 0.0100 0.0617 0.0032 C8 N2 0.0100 0.0555 0.0066 C9 C10 0.0100 0.0740 -0.0050 C9 C11 0.0100 0.0700 0.0031 C9 N2 0.0100 0.0476 -0.0002 C10 C11 0.0100 0.0752 0.0071 C10 C12 0.0100 0.0552 0.0050 C11 C12 0.0100 0.0495 0.0047 C11 N2 0.0100 0.0479 0.0023 C11 C13 0.0100 0.0607 0.0059 C12 N2 0.0100 0.0527 0.0028 C12 C13 0.0100 0.0598 -0.0010 C12 O2 0.0100 0.0615 -0.0017 C12 N3 0.0100 0.0531 -0.0017 N2 C13 0.0100 0.0558 -0.0032 C13 O2 0.0100 0.0508 0.0025 C13 N3 0.0100 0.0517 -0.0023 C13 C14 0.0100 0.0545 0.0018 O2 N3 0.0100 0.0491 -0.0003 N3 C14 0.0100 0.0511 -0.0010 N3 C15 0.0100 0.0580 -0.0085 N3 C19 0.0100 0.0497 -0.0057 C14 C15 0.0100 0.0520 -0.0055 C14 C16 0.0100 0.0499 -0.0003 C14 C18 0.0100 0.0531 0.0012 C14 C19 0.0100 0.0537 -0.0011 C15 C16 0.0100 0.0724 -0.0068 C15 C17 0.0100 0.0665 0.0003 C15 C19 0.0100 0.0521 0.0005 C16 C17 0.0100 0.0827 0.0032 C16 C18 0.0100 0.0589 -0.0002 C17 C18 0.0100 0.0595 0.0032 C17 C19 0.0100 0.0465 -0.0008 C18 C19 0.0100 0.0503 0.0020 C20 C21 0.0100 0.0581 0.0009 C20 C22 0.0100 0.0521 0.0015 C20 C24 0.0100 0.0579 0.0004 C20 C25 0.0100 0.0640 -0.0004 C21 C22 0.0100 0.0644 0.0059 C21 C23 0.0100 0.0805 0.0004 C21 C25 0.0100 0.0724 -0.0034 C22 C23 0.0100 0.1273 -0.0092 C22 C24 0.0100 0.1119 0.0002 C23 C24 0.0100 0.1212 0.0013 C23 C25 0.0100 0.0704 0.0011 C24 C25 0.0100 0.0637 0.0068 C26 C27 0.0100 0.0591 -0.0079 C26 C28 0.0100 0.0547 0.0038 C26 C30 0.0100 0.0572 0.0027 C26 C31 0.0100 0.0568 0.0007 C27 C28 0.0100 0.0651 -0.0034 C27 C29 0.0100 0.0630 -0.0007 C27 C31 0.0100 0.0623 0.0002 C28 C29 0.0100 0.0930 0.0078 C28 C30 0.0100 0.0837 -0.0007 C29 C30 0.0100 0.0940 0.0049 C29 C31 0.0100 0.0686 0.0034 C30 C31 0.0100 0.0626 0.0023 C32 C33 0.0100 0.0697 -0.0024 C32 C34 0.0100 0.0709 -0.0178 C32 C36 0.0100 0.0522 0.0039 C32 C37 0.0100 0.0645 -0.0071 C33 C34 0.0100 0.0620 0.0024 C33 C37 0.0100 0.0863 -0.0051 C36 C37 0.0100 0.0859 0.0008 C38 C39 0.0100 0.0531 -0.0073 C38 C40 0.0100 0.0462 0.0004 C38 C42 0.0100 0.0554 0.0025 C38 C43 0.0100 0.0608 -0.0018 C39 C40 0.0100 0.0614 -0.0012 C39 C41 0.0100 0.0656 0.0032 C39 C43 0.0100 0.0642 -0.0013 C40 C41 0.0100 0.1074 0.0142 C40 C42 0.0100 0.0971 0.0057 C41 C42 0.0100 0.0939 0.0059 C41 C43 0.0100 0.0584 0.0034 C42 C43 0.0100 0.0524 -0.0026 loop_ _atom_site_anharm_gc_c_label _atom_site_anharm_gc_c_111 _atom_site_anharm_gc_c_112 _atom_site_anharm_gc_c_113 _atom_site_anharm_gc_c_122 _atom_site_anharm_gc_c_123 _atom_site_anharm_gc_c_133 _atom_site_anharm_gc_c_222 _atom_site_anharm_gc_c_223 _atom_site_anharm_gc_c_233 _atom_site_anharm_gc_c_333 Au 0.00000003(4) -0.00000003(2) 0.000000003(11) 0.00000003(2) -0.000000008(8) 0.000000007(6) 0.00000043(4) -0.000000114(12) 0.000000059(6) -0.000000018(7) loop_ _atom_site_anharm_gc_d_label _atom_site_anharm_gc_d_1111 _atom_site_anharm_gc_d_1112 _atom_site_anharm_gc_d_1113 _atom_site_anharm_gc_d_1122 _atom_site_anharm_gc_d_1123 _atom_site_anharm_gc_d_1133 _atom_site_anharm_gc_d_1222 _atom_site_anharm_gc_d_1223 _atom_site_anharm_gc_d_1233 _atom_site_anharm_gc_d_1333 _atom_site_anharm_gc_d_2222 _atom_site_anharm_gc_d_2223 _atom_site_anharm_gc_d_2233 _atom_site_anharm_gc_d_2333 _atom_site_anharm_gc_d_3333 Au 0.000000044(3) 0.0000000061(16) 0.0000000002(7) 0.0000000163(11) 0.0000000002(5) 0.0000000030(3) 0.0000000042(17) -0.0000000005(4) 0.0000000003(3) 0.0000000001(2) 0.000000028(3) -0.0000000027(10) 0.0000000024(3) -0.0000000007(3) 0.0000000018(3) loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 0.000 0.000 0.500 547.8 132.2 ? 2 0.000 0.500 0.000 547.8 132.2 ?