#------------------------------------------------------------------------------ #$Date: 2026-05-28 01:36:47 +0100 (Thu, 28 May 2026) $ #$Revision: 306108 $ #$URL: svn://www.crystallography.net/cod/cif/7/06/44/7064421.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7064421 loop_ _publ_author_name 'Yan, Bo' 'Ji, Wen-Juan' 'Fan, Shucong' 'Pei, Wei-Wei' 'Liu, Gui-Fang' 'Wang, Bingqiang' 'Zhai, Quan-Guo' 'Fu, Yunlong' _publ_section_title ; Atomic Precision Engineering of Heterometallic Hexanuclear Al/M MOFs for Supercapacitor Applications ; _journal_name_full 'New Journal of Chemistry' _journal_paper_doi 10.1039/D6NJ00933F _journal_year 2026 _chemical_formula_moiety '4(C84 H45 Al4 N2 Ni2 O23), 9[C2H5NO], 9[H2O]' _chemical_formula_sum 'C102 H108 Al4 N11 Ni2 O41' _chemical_formula_weight 2369.33 _space_group_crystal_system cubic _space_group_IT_number 197 _space_group_name_Hall 'I 2 2 3' _space_group_name_H-M_alt 'I 2 3' _atom_sites_solution_hydrogens mixed _audit_block_doi 10.5517/ccdc.csd.cc2rnlhj _audit_creation_date 2026-05-20 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408) ; _audit_update_record ; 2026-05-22 deposited with the CCDC. 2026-05-27 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 6 _cell_length_a 27.3691(7) _cell_length_b 27.3691(7) _cell_length_c 27.3691(7) _cell_measurement_reflns_used 9990 _cell_measurement_temperature 273(2) _cell_measurement_theta_max 22.33 _cell_measurement_theta_min 2.35 _cell_volume 20501.3(9) _computing_cell_refinement 'Bruker SMART' _computing_data_collection 'Bruker SMART' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2019/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXS (G. Sheldrick)' _diffrn_ambient_temperature 273.15 _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'CCD area detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1177 _diffrn_reflns_av_unetI/netI 0.0652 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 34 _diffrn_reflns_limit_h_min -34 _diffrn_reflns_limit_k_max 26 _diffrn_reflns_limit_k_min -34 _diffrn_reflns_limit_l_max 34 _diffrn_reflns_limit_l_min -34 _diffrn_reflns_number 104432 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.368 _diffrn_reflns_theta_min 2.353 _exptl_absorpt_coefficient_mu 0.376 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_correction_T_min 0.6773 _exptl_absorpt_correction_type none _exptl_absorpt_process_details ; SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_crystal_colour green _exptl_crystal_colour_primary green _exptl_crystal_density_diffrn 1.151 _exptl_crystal_description block _exptl_crystal_F_000 7398 _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.27 _exptl_crystal_size_min 0.22 _refine_diff_density_max 1.293 _refine_diff_density_min -0.530 _refine_diff_density_rms 0.093 _refine_ls_abs_structure_details ; Refined as an inversion twin. ; _refine_ls_abs_structure_Flack 0.49(6) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.039 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 293 _refine_ls_number_reflns 7006 _refine_ls_number_restraints 400 _refine_ls_restrained_S_all 1.049 _refine_ls_R_factor_all 0.1628 _refine_ls_R_factor_gt 0.0920 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1717P)^2^+29.4214P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2448 _refine_ls_wR_factor_ref 0.3020 _reflns_Friedel_coverage 0.878 _reflns_Friedel_fraction_full 0.999 _reflns_Friedel_fraction_max 0.999 _reflns_number_gt 3993 _reflns_number_total 7006 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d6nj00933f2.cif _cod_data_source_block mo_20180906ak_0m_sq _cod_original_cell_volume 20501.3(16) _cod_database_code 7064421 _shelx_shelxl_version_number 2019/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.922 _shelx_estimated_absorpt_t_min 0.896 _olex2_refinement_description ; 1. Twinned data refinement Scales: 0.51139 0.48861 2. Restrained distances C20-O5A \\sim C1B-O5 with sigma of 0.01 O5A-C1A \\sim C19-O5 with sigma of 0.01 O5-C22 \\sim O5A-C22 with sigma of 0.01 C2-C1 \\sim C22-C21 with sigma of 0.01 3. Restrained planarity N1, C19, C20, C21, C22, O5A, C1A, C1B, O5 with sigma of 0.01 4. Uiso/Uaniso restraints and constraints N1 \\sim C1A \\sim C1B \\sim C21 \\sim C20 \\sim C19 \\sim C22 \\sim O5A \\sim O5: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.002 within 2A Uanis(C19) \\sim Ueq, Uanis(N1) \\sim Ueq, Uanis(C1A) \\sim Ueq, Uanis(C1B) \\sim Ueq, Uanis(C21) \\sim Ueq, Uanis(C20) \\sim Ueq, Uanis(C22) \\sim Ueq, Uanis(O5A) \\sim Ueq, Uanis(O5) \\sim Ueq: with sigma of 0.05 and sigma for terminal atoms of 0.01 5. Rigid body (RIGU) restrains C7, Ni1, N1, O1, O3, O6, C19, C1, C10, Al1, C20, O2, C2, O4, C11, O7, C21, C3, C12, C16, C22, C4, C6, C13, C15, C5, C14, C8, C17, C9, C18 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001 Ni1, N1, C19, C20, C21, C1B, C1A, C22, O5, O5A with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001 6. Others Fixed Sof: N1(0.5) C19(0.5) H19(0.5) C20(0.5) H20(0.5) C21(0.5) C1B(0.5) H1B(0.5) C1A(0.5) H1A(0.5) O7(0.25) H7(0.25) C22(0.5) O5A(0.5) O5(0.5) 7.a Riding coordinates: O7(H7) 7.b Aromatic/amide H refined with riding coordinates: C19(H19), C20(H20), C1B(H1B), C1A(H1A), C3(H3), C4(H4), C6(H6), C7(H7A), C9(H9), C12(H12), C13(H13), C15(H15), C16(H16) 7.c Fitted hexagon refined as free rotating group: N1(C19,C20,C21,C1B,C1A) ; _shelx_res_file ; TITL N in I23 #197 mo_20180906ak_0m_sq.res created by SHELXL-2019/3 at 14:19:18 on 19-May-2026 REM CONF CELL 0.71073 27.3691 27.3691 27.3691 90 90 90 ZERR 6 0.0007 0.0007 0.0007 0 0 0 LATT -2 SYMM +Z,+X,+Y SYMM +Y,+Z,+X SYMM -Y,-Z,+X SYMM +Z,-X,-Y SYMM -Y,+Z,-X SYMM -Z,-X,+Y SYMM -Z,+X,-Y SYMM +Y,-Z,-X SYMM -X,-Y,+Z SYMM +X,-Y,-Z SYMM -X,+Y,-Z SFAC C H Al N Ni O UNIT 612 648 24 66 12 246 RIGU 0.001 0.001 C7 Ni1 N1 O1 O3 O6 C19 C1 C10 Al1 C20 O2 C2 O4 C11 O7 C21 = C3 C12 C16 C22 C4 C6 C13 C15 C5 C14 C8 C17 C9 C18 SADI 0.01 C20 O5A C1B O5 SADI 0.01 O5A C1A C19 O5 FLAT 0.01 N1 C19 C20 C21 C22 O5A C1A C1B O5 SADI 0.01 O5 C22 O5A C22 SADI 0.01 C2 C1 C22 C21 RIGU 0.001 0.001 Ni1 N1 C19 C20 C21 C1B C1A C22 O5 O5A ISOR 0.05 0.01 C19 N1 C1A C1B C21 C20 C22 O5A O5 SIMU 0.01 0.002 2 N1 C1A C1B C21 C20 C19 C22 O5A O5 L.S. 12 0 0 PLAN 29 SIZE 0.3 0.27 0.22 TEMP 0 CONN 5 Al1 LIST 8 BOND $h HTAB ABIN fmap 2 acta SHEL 999 0.8 TWIN -1 0 0 0 -1 0 0 0 -1 2 OMIT 0 0 4 OMIT 0 0 8 OMIT 0 0 10 REM REM REM WGHT 0.171700 29.421400 BASF 0.48861 FVAR 0.03450 NI1 5 0.500000 0.000000 0.173660 10.50000 0.04164 0.04908 = 0.04806 0.00000 0.00000 0.00101 AL1 3 0.553684 0.000410 0.058608 11.00000 0.04595 0.06856 = 0.04758 -0.00113 0.00139 0.00700 PART -1 AFIX 66 N1 4 0.504028 -0.000809 0.250041 10.50000 0.10111 0.08496 = 0.05912 -0.00195 0.00276 0.02705 C19 1 0.547103 0.005471 0.276203 10.50000 0.10499 0.09131 = 0.07151 0.00275 -0.00399 0.02735 AFIX 43 H19 2 0.575402 0.015375 0.260213 10.50000 -1.20000 AFIX 65 C20 1 0.547881 -0.003054 0.326263 10.50000 0.10381 0.12300 = 0.07375 0.01348 -0.00015 0.01838 AFIX 43 H20 2 0.576701 0.001148 0.343767 10.50000 -1.20000 AFIX 65 C21 1 0.505584 -0.017858 0.350162 10.50000 0.11138 0.14038 = 0.10697 0.03100 0.01595 0.02151 C1B 1 0.462509 -0.024137 0.324001 10.50000 0.10561 0.13561 = 0.10422 0.02376 0.02325 0.01930 AFIX 43 H1B 2 0.434210 -0.034042 0.339991 10.50000 -1.20000 AFIX 65 C1A 1 0.461730 -0.015613 0.273940 10.50000 0.10994 0.12110 = 0.10159 0.01313 0.01753 0.01926 AFIX 43 H1A 2 0.432910 -0.019814 0.256437 10.50000 -1.20000 AFIX 0 PART 0 O1 6 0.552272 0.052714 0.175173 11.00000 0.05141 0.06814 = 0.09981 -0.01064 -0.00825 -0.00897 O2 6 0.586837 0.047231 0.100681 11.00000 0.15156 0.14788 = 0.13027 -0.05731 0.04322 -0.09141 O3 6 0.554197 -0.052266 0.176883 11.00000 0.06804 0.07297 = 0.07412 -0.00460 -0.00545 0.02428 O4 6 0.566280 -0.069007 0.099276 11.00000 0.11409 0.09326 = 0.07765 -0.01451 -0.02172 0.04448 O6 6 0.500000 0.000000 0.098854 10.50000 0.06387 0.07940 = 0.04874 0.00000 0.00000 0.00858 O7 6 0.604474 0.000000 0.000000 10.25000 0.03786 0.20295 = 0.06997 -0.00771 0.00000 0.00000 AFIX 3 H7 2 0.635535 0.000000 0.000000 10.25000 -1.20000 AFIX 0 C1 1 0.578671 0.067770 0.146426 11.00000 0.06568 0.09234 = 0.09821 -0.01447 -0.00609 -0.02570 C2 1 0.619654 0.101545 0.161190 11.00000 0.08090 0.10459 = 0.08964 0.00901 -0.01897 -0.04089 C3 1 0.655369 0.120195 0.121071 11.00000 0.08231 0.10950 = 0.08273 0.00663 -0.01913 -0.03930 AFIX 43 H3 2 0.651277 0.111606 0.088450 11.00000 -1.20000 AFIX 0 C4 1 0.691442 0.148469 0.134988 11.00000 0.07196 0.08881 = 0.08354 0.02220 -0.02749 -0.02691 AFIX 43 H4 2 0.710363 0.164006 0.111425 11.00000 -1.20000 AFIX 0 C5 1 0.702441 0.156028 0.185671 11.00000 0.07692 0.07641 = 0.08456 0.02235 -0.02728 -0.02672 C6 1 0.674097 0.134550 0.219531 11.00000 0.09516 0.08780 = 0.08308 0.01270 -0.02158 -0.04225 AFIX 43 H6 2 0.683275 0.136571 0.252185 11.00000 -1.20000 AFIX 0 C7 1 0.630411 0.108730 0.207296 11.00000 0.08045 0.06021 = 0.08651 0.01622 -0.01845 -0.02412 AFIX 43 H7A 2 0.609854 0.097161 0.231754 11.00000 -1.20000 AFIX 0 C8 1 0.746103 0.184807 0.199623 11.00000 0.08016 0.07538 = 0.07671 0.02000 -0.02840 -0.02622 C9 1 0.763099 0.224786 0.171755 11.00000 0.07660 0.09363 = 0.08391 0.03714 -0.04576 -0.03543 AFIX 43 H9 2 0.747395 0.231402 0.142357 11.00000 -1.20000 AFIX 0 C10 1 0.581628 -0.067967 0.141193 11.00000 0.08188 0.08410 = 0.07242 -0.00952 -0.00834 0.03756 C11 1 0.623089 -0.101773 0.157639 11.00000 0.06711 0.06034 = 0.08749 -0.01730 -0.01685 0.01858 C12 1 0.644562 -0.127184 0.125701 11.00000 0.08274 0.08685 = 0.08701 -0.03129 -0.03170 0.03890 AFIX 43 H12 2 0.631528 -0.129219 0.094386 11.00000 -1.20000 AFIX 0 C13 1 0.689054 -0.153132 0.137065 11.00000 0.10401 0.12641 = 0.09331 -0.04893 -0.04180 0.06778 AFIX 43 H13 2 0.707236 -0.167731 0.112349 11.00000 -1.20000 AFIX 0 C14 1 0.703745 -0.155913 0.183357 11.00000 0.07882 0.07692 = 0.09072 -0.03819 -0.03414 0.03278 C15 1 0.672320 -0.134422 0.220072 11.00000 0.09061 0.09603 = 0.09022 -0.03408 -0.03096 0.04617 AFIX 43 H15 2 0.677330 -0.141144 0.253001 11.00000 -1.20000 AFIX 0 C16 1 0.637124 -0.105713 0.206615 11.00000 0.06544 0.08432 = 0.08465 -0.01352 -0.01260 0.02644 AFIX 43 H16 2 0.620829 -0.087311 0.230078 11.00000 -1.20000 AFIX 0 C17 1 0.747249 -0.185541 0.198910 11.00000 0.08687 0.07822 = 0.08402 -0.03915 -0.03300 0.03931 C18 1 0.758475 -0.226105 0.171930 11.00000 0.09084 0.07501 = 0.07421 -0.03287 -0.02180 0.03488 PART -1 C22 1 0.507477 -0.026956 0.404690 10.50000 0.12200 0.15331 = 0.10925 0.04367 0.02237 0.03999 O5A 6 0.552595 -0.019802 0.431288 10.50000 0.12156 0.15275 = 0.10697 0.04841 0.02317 0.04075 O5 6 0.463161 -0.042605 0.428707 10.50000 0.12220 0.15312 = 0.11060 0.04012 0.02271 0.04013 HKLF 4 REM N in I23 #197 REM wR2 = 0.3020, GooF = S = 1.039, Restrained GooF = 1.049 for all data REM R1 = 0.0920 for 3993 Fo > 4sig(Fo) and 0.1628 for all 7006 data REM 293 parameters refined using 400 restraints END WGHT 0.1720 29.3616 REM Instructions for potential hydrogen bonds EQIV $3 -x+1, -y, z HTAB C1A O1_$3 REM Highest difference peak 1.293, deepest hole -0.530, 1-sigma level 0.093 Q1 1 0.5000 0.0000 0.2058 10.50000 0.05 1.29 Q2 1 0.5618 0.0007 0.4451 11.00000 0.05 1.02 Q3 1 0.5000 0.0000 0.4759 10.50000 0.05 0.89 Q4 1 0.5000 0.0000 0.4385 10.50000 0.05 0.68 Q5 1 0.5987 0.0018 0.3264 11.00000 0.05 0.60 Q6 1 0.5536 -0.0917 0.1109 11.00000 0.05 0.51 Q7 1 0.5000 0.0000 0.3803 10.50000 0.05 0.48 Q8 1 0.5494 0.0634 0.1677 11.00000 0.05 0.44 Q9 1 0.5534 0.0907 0.1100 11.00000 0.05 0.42 Q10 1 0.5495 -0.0624 0.1697 11.00000 0.05 0.38 Q11 1 0.5658 0.0839 0.1595 11.00000 0.05 0.37 Q12 1 0.5935 -0.0251 0.4209 11.00000 0.05 0.36 Q13 1 0.5684 -0.0565 0.0775 11.00000 0.05 0.35 Q14 1 0.4951 -0.0715 0.3825 11.00000 0.05 0.35 Q15 1 0.5823 0.0612 0.1320 11.00000 0.05 0.35 Q16 1 0.5814 -0.0620 0.1296 11.00000 0.05 0.34 Q17 1 0.5908 0.0000 0.0000 10.50000 0.05 0.34 Q18 1 0.4986 -0.0734 0.3904 11.00000 0.05 0.33 Q19 1 0.5658 -0.0825 0.1608 11.00000 0.05 0.32 Q20 1 0.6011 0.0003 0.2799 11.00000 0.05 0.31 Q21 1 0.5287 -0.0822 0.0969 11.00000 0.05 0.31 Q22 1 0.7304 -0.2377 0.1444 11.00000 0.05 0.31 Q23 1 0.6966 0.1502 0.1571 11.00000 0.05 0.31 Q24 1 0.6243 0.0887 0.1432 11.00000 0.05 0.30 Q25 1 0.6839 -0.1375 0.2170 11.00000 0.05 0.29 Q26 1 0.5000 0.0000 0.1193 10.50000 0.05 0.29 Q27 1 0.5903 -0.0503 0.0022 11.00000 0.05 0.29 Q28 1 0.6072 0.0448 0.1100 11.00000 0.05 0.29 Q29 1 0.5747 -0.0636 0.1266 11.00000 0.05 0.28 ; _shelx_res_checksum 65343 _shelx_hkl_file ; 1 0 3 20.17 0.95 -2 1 3 74.62 3.62 2 -1 3 78.58 3.62 2 -1 3 79.11 3.63 -3 2 1 73.70 3.63 -3 2 1 77.34 3.59 -1 3 2 71.91 3.62 -1 3 2 75.48 3.63 -1 3 2 77.99 3.58 3 -2 1 80.64 3.62 3 -2 1 82.19 3.61 3 2 -1 81.09 3.62 1 -3 2 82.52 3.63 1 -3 2 76.94 3.60 1 3 -2 73.21 3.63 -3 -2 -1 79.25 3.60 2 1 3 77.27 3.62 1 3 2 76.29 3.64 3 2 1 83.08 3.62 3 2 1 77.22 3.63 -1 -3 2 78.51 3.62 -2 -1 3 75.34 3.62 -2 -1 3 75.16 3.61 1 3 2 80.00 3.60 -1 -3 2 76.27 3.63 -1 3 -2 74.91 3.62 2 1 3 82.40 3.64 -3 2 -1 78.18 3.59 -3 -2 1 75.41 3.62 -3 -2 1 76.31 3.58 -3 2 -1 75.48 3.63 -3 -1 -2 181.50 8.33 1 2 -3 185.76 8.38 -3 1 2 187.42 8.38 3 -1 2 169.06 8.34 3 -1 2 177.22 8.37 -2 3 1 190.75 8.39 -2 3 1 179.98 8.36 -1 2 3 185.32 8.37 2 -3 1 181.12 8.37 2 -3 1 175.82 8.34 2 3 -1 185.81 8.37 1 -2 3 179.74 8.37 1 -2 3 180.16 8.36 -1 2 3 170.15 8.35 3 1 2 184.27 8.38 2 3 1 180.97 8.38 1 2 3 184.35 8.38 1 2 3 181.05 8.36 3 1 2 178.07 8.34 -1 -2 3 179.11 8.36 -1 -2 3 185.89 8.36 -1 2 -3 183.00 8.37 -3 -1 2 186.84 8.38 -3 -1 2 179.85 8.33 2 3 1 183.62 8.36 1 2 3 175.57 8.32 -2 -3 1 181.78 8.37 -2 3 -1 176.83 8.35 -3 -3 0 164.51 7.40 -3 0 -3 160.82 7.36 -3 0 -3 140.11 7.41 -3 0 3 168.06 7.42 -3 3 0 167.87 7.43 -3 3 0 165.16 7.38 0 -3 -3 142.17 7.38 0 -3 3 163.15 7.41 0 3 3 167.57 7.43 3 -3 0 148.54 7.37 3 -3 0 153.41 7.37 3 0 3 163.60 7.36 3 0 3 162.66 7.39 3 0 3 164.51 7.39 3 0 3 160.70 7.42 3 3 0 166.76 7.41 -3 -3 -2 1.31 0.14 -3 -3 -2 1.35 0.18 -3 -3 -2 1.35 0.20 3 -2 3 1.85 0.20 3 -2 3 1.66 0.18 3 -2 3 1.02 0.17 3 -2 3 1.87 0.22 -3 -2 -3 1.72 0.12 -3 -2 -3 1.51 0.19 -3 -2 -3 1.38 0.20 3 3 -2 1.62 0.21 -2 3 3 1.85 0.21 2 -3 3 1.92 0.19 -3 2 3 1.74 0.19 2 3 -3 1.81 0.21 2 3 -3 1.63 0.21 2 3 -3 1.14 0.16 -3 3 2 2.12 0.23 -3 3 2 1.68 0.18 -2 -3 -3 1.49 0.21 -2 -3 -3 1.14 0.17 3 -3 2 2.18 0.24 3 -3 2 1.55 0.17 3 3 -2 1.64 0.20 3 3 -2 1.45 0.17 3 2 -3 1.74 0.21 3 2 -3 1.93 0.21 3 2 -3 1.41 0.16 -2 3 3 1.35 0.20 3 -3 2 1.61 0.19 3 -3 2 1.38 0.16 2 -3 3 1.74 0.20 2 -3 3 1.29 0.18 -2 -3 3 1.80 0.22 -3 2 -3 1.86 0.21 -3 3 -2 1.29 0.20 -3 3 -2 1.12 0.17 2 -3 -3 2.09 0.23 2 -3 -3 1.31 0.17 -3 -3 2 1.54 0.20 2 3 3 1.52 0.21 2 3 3 1.56 0.20 3 -3 -2 2.30 0.24 3 -3 -2 1.49 0.18 -2 -3 3 1.57 0.20 -2 -3 3 1.63 0.19 -3 2 -3 1.36 0.17 3 -2 -3 2.03 0.23 3 -2 -3 1.48 0.17 -3 -3 2 1.66 0.19 -3 -3 2 1.43 0.16 -2 3 -3 1.30 0.18 -3 -2 3 1.91 0.22 -3 -2 3 1.77 0.20 -3 -2 3 1.41 0.16 3 2 3 1.44 0.12 3 2 3 1.64 0.21 3 2 3 1.46 0.21 -2 3 -3 1.91 0.21 -2 3 -3 1.20 0.20 3 3 2 1.62 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3 5 34 14.76 12.28 5 5 34 -5.14 -19.60 7 5 34 -13.32 -17.43 9 5 34 -12.66 20.77 11 5 34 -11.27 6.88 0 6 34 0.74 -10.00 2 6 34 4.85 18.76 4 6 34 10.03 -10.51 6 6 34 -0.88 -9.95 8 6 34 -1.71 -14.59 10 6 34 -14.19 12.45 12 6 34 0.75 5.71 1 7 34 2.58 -19.32 3 7 34 -3.31 18.40 5 7 34 -8.29 9.47 7 7 34 -4.67 -18.20 9 7 34 -3.81 11.27 11 7 34 -9.68 0.96 0 8 34 16.15 -2.14 2 8 34 -2.63 -4.55 4 8 34 -8.36 10.63 6 8 34 -14.33 13.54 8 8 34 -3.17 -9.69 10 8 34 -7.98 9.97 1 9 34 5.14 -15.70 3 9 34 -5.80 19.70 5 9 34 -4.36 13.38 7 9 34 6.04 -13.32 9 9 34 2.08 12.78 0 10 34 9.00 -0.77 2 10 34 -12.99 20.13 4 10 34 -7.44 4.42 6 10 34 13.92 -2.56 8 10 34 8.29 -12.33 1 11 34 1.40 -9.97 3 11 34 -4.02 16.94 5 11 34 5.34 -17.39 7 11 34 6.63 -10.19 0 12 34 -9.94 -2.16 2 12 34 -0.70 6.78 4 12 34 10.12 -8.87 6 12 34 -3.89 -0.54 1 13 34 -9.58 -12.11 3 13 34 6.44 8.49 1 0 35 2.65 1.58 3 0 35 5.76 3.49 5 0 35 1.59 5.51 7 0 35 -5.48 2.57 9 0 35 -4.07 -1.10 0 1 35 0.97 -4.81 2 1 35 2.84 -16.13 4 1 35 1.71 16.82 6 1 35 -0.93 16.66 8 1 35 5.02 -14.33 10 1 35 -5.95 -12.81 1 2 35 9.34 -28.33 3 2 35 -8.85 4.53 5 2 35 2.21 20.75 7 2 35 20.86 -2.57 9 2 35 8.93 -15.06 0 3 35 12.97 -5.86 2 3 35 -2.83 -8.56 4 3 35 -1.77 -0.30 6 3 35 17.01 0.72 8 3 35 10.00 -6.48 10 3 35 10.20 -6.82 1 4 35 2.07 -22.89 3 4 35 -10.31 0.67 5 4 35 6.42 -13.78 7 4 35 -0.57 8.13 9 4 35 -9.00 2.85 0 5 35 -0.45 -13.55 2 5 35 5.65 10.97 4 5 35 8.90 -15.36 6 5 35 -5.72 -1.71 8 5 35 -10.58 13.36 1 6 35 7.18 -24.43 3 6 35 15.06 18.77 5 6 35 -1.09 -12.72 7 6 35 -4.33 -12.38 0 7 35 -6.21 -18.41 2 7 35 -2.53 12.34 4 7 35 1.32 4.50 6 7 35 -15.81 -1.05 1 8 35 4.32 -11.01 3 8 35 -6.74 10.07 5 8 35 -3.63 4.48 0 9 35 7.05 -1.66 2 9 35 -0.64 3.49 4 9 35 -3.79 -0.97 1 10 35 -3.80 -10.76 3 10 35 -17.64 12.86 0 0 36 10.12 2.40 2 0 36 -0.35 -2.02 4 0 36 -3.16 8.17 6 0 36 -8.83 7.89 1 1 36 7.16 -7.67 3 1 36 6.31 1.07 5 1 36 4.08 11.90 0 2 36 18.77 2.25 2 2 36 -8.55 -9.16 4 2 36 1.66 17.02 6 2 36 16.85 8.03 1 3 36 3.55 -11.57 3 3 36 -20.83 -5.78 5 3 36 -2.60 7.86 0 4 36 11.03 -3.17 2 4 36 -6.95 -8.77 4 4 36 -4.30 -10.52 1 5 36 1.08 -7.96 3 5 36 13.25 3.48 0 6 36 0.51 -11.77 2 6 36 3.49 9.66 0 1 1 415.23 -5.29 0 0 2 24.20 0.07 1 1 2 -33.10 -12.24 0 2 2 -422.31 12.40 2 2 2 270.03 -19.20 0 1 3 33.89 10.02 0 0 4 161.33 -1.23 0 0 8 52.31 -0.45 0 0 10 24.76 -0.42 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 240625) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 0.000 0.000 5478 1128 ' ' 2 0.500 0.500 0.500 5478 1128 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 0 1 1 1.052 0 0 2 1.488 1 1 2 1.823 0 2 2 2.105 2 2 2 2.578 0 1 3 2.353 0 0 4 2.977 0 0 8 5.962 0 0 10 7.460 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL N in I23 #197 CELL 27.3691 27.3691 27.3691 90.00 90.00 90.00 SPGR I23 # Solvent Accessible Volume = 11002 # Electrons Found in S.A.V. = 2175 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 0.357 0.262-0.002 ! 2.69 eA-3 C102 0.787 0.507 0.155 ! 2.38 eA-3 C103 0.487 0.140 0.281 ! 2.30 eA-3 C104 0.853 0.850 0.150 ! 2.25 eA-3 C105 0.740 0.994 0.336 ! 2.25 eA-3 C106 0.134 0.734 0.493 ! 2.14 eA-3 C107 0.819 0.705 0.482 ! 2.14 eA-3 C108 0.112 0.885 0.112 ! 2.12 eA-3 C109 0.478 0.836 0.210 ! 2.11 eA-3 C110 0.978 0.336 0.710 ! 2.11 eA-3 C111 0.134 0.859 0.124 ! 2.02 eA-3 C112 0.673 0.830 0.005 ! 1.98 eA-3 C113 0.820 0.907 0.141 ! 1.97 eA-3 C114 0.666 0.789 0.493 ! 1.96 eA-3 C115 0.274 0.008 0.143 ! 1.96 eA-3 C116 0.850 0.900 0.145 ! 1.91 eA-3 C117 0.122 0.825 0.111 ! 1.82 eA-3 C118 0.330 0.607 0.622 ! 1.79 eA-3 C119 0.905 0.131 0.137 ! 1.75 eA-3 C120 0.405 0.631 0.637 ! 1.75 eA-3 C121 0.303 0.563 0.345 ! 1.74 eA-3 C122 0.860 0.156 0.077 ! 1.71 eA-3 C123 0.960 0.679 0.259 ! 1.71 eA-3 C124 0.078 0.858 0.157 ! 1.70 eA-3 C125 0.634 0.797 0.492 ! 1.69 eA-3 C126 0.478 0.181 0.230 ! 1.69 eA-3 C127 0.647 0.392 0.599 ! 1.68 eA-3 C128 0.728 0.491 0.171 ! 1.67 eA-3 C129 0.834 0.735 0.488 ! 1.63 eA-3 C130 0.802 0.999 0.345 ! 1.60 eA-3 C131 0.664 0.350 0.611 ! 1.59 eA-3 C132 0.164 0.850 0.111 ! 1.59 eA-3 C133 0.488 0.185 0.797 ! 1.58 eA-3 C134 0.150 0.923 0.167 ! 1.56 eA-3 C135 0.470 0.162 0.249 ! 1.56 eA-3 C136 0.655 0.342 0.373 ! 1.56 eA-3 C137 0.853 0.930 0.117 ! 1.54 eA-3 C138 0.179 0.508 0.173 ! 1.50 eA-3 C139 0.370 0.372 0.659 ! 1.49 eA-3 C140 0.870 0.872 0.159 ! 1.49 eA-3 C141 0.874 0.875 0.124 ! 1.49 eA-3 C142 0.365 0.171 0.015 ! 1.49 eA-3 C143 0.155 0.870 0.879 ! 1.48 eA-3 C144 0.922 0.166 0.085 ! 1.47 eA-3 C145 0.283 0.116 0.008 ! 1.47 eA-3 C146 0.853 0.758 0.016 ! 1.47 eA-3 C147 0.070 0.836 0.121 ! 1.46 eA-3 Q148 0.947 0.665 0.282 ! 1.46 eA-3 C149 0.376 0.202 0.018 ! 1.42 eA-3 Q150 1.000 0.504 0.289 ! 1.42 eA-3 C151 0.056 0.867 0.125 ! 1.41 eA-3 C152 0.869 0.897 0.183 ! 1.41 eA-3 C153 0.875 0.015 0.271 ! 1.41 eA-3 C154 0.821 0.751 0.001 ! 1.39 eA-3 C155 0.710 0.492 0.196 ! 1.38 eA-3 C156 0.274 0.972 0.137 ! 1.37 eA-3 C157 0.608 0.592 0.455 ! 1.36 eA-3 C158 0.678 0.663 0.577 ! 1.34 eA-3 C159 0.178 0.163 0.077 ! 1.34 eA-3 C160 0.117 0.165 0.918 ! 1.34 eA-3 C161 0.639 0.361 0.663 ! 1.34 eA-3 C162 0.139 0.861 0.163 ! 1.34 eA-3 C163 0.510 0.205 0.260 ! 1.33 eA-3 C164 0.203 0.951 0.166 ! 1.32 eA-3 C165 0.445 0.644 0.265 ! 1.31 eA-3 C166 0.859 0.883 0.089 ! 1.31 eA-3 C167 0.170 0.829 0.047 ! 1.29 eA-3 C168 0.814 0.255 0.029 ! 1.29 eA-3 Q169 0.054 0.351 0.028 ! 1.29 eA-3 C170 0.797 0.496 0.406 ! 1.29 eA-3 C171 0.140 0.766 0.949 ! 1.28 eA-3 C172 0.873 0.094 0.082 ! 1.28 eA-3 C173 0.209 0.173 0.040 ! 1.28 eA-3 C174 0.751 0.462 0.383 ! 1.27 eA-3 C175 0.540 0.321 0.352 ! 1.27 eA-3 C176 0.865 0.927 0.189 ! 1.26 eA-3 C177 0.899 0.133 0.059 ! 1.26 eA-3 C178 0.825 0.892 0.062 ! 1.26 eA-3 C179 0.769 0.485 0.324 ! 1.26 eA-3 C180 0.197 0.540 0.198 ! 1.26 eA-3 C181 0.605 0.341 0.672 ! 1.25 eA-3 C182 0.521 0.670 0.281 ! 1.25 eA-3 C183 0.907 0.892 0.174 ! 1.25 eA-3 Q184 0.335 0.625 0.032 ! 1.24 eA-3 C185 0.186 0.280 0.525 ! 1.23 eA-3 Q186 0.823 0.832 0.159 ! 1.23 eA-3 C187 0.813 0.648 0.491 ! 1.22 eA-3 C188 0.835 0.900 0.089 ! 1.21 eA-3 C189 0.570 0.622 0.470 ! 1.21 eA-3 C190 0.398 0.497 0.231 ! 1.21 eA-3 C191 0.436 0.712 0.353 ! 1.21 eA-3 C192 0.815 0.705 0.024 ! 1.21 eA-3 C193 0.743 0.959 0.158 ! 1.20 eA-3 C194 0.163 0.015 0.234 ! 1.20 eA-3 Q195 0.986 0.031 0.318 ! 1.20 eA-3 C196 0.951 0.711 0.250 ! 1.19 eA-3 C197 0.931 0.973 0.274 ! 1.19 eA-3 C198 0.216 0.943 0.885 ! 1.18 eA-3 C199 0.713 0.448 0.305 ! 1.18 eA-3 ) ; _shelx_fab_checksum 86174 _platon_squeeze_special_details ; A solvent mask was calculated and 2256 electrons were found in a volume of 10956\%A^3^ in 1 void per unit cell. This is consistent with the presence of 9 C2H5NO and 9 H2O per Formula Unit which account for 2268 electrons per unit cell. ; _platon_squeeze_void_probe_radius 1.20 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' 'z, x, y' 'y, z, x' '-y, -z, x' 'z, -x, -y' '-y, z, -x' '-z, -x, y' '-z, x, -y' 'y, -z, -x' '-x, -y, z' 'x, -y, -z' '-x, y, -z' 'x+1/2, y+1/2, z+1/2' 'z+1/2, x+1/2, y+1/2' 'y+1/2, z+1/2, x+1/2' '-y+1/2, -z+1/2, x+1/2' 'z+1/2, -x+1/2, -y+1/2' '-y+1/2, z+1/2, -x+1/2' '-z+1/2, -x+1/2, y+1/2' '-z+1/2, x+1/2, -y+1/2' 'y+1/2, -z+1/2, -x+1/2' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x+1/2, y+1/2, -z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ni1 Ni 0.500000 0.000000 0.17366(4) 0.0463(4) Uani 1 2 d S T P . . Al1 Al 0.55368(8) 0.00041(18) 0.05861(8) 0.0540(6) Uani 1 1 d . . . . . N1 N 0.5040(10) -0.0008(10) 0.2500(3) 0.082(3) Uani 0.5 1 d G U P A -1 C19 C 0.5471(9) 0.0055(9) 0.2762(4) 0.089(4) Uani 0.5 1 d DG U P A -1 H19 H 0.575402 0.015375 0.260213 0.107 Uiso 0.5 1 calc R U P A -1 C20 C 0.5479(7) -0.0031(7) 0.3263(4) 0.100(4) Uani 0.5 1 d DG U P A -1 H20 H 0.576701 0.001148 0.343767 0.120 Uiso 0.5 1 calc R U P A -1 C21 C 0.5056(6) -0.0179(4) 0.3502(3) 0.120(4) Uani 0.5 1 d DG U P A -1 C1B C 0.4625(7) -0.0241(7) 0.3240(5) 0.115(5) Uani 0.5 1 d DG U P A -1 H1B H 0.434210 -0.034042 0.339991 0.138 Uiso 0.5 1 calc R U P A -1 C1A C 0.4617(9) -0.0156(9) 0.2739(5) 0.111(5) Uani 0.5 1 d DG U P A -1 H1A H 0.432910 -0.019814 0.256437 0.133 Uiso 0.5 1 calc R U P A -1 O1 O 0.5523(3) 0.0527(3) 0.1752(4) 0.073(2) Uani 1 1 d . . . . . O2 O 0.5868(5) 0.0472(4) 0.1007(4) 0.143(5) Uani 1 1 d . . . . . O3 O 0.5542(3) -0.0523(3) 0.1769(3) 0.072(2) Uani 1 1 d . . . . . O4 O 0.5663(3) -0.0690(3) 0.0993(3) 0.095(3) Uani 1 1 d . . . . . O6 O 0.500000 0.000000 0.0989(2) 0.0640(16) Uani 1 2 d S T P A . O7 O 0.6045(6) 0.000000 0.000000 0.104(6) Uani 0.5 2 d S T P A . H7 H 0.635535 0.000000 0.000000 0.124 Uiso 0.5 2 d R U P . . C1 C 0.5787(5) 0.0678(6) 0.1464(6) 0.085(4) Uani 1 1 d D . . . . C2 C 0.6197(5) 0.1015(6) 0.1612(6) 0.092(4) Uani 1 1 d D . . . . C3 C 0.6554(5) 0.1202(6) 0.1211(5) 0.092(4) Uani 1 1 d . . . . . H3 H 0.651277 0.111606 0.088450 0.110 Uiso 1 1 calc R U . . . C4 C 0.6914(5) 0.1485(5) 0.1350(5) 0.081(4) Uani 1 1 d . . . . . H4 H 0.710363 0.164006 0.111425 0.098 Uiso 1 1 calc R U . . . C5 C 0.7024(6) 0.1560(6) 0.1857(5) 0.079(4) Uani 1 1 d . . . . . C6 C 0.6741(6) 0.1345(5) 0.2195(6) 0.089(4) Uani 1 1 d . . . . . H6 H 0.683275 0.136571 0.252185 0.106 Uiso 1 1 calc R U . . . C7 C 0.6304(5) 0.1087(5) 0.2073(5) 0.076(3) Uani 1 1 d . . . . . H7A H 0.609854 0.097161 0.231754 0.091 Uiso 1 1 calc R U . . . C8 C 0.7461(6) 0.1848(5) 0.1996(5) 0.077(4) Uani 1 1 d . . . . . C9 C 0.7631(6) 0.2248(5) 0.1718(6) 0.085(5) Uani 1 1 d . . . . . H9 H 0.747395 0.231402 0.142357 0.102 Uiso 1 1 calc R U . . . C10 C 0.5816(5) -0.0680(5) 0.1412(5) 0.079(3) Uani 1 1 d . . . . . C11 C 0.6231(5) -0.1018(5) 0.1576(5) 0.072(3) Uani 1 1 d . . . . . C12 C 0.6446(5) -0.1272(5) 0.1257(5) 0.086(4) Uani 1 1 d . . . . . H12 H 0.631528 -0.129219 0.094386 0.103 Uiso 1 1 calc R U . . . C13 C 0.6891(6) -0.1531(6) 0.1371(6) 0.108(6) Uani 1 1 d . . . . . H13 H 0.707236 -0.167731 0.112349 0.129 Uiso 1 1 calc R U . . . C14 C 0.7037(6) -0.1559(5) 0.1834(6) 0.082(4) Uani 1 1 d . . . . . C15 C 0.6723(6) -0.1344(6) 0.2201(6) 0.092(5) Uani 1 1 d . . . . . H15 H 0.677330 -0.141144 0.253001 0.111 Uiso 1 1 calc R U . . . C16 C 0.6371(5) -0.1057(5) 0.2066(5) 0.078(4) Uani 1 1 d . . . . . H16 H 0.620829 -0.087311 0.230078 0.094 Uiso 1 1 calc R U . . . C17 C 0.7472(6) -0.1855(5) 0.1989(6) 0.083(4) Uani 1 1 d . . . . . C18 C 0.7585(6) -0.2261(5) 0.1719(6) 0.080(4) Uani 1 1 d . . . . . C22 C 0.5075(6) -0.0270(5) 0.4047(7) 0.128(4) Uani 0.5 1 d D U P A -1 O5A O 0.5526(7) -0.0198(6) 0.4313(6) 0.127(4) Uani 0.5 1 d D U P A -1 O5 O 0.4632(8) -0.0426(7) 0.4287(6) 0.129(4) Uani 0.5 1 d D U P A -1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ni1 0.0416(7) 0.0491(7) 0.0481(8) 0.000 0.000 0.0010(12) Al1 0.0460(12) 0.0686(14) 0.0476(12) -0.001(2) 0.0014(9) 0.007(2) N1 0.101(8) 0.085(7) 0.059(4) -0.002(7) 0.003(5) 0.027(8) C19 0.105(8) 0.091(10) 0.072(6) 0.003(8) -0.004(5) 0.027(9) C20 0.104(8) 0.123(11) 0.074(5) 0.013(8) 0.000(5) 0.018(10) C21 0.111(8) 0.140(10) 0.107(5) 0.031(7) 0.016(5) 0.022(9) C1B 0.106(9) 0.136(12) 0.104(6) 0.024(8) 0.023(6) 0.019(9) C1A 0.110(9) 0.121(12) 0.102(6) 0.013(8) 0.018(6) 0.019(9) O1 0.051(4) 0.068(3) 0.100(5) -0.011(4) -0.008(4) -0.009(4) O2 0.152(8) 0.148(8) 0.130(6) -0.057(6) 0.043(6) -0.091(7) O3 0.068(5) 0.073(3) 0.074(4) -0.005(4) -0.005(4) 0.024(4) O4 0.114(6) 0.093(4) 0.078(4) -0.015(3) -0.022(4) 0.044(5) O6 0.064(3) 0.079(4) 0.049(3) 0.000 0.000 0.009(4) O7 0.038(7) 0.203(18) 0.070(6) -0.008(7) 0.000 0.000 C1 0.066(6) 0.092(8) 0.098(5) -0.014(4) -0.006(4) -0.026(5) C2 0.081(7) 0.105(9) 0.090(5) 0.009(5) -0.019(4) -0.041(7) C3 0.082(7) 0.109(9) 0.083(6) 0.007(6) -0.019(5) -0.039(6) C4 0.072(6) 0.089(8) 0.084(5) 0.022(6) -0.027(5) -0.027(6) C5 0.077(6) 0.076(8) 0.085(5) 0.022(5) -0.027(4) -0.027(5) C6 0.095(7) 0.088(9) 0.083(6) 0.013(6) -0.022(5) -0.042(7) C7 0.080(7) 0.060(7) 0.087(5) 0.016(5) -0.018(5) -0.024(5) C8 0.080(7) 0.075(8) 0.077(8) 0.020(6) -0.028(6) -0.026(6) C9 0.077(8) 0.094(8) 0.084(9) 0.037(7) -0.046(7) -0.035(7) C10 0.082(7) 0.084(8) 0.072(4) -0.010(4) -0.008(3) 0.038(6) C11 0.067(6) 0.060(6) 0.087(5) -0.017(4) -0.017(4) 0.019(5) C12 0.083(7) 0.087(8) 0.087(6) -0.031(6) -0.032(5) 0.039(6) C13 0.104(9) 0.126(12) 0.093(6) -0.049(7) -0.042(6) 0.068(9) C14 0.079(7) 0.077(8) 0.091(6) -0.038(6) -0.034(5) 0.033(6) C15 0.091(8) 0.096(10) 0.090(6) -0.034(6) -0.031(5) 0.046(7) C16 0.065(7) 0.084(8) 0.085(5) -0.014(6) -0.013(5) 0.026(6) C17 0.087(7) 0.078(7) 0.084(8) -0.039(6) -0.033(6) 0.039(6) C18 0.091(10) 0.075(7) 0.074(8) -0.033(6) -0.022(7) 0.035(7) C22 0.122(7) 0.153(8) 0.109(5) 0.044(6) 0.022(5) 0.040(6) O5A 0.122(7) 0.153(8) 0.107(5) 0.048(6) 0.023(5) 0.041(6) O5 0.122(7) 0.153(8) 0.111(5) 0.040(6) 0.023(5) 0.040(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Ni1 N1 90.5(9) 10_655 . ? O1 Ni1 N1 87.1(9) . . ? O1 Ni1 O1 177.7(6) . 10_655 ? O1 Ni1 O3 89.2(2) 10_655 10_655 ? O1 Ni1 O3 90.7(2) . 10_655 ? O1 Ni1 O3 89.2(2) . . ? O1 Ni1 O3 90.7(2) 10_655 . ? O1 Ni1 O6 91.2(3) 10_655 . ? O1 Ni1 O6 91.2(3) . . ? O3 Ni1 N1 90.1(7) 10_655 . ? O3 Ni1 N1 85.0(7) . . ? O3 Ni1 O3 175.1(5) . 10_655 ? O6 Ni1 N1 176.9(7) . . ? O6 Ni1 O3 92.4(2) . 10_655 ? O6 Ni1 O3 92.5(2) . . ? O2 Al1 Al1 118.1(4) . 10_655 ? O2 Al1 O4 101.2(5) . . ? O2 Al1 O7 98.3(4) . . ? O4 Al1 Al1 98.5(3) . 10_655 ? O6 Al1 Al1 36.86(18) . 10_655 ? O6 Al1 O2 91.3(4) . . ? O6 Al1 O4 79.6(3) . . ? O6 Al1 O7 167.8(4) . . ? O7 Al1 Al1 130.9(3) . 10_655 ? O7 Al1 O4 105.8(3) . . ? C19 N1 Ni1 123.9(12) . . ? C19 N1 C1A 120.0 . . ? C1A N1 Ni1 115.4(12) . . ? N1 C19 H19 120.0 . . ? N1 C19 C20 120.0 . . ? C20 C19 H19 120.0 . . ? C19 C20 H20 120.0 . . ? C21 C20 C19 120.0 . . ? C21 C20 H20 120.0 . . ? C20 C21 C1B 120.0 . . ? C20 C21 C22 118.9(7) . . ? C1B C21 C22 121.1(7) . . ? C21 C1B H1B 120.0 . . ? C1A C1B C21 120.0 . . ? C1A C1B H1B 120.0 . . ? N1 C1A H1A 120.0 . . ? C1B C1A N1 120.0 . . ? C1B C1A H1A 120.0 . . ? C1 O1 Ni1 133.3(10) . . ? C1 O2 Al1 136.4(9) . . ? C10 O3 Ni1 127.6(8) . . ? C10 O4 Al1 120.1(9) . . ? Al1 O6 Ni1 126.86(18) 10_655 . ? Al1 O6 Ni1 126.86(18) . . ? Al1 O6 Al1 106.3(4) 10_655 . ? Al1 O7 Al1 98.2(6) . 11 ? Al1 O7 H7 130.9 11 . ? Al1 O7 H7 130.9 . . ? O1 C1 O2 125.1(13) . . ? O1 C1 C2 120.4(14) . . ? O2 C1 C2 111.7(13) . . ? C1 C2 C3 118.6(13) . . ? C7 C2 C1 121.1(14) . . ? C7 C2 C3 119.3(12) . . ? C2 C3 H3 121.3 . . ? C4 C3 C2 117.5(13) . . ? C4 C3 H3 121.3 . . ? C3 C4 H4 119.2 . . ? C3 C4 C5 121.6(14) . . ? C5 C4 H4 119.2 . . ? C4 C5 C8 119.7(13) . . ? C6 C5 C4 118.9(13) . . ? C6 C5 C8 121.4(13) . . ? C5 C6 H6 118.7 . . ? C5 C6 C7 122.5(14) . . ? C7 C6 H6 118.7 . . ? C2 C7 C6 119.2(14) . . ? C2 C7 H7A 120.4 . . ? C6 C7 H7A 120.4 . . ? C9 C8 C5 122.6(13) . . ? C9 C8 C5 122.2(13) 6_656 . ? C9 C8 C9 114.9(14) 6_656 . ? C8 C9 C8 124.5(14) 7_665 . ? C8 C9 H9 117.8 . . ? C8 C9 H9 117.8 7_665 . ? O3 C10 C11 113.9(12) . . ? O4 C10 O3 120.8(12) . . ? O4 C10 C11 121.1(12) . . ? C12 C11 C10 118.3(13) . . ? C12 C11 C16 119.6(12) . . ? C16 C11 C10 122.1(12) . . ? C11 C12 H12 119.5 . . ? C11 C12 C13 121.0(13) . . ? C13 C12 H12 119.5 . . ? C12 C13 H13 120.4 . . ? C14 C13 C12 119.2(14) . . ? C14 C13 H13 120.4 . . ? C13 C14 C15 117.3(13) . . ? C13 C14 C17 122.7(13) . . ? C15 C14 C17 119.6(13) . . ? C14 C15 H15 120.3 . . ? C16 C15 C14 119.4(15) . . ? C16 C15 H15 120.3 . . ? C11 C16 H16 119.2 . . ? C15 C16 C11 121.5(14) . . ? C15 C16 H16 119.2 . . ? C18 C17 C14 117.6(13) . . ? C18 C17 C14 119.8(12) 9_656 . ? C18 C17 C18 122.6(14) . 9_656 ? C17 C18 C17 117.3(14) . 8_645 ? O5A C22 C21 120.2(11) . . ? O5 C22 C21 117.9(11) . . ? O5 C22 O5A 121.9(17) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ni1 N1 2.094(7) . ? Ni1 O1 2.032(9) . ? Ni1 O1 2.032(9) 10_655 ? Ni1 O3 2.063(8) . ? Ni1 O3 2.063(8) 10_655 ? Ni1 O6 2.047(7) . ? Al1 Al1 2.939(4) 10_655 ? Al1 O2 1.947(11) . ? Al1 O4 2.229(9) . ? Al1 O6 1.836(5) . ? Al1 O7 2.123(10) . ? N1 C19 1.3900 . ? N1 C1A 1.3900 . ? C19 H19 0.9300 . ? C19 C20 1.3900 . ? C20 H20 0.9300 . ? C20 C21 1.3900 . ? C21 C1B 1.3900 . ? C21 C22 1.514(18) . ? C1B H1B 0.9300 . ? C1B C1A 1.3900 . ? C1A H1A 0.9300 . ? O1 C1 1.145(16) . ? O2 C1 1.391(17) . ? O3 C10 1.305(15) . ? O4 C10 1.222(15) . ? O7 H7 0.8501 . ? C1 C2 1.509(16) . ? C2 C3 1.56(2) . ? C2 C7 1.311(19) . ? C3 H3 0.9300 . ? C3 C4 1.311(17) . ? C4 H4 0.9300 . ? C4 C5 1.434(19) . ? C5 C6 1.344(19) . ? C5 C8 1.481(17) . ? C6 H6 0.9300 . ? C6 C7 1.429(19) . ? C7 H7A 0.9300 . ? C8 C9 1.413(18) . ? C8 C9 1.343(16) 6_656 ? C9 H9 0.9300 . ? C10 C11 1.532(16) . ? C11 C12 1.262(16) . ? C11 C16 1.399(18) . ? C12 H12 0.9300 . ? C12 C13 1.444(18) . ? C13 H13 0.9300 . ? C13 C14 1.331(19) . ? C14 C15 1.448(19) . ? C14 C17 1.502(17) . ? C15 H15 0.9300 . ? C15 C16 1.297(18) . ? C16 H16 0.9300 . ? C17 C18 1.368(16) . ? C17 C18 1.425(17) 9_656 ? C22 O5A 1.447(17) . ? C22 O5 1.444(17) . ? loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 0.000 0.000 5478 1128 '27 C2H5NO,27 H2O' 2 0.500 0.500 0.500 5478 1128 '27 C2H5NO,27 H2O' loop_ _twin_individual_id _twin_individual_mass_fraction_refined 1 0.51139 2 0.48861