#------------------------------------------------------------------------------ #$Date: 2026-06-06 02:00:03 +0100 (Sat, 06 Jun 2026) $ #$Revision: 306517 $ #$URL: svn://www.crystallography.net/cod/cif/7/06/44/7064437.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7064437 loop_ _publ_author_name 'Varmuzova, Vera' 'Cisarova, Ivana' '\ 2\s(I)' _cod_data_source_file d6nj01330a2.cif _cod_data_source_block vv457 _cod_database_code 7064437 _shelx_shelxl_version_number 2019/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.644 _shelx_estimated_absorpt_t_max 0.889 _shelx_res_file ; TITL vv457, 10 K, in P2(1)2(1)2(1) vv457.res created by SHELXL-2025/1 at 20:08:10 on 03-Jun-2026 CELL 0.71073 11.3698 19.8046 24.4266 90.000 90.000 90.000 ZERR 4 0.0006 0.0011 0.0015 0.000 0.000 0.000 LATT -1 SYMM 1/2-X, -Y, 1/2+Z SYMM -X, 1/2+Y, 1/2-Z SYMM 1/2+X, 1/2-Y, -Z SFAC C H CL FE N O P PD UNIT 224 192 32 8 16 8 8 4 TEMP -173 SIZE 0.09 0.14 0.36 L.S. 9 DFIX 1.760 0.002 C2S Cl5D BOND $H ACTA LIST 4 FMAP 2 EADP Cl5S Cl5D PLAN -10 WGHT 0.020900 2.416000 FVAR 0.23476 0.85209 PD1 8 0.281048 0.613511 0.280545 11.00000 0.00855 0.01013 = 0.01149 0.00074 0.00155 0.00024 CL1 3 0.316831 0.724858 0.300686 11.00000 0.01399 0.01196 = 0.02946 -0.00361 -0.00088 0.00074 CL2 3 0.248023 0.503060 0.254886 11.00000 0.01448 0.01245 = 0.02498 -0.00214 -0.00082 0.00000 FE1 4 0.513154 0.601558 0.425306 11.00000 0.01119 0.01278 = 0.01361 0.00096 0.00091 0.00032 FE2 4 0.040580 0.629932 0.141670 11.00000 0.01003 0.01275 = 0.01220 0.00089 0.00014 -0.00020 P1 7 0.486265 0.602411 0.282651 11.00000 0.00942 0.01058 = 0.01311 0.00077 0.00177 0.00032 P2 7 0.075346 0.626822 0.282367 11.00000 0.00918 0.01153 = 0.01216 0.00033 0.00168 -0.00019 O1 6 0.450474 0.409386 0.413230 11.00000 0.01820 0.01771 = 0.02288 -0.00079 -0.00178 -0.00235 O2 6 0.087937 0.817667 0.154925 11.00000 0.02483 0.01802 = 0.01843 0.00155 -0.00462 -0.00255 N1 5 0.668452 0.456946 0.511981 11.00000 0.01664 0.01996 = 0.01910 0.00215 -0.00047 -0.00380 N2 5 0.662594 0.362841 0.462065 11.00000 0.01688 0.01711 = 0.01845 0.00145 0.00274 0.00283 N3 5 -0.035977 0.796722 0.024132 11.00000 0.01804 0.02320 = 0.01939 0.00128 -0.00362 0.00540 N4 5 -0.118427 0.855499 0.091915 11.00000 0.01454 0.01701 = 0.02079 -0.00013 0.00082 -0.00029 C1 1 0.452862 0.513788 0.458904 11.00000 0.01623 0.01342 = 0.01517 0.00160 0.00357 -0.00119 C2 1 0.362213 0.545200 0.426487 11.00000 0.01036 0.01809 = 0.02245 0.00127 0.00266 -0.00123 AFIX 43 H2 2 0.323601 0.525868 0.395764 11.00000 -1.20000 AFIX 0 C3 1 0.341042 0.610345 0.448810 11.00000 0.01290 0.01916 = 0.02793 0.00030 0.00542 0.00161 AFIX 43 H3 2 0.285884 0.642318 0.435341 11.00000 -1.20000 AFIX 0 C4 1 0.416201 0.619613 0.494637 11.00000 0.02049 0.01829 = 0.01838 -0.00217 0.00670 0.00060 AFIX 43 H4 2 0.419253 0.658649 0.517196 11.00000 -1.20000 AFIX 0 C5 1 0.486119 0.560607 0.501058 11.00000 0.02306 0.01730 = 0.01397 0.00230 0.00304 0.00001 AFIX 43 H5 2 0.544364 0.553441 0.528331 11.00000 -1.20000 AFIX 0 C6 1 0.559663 0.623139 0.346132 11.00000 0.01142 0.01328 = 0.01405 0.00187 0.00130 -0.00024 C7 1 0.548458 0.683836 0.377946 11.00000 0.01771 0.01208 = 0.01605 0.00105 0.00109 -0.00116 AFIX 43 H7 2 0.495925 0.720060 0.370727 11.00000 -1.20000 AFIX 0 C8 1 0.629761 0.680234 0.422150 11.00000 0.01921 0.01862 = 0.01664 -0.00072 -0.00050 -0.00623 AFIX 43 H8 2 0.641190 0.713777 0.449438 11.00000 -1.20000 AFIX 0 C9 1 0.690900 0.617821 0.418436 11.00000 0.01041 0.02243 = 0.01865 0.00111 -0.00144 -0.00197 AFIX 43 H9 2 0.750111 0.602403 0.442864 11.00000 -1.20000 AFIX 0 C10 1 0.648145 0.582389 0.371817 11.00000 0.00927 0.01828 = 0.01841 0.00033 0.00287 0.00125 AFIX 43 H10 2 0.673781 0.539211 0.359790 11.00000 -1.20000 AFIX 0 C11 1 0.547623 0.660782 0.232676 11.00000 0.00886 0.01251 = 0.01646 0.00262 0.00269 0.00284 C12 1 0.617611 0.715524 0.247143 11.00000 0.01378 0.01847 = 0.01714 0.00154 0.00295 -0.00126 AFIX 43 H12 2 0.638911 0.722409 0.284333 11.00000 -1.20000 AFIX 0 C13 1 0.656329 0.760122 0.207132 11.00000 0.01890 0.01703 = 0.02520 0.00389 0.00425 -0.00430 AFIX 43 H13 2 0.702758 0.797964 0.217340 11.00000 -1.20000 AFIX 0 C14 1 0.628273 0.750217 0.152729 11.00000 0.01765 0.01961 = 0.02480 0.01050 0.00454 0.00008 AFIX 43 H14 2 0.655785 0.780866 0.125690 11.00000 -1.20000 AFIX 0 C15 1 0.559410 0.695053 0.137664 11.00000 0.01878 0.02435 = 0.01507 0.00525 -0.00015 0.00439 AFIX 43 H15 2 0.540881 0.687567 0.100229 11.00000 -1.20000 AFIX 0 C16 1 0.517963 0.651084 0.177465 11.00000 0.01475 0.01627 = 0.01884 0.00186 -0.00085 -0.00057 AFIX 43 H16 2 0.469226 0.614202 0.167279 11.00000 -1.20000 AFIX 0 C17 1 0.554122 0.521517 0.266237 11.00000 0.01044 0.01238 = 0.01539 -0.00113 -0.00063 0.00110 C18 1 0.512856 0.463332 0.292532 11.00000 0.01285 0.01675 = 0.01471 0.00046 0.00047 -0.00075 AFIX 43 H18 2 0.445460 0.465692 0.315440 11.00000 -1.20000 AFIX 0 C19 1 0.570529 0.402088 0.285113 11.00000 0.02104 0.01248 = 0.02316 0.00191 -0.00433 -0.00242 AFIX 43 H19 2 0.542248 0.362604 0.302846 11.00000 -1.20000 AFIX 0 C20 1 0.669223 0.398527 0.251890 11.00000 0.02021 0.01353 = 0.02897 -0.00487 -0.00407 0.00305 AFIX 43 H20 2 0.708335 0.356602 0.246820 11.00000 -1.20000 AFIX 0 C21 1 0.710865 0.456089 0.226069 11.00000 0.01526 0.02099 = 0.02424 -0.00476 0.00414 0.00203 AFIX 43 H21 2 0.778628 0.453656 0.203401 11.00000 -1.20000 AFIX 0 C22 1 0.653410 0.517337 0.233372 11.00000 0.01340 0.01584 = 0.01907 0.00106 0.00075 -0.00135 AFIX 43 H22 2 0.682351 0.556712 0.215710 11.00000 -1.20000 AFIX 0 C23 1 0.501056 0.446370 0.445767 11.00000 0.01651 0.01564 = 0.01502 0.00323 0.00517 -0.00143 C24 1 0.610476 0.423847 0.473054 11.00000 0.01669 0.01515 = 0.01578 0.00275 0.00375 -0.00056 C25 1 0.759582 0.415665 0.526142 11.00000 0.01678 0.02574 = 0.01839 0.00681 -0.00040 -0.00165 AFIX 43 H25 2 0.816692 0.425835 0.553308 11.00000 -1.20000 AFIX 0 C26 1 0.757351 0.357672 0.495852 11.00000 0.01434 0.02460 = 0.02168 0.00809 0.00288 0.00186 AFIX 43 H26 2 0.811170 0.321071 0.497956 11.00000 -1.20000 AFIX 0 C27 1 0.628153 0.311505 0.422220 11.00000 0.03362 0.02226 = 0.02388 -0.00637 -0.00157 0.00726 AFIX 137 H27A 2 0.682081 0.273019 0.424643 11.00000 -1.50000 H27B 2 0.631451 0.330698 0.385273 11.00000 -1.50000 H27C 2 0.547824 0.296360 0.430017 11.00000 -1.50000 AFIX 0 C31 1 0.105491 0.715889 0.105730 11.00000 0.01221 0.01810 = 0.01475 0.00511 0.00199 -0.00160 C32 1 0.192944 0.684919 0.140785 11.00000 0.01094 0.01995 = 0.01386 0.00278 0.00053 -0.00239 AFIX 43 H32 2 0.229845 0.705253 0.171538 11.00000 -1.20000 AFIX 0 C33 1 0.213451 0.618688 0.120827 11.00000 0.01204 0.02119 = 0.01662 0.00333 0.00366 0.00248 AFIX 43 H33 2 0.266998 0.586958 0.135977 11.00000 -1.20000 AFIX 0 C34 1 0.140551 0.607687 0.074385 11.00000 0.01847 0.01859 = 0.01607 0.00006 0.00575 0.00156 AFIX 43 H34 2 0.137363 0.567510 0.053189 11.00000 -1.20000 AFIX 0 C35 1 0.073162 0.667157 0.065076 11.00000 0.01638 0.01778 = 0.01386 0.00235 0.00160 -0.00023 AFIX 43 H35 2 0.016685 0.673432 0.036869 11.00000 -1.20000 AFIX 0 C36 1 -0.005424 0.607663 0.220684 11.00000 0.01016 0.01606 = 0.01355 0.00155 0.00216 -0.00131 C37 1 0.000810 0.547563 0.187869 11.00000 0.01788 0.01299 = 0.01505 0.00125 -0.00079 -0.00292 AFIX 43 H37 2 0.050926 0.510000 0.194267 11.00000 -1.20000 AFIX 0 C38 1 -0.080996 0.554033 0.144170 11.00000 0.01815 0.01667 = 0.01707 0.00103 -0.00105 -0.00633 AFIX 43 H38 2 -0.095344 0.521454 0.116416 11.00000 -1.20000 AFIX 0 C39 1 -0.137745 0.617904 0.149236 11.00000 0.01012 0.02461 = 0.01864 0.00116 0.00059 -0.00106 AFIX 43 H39 2 -0.196103 0.635330 0.125255 11.00000 -1.20000 AFIX 0 C40 1 -0.092451 0.650890 0.195986 11.00000 0.00998 0.01958 = 0.01527 0.00015 0.00137 -0.00003 AFIX 43 H40 2 -0.115437 0.694160 0.208922 11.00000 -1.20000 AFIX 0 C41 1 0.016404 0.570487 0.334115 11.00000 0.00983 0.01415 = 0.01646 0.00379 0.00442 0.00367 C42 1 0.060497 0.576809 0.387181 11.00000 0.02072 0.02618 = 0.01888 0.00393 0.00125 0.00252 AFIX 43 H42 2 0.118816 0.609827 0.394866 11.00000 -1.20000 AFIX 0 C43 1 0.019754 0.535170 0.428890 11.00000 0.03634 0.03479 = 0.01757 0.00819 0.00644 0.01025 AFIX 43 H43 2 0.050123 0.539708 0.464935 11.00000 -1.20000 AFIX 0 C44 1 -0.065234 0.487073 0.417694 11.00000 0.03123 0.02685 = 0.03222 0.01655 0.02009 0.01224 AFIX 43 H44 2 -0.093635 0.458747 0.446161 11.00000 -1.20000 AFIX 0 C45 1 -0.108722 0.480202 0.365338 11.00000 0.01839 0.01435 = 0.04317 0.00783 0.01378 0.00259 AFIX 43 H45 2 -0.166176 0.446602 0.357904 11.00000 -1.20000 AFIX 0 C46 1 -0.069526 0.521906 0.323122 11.00000 0.01239 0.01433 = 0.02706 0.00407 0.00266 0.00268 AFIX 43 H46 2 -0.100909 0.517340 0.287269 11.00000 -1.20000 AFIX 0 C47 1 0.012689 0.708765 0.300121 11.00000 0.00961 0.01361 = 0.01506 -0.00145 -0.00023 0.00009 C48 1 -0.079781 0.714532 0.337499 11.00000 0.01635 0.01679 = 0.02119 -0.00103 0.00373 0.00034 AFIX 43 H48 2 -0.107177 0.675873 0.356670 11.00000 -1.20000 AFIX 0 C49 1 -0.131664 0.777423 0.346506 11.00000 0.01914 0.02514 = 0.02932 -0.00574 0.00856 0.00466 AFIX 43 H49 2 -0.194167 0.781592 0.372094 11.00000 -1.20000 AFIX 0 C50 1 -0.092376 0.833952 0.318245 11.00000 0.02379 0.01784 = 0.03654 -0.00433 0.00191 0.00600 AFIX 43 H50 2 -0.127939 0.876650 0.324576 11.00000 -1.20000 AFIX 0 C51 1 -0.001834 0.828138 0.281027 11.00000 0.02104 0.01502 = 0.02560 0.00098 0.00014 0.00215 AFIX 43 H51 2 0.024316 0.866815 0.261505 11.00000 -1.20000 AFIX 0 C52 1 0.051611 0.765735 0.271876 11.00000 0.01311 0.01765 = 0.01693 0.00070 0.00044 0.00058 AFIX 43 H52 2 0.114465 0.762055 0.246425 11.00000 -1.20000 AFIX 0 C53 1 0.055481 0.783208 0.116046 11.00000 0.01582 0.01518 = 0.01462 0.00452 0.00042 -0.00308 C54 1 -0.033633 0.809519 0.077333 11.00000 0.01396 0.01482 = 0.01778 0.00157 -0.00010 -0.00101 C55 1 -0.124146 0.836276 0.003924 11.00000 0.02355 0.02997 = 0.02067 0.00041 -0.00605 0.00963 AFIX 43 H55 2 -0.146229 0.838488 -0.033543 11.00000 -1.20000 AFIX 0 C56 1 -0.176236 0.872229 0.044989 11.00000 0.01873 0.02335 = 0.02755 0.00018 -0.00662 0.00356 AFIX 43 H56 2 -0.240129 0.902844 0.041524 11.00000 -1.20000 AFIX 0 C57 1 -0.147007 0.882949 0.145846 11.00000 0.02115 0.02204 = 0.02311 -0.00424 0.00733 -0.00525 AFIX 137 H57A 2 -0.120278 0.851559 0.174256 11.00000 -1.50000 H57B 2 -0.232286 0.889123 0.148827 11.00000 -1.50000 H57C 2 -0.107617 0.926569 0.150612 11.00000 -1.50000 AFIX 0 REM solvent C1S 1 0.117841 0.557048 0.629899 11.00000 0.02432 0.02448 = 0.02350 0.00339 -0.00013 -0.00250 AFIX 13 H1S 2 0.148583 0.532873 0.662870 11.00000 -1.20000 AFIX 0 CL1S 3 0.059520 0.634932 0.650992 11.00000 0.03447 0.03226 = 0.04229 -0.00473 0.00496 0.00619 CL2S 3 0.010265 0.506181 0.598882 11.00000 0.03569 0.03489 = 0.05139 0.00603 -0.00619 -0.01660 CL3S 3 0.234313 0.568769 0.583841 11.00000 0.03308 0.04565 = 0.04338 -0.01780 0.01597 -0.01355 C2S 1 0.773966 0.685176 0.579222 11.00000 0.03431 0.03686 = 0.02842 -0.00341 -0.00546 -0.01401 AFIX 13 H2S 2 0.809894 0.697249 0.615285 11.00000 -1.20000 AFIX 0 CL4S 3 0.643545 0.731229 0.570661 11.00000 0.03417 0.04632 = 0.04352 -0.02060 0.00199 -0.00445 PART 1 CL5S 3 0.746416 0.596185 0.577614 21.00000 0.03522 0.03405 = 0.06703 0.02006 -0.01278 -0.01126 PART 2 CL5D 3 0.711098 0.609113 0.600115 -21.00000 0.03522 0.03405 = 0.06703 0.02006 -0.01278 -0.01126 PART 0 CL6S 3 0.874662 0.702189 0.527363 11.00000 0.03676 0.03667 = 0.03829 -0.00207 0.00415 -0.00512 HKLF 4 REM vv457, 10 K, in P2(1)2(1)2(1) REM wR2 = 0.0504, GooF = S = 1.042, Restrained GooF = 1.044 for all data REM R1 = 0.0225 for 13153 Fo > 4sig(Fo) and 0.0242 for all 13612 data REM 682 parameters refined using 1 restraints END WGHT 0.0209 2.4161 REM Highest difference peak 0.650, deepest hole -0.522, 1-sigma level 0.057 Q1 1 0.7447 0.6230 0.6027 11.00000 0.05 0.65 Q2 1 0.6056 0.7589 0.5545 11.00000 0.05 0.48 Q3 1 0.2701 0.6200 0.2447 11.00000 0.05 0.36 Q4 1 0.2026 0.6038 0.5734 11.00000 0.05 0.35 Q5 1 -0.0443 0.5268 0.5942 11.00000 0.05 0.35 Q6 1 0.2848 0.6072 0.3156 11.00000 0.05 0.33 Q7 1 0.0526 0.6057 0.3139 11.00000 0.05 0.33 Q8 1 0.5364 0.6588 0.2049 11.00000 0.05 0.30 Q9 1 0.5615 0.6594 0.3559 11.00000 0.05 0.28 Q10 1 0.0176 0.5121 0.6317 11.00000 0.05 0.28 ; _shelx_res_checksum 96570 _shelx_hkl_file ; -2 0 0 4685.93 150.78 3 0 0 2.40 1.00 -3 0 0 2.60 4.00 -3 0 0 5.40 4.30 4 0 0 3312.07 102.99 -4 0 0 3202.48 110.09 -4 0 0 3179.08 109.39 5 0 0 2.20 1.60 -5 0 0 4.80 6.30 -5 0 0 2.30 6.70 6 0 0 9.70 2.20 -6 0 0 7.60 7.30 -6 0 0 -0.40 6.10 -7 0 0 12.20 7.30 -7 0 0 5.60 5.80 7 0 0 3.90 1.80 8 0 0 708.03 25.40 -8 0 0 682.23 38.80 -8 0 0 658.93 38.60 -9 0 0 -9.30 7.00 9 0 0 0.90 2.00 -9 0 0 -3.10 6.80 10 0 0 124.29 7.70 -10 0 0 97.59 20.60 -10 0 0 99.39 17.00 -11 0 0 -0.90 6.80 11 0 0 1.50 2.50 -11 0 0 9.80 12.80 12 0 0 -0.10 2.30 -12 0 0 -9.50 7.40 -12 0 0 12.60 10.90 13 0 0 4.30 2.70 -13 0 0 -5.20 13.30 -13 0 0 1.20 10.10 -14 0 0 273.67 42.40 -14 0 0 286.67 27.20 14 0 0 272.07 14.20 -15 0 0 6.50 10.40 -15 0 0 6.60 17.90 15 0 0 -0.60 2.80 -1 -1 0 916.91 28.80 -1 1 0 889.41 28.70 1 1 0 851.01 29.10 -1 1 0 993.60 31.90 2 1 0 63.89 2.50 2 1 0 69.59 3.30 -2 1 0 61.59 6.00 3 -1 0 356.36 12.30 3 1 0 363.46 12.90 -3 1 0 352.36 17.30 -3 -1 0 365.56 18.10 -3 -1 0 345.47 17.10 -4 -1 0 4142.69 142.39 -4 1 0 4383.46 141.59 -4 -1 0 4281.07 142.59 -4 1 0 4246.88 142.39 5 1 0 2029.60 64.69 5 -1 0 1955.90 64.09 -5 1 0 1922.01 71.69 -5 1 0 1971.00 73.69 -5 -1 0 1978.30 73.59 -5 -1 0 2039.90 73.29 6 1 0 352.36 14.10 -6 1 0 359.76 23.10 -6 -1 0 354.16 22.20 6 -1 0 365.16 13.80 -6 -1 0 333.37 22.80 -6 1 0 366.56 21.60 -7 -1 0 2.20 7.30 -7 -1 0 12.40 7.00 -7 1 0 16.80 7.30 -7 1 0 8.20 8.00 7 1 0 11.20 2.50 7 -1 0 9.90 2.20 8 -1 0 689.93 25.00 -8 -1 0 707.33 39.60 8 1 0 695.73 27.00 -8 1 0 644.64 38.20 -8 1 0 670.63 40.00 -8 -1 0 707.93 36.80 -9 1 0 79.49 14.20 9 -1 0 92.99 7.10 -9 1 0 111.39 19.30 9 1 0 87.19 6.30 -9 -1 0 101.39 16.00 -9 -1 0 117.29 20.20 -10 -1 0 47.60 12.90 -10 1 0 47.60 16.80 -10 1 0 35.40 10.70 10 -1 0 33.20 4.50 -10 -1 0 37.60 14.00 10 1 0 38.80 5.20 -11 -1 0 63.79 14.70 -11 1 0 64.09 14.20 -11 1 0 62.69 17.40 11 1 0 63.49 5.90 11 -1 0 58.69 5.40 -11 -1 0 65.79 19.00 -12 1 0 56.09 14.20 12 1 0 52.79 6.30 -12 -1 0 58.59 15.10 12 -1 0 48.40 5.30 -12 1 0 52.29 18.50 -12 -1 0 83.39 22.70 -13 -1 0 50.59 20.30 -13 -1 0 95.59 18.30 13 -1 0 80.99 6.90 13 1 0 93.89 7.60 -13 1 0 53.69 21.00 -13 1 0 93.29 20.40 14 1 0 55.49 7.40 -14 -1 0 61.79 23.40 -14 -1 0 74.79 16.70 -14 1 0 35.90 22.00 -14 1 0 80.39 17.90 14 -1 0 51.29 6.40 15 1 0 29.70 5.80 -15 -1 0 46.40 21.80 -15 -1 0 54.09 16.80 -15 1 0 41.30 22.60 -15 1 0 21.40 12.20 15 -1 0 44.20 6.20 0 -2 0 278.47 9.30 0 2 0 282.47 10.00 0 -2 0 283.27 9.30 0 -2 0 263.67 9.10 -1 -2 0 3.50 0.80 1 2 0 4.00 0.90 1 2 0 6.80 0.90 1 -2 0 4.70 0.50 -1 2 0 4.70 0.80 1 -2 0 4.30 0.60 -1 -2 0 4.80 1.80 1 -2 0 5.00 0.80 -1 -2 0 4.80 1.00 -1 -2 0 3.90 0.70 1 2 0 3.40 0.70 2 2 0 23.80 2.20 2 2 0 26.70 1.90 -2 -2 0 23.70 1.60 -2 -2 0 24.90 2.20 -2 -2 0 27.20 4.70 -2 -2 0 24.60 1.90 -2 2 0 27.30 1.60 -2 2 0 28.80 5.50 -2 2 0 25.30 4.30 2 2 0 23.20 1.60 2 -2 0 26.20 1.50 3 2 0 268.97 10.00 -3 -2 0 264.47 14.30 -3 -2 0 251.77 8.80 -3 2 0 244.88 13.20 -3 2 0 268.97 14.50 3 2 0 250.67 8.80 3 2 0 260.07 9.20 -3 -2 0 248.68 15.60 -4 2 0 5866.71 190.68 -4 -2 0 5908.11 193.58 -4 -2 0 6102.89 192.88 -4 2 0 5808.52 192.48 4 2 0 5606.64 184.68 -5 2 0 2341.07 86.99 -5 -2 0 2427.76 87.49 5 2 0 2375.46 77.99 -5 -2 0 2484.25 87.59 5 -2 0 2394.36 76.99 -5 2 0 2400.26 84.59 -6 2 0 36.00 10.20 6 -2 0 26.80 2.70 6 2 0 32.20 3.80 -6 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-2 82.09 8.90 3 -5 2 71.39 3.80 3 5 -2 74.29 4.50 -3 -5 -2 76.69 4.10 3 5 -2 72.59 4.70 -3 5 2 84.59 8.40 3 5 -2 67.69 3.90 3 5 2 84.29 5.00 3 5 2 78.09 4.50 -3 -5 2 84.89 4.40 -3 -5 2 92.19 8.40 -3 -5 2 100.29 12.30 -3 5 -2 93.99 3.90 -3 5 -2 97.39 8.20 3 -5 -2 91.89 4.40 -3 -5 2 82.09 5.30 3 -5 -2 90.09 4.20 3 5 2 81.89 4.30 -4 5 2 192.58 14.30 4 5 -2 194.18 8.60 -4 -5 -2 186.68 8.00 4 5 -2 191.38 8.00 -4 -5 -2 200.88 16.10 -4 -5 -2 211.58 9.40 -4 -5 -2 198.58 7.90 -4 -5 -2 186.58 20.30 4 -5 2 203.48 7.80 -4 5 2 199.68 12.30 4 5 -2 189.08 9.10 -4 5 2 201.28 7.90 -4 -5 2 208.58 14.60 -4 5 -2 215.98 14.10 4 -5 -2 212.48 8.20 4 5 2 196.28 8.40 -4 -5 2 202.28 18.20 -4 -5 2 213.58 8.30 -4 5 -2 222.48 20.50 4 5 2 212.28 9.50 4 5 2 192.28 8.20 -4 5 -2 209.98 8.20 4 -5 -2 205.38 8.70 5 5 -2 1864.11 61.59 -5 -5 -2 1881.31 73.39 5 -5 2 1931.11 59.89 5 5 -2 1911.01 61.09 -5 -5 -2 1801.62 76.49 -5 -5 -2 1968.20 63.09 -5 -5 -2 1889.51 60.99 -5 5 2 1863.31 67.29 -5 5 2 1924.81 60.69 5 -5 2 1848.22 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476.45 19.10 -1 -8 -4 498.15 18.80 -1 -8 -4 534.75 18.80 1 8 -4 502.15 18.70 -1 -8 -4 521.85 23.30 1 -8 -4 495.65 18.80 1 -8 -4 506.95 17.80 -1 8 -4 487.05 16.90 -1 8 -4 455.35 20.50 -1 -8 4 502.95 21.00 -1 8 -4 465.55 17.90 1 8 4 452.75 17.70 -1 -8 4 493.95 18.00 1 -8 -4 502.05 18.10 1 -8 -4 481.45 17.30 1 8 4 483.75 18.10 -1 8 -4 496.05 18.10 -1 -8 4 471.75 19.00 2 -8 4 2075.19 66.69 2 -8 4 1988.20 65.99 2 8 -4 1990.40 66.09 -2 -8 -4 1988.70 72.79 2 8 -4 2015.30 66.69 -2 8 4 2042.50 66.19 -2 -8 -4 1972.00 66.39 -2 8 4 2056.19 65.79 2 8 -4 2023.80 66.49 -2 -8 -4 2061.79 65.99 2 8 4 2003.20 66.39 -2 8 -4 2039.00 66.39 -2 -8 4 2137.29 66.69 -2 -8 4 2083.49 71.59 2 8 4 1951.50 66.69 2 8 4 2060.69 66.89 2 -8 -4 2132.29 65.79 2 -8 -4 1933.21 66.09 -2 -8 4 2153.38 68.19 -2 8 -4 2018.00 66.49 2 -8 -4 2009.10 65.89 -2 8 -4 1991.50 70.89 2 -8 -4 1990.10 66.49 -2 8 -4 2047.20 64.89 -3 -8 -4 314.37 20.20 3 -8 4 317.97 13.10 -3 -8 -4 268.17 24.70 3 8 -4 319.57 13.40 -3 -8 -4 318.87 12.60 -3 8 4 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22.10 -4 16 4 150.78 9.40 -4 16 4 136.99 8.50 4 16 -4 137.29 9.60 4 16 -4 132.19 9.40 -4 -16 -4 115.89 25.20 4 16 -4 139.19 9.70 4 -16 -4 149.19 9.10 -4 16 -4 143.29 8.10 -4 -16 4 130.29 10.40 -4 16 -4 144.39 9.20 4 16 4 143.99 8.90 4 16 4 126.59 9.30 4 16 4 133.69 9.40 -4 -16 4 144.29 15.40 4 -16 -4 133.39 7.10 -4 16 -4 123.49 5.60 -5 -16 -4 -4.60 6.90 -5 16 4 6.60 2.80 5 16 -4 5.30 3.10 -5 -16 -4 5.40 14.50 -5 -16 -4 7.30 3.10 5 16 -4 8.90 4.00 -5 16 4 3.10 3.40 5 16 -4 6.50 3.40 -5 16 -4 3.20 2.60 5 16 4 7.70 3.80 5 -16 -4 8.30 1.90 5 16 4 5.70 3.10 -5 -16 4 14.60 9.00 5 16 4 4.20 3.20 -5 -16 4 6.30 4.30 5 -16 -4 6.60 2.70 -5 -16 4 3.10 10.30 -6 -16 -4 613.34 25.10 -6 -16 -4 647.04 46.80 6 16 -4 602.64 25.40 6 16 -4 602.94 26.40 6 16 -4 620.54 25.40 -6 -16 -4 569.34 49.00 -6 16 4 623.14 24.90 6 -16 -4 612.24 23.60 -6 -16 4 514.35 34.90 6 16 4 601.54 24.50 6 -16 -4 556.74 20.70 6 16 4 615.94 23.70 -6 16 -4 581.24 23.60 -6 -16 4 530.65 43.00 -6 16 -4 506.35 29.30 -7 -16 -4 370.36 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841.52 29.70 -6 9 5 854.01 29.60 -6 -9 -5 819.42 29.60 -6 -9 5 931.81 46.50 -6 -9 5 865.31 42.60 -6 9 -5 847.32 40.70 6 9 5 913.21 31.70 -6 9 -5 916.11 31.60 6 9 5 928.41 33.60 6 9 5 923.81 32.30 6 -9 -5 924.21 31.60 7 -9 5 271.27 12.30 -7 -9 -5 274.37 14.80 -7 -9 -5 282.27 30.50 7 9 -5 266.77 13.90 -7 -9 -5 234.58 24.50 -7 9 5 276.57 11.60 -7 9 5 282.97 17.10 7 9 -5 273.57 11.90 7 9 -5 260.17 12.70 -7 -9 -5 267.97 10.80 -7 -9 5 271.27 24.70 7 -9 -5 295.57 11.90 7 9 5 279.47 13.90 7 9 5 293.17 12.80 7 9 5 300.07 12.30 7 -9 -5 286.77 11.90 -7 -9 5 292.77 23.30 -7 9 -5 264.67 20.90 -7 9 -5 278.47 11.80 8 9 -5 168.98 10.80 -8 9 5 161.28 13.70 -8 9 5 166.48 11.20 -8 -9 -5 175.38 28.80 8 9 -5 171.48 9.30 -8 9 5 171.58 17.70 8 -9 5 167.38 9.00 8 9 -5 151.38 8.30 -8 -9 -5 165.28 24.20 8 -9 -5 159.88 7.70 8 9 5 159.18 8.80 -8 9 -5 160.58 17.40 8 -9 -5 150.98 7.90 -8 9 -5 161.18 7.50 -8 -9 5 112.09 18.10 8 9 5 130.29 9.30 -8 -9 5 161.38 21.20 8 9 5 162.28 8.10 9 9 -5 66.09 8.00 -9 9 5 50.49 10.30 9 9 -5 51.39 5.70 9 -9 5 57.69 5.10 -9 -9 -5 88.69 19.80 -9 -9 -5 84.39 23.30 9 9 -5 56.79 5.00 -9 9 5 55.49 13.90 -9 -9 5 54.79 14.10 9 -9 -5 60.59 4.30 -9 -9 5 69.39 15.60 9 9 5 65.49 6.90 9 9 5 49.80 5.50 9 -9 -5 59.59 4.90 -9 9 -5 60.69 4.10 -9 9 -5 61.89 13.30 -10 -9 -5 142.79 26.80 10 9 -5 146.19 8.80 10 -9 5 141.09 8.40 -10 -9 -5 106.99 22.50 -10 9 5 150.88 26.20 -10 9 5 131.79 13.90 10 9 -5 141.09 11.80 10 -9 -5 163.08 8.00 10 9 5 168.48 15.30 10 -9 -5 160.98 8.70 10 -9 -5 144.79 7.40 -10 -9 5 146.19 23.00 -10 9 -5 165.18 22.20 -10 -9 5 173.68 20.00 -11 9 5 85.69 13.60 -11 9 5 74.89 17.80 11 -9 5 66.09 6.20 -11 -9 -5 41.40 19.50 -11 -9 -5 54.89 18.40 11 9 -5 62.39 8.00 11 9 -5 69.59 6.00 11 9 5 60.49 5.60 11 -9 -5 67.89 5.00 11 9 5 49.99 7.10 11 -9 -5 60.69 4.40 -11 9 -5 59.59 14.50 -11 -9 5 69.59 15.70 -11 -9 5 54.09 16.80 11 -9 -5 76.99 5.70 12 9 -5 115.09 7.50 -12 -9 -5 90.99 23.00 -12 -9 -5 93.09 26.60 12 -9 5 88.69 7.60 12 9 -5 110.99 10.00 -12 9 5 106.69 16.00 -12 9 5 147.39 26.20 12 9 5 104.89 9.40 -12 -9 5 123.49 19.80 -12 -9 5 64.09 19.10 -12 9 -5 108.09 19.50 12 -9 -5 116.59 7.40 12 -9 -5 112.89 9.00 12 -9 -5 100.09 6.00 13 9 -5 3.20 2.70 -13 -9 -5 -1.80 12.00 -13 9 5 -3.60 6.30 -13 9 5 10.10 16.50 -13 -9 -5 11.30 16.40 13 9 -5 5.90 4.00 -13 -9 5 1.40 8.60 -13 9 -5 3.30 10.00 13 9 5 6.40 3.40 13 -9 -5 4.40 2.20 -13 -9 5 18.60 16.10 -14 -9 -5 26.40 16.80 -14 -9 -5 -2.80 14.20 -14 9 5 4.30 8.30 -14 9 5 12.50 16.30 14 9 -5 7.30 3.10 14 -9 -5 4.40 2.40 14 9 5 4.70 4.00 -14 9 -5 11.60 11.30 -14 -9 5 5.00 9.20 -14 -9 5 21.40 18.20 0 -10 -5 344.77 14.10 0 10 5 330.47 14.00 0 10 5 324.67 13.30 0 -10 -5 335.57 13.50 0 10 -5 325.67 14.00 0 -10 -5 320.27 16.70 0 -10 -5 318.67 13.50 0 -10 5 336.47 15.00 0 -10 5 332.27 13.80 0 10 -5 342.67 13.90 0 10 -5 338.97 13.20 1 10 -5 1918.01 64.09 -1 -10 -5 1913.91 64.19 1 -10 5 2016.30 65.49 -1 10 5 1898.41 63.59 -1 -10 -5 1939.71 64.29 1 10 -5 1945.51 64.39 -1 -10 -5 1938.61 70.09 -1 -10 -5 1950.60 64.49 -1 10 5 1962.80 64.59 1 -10 -5 1889.11 64.79 -1 10 -5 1913.71 63.39 1 -10 -5 1911.61 63.49 -1 -10 5 1900.11 64.89 -1 10 -5 1835.42 63.29 1 -10 -5 1822.72 62.49 1 10 5 1994.00 63.29 -1 -10 5 1985.10 67.79 1 -10 -5 1920.11 62.99 -1 -10 5 1918.01 63.39 -1 10 -5 1906.81 61.99 1 10 5 1944.71 63.69 2 10 -5 360.86 15.30 2 10 -5 346.57 14.70 2 10 -5 361.46 14.80 -2 -10 -5 356.66 14.80 -2 10 5 365.66 14.20 2 -10 5 370.86 15.50 -2 -10 -5 368.66 21.10 -2 10 5 339.67 14.60 -2 -10 -5 340.77 14.50 -2 -10 5 366.66 19.50 -2 10 -5 366.36 15.20 2 -10 -5 370.86 14.30 -2 10 -5 347.37 18.80 2 -10 -5 373.36 14.50 2 -10 -5 384.86 14.80 2 10 5 361.06 15.30 -2 -10 5 384.76 16.80 -2 10 -5 397.16 15.10 2 10 5 381.06 16.60 -2 10 -5 376.26 13.40 2 -10 -5 388.56 15.30 -3 -10 -5 531.45 19.50 3 10 -5 465.35 19.70 3 10 -5 474.15 19.70 -3 -10 -5 538.15 28.20 -3 10 5 501.05 19.40 -3 10 5 517.65 19.40 -3 -10 -5 499.45 19.90 -3 -10 -5 489.15 19.00 3 10 -5 500.35 19.30 3 -10 5 514.25 20.10 -3 10 -5 481.85 17.70 3 -10 -5 483.55 17.70 3 10 5 447.06 18.30 3 10 5 454.55 18.50 -3 -10 5 485.75 20.00 -3 10 -5 454.25 15.60 -3 -10 5 467.05 23.80 -3 10 -5 457.65 18.00 3 -10 -5 457.45 18.00 -3 10 -5 455.45 23.20 3 -10 -5 500.95 17.10 -4 -10 -5 187.18 10.00 -4 10 5 186.48 10.20 4 -10 5 198.08 9.80 4 10 -5 176.08 9.20 -4 -10 -5 179.98 9.00 -4 -10 -5 216.48 18.20 -4 -10 -5 201.98 26.90 -4 10 5 196.08 9.40 4 10 -5 183.08 10.00 4 10 -5 186.58 9.90 -4 -10 -5 185.48 9.40 4 10 5 205.78 10.20 4 10 5 183.98 9.00 -4 -10 5 192.58 14.90 4 10 5 175.68 9.40 -4 10 -5 197.98 8.60 -4 10 -5 189.48 14.10 4 -10 -5 188.68 8.80 4 -10 -5 185.48 9.10 -4 10 -5 181.88 9.00 5 10 -5 33.30 4.10 -5 -10 -5 32.20 4.00 -5 -10 -5 39.00 11.10 5 -10 5 32.10 4.20 -5 -10 -5 44.40 4.50 -5 -10 -5 32.10 15.70 -5 -10 -5 36.60 5.10 5 10 -5 34.70 4.90 5 10 -5 33.80 4.80 5 -10 -5 31.10 4.10 -5 -10 5 35.90 9.40 -5 10 -5 26.40 7.50 5 -10 -5 34.10 3.20 5 10 5 24.80 3.70 5 -10 -5 37.20 5.00 -5 -10 5 48.70 13.30 5 10 5 28.90 4.40 -5 10 -5 35.00 2.90 5 10 5 31.50 3.80 -6 10 5 228.78 10.30 6 10 -5 223.38 12.10 -6 -10 -5 232.88 10.10 -6 -10 -5 213.88 22.00 -6 -10 -5 208.28 10.40 -6 -10 -5 259.77 29.40 -6 -10 -5 202.68 11.50 6 10 -5 230.68 11.50 6 10 -5 207.18 10.40 6 -10 5 222.88 10.90 6 10 5 221.48 10.80 6 -10 -5 218.18 10.00 6 -10 -5 227.78 9.80 6 10 5 209.38 11.50 -6 -10 5 264.87 23.90 -6 -10 5 210.58 19.00 -6 10 -5 187.18 16.50 6 10 5 227.48 10.30 -6 10 -5 209.68 9.90 7 10 -5 17.90 3.40 -7 -10 -5 17.60 3.00 7 -10 5 21.70 3.80 -7 10 5 23.70 7.10 -7 -10 -5 27.80 14.50 -7 10 5 16.60 3.20 -7 -10 -5 29.60 11.50 7 10 -5 16.10 4.40 7 10 -5 21.10 4.10 -7 10 -5 14.10 2.70 -7 -10 5 13.40 11.20 -7 -10 5 10.30 7.60 -7 10 -5 13.10 7.10 7 10 5 16.50 3.70 7 -10 -5 14.90 2.50 7 10 5 10.30 3.70 7 -10 -5 14.60 2.40 7 10 5 16.70 3.10 7 -10 -5 17.00 3.00 -8 -10 -5 79.99 18.00 8 10 -5 50.49 6.70 8 10 -5 64.79 6.50 8 -10 5 66.99 5.80 8 10 -5 65.99 5.40 -8 10 5 76.29 11.50 -8 -10 -5 66.39 20.90 -8 10 5 62.19 4.80 8 10 5 64.09 5.70 -8 10 -5 43.10 11.00 8 10 5 58.69 6.30 -8 10 -5 62.49 4.60 8 -10 -5 67.59 4.80 -8 -10 5 102.09 20.90 8 10 5 63.49 5.10 8 -10 -5 65.99 4.50 8 -10 -5 60.49 4.30 -8 -10 5 45.00 12.70 9 -10 5 235.38 11.70 -9 -10 -5 214.18 30.10 9 10 -5 227.88 11.00 9 10 -5 245.88 14.10 -9 10 5 245.78 10.30 -9 10 5 236.28 17.70 9 10 -5 241.48 12.10 -9 -10 -5 232.88 33.20 9 10 5 225.08 12.90 -9 -10 5 218.38 23.00 9 10 5 219.28 11.00 -9 10 -5 199.38 20.00 9 -10 -5 207.68 9.50 9 -10 -5 227.78 9.70 -9 -10 5 229.28 23.10 9 -10 -5 211.58 9.80 -9 10 -5 212.88 9.40 10 10 -5 329.77 14.20 10 -10 5 301.67 14.80 -10 -10 -5 364.06 35.30 10 10 -5 349.67 15.40 10 10 -5 331.57 17.70 -10 -10 -5 312.27 35.00 -10 10 5 372.06 22.80 -10 10 -5 283.97 27.40 10 -10 -5 326.77 13.20 10 10 5 310.57 14.40 10 10 5 340.77 17.10 10 -10 -5 327.87 13.50 10 -10 -5 333.57 13.60 -10 -10 5 354.56 28.30 -10 -10 5 305.27 29.90 -11 10 5 26.00 8.60 11 10 -5 21.40 5.80 11 10 -5 22.30 4.10 -11 -10 -5 21.70 18.00 11 -10 5 28.60 4.90 11 10 -5 26.50 3.80 -11 -10 -5 28.20 17.90 -11 10 -5 35.10 12.50 -11 -10 5 28.50 12.90 11 -10 -5 25.40 3.50 11 -10 -5 29.10 3.40 11 10 5 28.00 4.30 11 10 5 35.10 6.30 -11 -10 5 23.30 12.50 -12 10 5 15.40 8.20 -12 10 5 20.10 14.50 12 -10 5 15.20 3.80 -12 -10 -5 -5.70 12.70 12 10 -5 15.80 3.40 12 10 -5 14.10 4.90 -12 -10 -5 7.00 15.00 -12 -10 5 -5.10 11.30 -12 -10 5 8.70 8.50 12 10 5 15.40 4.80 12 10 5 14.40 3.10 -12 10 -5 8.20 9.80 12 -10 -5 8.30 2.30 12 -10 -5 11.70 4.00 12 -10 -5 18.20 2.80 13 10 -5 26.90 6.10 -13 -10 -5 44.60 17.10 -13 10 5 30.00 10.00 13 10 -5 32.70 4.90 -13 -10 -5 3.00 15.10 -13 -10 5 -2.30 12.00 13 10 5 18.20 5.10 -13 -10 5 42.00 13.20 -13 10 -5 23.60 10.60 13 -10 -5 20.60 3.60 0 11 -5 2061.49 69.09 0 -11 -5 2058.89 68.59 0 -11 5 2100.79 71.89 0 -11 -5 2134.99 73.09 0 -11 5 2169.88 70.59 0 11 5 2032.50 69.29 0 -11 -5 2071.59 68.79 0 11 -5 2068.69 68.19 0 11 -5 2111.19 69.09 0 -11 5 2122.99 68.99 0 11 5 1988.20 68.29 1 11 -5 428.66 17.30 1 11 -5 430.76 17.90 -1 -11 -5 430.06 17.50 -1 11 5 441.26 17.80 1 -11 5 462.55 18.80 1 -11 5 431.96 19.10 -1 -11 -5 442.36 17.60 -1 -11 -5 478.55 23.10 -1 11 5 465.45 17.10 1 -11 -5 442.96 18.10 1 -11 -5 462.55 19.60 1 11 5 448.86 18.20 1 -11 -5 423.16 17.40 -1 -11 5 461.45 19.30 -1 11 -5 439.46 17.90 -1 11 -5 447.46 16.60 1 11 5 472.85 17.80 -1 -11 5 466.05 17.90 -1 11 -5 480.15 18.20 1 -11 -5 425.76 17.00 -1 -11 5 474.05 21.70 2 11 -5 609.84 23.70 -2 -11 -5 644.54 23.40 -2 -11 -5 586.44 23.00 2 11 -5 609.14 23.60 2 -11 5 667.53 24.50 2 11 -5 610.34 23.40 -2 -11 -5 601.44 23.50 -2 11 5 640.94 22.70 -2 11 5 636.64 23.50 -2 -11 -5 611.84 30.20 -2 -11 5 579.44 27.40 -2 11 -5 622.64 22.80 -2 11 -5 563.04 22.20 2 -11 -5 613.14 22.30 -2 -11 5 599.24 22.60 2 -11 -5 615.24 21.60 2 11 5 586.64 22.50 -2 -11 5 640.04 24.50 -2 11 -5 569.74 26.00 2 11 5 588.14 22.90 2 -11 -5 605.44 22.60 -2 11 -5 595.04 20.60 2 -11 -5 606.34 22.20 -3 -11 -5 474.95 19.30 -3 11 5 457.95 18.60 -3 -11 -5 485.25 18.90 3 -11 5 468.85 19.50 -3 -11 -5 474.25 18.60 3 11 -5 470.35 18.80 3 11 -5 501.95 19.60 -3 11 5 468.55 18.50 -3 -11 -5 499.85 27.40 3 11 -5 467.25 19.20 3 11 5 439.26 18.00 -3 11 -5 467.25 17.30 -3 11 -5 422.66 15.00 3 -11 -5 455.15 16.50 3 -11 -5 434.46 17.60 -3 -11 5 463.25 24.20 -3 11 -5 417.66 22.20 3 -11 -5 452.55 17.40 3 11 5 423.96 17.90 -3 -11 5 470.35 19.60 -3 11 -5 465.75 17.80 -4 -11 -5 7.00 2.40 -4 11 5 12.70 3.10 4 -11 5 10.00 2.90 4 11 -5 9.20 3.10 -4 -11 -5 10.00 12.90 -4 -11 -5 17.10 8.20 4 11 -5 7.80 2.80 -4 -11 -5 9.50 2.70 -4 -11 -5 8.90 3.40 4 11 -5 9.80 3.00 -4 11 5 13.40 3.30 4 11 5 3.50 2.00 -4 -11 5 2.20 4.90 4 11 5 7.20 2.40 -4 -11 5 5.60 3.00 4 -11 -5 6.10 1.70 4 -11 -5 5.20 2.30 -4 11 -5 3.20 4.50 -4 11 -5 4.20 2.00 -4 11 -5 5.30 2.00 4 11 5 3.90 2.20 4 -11 -5 2.60 1.70 -5 -11 -5 79.99 6.70 5 -11 5 75.99 6.30 -5 -11 -5 89.49 6.10 -5 -11 -5 78.29 5.70 -5 -11 -5 72.39 13.50 5 11 -5 84.39 6.10 5 11 -5 90.49 7.20 5 11 -5 75.59 6.50 -5 -11 -5 92.99 22.40 -5 11 -5 95.59 6.30 -5 -11 5 78.59 12.60 5 11 5 82.79 6.40 5 -11 -5 87.69 6.00 5 -11 -5 90.69 5.70 -5 11 -5 77.09 11.40 5 11 5 88.49 6.00 5 -11 -5 98.59 5.70 5 11 5 83.99 6.60 -5 -11 5 105.39 18.00 -5 11 -5 95.29 5.10 6 11 -5 606.34 23.20 6 -11 5 576.44 22.80 -6 11 5 585.94 22.00 6 11 -5 599.14 24.20 -6 -11 -5 579.04 21.90 6 11 -5 579.44 22.30 -6 -11 -5 514.25 35.70 -6 -11 -5 537.85 42.80 -6 -11 5 500.05 35.10 6 11 5 510.05 20.00 6 -11 -5 522.25 19.90 -6 11 -5 462.55 28.00 -6 11 -5 519.45 20.00 -6 -11 5 482.55 30.40 6 11 5 557.84 22.10 6 -11 -5 523.35 19.60 6 11 5 529.25 20.70 7 11 -5 111.39 8.70 7 11 -5 112.19 8.00 7 -11 5 117.89 7.70 -7 -11 -5 112.69 20.50 -7 -11 -5 129.89 7.00 -7 -11 -5 110.79 26.20 -7 11 5 120.09 7.20 7 11 -5 114.59 7.40 7 11 5 124.49 7.50 7 11 5 121.69 9.00 7 -11 -5 129.29 7.10 7 -11 -5 137.19 8.60 -7 11 -5 130.99 7.30 -7 -11 5 120.69 18.50 7 11 5 116.49 7.80 -7 -11 5 149.39 23.40 7 -11 -5 120.99 6.80 -7 11 -5 98.99 15.10 8 -11 5 124.69 9.30 8 11 -5 130.49 8.00 -8 11 5 139.29 7.60 -8 11 5 126.49 12.50 8 11 -5 127.69 9.80 -8 -11 -5 177.88 31.90 8 11 -5 129.09 8.70 8 -11 -5 132.09 7.30 8 11 5 138.19 7.90 -8 -11 5 114.49 23.80 8 11 5 137.59 8.40 -8 11 -5 107.89 16.20 8 -11 -5 130.49 7.40 8 -11 -5 142.09 6.90 -8 -11 5 142.19 22.40 8 11 5 114.49 8.90 -8 11 -5 130.49 7.20 -9 -11 -5 16.40 15.20 9 11 -5 30.90 4.70 -9 11 5 25.80 8.20 -9 11 5 25.50 3.60 -9 -11 -5 8.50 12.60 9 -11 5 35.00 4.90 -9 11 -5 16.20 2.80 -9 -11 5 25.90 13.60 9 -11 -5 16.80 3.30 9 -11 -5 18.70 3.10 -9 11 -5 27.20 10.60 -9 -11 5 11.00 10.30 9 -11 -5 20.40 2.70 10 -11 5 197.28 10.90 -10 11 5 196.58 16.80 -10 -11 -5 167.78 30.20 10 11 -5 199.18 10.20 10 11 -5 193.68 12.70 10 11 -5 200.08 11.00 -10 -11 -5 213.08 35.20 -10 11 -5 197.18 20.90 10 -11 -5 207.38 8.80 10 -11 -5 198.68 9.10 10 -11 -5 201.28 10.00 -10 -11 5 203.98 23.30 -10 -11 5 138.19 23.80 10 11 5 183.48 10.50 10 -11 -5 196.88 8.80 10 11 5 189.98 12.60 11 -11 5 54.39 6.30 -11 -11 -5 42.70 17.80 -11 11 5 34.30 11.00 -11 -11 -5 41.70 19.10 11 11 -5 52.29 7.80 11 11 -5 54.09 6.30 11 11 -5 53.69 5.10 11 -11 -5 41.00 4.60 -11 -11 5 65.89 15.80 11 11 5 41.90 5.30 -11 -11 5 28.70 14.40 -11 11 -5 31.10 12.80 11 11 5 49.10 7.50 11 -11 -5 45.50 3.60 11 -11 -5 45.00 3.80 -12 -11 -5 84.49 22.90 12 11 -5 153.18 11.80 -12 -11 -5 123.59 28.00 12 11 -5 145.39 9.30 -12 11 5 143.19 15.70 12 -11 5 122.89 14.80 12 11 -5 144.09 8.00 -12 11 -5 150.98 22.80 12 11 5 118.79 7.80 12 11 5 117.59 10.10 12 -11 -5 134.59 6.60 -12 -11 5 143.39 21.30 12 -11 -5 123.09 6.60 -12 -11 5 110.79 25.70 12 -11 -5 126.29 7.40 -13 11 5 138.29 18.20 -13 -11 -5 104.49 26.60 13 11 -5 124.19 11.30 13 11 -5 127.59 8.60 -13 -11 -5 96.69 29.10 -13 -11 5 110.29 19.20 13 11 5 124.29 10.50 13 -11 -5 105.59 5.80 -13 11 -5 116.39 19.80 -13 -11 5 118.29 27.40 0 -12 5 1346.07 46.60 0 -12 -5 1320.47 46.40 0 12 5 1422.16 46.20 0 12 5 1360.56 47.10 0 -12 -5 1398.96 50.89 0 12 -5 1342.27 46.80 0 -12 -5 1343.87 46.20 0 12 -5 1294.27 46.60 0 -12 -5 1398.36 47.00 0 12 -5 1346.27 45.80 0 -12 5 1384.86 50.09 0 -12 5 1361.56 48.20 -1 12 5 337.77 15.40 1 -12 5 368.46 15.40 -1 -12 -5 364.86 15.30 -1 12 5 393.96 14.90 1 12 -5 357.56 14.90 -1 -12 -5 355.96 20.20 1 12 -5 371.86 15.80 1 -12 5 368.06 16.60 -1 12 -5 346.37 14.80 1 -12 -5 353.76 14.10 1 -12 -5 356.26 16.70 -1 -12 5 364.56 18.70 -1 12 -5 346.87 13.40 1 12 5 322.17 14.30 -1 12 -5 339.47 14.60 1 12 5 326.87 15.00 1 -12 -5 335.27 14.40 1 -12 -5 354.76 15.00 -1 -12 5 353.56 14.80 -2 -12 -5 55.69 4.80 2 -12 5 46.50 4.70 2 -12 5 56.19 5.50 2 12 -5 56.59 5.30 -2 -12 -5 72.19 12.40 -2 12 5 48.70 4.90 -2 -12 -5 52.89 4.80 -2 -12 -5 57.79 4.90 -2 12 5 63.39 4.70 2 12 -5 54.69 5.00 2 12 -5 52.09 4.80 -2 -12 5 56.79 8.90 2 -12 -5 56.99 4.20 -2 -12 5 46.30 4.70 2 12 5 61.09 5.40 2 -12 -5 51.79 4.80 -2 -12 5 47.00 6.00 2 -12 -5 48.50 4.30 -2 12 -5 49.10 3.40 -2 12 -5 51.49 4.70 2 12 5 46.20 4.50 -2 12 -5 54.59 5.00 -3 -12 -5 625.04 24.90 -3 -12 -5 600.34 22.90 3 12 -5 621.54 23.70 3 12 -5 585.34 23.40 -3 12 5 612.54 22.50 -3 12 5 590.74 23.10 -3 -12 -5 617.74 32.10 3 -12 5 575.24 23.70 -3 -12 -5 599.14 23.00 3 12 -5 572.14 23.00 3 -12 -5 625.64 22.30 3 -12 -5 632.34 23.60 3 12 5 600.54 23.90 -3 12 -5 637.74 29.00 -3 12 -5 645.14 23.90 -3 12 -5 673.63 23.40 -3 -12 5 620.04 30.60 3 -12 -5 629.94 23.40 3 12 5 596.04 23.90 -3 12 -5 604.24 20.80 -3 -12 5 608.94 25.50 4 -12 5 757.02 28.40 -4 -12 -5 709.13 45.70 4 12 -5 788.72 27.90 -4 12 5 714.33 27.40 -4 -12 -5 729.83 27.30 -4 -12 -5 736.23 27.50 4 12 -5 749.53 28.10 -4 12 5 740.43 28.10 -4 -12 -5 733.43 28.40 4 12 -5 733.13 28.30 -4 -12 -5 741.73 39.00 4 -12 -5 737.53 25.10 -4 12 -5 720.13 26.80 -4 -12 5 659.33 34.30 -4 12 -5 762.22 33.80 -4 -12 5 739.23 29.10 4 -12 -5 756.12 26.90 4 12 5 667.13 27.20 4 12 5 696.43 26.50 4 -12 -5 707.73 26.20 4 12 5 744.73 27.30 -5 -12 -5 642.04 38.20 -5 -12 -5 682.73 27.20 -5 12 5 699.53 27.60 5 12 -5 666.43 26.30 -5 -12 -5 721.93 25.80 5 12 -5 642.04 26.70 -5 12 5 689.43 26.20 -5 -12 -5 627.84 46.20 5 12 -5 707.83 26.00 -5 -12 -5 693.93 25.90 5 -12 -5 710.13 25.60 5 -12 -5 683.33 25.40 -5 -12 5 605.34 38.50 5 12 5 664.93 26.00 5 12 5 708.73 26.90 -5 -12 5 661.13 35.00 5 12 5 700.03 25.50 -5 12 -5 669.03 24.00 5 -12 -5 709.53 23.80 -5 12 -5 682.23 25.50 -5 12 -5 642.94 32.70 6 -12 5 167.28 10.20 -6 -12 -5 149.99 21.90 6 12 -5 167.38 10.60 6 12 -5 163.98 9.70 -6 -12 -5 189.98 31.70 -6 -12 -5 172.88 9.20 6 12 -5 162.68 9.30 -6 12 5 161.08 9.00 -6 -12 5 175.28 24.80 6 -12 -5 181.48 9.20 6 12 5 150.28 9.80 6 12 5 152.38 9.50 6 -12 -5 177.98 9.00 6 12 5 164.28 8.90 -6 12 -5 169.18 15.90 -6 -12 5 118.99 17.30 -7 12 5 28.70 4.00 7 12 -5 20.50 3.80 7 12 -5 18.10 4.40 -7 -12 -5 -1.80 13.80 7 -12 5 24.50 4.10 -7 -12 -5 27.00 12.30 -7 -12 -5 23.50 3.80 7 12 -5 25.90 4.50 7 12 5 25.80 4.30 -7 -12 5 39.50 15.60 -7 12 -5 13.10 7.00 -7 -12 5 4.90 8.50 7 -12 -5 21.60 3.50 7 12 5 17.90 3.50 7 12 5 17.80 4.30 -7 12 -5 16.50 3.30 -8 -12 -5 510.05 44.40 -8 12 5 535.85 20.40 -8 -12 -5 520.85 19.50 8 12 -5 499.85 20.70 8 12 -5 553.64 23.80 8 12 -5 525.95 21.70 -8 -12 -5 497.05 38.10 8 -12 5 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257.47 12.00 -10 -14 7 246.18 26.10 -10 14 -7 199.78 21.40 10 14 7 254.37 15.30 -11 -14 -7 2.20 16.20 11 14 -7 10.90 3.80 -11 -14 -7 14.20 17.20 11 14 -7 8.60 4.80 11 14 -7 8.00 3.40 -11 -14 7 11.90 11.80 -11 14 -7 17.60 9.60 11 14 7 16.30 4.50 11 -14 -7 16.00 3.20 11 -14 -7 13.20 2.30 11 14 7 16.60 5.50 -11 -14 7 26.20 12.70 -12 -14 -7 240.08 39.90 -12 -14 -7 252.67 42.40 12 14 -7 258.07 14.30 12 14 -7 275.47 17.40 -12 -14 7 222.48 24.30 -12 -14 7 227.08 33.50 12 14 7 211.08 12.90 -12 14 -7 240.58 24.60 0 -15 -7 1042.40 38.50 0 -15 -7 1084.79 44.40 0 15 -7 1075.59 39.10 0 15 7 1066.39 39.40 0 15 -7 1064.89 39.20 0 -15 -7 1052.59 38.90 0 15 -7 1063.29 37.50 0 15 7 1070.69 38.20 0 -15 7 1105.29 44.10 1 15 -7 1972.30 67.09 -1 15 7 2042.20 67.19 -1 -15 -7 1964.60 67.79 -1 15 7 2010.70 68.49 1 15 -7 2024.20 68.29 1 15 -7 2015.90 68.29 1 -15 7 1960.40 71.39 -1 -15 -7 1960.20 67.89 1 -15 -7 1942.91 68.99 1 -15 -7 1917.51 64.59 -1 -15 7 1850.71 71.49 -1 15 -7 1939.51 65.89 -1 15 -7 1940.01 63.59 1 15 7 1962.60 66.19 1 15 7 1884.91 64.89 1 -15 -7 1895.61 65.49 -1 15 -7 1921.41 65.49 -2 -15 -7 251.87 20.10 2 15 -7 225.18 12.50 2 15 -7 229.98 12.00 2 15 -7 236.48 12.70 -2 -15 -7 237.68 12.30 -2 -15 -7 221.38 12.20 -2 15 7 239.18 12.60 -2 15 7 247.08 11.90 2 15 7 224.58 11.80 2 -15 -7 231.08 12.10 -2 -15 7 206.78 16.90 2 -15 -7 245.28 13.80 2 15 7 223.18 12.50 2 -15 -7 232.18 11.00 -2 15 -7 228.98 11.70 -2 15 -7 235.28 10.00 -2 15 -7 234.58 12.40 3 15 -7 235.18 12.60 3 15 -7 250.17 12.80 -3 -15 -7 243.88 21.00 3 15 -7 237.98 13.00 -3 -15 -7 220.38 12.20 -3 15 7 234.48 12.10 -3 15 7 233.78 12.50 3 15 7 261.07 13.30 -3 15 -7 244.58 9.80 3 -15 -7 243.28 11.40 3 -15 -7 253.47 13.00 -3 -15 7 264.97 19.80 -3 -15 7 255.87 15.30 3 15 7 240.28 13.30 -3 15 -7 261.67 13.10 -3 15 -7 257.37 12.30 -4 -15 -7 65.69 6.40 -4 15 7 59.39 6.10 4 15 -7 70.19 7.90 -4 -15 -7 68.89 21.00 -4 -15 -7 70.79 15.70 4 15 -7 68.09 7.60 4 15 -7 63.99 6.70 -4 15 -7 66.49 11.90 4 -15 -7 82.29 5.50 4 -15 -7 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9.50 4.10 3 23 9 12.50 5.30 -3 -23 9 -8.10 6.90 -4 -23 -9 -12.00 17.60 -4 23 9 12.50 5.20 -4 -23 -9 -0.40 9.00 4 23 -9 11.10 4.80 4 23 -9 5.20 4.10 4 23 -9 -0.20 3.70 -4 23 9 0.60 2.60 4 -23 9 10.80 6.40 -4 23 -9 -0.30 2.60 4 23 9 4.20 4.30 4 23 9 11.70 4.60 -4 23 -9 2.50 3.10 -4 -23 9 12.50 10.10 -5 -23 -9 146.19 25.10 -5 23 9 160.28 13.00 5 23 -9 121.09 10.90 5 23 -9 127.09 11.40 5 -23 9 130.79 13.90 -5 -23 -9 72.29 30.60 5 23 -9 136.39 12.60 5 23 9 124.19 11.30 -5 -23 9 125.69 21.90 5 23 9 110.89 10.50 6 -23 9 77.49 11.10 6 23 -9 74.09 9.80 6 23 -9 78.19 11.60 -6 -23 -9 65.29 28.50 6 23 -9 79.99 9.70 -6 -23 -9 80.29 21.50 6 23 9 98.89 10.30 -6 -23 9 100.69 20.60 -6 -23 9 80.09 24.30 0 -24 -9 22.40 11.00 0 24 -9 27.70 5.60 0 24 -9 18.20 4.40 0 24 9 15.80 4.90 0 -24 9 25.40 9.80 0 24 -9 15.70 5.50 -1 24 9 110.89 11.20 -1 -24 -9 108.49 17.90 -1 24 9 96.29 9.60 1 24 -9 87.59 8.20 1 24 -9 92.89 10.10 1 24 -9 99.99 10.10 1 -24 9 98.79 16.10 -1 -24 9 102.89 18.00 -1 24 -9 91.29 7.40 -1 24 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6.00 -1 25 -9 26.70 7.20 -1 25 -9 22.80 4.30 2 25 -9 176.68 12.00 -2 25 9 162.38 12.60 -2 25 9 194.78 15.00 -2 -25 -9 200.78 25.40 2 25 -9 144.39 13.10 2 -25 9 183.58 18.40 2 25 -9 191.18 13.50 -2 25 -9 175.28 13.80 -2 25 -9 171.48 12.30 -2 -25 9 171.98 23.70 2 25 9 192.48 14.60 2 25 9 161.38 12.60 0 0 -10 24.90 3.30 0 0 -10 23.00 3.70 0 0 10 32.70 5.10 0 0 -10 34.50 7.90 0 0 10 31.70 3.60 1 0 10 1860.21 66.39 -1 0 10 2020.80 64.69 -1 0 -10 2041.90 73.19 -1 0 -10 2013.00 66.19 1 0 -10 1882.41 66.79 1 0 10 1981.60 64.79 -1 0 10 1973.70 69.19 1 0 -10 1968.40 69.19 1 0 -10 1970.40 64.89 -1 0 -10 2117.69 65.39 2 0 -10 92.79 7.80 2 0 10 84.69 5.60 -2 0 -10 89.19 5.80 2 0 10 76.69 5.90 -2 0 -10 110.89 15.90 -2 0 -10 88.99 5.50 -2 0 10 85.29 5.30 3 0 10 93.29 5.90 -3 0 -10 139.59 18.10 -3 0 -10 91.99 5.40 3 0 -10 93.29 8.40 -3 0 -10 114.29 20.80 -3 0 -10 92.89 5.90 -3 0 10 91.99 6.80 3 0 10 88.19 6.00 -3 0 10 91.79 5.60 3 0 -10 96.19 5.90 -4 0 -10 715.23 24.30 -4 0 -10 659.83 43.40 -4 0 -10 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57.89 9.40 -4 -1 -21 68.59 17.60 -4 1 21 52.09 6.20 4 1 -21 77.39 7.90 4 -1 21 70.29 7.30 4 1 21 64.99 7.10 -4 1 -21 66.69 16.20 4 -1 -21 78.49 8.40 4 1 21 59.09 9.30 -5 -1 -21 250.57 27.70 -5 1 21 289.07 18.00 -5 1 21 259.57 13.70 5 -1 21 246.28 16.60 5 1 -21 271.57 14.80 5 -1 21 295.57 14.60 5 1 21 275.17 17.10 5 1 21 292.67 14.90 -5 1 -21 302.27 17.70 -5 1 -21 240.08 26.20 5 -1 -21 278.57 14.90 -5 -1 21 267.27 18.30 -6 1 21 74.49 11.00 -6 -1 -21 63.79 8.90 6 -1 21 76.49 10.40 6 -1 21 51.09 7.00 6 1 -21 65.49 7.70 -6 -1 -21 55.29 15.40 -6 -1 21 58.69 11.00 6 1 21 80.59 10.20 6 1 21 80.59 9.30 6 -1 -21 58.69 7.60 -6 1 -21 73.59 9.10 -6 1 -21 101.19 21.40 7 1 -21 113.19 8.70 -7 -1 -21 102.99 9.10 7 -1 21 112.99 10.60 -7 1 21 111.99 14.90 -7 -1 -21 67.79 31.20 -7 -1 21 119.69 15.90 7 1 21 117.09 9.10 7 1 21 100.49 10.10 -7 1 -21 128.59 9.20 7 -1 -21 119.69 9.10 -8 -1 -21 170.58 8.40 -8 -1 -21 185.38 10.30 8 1 -21 155.58 10.60 8 -1 21 164.28 12.90 -8 1 21 176.48 16.50 -8 -1 -21 169.68 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5 10 22 13.80 6.00 -5 10 -22 3.40 4.00 5 10 22 1.20 2.90 -5 10 -22 13.80 8.50 5 -10 -22 12.90 4.20 5 -10 -22 3.10 10.90 -5 10 -22 10.60 3.10 -5 -10 22 -6.10 5.10 6 10 -22 1.90 3.40 -6 -10 -22 0.10 15.70 6 10 -22 8.10 5.70 6 10 -22 6.40 3.40 -6 10 22 -1.20 1.50 -6 -10 -22 -6.90 19.90 -6 10 -22 0.30 3.30 6 10 22 9.00 5.10 -6 -10 22 8.20 8.30 6 10 22 4.00 4.60 -6 10 -22 -7.90 7.60 6 -10 -22 32.30 13.40 -7 -10 -22 48.10 23.80 7 10 -22 72.59 10.40 7 10 -22 82.99 12.30 7 10 -22 56.49 8.40 -7 -10 -22 56.99 26.60 -7 10 -22 47.60 14.60 -7 10 -22 58.59 6.60 7 10 22 65.49 9.10 7 -10 -22 44.70 6.60 -7 10 -22 54.19 7.90 7 10 22 69.79 10.50 -7 -10 22 53.69 13.90 8 10 -22 135.79 10.70 8 10 -22 111.19 13.40 -8 -10 -22 163.18 34.10 -8 -10 -22 109.29 33.50 8 10 22 118.79 10.60 -8 10 -22 71.99 17.30 -8 -10 22 105.09 19.50 8 10 22 94.09 10.20 -8 10 -22 106.49 7.30 -9 -10 -22 81.09 33.80 9 10 -22 95.89 9.20 9 10 -22 83.89 11.70 -9 -10 -22 67.99 25.40 -9 -10 22 65.49 15.60 -9 10 -22 59.39 17.90 9 10 22 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2 -1 23 39.10 9.20 2 1 -23 43.70 6.40 2 1 -23 48.50 7.80 -2 1 23 28.50 5.10 2 -1 -23 40.80 6.00 2 1 23 31.20 8.50 2 -1 -23 49.90 9.60 -2 1 -23 35.10 10.90 -2 -1 23 45.30 6.20 2 1 23 36.80 6.20 3 -1 23 6.80 5.00 3 1 -23 -3.10 2.70 -3 -1 -23 19.10 12.80 3 -1 -23 0.90 2.50 3 1 23 -2.80 4.40 -3 1 -23 -4.70 8.40 3 1 23 -4.30 2.80 3 -1 -23 -0.80 5.00 -4 -1 -23 127.99 22.40 4 1 -23 98.79 9.30 4 -1 23 115.79 12.50 4 -1 23 105.99 9.20 -4 1 23 109.19 8.60 4 1 23 89.09 12.00 4 1 23 107.89 9.20 -4 1 -23 100.49 19.80 4 -1 -23 98.89 9.20 5 -1 23 494.85 27.50 -5 1 23 501.25 27.10 5 1 -23 549.45 24.10 -5 -1 -23 539.25 40.00 -5 1 23 546.25 22.80 5 -1 23 544.85 23.70 -5 -1 23 562.34 29.30 -5 1 -23 584.24 27.70 5 1 23 562.74 24.60 -5 1 -23 535.25 39.10 5 -1 -23 582.44 25.10 5 1 23 503.55 27.70 -6 -1 -23 168.18 39.80 6 -1 23 157.68 13.80 -6 -1 -23 171.88 13.80 6 1 -23 183.58 11.90 6 -1 23 151.78 11.00 -6 1 23 178.68 15.60 -6 1 -23 146.89 12.30 -6 1 -23 142.19 24.40 -6 -1 23 161.48 15.20 6 1 23 149.69 10.90 6 1 23 181.48 16.40 6 -1 -23 154.98 11.10 7 1 -23 70.79 8.30 7 -1 23 65.69 9.90 -7 -1 -23 66.59 8.60 -7 1 23 72.29 12.10 -7 -1 -23 58.19 19.80 7 -1 -23 81.79 8.10 7 1 23 80.99 8.40 -7 1 -23 75.89 18.40 7 1 23 66.39 11.80 -7 1 -23 68.49 8.30 -8 -1 -23 8.90 3.30 -8 -1 -23 6.90 12.30 8 -1 23 4.00 7.40 8 1 -23 11.70 4.20 -8 1 23 16.10 7.80 8 1 23 12.70 4.90 8 -1 -23 5.00 3.50 -8 -1 23 0.60 7.10 -8 1 -23 0.40 12.20 8 1 23 6.90 4.00 -8 1 -23 8.20 3.40 9 1 -23 77.19 8.40 9 -1 23 80.09 10.80 -9 -1 -23 83.59 22.80 -9 -1 23 114.99 17.40 9 -1 -23 89.09 8.50 9 1 23 90.19 11.60 -9 1 -23 66.99 20.80 9 1 23 87.09 8.50 10 -1 23 64.69 9.60 -10 1 23 72.09 15.30 -10 -1 -23 46.50 20.00 -10 1 -23 48.40 17.50 -10 -1 23 93.09 17.60 10 1 23 69.59 10.00 0 -2 -23 95.09 17.30 0 2 23 77.39 13.20 0 -2 -23 94.39 8.40 0 2 -23 88.19 8.30 0 2 -23 110.59 12.60 0 2 23 111.29 9.00 1 2 -23 281.97 16.80 -1 2 23 265.47 14.90 -1 -2 -23 287.07 15.90 1 -2 23 284.77 14.80 1 2 -23 294.47 18.10 -1 -2 -23 327.27 27.00 1 2 23 263.27 19.90 1 -2 -23 283.37 15.40 -1 2 -23 280.37 21.80 1 -2 -23 274.17 22.70 1 2 23 281.17 15.00 -2 -2 -23 196.58 26.10 -2 2 23 155.38 10.80 2 2 -23 146.99 10.60 2 2 -23 152.28 10.90 2 -2 23 163.78 10.70 2 -2 23 142.89 14.50 2 2 23 144.39 14.40 2 -2 -23 146.89 16.10 -2 2 -23 167.48 18.40 2 -2 -23 146.29 10.60 2 2 23 162.78 11.00 3 -2 23 143.69 14.20 -3 2 23 124.29 9.70 3 2 -23 132.29 10.20 3 -2 23 125.49 9.60 -3 -2 -23 160.98 24.30 3 2 23 118.29 9.80 -3 2 -23 122.89 19.50 3 2 23 114.29 12.20 3 -2 -23 109.39 9.30 3 -2 -23 146.19 13.40 4 -2 23 18.10 6.50 -4 -2 -23 14.20 14.00 -4 2 23 13.90 4.20 4 2 -23 13.30 4.30 -4 2 -23 7.20 9.20 4 -2 -23 11.50 6.90 4 2 23 10.60 3.80 4 2 23 12.00 5.40 -4 2 -23 6.70 5.70 4 -2 -23 14.70 4.20 5 2 -23 273.17 15.40 -5 -2 -23 246.98 28.30 -5 2 23 312.67 18.90 -5 2 23 274.97 14.40 5 -2 23 255.67 18.40 5 2 23 252.37 14.80 -5 -2 23 277.87 19.30 5 -2 -23 267.47 15.20 -5 2 -23 265.87 27.30 5 2 23 256.07 20.00 -5 2 -23 267.47 17.10 -6 2 23 108.39 8.30 -6 2 23 112.29 12.10 6 2 -23 93.99 9.10 6 -2 23 115.09 13.70 -6 2 -23 104.89 21.20 6 2 23 98.49 9.10 -6 2 -23 84.89 10.30 6 -2 -23 116.39 9.50 7 -2 23 -5.00 4.00 -7 2 23 9.40 6.70 -7 -2 -23 2.70 4.60 7 2 -23 6.60 3.80 -7 -2 -23 9.60 13.50 -7 2 -23 4.40 4.30 7 2 23 4.60 3.80 7 2 23 3.70 4.40 -7 -2 23 3.40 6.20 -7 2 -23 4.50 10.90 7 -2 -23 6.60 3.70 -8 -2 -23 112.39 8.00 -8 2 23 104.79 14.70 -8 -2 -23 96.79 24.50 -8 -2 -23 104.99 8.60 8 -2 23 108.09 11.40 8 2 -23 92.79 8.90 -8 2 -23 83.09 20.40 -8 2 -23 91.69 7.30 8 -2 -23 92.19 8.60 8 2 23 107.89 9.00 8 2 23 101.69 12.10 -8 -2 23 99.69 16.30 -9 2 23 8.60 7.90 9 2 -23 7.50 3.50 -9 -2 -23 2.40 13.30 -9 -2 23 9.80 8.50 9 2 23 10.30 4.70 9 2 23 2.30 3.70 -9 2 -23 6.90 12.00 9 -2 -23 4.60 3.20 -10 -2 -23 57.09 21.20 -10 2 23 133.99 26.40 10 -2 23 116.09 11.60 -10 -2 23 114.99 18.90 -10 2 -23 90.79 22.00 10 2 23 101.99 10.60 10 2 23 80.09 8.40 0 3 -23 811.92 37.20 0 3 -23 812.42 32.50 0 -3 -23 784.82 32.40 0 3 23 829.22 32.30 0 -3 -23 795.32 44.30 0 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-27 107.39 20.80 6 5 27 94.49 9.60 -6 5 -27 103.09 10.20 -7 5 27 100.99 13.70 -7 -5 -27 79.79 22.70 -7 -5 27 79.79 15.80 -7 5 -27 101.39 20.50 7 5 27 89.89 13.20 7 5 27 73.19 9.70 -7 5 -27 78.19 9.30 0 6 -27 300.07 21.00 0 6 27 271.57 16.70 0 -6 -27 289.17 30.00 0 6 27 270.57 23.00 -1 -6 -27 314.17 32.20 -1 6 27 311.07 17.40 1 6 -27 287.37 21.20 1 6 -27 305.17 16.10 -1 6 27 308.17 24.80 1 -6 -27 310.17 30.30 1 6 27 265.67 16.70 -1 6 -27 287.17 20.70 -1 6 -27 306.17 20.90 1 6 27 281.47 22.60 2 6 -27 25.50 8.50 -2 -6 -27 46.50 19.30 -2 6 27 25.80 5.70 -2 6 -27 39.40 11.00 2 -6 -27 63.69 17.10 2 6 27 40.70 7.10 -2 6 -27 18.30 8.00 2 6 27 42.30 9.80 3 6 -27 109.39 15.30 -3 -6 -27 115.79 40.10 3 6 -27 96.09 9.70 -3 6 27 100.29 9.80 -3 6 -27 97.49 12.40 -3 6 -27 103.09 16.40 3 -6 -27 123.99 20.10 3 6 27 121.89 16.00 3 6 27 104.09 10.60 3 -6 -27 114.49 10.20 -4 6 27 83.89 10.50 4 6 -27 58.49 8.20 4 6 -27 80.59 13.50 -4 6 27 76.39 9.00 -4 -6 -27 80.99 23.20 -4 6 -27 63.29 10.00 4 6 27 100.59 14.10 4 6 27 84.39 10.80 -4 -6 27 88.99 13.70 4 -6 -27 70.39 9.00 -4 6 -27 92.89 16.90 -5 6 27 30.00 7.30 -5 -6 -27 32.20 17.90 5 -6 -27 34.50 17.70 5 6 27 20.50 5.70 5 6 27 24.70 7.40 -5 6 -27 22.30 11.00 -5 6 -27 21.90 6.80 -5 -6 27 26.50 9.90 -6 -6 -27 10.10 15.20 -6 6 27 23.00 7.90 -6 -6 27 27.50 10.30 6 6 27 29.40 8.50 6 6 27 25.70 5.90 -6 6 -27 10.20 10.70 -6 6 -27 29.50 6.40 7 6 -27 49.80 11.70 -7 -6 -27 102.29 27.00 -7 6 -27 71.69 18.30 -7 6 -27 69.69 8.60 7 6 27 73.49 12.70 -7 -6 27 50.29 12.70 7 6 27 61.49 13.70 0 7 27 340.87 18.60 0 7 27 324.97 24.80 0 7 -27 318.37 21.90 0 -7 -27 361.56 34.90 1 7 -27 45.90 6.30 -1 -7 -27 59.89 19.00 1 7 -27 41.20 9.00 -1 7 27 46.70 8.00 -1 7 27 51.89 12.10 -1 7 -27 41.30 8.90 1 7 27 31.50 6.50 -1 7 -27 42.90 9.70 1 -7 -27 50.19 17.60 1 7 27 44.30 10.20 2 7 -27 21.40 8.10 -2 -7 -27 42.20 19.40 -2 7 27 18.70 5.70 -2 7 27 21.10 9.30 2 7 27 9.90 4.40 -2 7 -27 16.40 7.70 2 7 27 18.40 7.30 2 -7 -27 31.60 15.50 -2 7 -27 16.80 7.20 3 7 -27 26.20 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36.30 9.20 -3 11 -27 43.00 7.80 -3 -11 27 46.50 12.00 -3 11 -27 37.50 10.40 3 11 27 63.49 9.90 -4 -11 -27 222.08 39.10 4 11 -27 191.08 28.10 4 11 27 195.78 30.30 -4 -11 27 196.58 21.20 -4 11 -27 239.28 16.40 4 11 27 218.58 15.70 4 -11 -27 254.47 37.60 -4 11 -27 220.18 20.50 5 11 -27 89.19 10.70 -5 -11 -27 78.49 25.60 5 11 -27 76.89 12.20 5 11 27 82.19 10.20 5 11 27 92.79 13.60 5 -11 -27 130.99 24.90 -5 -11 27 68.39 15.70 -5 11 -27 79.39 15.90 -5 11 -27 110.29 10.50 0 -12 -27 13.10 18.30 0 12 -27 1.80 5.00 0 12 27 11.40 6.90 -1 12 27 65.99 8.90 1 12 -27 90.79 12.10 -1 -12 -27 88.49 28.20 -1 12 27 68.09 13.60 1 -12 -27 66.69 25.70 -1 12 -27 90.19 11.80 -1 12 -27 70.29 10.50 1 12 27 76.79 9.60 1 12 27 81.69 13.20 -2 -12 -27 26.10 22.50 -2 12 27 34.30 6.80 2 12 -27 46.10 15.30 -2 12 27 34.90 10.50 -2 12 -27 51.99 8.80 2 -12 -27 51.69 22.70 2 12 27 20.30 6.10 2 12 27 35.70 13.50 -2 12 -27 31.60 9.00 -3 -12 -27 149.19 34.10 -3 12 27 130.19 11.70 3 12 -27 124.89 14.80 -3 12 27 153.38 21.60 3 12 -27 154.88 12.70 -3 12 -27 142.79 18.00 -3 12 -27 129.29 12.00 3 12 27 150.48 12.80 3 -12 -27 134.89 29.60 3 12 27 122.29 18.40 -3 -12 27 98.69 17.00 -4 -12 -27 19.20 18.90 4 12 -27 33.30 8.40 4 12 -27 39.40 6.90 4 12 27 40.60 9.10 -4 12 -27 20.20 6.10 -4 12 -27 31.30 7.00 4 -12 -27 32.60 18.70 4 12 27 36.20 7.80 -4 -12 27 33.30 12.50 -4 12 -27 17.80 9.10 0 13 -27 150.98 24.50 0 13 -27 149.29 12.90 0 13 27 157.38 13.40 0 -13 -27 123.69 32.30 1 13 -27 33.70 7.00 -1 -13 -27 8.90 20.20 1 13 -27 22.00 9.30 -1 13 27 34.10 6.60 1 13 27 34.70 7.30 1 -13 -27 62.89 23.40 -1 13 -27 33.20 8.20 -1 13 -27 32.00 8.10 -1 13 -27 44.60 8.40 1 13 27 24.20 12.20 2 13 -27 26.20 6.50 2 13 -27 32.80 7.60 -2 -13 -27 -2.30 16.50 -2 13 27 15.30 5.30 2 13 27 23.40 6.10 -2 -13 27 14.90 7.40 -2 13 -27 19.70 5.90 2 13 27 17.40 7.50 -2 13 -27 19.20 6.80 2 -13 -27 24.90 19.60 -2 13 -27 24.10 8.00 -3 13 27 27.90 7.40 3 13 -27 35.20 6.70 -3 -13 -27 5.80 18.20 -3 13 27 34.10 16.60 3 13 -27 39.90 8.70 3 13 27 54.39 10.30 -3 13 -27 43.40 8.40 3 13 27 52.39 9.60 3 -13 -27 3.70 14.90 -3 13 -27 46.70 11.40 -3 -13 27 36.10 12.50 -3 13 -27 58.99 9.60 0 14 27 128.49 12.40 0 14 27 142.89 19.20 0 14 -27 110.39 12.70 0 -14 -27 102.79 29.90 0 14 -27 112.89 13.70 -1 14 27 88.29 15.10 -1 -14 -27 74.49 28.20 1 14 -27 86.59 12.20 1 14 -27 64.49 9.00 1 14 27 61.29 9.80 1 14 27 82.39 14.00 1 -14 -27 38.70 23.80 -1 14 -27 72.69 11.60 -1 14 -27 91.69 11.30 -2 14 27 12.60 7.50 2 14 -27 15.40 5.60 -2 -14 -27 23.50 19.80 2 14 -27 14.70 5.80 -2 14 27 17.70 7.10 -2 -14 27 15.20 9.00 2 14 27 24.10 6.70 2 14 27 30.00 8.10 2 -14 -27 10.80 20.50 -2 14 -27 25.80 8.00 0 0 28 1180.08 45.50 0 0 -28 1196.28 54.09 -1 0 -28 32.10 11.00 1 0 -28 40.10 9.60 -1 0 28 36.30 6.40 1 0 28 32.80 6.10 2 0 28 90.09 9.30 2 0 -28 84.19 10.90 -2 0 -28 58.49 15.10 3 0 28 10.70 5.90 -3 0 -28 39.30 12.80 3 0 28 11.70 4.00 3 0 -28 21.20 4.70 4 0 -28 202.58 19.20 4 0 28 207.38 14.20 -4 0 -28 249.68 48.60 4 0 28 203.78 19.30 -5 0 28 15.10 8.30 5 0 28 16.50 7.10 5 0 28 6.90 4.80 -5 0 -28 18.10 13.90 -5 0 -28 -1.90 6.20 -6 0 -28 21.30 13.80 6 0 28 -5.50 4.60 -6 0 -28 3.60 5.10 -6 0 28 5.20 7.10 -7 0 -28 8.80 12.90 -7 0 28 6.50 7.30 7 0 28 7.40 5.40 -7 0 -28 3.50 4.50 0 1 28 144.09 11.90 0 1 -28 168.98 16.10 0 -1 -28 165.78 18.60 1 1 -28 146.19 14.30 -1 1 28 133.99 11.10 -1 -1 -28 168.08 23.10 1 -1 -28 155.58 17.30 1 1 28 154.58 11.90 -1 1 -28 174.88 18.40 -2 -1 -28 64.89 16.20 -2 1 28 40.00 6.80 2 1 28 50.79 7.80 -2 1 -28 41.20 12.60 2 1 28 48.60 11.30 3 1 -28 3.40 3.20 -3 1 28 3.70 2.90 -3 -1 -28 4.40 11.90 3 1 28 3.50 5.90 -3 1 -28 -1.60 7.60 3 -1 -28 5.20 3.50 3 1 28 0.80 3.00 -4 -1 -28 53.19 21.20 4 -1 28 55.69 11.80 -4 1 -28 61.39 10.90 4 1 28 60.39 12.40 4 1 28 41.90 7.00 4 -1 -28 37.30 8.20 -4 1 -28 42.10 15.90 -5 1 28 217.98 18.20 -5 -1 -28 188.48 29.30 5 -1 28 223.78 19.40 -5 -1 -28 270.27 19.60 -5 -1 28 210.88 19.10 -5 1 -28 234.48 31.80 5 1 28 210.38 14.60 5 1 28 284.57 21.50 -5 1 -28 247.78 18.40 -6 -1 -28 -1.50 5.10 6 -1 28 17.00 6.80 -6 1 28 11.40 7.00 -6 -1 -28 0.40 11.20 -6 -1 28 4.70 7.40 -6 1 -28 -9.20 11.30 6 1 28 2.30 4.50 6 1 28 14.90 6.30 -6 1 -28 0.30 5.10 -7 -1 -28 32.90 7.70 -7 -1 -28 33.60 17.00 -7 1 28 34.00 10.80 7 -1 28 46.10 11.00 -7 1 -28 21.40 14.30 -7 1 -28 19.60 6.00 -7 -1 28 29.70 10.40 7 1 28 40.40 9.70 0 -2 -28 43.80 13.40 0 2 -28 33.30 9.20 1 2 -28 26.70 7.40 -1 2 28 23.90 6.60 -1 -2 -28 33.70 12.70 1 2 28 28.60 5.60 1 2 28 30.70 9.10 1 -2 -28 43.80 11.90 -1 2 -28 40.10 11.70 -2 2 28 2.60 3.60 -2 -2 -28 13.60 11.30 2 2 28 16.30 7.30 -2 2 -28 7.30 8.60 2 2 28 4.30 3.90 2 -2 -28 7.50 8.10 3 2 -28 83.49 10.30 -3 -2 -28 93.39 20.10 -3 2 28 73.69 9.10 -3 2 -28 79.59 12.70 -3 2 -28 88.69 17.20 3 2 28 61.99 12.90 3 -2 -28 61.59 8.20 3 2 28 80.79 9.20 4 2 -28 282.87 19.30 -4 2 28 275.87 16.00 -4 -2 -28 270.07 29.70 4 2 28 275.07 21.40 -4 -2 28 240.18 18.90 4 -2 -28 212.98 17.20 -4 2 -28 261.87 19.20 -4 2 -28 232.08 24.90 4 2 28 234.78 15.20 -5 2 28 297.97 20.50 -5 -2 -28 263.67 35.70 5 -2 28 265.37 22.20 -5 -2 28 258.87 21.10 5 2 28 252.67 20.30 -5 2 -28 252.47 18.20 5 2 28 233.48 15.50 -5 2 -28 228.58 26.90 -6 -2 -28 13.50 13.80 6 -2 28 26.40 8.50 -6 2 28 30.30 10.40 -6 -2 -28 29.60 7.90 -6 2 -28 32.40 7.00 6 2 28 39.90 9.60 6 2 28 17.80 5.00 -6 -2 28 34.40 10.00 -6 2 -28 22.90 14.90 -7 2 28 56.59 11.50 7 -2 28 38.70 8.80 -7 -2 -28 36.90 17.40 -7 -2 -28 38.90 8.30 -7 2 -28 30.60 6.60 -7 -2 28 44.20 12.20 -7 2 -28 24.00 14.40 7 2 28 53.19 10.80 7 2 28 33.30 9.80 0 3 -28 298.37 20.70 0 -3 -28 375.26 28.50 0 3 28 330.87 18.50 1 3 -28 152.18 12.40 -1 3 28 166.08 12.60 -1 -3 -28 189.88 26.10 -1 3 -28 156.58 16.70 1 -3 -28 182.08 19.00 1 3 28 161.88 12.50 1 3 28 151.78 20.00 -2 3 28 99.49 9.40 -2 -3 -28 140.99 23.00 -2 3 -28 112.59 18.00 2 3 28 94.59 10.00 2 3 28 118.79 17.00 -2 3 -28 109.29 14.50 -3 3 28 89.19 10.50 -3 -3 -28 90.79 21.50 -3 3 -28 98.49 13.30 -3 3 -28 83.49 16.80 3 3 28 102.99 11.50 3 -3 -28 59.99 8.10 3 3 28 85.99 14.20 3 -3 -28 91.59 12.80 -4 3 28 154.88 12.10 4 3 -28 183.28 12.90 -4 -3 -28 170.48 28.50 4 3 28 189.58 18.00 -4 3 -28 209.08 22.80 -4 -3 28 190.78 16.80 4 3 28 180.98 13.70 -4 3 -28 206.78 16.80 -5 3 28 443.86 25.50 -5 -3 -28 341.77 36.00 5 3 28 408.16 26.60 -5 3 -28 405.06 23.20 -5 -3 28 368.86 25.80 5 3 28 385.86 20.70 -5 3 -28 405.46 33.80 6 -3 28 38.20 9.90 -6 3 28 44.30 9.60 -6 -3 -28 46.10 18.10 -6 -3 28 39.20 11.00 -6 3 -28 32.60 13.70 6 3 28 40.80 6.60 6 3 28 42.50 10.50 -6 3 -28 48.90 8.60 -7 3 28 11.20 7.20 -7 -3 -28 6.70 12.60 7 -3 28 10.40 6.80 -7 -3 -28 3.10 5.50 -7 -3 28 11.10 8.70 7 3 28 6.70 5.00 -7 3 -28 -13.80 10.10 7 3 28 11.40 5.60 -7 3 -28 9.40 4.60 0 4 -28 725.53 34.80 0 4 28 744.03 32.00 0 4 28 730.93 41.70 0 -4 -28 770.72 45.10 -1 -4 -28 286.17 28.60 -1 4 28 272.57 16.20 1 4 -28 256.77 15.80 1 4 28 236.38 15.50 1 -4 -28 259.27 25.10 -1 4 -28 248.68 20.20 -1 4 -28 233.88 19.30 1 4 28 281.97 23.00 -2 4 28 66.19 8.60 -2 -4 -28 100.89 21.00 -2 4 -28 64.79 13.20 2 4 28 83.89 14.50 -2 4 -28 77.19 12.30 2 4 28 64.29 9.60 2 -4 -28 79.49 15.50 3 4 -28 58.69 8.20 -3 4 28 71.99 8.30 -3 -4 -28 58.09 20.20 3 -4 -28 57.29 8.30 3 -4 -28 92.09 14.20 3 4 28 83.59 13.50 3 4 28 77.29 9.00 -3 4 -28 56.19 14.50 -3 4 -28 80.09 12.00 4 4 -28 169.88 13.70 -4 -4 -28 248.28 35.10 -4 4 28 226.68 14.20 4 4 28 219.38 15.00 -4 -4 28 199.18 17.90 -4 4 -28 231.68 17.40 4 4 28 216.78 19.30 -4 4 -28 240.28 23.30 -5 -4 -28 118.29 25.70 -5 4 28 139.79 13.90 -5 4 -28 135.59 13.00 -5 4 -28 145.39 23.40 5 4 28 121.49 15.80 -5 -4 28 96.79 15.30 5 4 28 106.79 10.70 -6 -4 -28 62.29 19.70 -6 4 28 74.99 12.40 6 4 28 62.89 10.60 -6 4 -28 56.99 16.80 -6 -4 28 64.49 13.80 -6 4 -28 56.89 9.00 6 4 28 67.99 9.20 -7 -4 -28 24.80 17.00 -7 4 28 22.70 8.80 -7 -4 -28 19.90 7.10 7 4 28 18.70 6.20 7 4 28 21.60 5.50 -7 4 -28 16.10 12.40 -7 4 -28 12.70 4.80 -7 -4 28 16.80 9.10 0 5 -28 209.48 18.20 0 5 28 184.88 19.20 0 5 -28 181.08 26.30 0 5 28 166.18 12.80 0 -5 -28 196.28 28.20 1 5 -28 33.50 9.40 1 5 -28 42.40 6.90 -1 -5 -28 49.10 17.90 -1 5 28 25.60 6.40 1 -5 -28 26.80 14.10 -1 5 -28 39.60 9.90 1 5 28 57.89 12.20 1 5 28 36.20 8.10 -1 5 -28 31.90 9.20 -2 5 28 63.99 8.30 -2 -5 -28 96.19 21.30 2 5 28 86.59 10.00 -2 5 -28 76.49 12.00 2 5 28 69.69 13.40 -2 5 -28 99.49 15.40 2 -5 -28 81.79 16.80 -3 5 28 26.00 6.50 -3 -5 -28 23.30 15.60 -3 5 -28 29.10 11.10 3 -5 -28 26.50 11.70 3 5 28 26.90 8.90 3 -5 -28 28.20 6.10 -3 5 -28 36.80 8.00 -4 5 28 463.65 22.50 -4 -5 -28 411.36 39.40 -4 5 28 444.26 23.80 4 5 28 441.66 28.10 -4 -5 28 429.56 27.50 -4 5 -28 460.25 24.70 4 5 28 455.35 22.50 -4 5 -28 468.15 32.90 4 -5 -28 391.86 27.50 -5 5 28 0.30 2.10 -5 5 28 11.40 6.20 -5 -5 -28 0.50 13.50 5 5 28 -0.50 3.60 5 5 28 14.50 6.60 -5 -5 28 5.00 6.90 -5 5 -28 1.70 10.10 -5 5 -28 19.50 6.10 -6 -5 -28 14.20 16.30 -6 5 28 26.40 8.00 -6 5 -28 9.00 5.10 6 5 28 7.30 3.90 -6 -5 28 19.80 9.10 6 5 28 18.10 7.40 -6 5 -28 10.70 11.90 -7 -5 -28 33.10 18.10 -7 5 28 14.40 7.90 -7 5 -28 25.30 13.50 -7 -5 28 16.00 8.70 7 5 28 41.60 9.40 7 5 28 32.20 6.30 0 6 -28 27.40 8.40 0 6 28 27.20 6.30 0 -6 -28 41.50 15.40 0 6 28 26.70 9.50 -1 6 28 47.40 13.10 -1 6 28 54.59 8.80 -1 -6 -28 49.10 16.70 1 6 -28 49.60 10.20 1 6 -28 58.79 11.50 1 -6 -28 44.70 13.60 1 6 28 62.99 13.70 -1 6 -28 31.30 8.80 -1 6 -28 64.49 11.80 2 6 -28 55.99 11.10 -2 6 28 64.19 9.30 -2 -6 -28 73.89 20.70 2 6 28 54.69 11.10 -2 6 -28 52.89 9.90 2 6 28 40.60 7.00 -2 6 -28 40.40 11.00 2 -6 -28 66.59 17.00 -3 6 28 4.20 4.00 3 6 -28 16.40 8.20 -3 -6 -28 18.60 15.70 3 6 28 10.50 5.10 3 -6 -28 -8.80 8.90 3 6 28 5.60 6.20 -3 6 -28 11.60 6.20 3 -6 -28 10.10 4.50 -3 6 -28 13.50 8.60 -4 -6 -28 73.29 22.10 -4 6 28 87.59 11.00 -4 6 28 97.09 11.70 4 6 -28 91.69 14.80 -4 6 -28 100.89 24.30 -4 6 -28 84.19 11.40 4 6 28 82.79 10.50 4 6 28 80.59 13.00 -4 -6 28 82.09 14.20 -5 6 28 155.08 13.50 5 6 -28 120.79 15.60 -5 -6 -28 113.99 26.60 -5 6 -28 155.28 23.20 -5 6 -28 143.99 13.00 -5 -6 28 122.99 17.30 5 6 28 158.78 15.80 5 6 28 121.79 11.80 -6 -6 -28 84.39 24.20 -6 6 28 94.79 12.70 6 6 -28 94.39 17.10 -6 6 -28 95.29 18.90 -6 -6 28 89.99 16.20 6 6 28 66.79 8.60 6 6 28 97.49 14.20 -6 6 -28 123.69 11.20 0 7 28 64.19 8.60 0 7 28 55.29 13.10 0 -7 -28 76.99 20.40 0 7 -28 78.69 12.60 1 7 -28 170.28 16.70 -1 -7 -28 175.78 29.00 -1 7 28 146.39 19.70 -1 7 28 147.49 12.30 -1 7 -28 158.98 15.50 -1 7 -28 146.09 14.20 1 7 28 187.78 18.90 1 -7 -28 176.08 27.50 -2 -7 -28 12.80 19.60 -2 7 28 16.40 5.50 2 7 -28 14.00 7.40 2 7 28 15.30 5.00 -2 7 -28 15.80 8.60 2 -7 -28 1.70 11.40 2 7 28 15.80 7.40 -2 7 -28 16.70 6.90 -3 -7 -28 31.50 18.30 3 7 -28 19.20 8.00 -3 7 28 27.00 5.90 3 7 28 53.89 11.70 3 -7 -28 57.09 17.90 3 7 28 43.40 8.20 3 -7 -28 36.10 11.00 -3 7 -28 50.99 12.50 -3 7 -28 38.90 8.60 -4 -7 -28 134.69 28.10 -4 7 28 172.48 13.20 4 7 -28 132.49 17.40 -4 -7 28 166.48 17.60 -4 7 -28 198.08 15.30 4 7 28 146.49 13.10 4 7 28 203.48 17.70 4 -7 -28 202.18 25.60 -5 -7 -28 277.27 39.70 -5 7 28 276.57 17.60 5 7 -28 239.88 21.20 -5 7 -28 272.27 25.60 -5 7 -28 259.77 17.40 5 7 28 259.87 16.50 5 7 28 255.47 20.70 -5 -7 28 247.78 22.60 -6 7 28 10.00 5.30 6 7 -28 33.30 15.80 -6 -7 -28 44.90 19.30 -6 7 -28 38.90 13.40 6 7 28 29.00 6.10 -6 7 -28 35.80 7.20 -6 -7 28 38.90 12.00 0 8 -28 496.75 25.90 0 8 -28 549.35 29.60 0 8 28 530.95 34.00 0 -8 -28 586.84 45.30 0 8 28 526.25 25.60 -1 -8 -28 202.88 32.50 -1 8 28 182.88 19.50 -1 8 28 163.28 13.30 1 8 -28 212.78 17.70 -1 8 -28 188.08 16.10 1 -8 -28 201.58 30.50 -1 8 -28 177.18 15.40 1 8 28 178.38 13.60 1 8 28 164.18 17.80 -2 8 28 7.30 4.90 -2 8 28 16.00 8.40 -2 -8 -28 24.50 17.10 2 8 -28 16.00 7.90 2 -8 -28 19.30 13.30 2 8 28 10.20 6.60 -2 8 -28 23.00 8.10 -2 8 -28 6.40 6.10 2 8 28 10.30 4.10 -3 8 28 122.99 11.00 3 8 -28 96.79 13.70 -3 -8 -28 88.69 23.80 3 -8 -28 102.29 21.20 3 8 28 92.09 11.30 3 8 28 115.19 15.30 -3 8 -28 104.29 12.40 -3 8 -28 103.79 16.00 -4 8 28 233.38 15.50 4 8 -28 231.38 19.50 -4 -8 -28 247.08 38.20 4 8 28 231.88 19.50 4 -8 -28 223.18 29.20 4 8 28 203.28 14.70 -4 8 -28 183.68 20.00 -4 8 -28 193.68 15.30 -4 -8 28 218.68 20.00 -5 -8 -28 101.79 27.40 5 8 28 98.09 21.20 -5 -8 28 61.79 14.10 5 -8 -28 135.79 21.40 -5 8 -28 91.09 10.90 -5 8 -28 106.49 19.30 5 8 28 69.09 9.30 -6 -8 -28 18.00 17.70 6 8 -28 17.50 8.10 -6 8 -28 9.10 9.40 6 8 28 28.70 8.80 -6 -8 28 15.20 8.60 -6 8 -28 13.70 4.90 0 9 28 262.87 16.90 0 9 -28 288.27 20.30 0 9 28 294.47 23.50 0 9 -28 243.78 15.90 0 -9 -28 264.37 37.20 -1 -9 -28 57.79 23.40 1 9 -28 44.90 9.50 -1 9 28 43.80 11.90 -1 9 28 49.90 7.40 1 9 28 68.99 12.60 -1 9 -28 59.59 10.40 1 9 28 39.10 7.10 1 -9 -28 55.39 20.50 -1 9 -28 52.99 10.10 -2 9 28 13.10 5.00 2 9 -28 22.30 8.00 -2 -9 -28 18.30 16.90 -2 9 28 9.80 7.20 2 9 28 22.90 7.90 2 -9 -28 -8.30 13.10 2 9 28 16.00 5.80 -2 9 -28 20.90 8.30 -2 9 -28 10.20 6.00 -3 -9 -28 62.09 20.60 3 9 -28 78.99 12.90 -3 9 28 67.29 9.60 -3 9 -28 62.59 9.70 3 9 28 60.29 8.40 -3 9 -28 80.49 13.60 3 -9 -28 114.79 23.30 -3 -9 28 68.09 13.40 3 9 28 60.99 11.80 4 9 28 210.88 15.70 4 -9 -28 250.67 32.70 -4 9 -28 238.08 16.80 4 9 28 273.57 35.80 -4 -9 28 224.58 21.40 -4 9 -28 229.68 21.60 5 9 -28 137.89 17.00 -5 -9 -28 169.08 34.50 -5 9 -28 140.99 12.30 5 -9 -28 131.29 23.10 -5 -9 28 109.39 18.70 5 9 28 136.09 12.60 -5 9 -28 143.49 20.70 5 9 28 155.38 15.30 0 10 28 202.98 19.40 0 10 -28 164.58 12.80 0 10 -28 236.88 18.00 0 -10 -28 217.68 35.70 -1 10 28 94.29 11.40 -1 10 28 82.39 14.90 -1 -10 -28 83.79 24.80 1 10 -28 74.49 11.70 1 10 28 110.49 12.70 1 10 28 108.89 16.60 -1 10 -28 99.69 12.90 -1 10 -28 95.39 12.20 1 -10 -28 126.69 27.00 -2 10 28 26.00 9.10 -2 -10 -28 4.40 15.20 -2 10 28 16.40 5.70 2 10 -28 23.50 7.10 2 -10 -28 21.90 16.30 2 10 28 11.40 4.90 -2 10 -28 13.40 7.40 2 10 28 12.60 6.10 -2 10 -28 8.20 5.10 -3 -10 -28 95.09 26.50 -3 10 28 130.09 11.60 3 -10 -28 143.19 28.10 3 10 28 94.79 11.90 -3 -10 28 104.89 16.80 -3 10 -28 134.69 15.60 -3 10 -28 148.69 13.10 -4 -10 -28 110.89 30.80 4 10 -28 88.59 13.00 -4 10 -28 117.39 18.30 4 -10 -28 118.09 24.20 4 10 28 100.99 12.00 4 10 28 121.49 16.30 -4 -10 28 85.19 15.90 -4 10 -28 100.99 12.20 -5 -10 -28 15.60 20.40 5 10 -28 12.80 7.50 5 -10 -28 36.70 17.30 -5 -10 28 27.30 11.10 5 10 28 20.10 7.40 -5 10 -28 25.30 10.20 -5 10 -28 7.80 5.20 5 10 28 11.90 5.10 0 -11 -28 85.39 25.80 0 11 -28 75.09 12.70 0 11 28 104.89 22.70 0 11 28 61.19 8.50 -1 11 28 95.29 11.80 -1 11 28 88.99 18.60 -1 -11 -28 108.39 29.10 -1 11 -28 70.09 10.50 1 -11 -28 65.09 23.00 -1 11 -28 77.09 10.90 1 11 28 87.49 11.30 2 11 -28 87.99 14.20 -2 -11 -28 115.39 30.40 -2 11 28 156.58 33.50 -2 11 28 78.59 10.10 -2 11 -28 91.49 13.70 -2 11 -28 101.59 12.10 2 11 28 79.99 10.10 2 -11 -28 74.19 26.20 2 11 28 84.59 16.30 3 11 -28 74.29 11.80 -3 -11 -28 77.49 27.10 -3 11 28 84.29 11.00 3 11 28 71.29 10.40 -3 -11 28 78.09 15.20 3 -11 -28 78.69 21.90 -3 11 -28 82.09 10.80 -3 11 -28 83.69 14.00 3 11 28 70.79 12.90 -4 -11 -28 69.89 25.70 4 11 -28 101.19 13.60 -4 11 -28 69.89 10.10 -4 11 -28 61.59 13.20 4 11 28 74.09 12.30 4 11 28 88.59 11.50 -4 -11 28 55.49 13.70 4 -11 -28 86.49 21.30 0 -12 -28 131.19 30.30 0 12 28 100.29 16.50 0 12 28 98.39 11.20 0 12 -28 87.59 16.40 -1 -12 -28 108.79 29.40 1 12 -28 109.69 13.60 -1 12 28 124.69 12.10 -1 12 28 125.99 18.30 1 12 28 131.09 17.60 1 -12 -28 101.99 27.60 1 12 28 115.79 13.60 -1 12 -28 88.29 10.30 -2 12 28 33.70 10.30 2 12 -28 34.70 9.00 -2 12 28 28.30 6.40 -2 -12 -28 35.60 25.10 2 12 28 38.80 8.10 -2 12 -28 43.60 8.70 -2 12 -28 38.50 8.80 2 12 28 62.09 12.20 2 -12 -28 75.79 25.00 -3 -12 -28 164.18 35.30 -3 12 28 135.79 20.40 3 12 -28 135.09 12.10 3 12 -28 112.29 13.80 3 12 28 128.09 16.70 -3 12 -28 136.09 12.40 -3 12 -28 118.69 16.50 3 12 28 127.69 12.40 3 -12 -28 120.29 28.80 -3 -12 28 91.69 16.20 0 13 -28 362.06 22.60 0 13 28 328.97 20.60 0 -13 -28 344.07 47.80 0 13 28 362.96 27.10 0 13 -28 354.36 20.40 1 13 -28 91.39 12.90 -1 -13 -28 115.09 29.60 -1 13 28 135.99 19.60 1 13 -28 128.49 11.60 -1 13 -28 146.59 13.50 -1 13 -28 110.89 12.90 1 -13 -28 194.88 36.90 1 13 28 132.09 13.00 1 13 28 125.99 17.40 -2 13 28 204.58 21.40 2 13 28 217.68 19.90 0 0 29 4.40 4.50 0 0 -29 15.40 8.10 -1 0 -29 0.50 7.60 2 0 29 12.00 5.20 -2 0 -29 -2.40 7.90 -3 0 -29 10.50 11.20 3 0 29 32.00 9.70 3 0 29 11.30 4.70 4 0 29 173.58 18.50 -4 0 29 190.18 16.50 4 0 29 177.08 13.10 -4 0 -29 205.08 28.90 -5 0 29 236.58 19.10 5 0 29 203.88 19.50 -5 0 -29 197.38 18.00 -5 0 -29 214.38 29.90 -6 0 -29 2.10 5.30 6 0 29 0.80 5.40 -6 0 -29 12.10 13.80 -6 0 29 15.40 8.70 0 1 -29 190.68 18.20 0 -1 -29 173.78 19.30 0 1 29 170.48 13.10 -1 1 29 45.30 7.50 1 1 -29 45.40 9.50 -1 -1 -29 68.59 14.60 1 -1 -29 44.20 11.10 -1 1 -29 59.99 13.40 -2 -1 -29 34.10 12.40 -2 1 -29 4.80 8.50 2 -1 -29 19.30 7.20 2 1 29 19.80 7.70 2 1 29 23.90 6.20 -3 -1 -29 21.00 12.80 3 -1 -29 22.80 6.00 3 1 29 31.30 6.20 3 1 29 38.30 10.00 -3 1 -29 47.20 14.30 4 -1 29 98.09 15.50 -4 -1 -29 102.79 21.30 4 1 29 59.59 8.60 -4 -1 29 88.49 13.10 -4 1 -29 75.49 12.20 -4 1 -29 110.99 22.10 4 1 29 97.19 14.90 -5 -1 -29 190.48 29.90 -5 -1 -29 169.18 16.90 -5 1 29 184.48 17.20 5 -1 29 170.48 18.00 5 1 29 152.38 12.60 -5 1 -29 157.78 15.90 -5 1 -29 161.68 25.80 5 1 29 181.28 18.30 -5 -1 29 182.88 17.50 -6 -1 -29 61.39 10.40 6 -1 29 73.09 13.20 -6 1 29 71.49 13.00 -6 -1 -29 54.49 19.10 6 1 29 65.49 8.90 -6 1 -29 58.69 18.70 -6 1 -29 72.49 10.70 -6 -1 29 67.09 13.50 6 1 29 71.79 13.10 0 -2 -29 629.04 37.30 0 2 29 542.55 26.20 0 2 -29 565.24 31.00 1 2 -29 124.59 12.50 -1 2 29 131.39 11.10 -1 -2 -29 167.18 23.50 -1 2 -29 127.99 18.00 1 -2 -29 142.19 18.80 -2 2 29 49.99 7.50 -2 -2 -29 86.19 18.90 2 2 29 52.39 7.50 -2 2 -29 68.29 14.90 2 -2 -29 53.99 11.00 2 2 29 46.50 11.80 -3 -2 -29 21.00 12.30 -3 2 29 6.00 4.20 -3 2 -29 -8.50 7.50 -3 2 -29 9.10 6.40 3 2 29 8.40 6.90 3 2 29 3.30 4.20 -4 -2 -29 157.78 27.30 -4 2 29 98.39 9.70 4 2 29 119.99 17.90 -4 2 -29 132.89 15.70 -4 -2 29 147.19 14.90 -4 2 -29 119.19 21.50 4 2 29 129.69 11.90 5 -2 29 93.89 14.90 -5 2 29 103.39 14.10 -5 -2 -29 133.19 26.80 -5 -2 29 115.09 16.90 5 2 29 120.19 16.80 -5 2 -29 117.39 21.90 -5 2 -29 113.59 13.90 5 2 29 133.79 11.50 -6 -2 -29 38.10 8.60 -6 -2 -29 42.00 17.40 -6 2 29 69.29 12.20 6 -2 29 68.29 12.50 -6 2 -29 62.39 17.80 -6 -2 29 33.70 11.00 6 2 29 47.30 10.70 6 2 29 44.50 7.20 -6 2 -29 47.90 8.70 0 -3 -29 144.49 22.20 0 3 29 102.29 11.80 0 3 -29 104.09 13.60 -1 3 29 273.07 15.60 -1 -3 -29 240.88 26.10 1 3 -29 205.48 14.90 1 -3 -29 239.68 22.60 1 3 29 213.78 21.20 -1 3 -29 250.87 20.50 1 3 29 268.97 20.00 -2 -3 -29 186.78 27.90 -2 3 29 173.28 12.50 2 -3 -29 173.58 27.50 2 3 29 191.38 19.50 2 3 29 173.68 13.30 -2 3 -29 162.78 17.50 -2 3 -29 200.58 17.50 -3 3 29 23.40 5.90 3 3 29 51.49 11.50 3 3 29 28.70 6.40 -3 3 -29 25.10 8.10 -3 3 -29 41.70 12.80 -4 -3 -29 46.90 18.10 -4 3 29 29.10 6.20 -4 3 29 36.80 7.80 -4 3 -29 51.49 14.70 -4 -3 29 33.50 9.30 -4 3 -29 13.00 7.00 4 3 29 34.90 9.60 4 3 29 29.90 6.90 -5 3 29 39.60 9.90 -5 -3 -29 15.00 15.30 5 3 29 45.80 7.50 5 3 29 59.29 11.20 -5 3 -29 47.00 14.80 -5 -3 29 39.50 10.70 -5 3 -29 61.29 10.10 -6 -3 -29 43.60 9.90 -6 3 29 75.69 12.00 -6 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-30 15.50 7.40 -1 -10 -30 38.50 18.20 1 10 30 37.10 11.10 -1 10 -30 29.40 7.90 1 -10 -30 32.60 17.20 0 0 -31 2.10 7.50 1 0 -31 12.40 8.00 -1 0 -31 6.90 9.10 -2 0 -31 -2.40 8.30 -3 0 -31 40.50 14.60 4 0 31 51.09 12.20 -4 0 -31 87.19 13.90 -4 0 31 77.29 12.60 -4 0 -31 47.60 16.30 0 1 -31 99.49 14.50 0 -1 -31 102.59 17.10 0 1 31 88.49 9.90 -1 1 31 17.20 5.30 -1 -1 -31 47.50 12.80 1 -1 -31 59.19 10.80 -1 1 -31 54.29 12.00 1 1 31 33.80 6.20 -2 -1 -31 44.20 13.70 -2 1 -31 29.00 11.50 2 1 31 16.50 5.10 -3 -1 -31 65.79 17.80 -3 1 -31 67.09 20.40 3 1 31 39.50 7.30 -3 1 -31 38.30 10.40 3 1 31 32.60 11.00 -4 1 31 13.10 6.70 -4 -1 -31 15.60 13.70 -4 -1 31 2.70 6.80 -4 1 -31 15.80 10.80 -4 1 -31 7.00 7.40 4 1 31 5.30 4.20 4 1 31 18.90 9.30 0 2 -31 12.30 7.50 0 2 31 12.50 5.70 0 -2 -31 23.90 10.70 -1 -2 -31 40.80 14.20 -1 2 31 32.80 6.40 -1 2 -31 42.50 11.40 1 2 31 27.80 6.40 1 -2 -31 40.60 11.30 -2 2 31 412.86 21.70 -2 -2 -31 425.96 32.90 2 2 31 397.66 21.30 -2 2 -31 387.86 29.10 -2 2 -31 431.76 27.20 -3 -2 -31 27.30 13.90 3 2 31 10.40 5.80 -3 2 -31 13.20 8.60 3 2 31 18.40 6.60 -4 2 31 59.69 11.50 -4 -2 -31 64.89 17.20 -4 2 -31 22.40 11.90 -4 -2 31 50.29 10.70 4 2 31 77.59 15.90 -4 2 -31 48.50 10.30 4 2 31 55.99 9.10 0 3 -31 -1.20 5.40 0 3 31 2.40 3.90 0 -3 -31 14.40 9.90 -1 3 31 152.98 12.40 -1 -3 -31 148.19 23.00 1 3 31 148.39 12.50 1 -3 -31 189.48 22.80 -1 3 -31 163.78 16.70 -1 3 -31 126.09 17.00 -2 -3 -31 41.30 20.60 2 3 31 11.10 8.40 -2 3 -31 24.30 9.40 2 3 31 4.00 4.30 2 -3 -31 12.70 10.00 -2 3 -31 4.90 8.20 -3 -3 -31 33.00 13.60 -3 3 31 33.30 6.10 -3 3 -31 32.50 9.10 3 3 31 28.10 14.40 -3 3 -31 47.10 15.40 3 3 31 35.10 7.80 -4 -3 -31 29.70 16.60 -4 3 31 15.70 7.10 -4 3 -31 12.40 7.20 4 3 31 5.00 5.00 -4 -3 31 8.80 7.00 -4 3 -31 8.70 9.00 0 4 -31 36.70 7.80 0 -4 -31 36.80 13.00 0 4 31 29.10 6.30 1 4 -31 9.40 9.30 -1 4 31 13.50 5.70 -1 -4 -31 3.20 10.60 -1 4 -31 10.80 6.80 1 -4 -31 22.80 10.40 -1 4 -31 17.10 9.60 1 4 31 9.80 4.80 -2 4 31 14.90 6.00 -2 -4 -31 25.50 14.30 -2 4 -31 8.90 8.40 -2 4 -31 29.60 8.40 2 -4 -31 24.90 10.30 2 4 31 12.70 5.00 -3 -4 -31 35.10 16.90 -3 4 31 27.30 5.70 -3 4 -31 26.40 12.40 3 4 31 25.20 6.50 -3 4 -31 37.20 8.70 3 4 31 15.80 9.00 4 4 31 22.00 9.30 0 5 31 12.90 5.20 0 5 -31 16.30 7.90 0 5 -31 7.10 9.60 0 -5 -31 47.40 14.30 -1 5 31 85.79 14.20 -1 -5 -31 87.09 19.40 1 5 -31 76.39 13.20 -1 5 -31 54.89 11.40 1 -5 -31 86.69 17.10 1 5 31 46.80 12.20 1 5 31 49.99 8.70 -2 5 31 32.30 7.10 -2 -5 -31 46.60 14.50 2 5 -31 37.30 10.10 2 -5 -31 40.80 13.20 2 5 31 26.30 9.70 -2 5 -31 28.20 9.40 -2 5 -31 33.30 10.60 2 5 31 35.50 6.70 3 5 -31 63.39 12.50 -3 5 31 47.50 7.40 -3 -5 -31 65.19 20.60 -3 5 -31 44.70 13.70 3 5 31 59.29 9.50 3 5 31 84.69 15.20 -3 5 -31 94.09 12.50 0 6 31 298.37 19.00 0 6 31 378.76 29.20 0 6 -31 309.57 23.70 0 -6 -31 369.06 32.80 -1 -6 -31 57.79 19.80 1 6 -31 75.59 13.00 1 -6 -31 108.59 20.20 1 6 31 111.39 13.10 -1 6 -31 87.79 13.00 -1 6 -31 74.69 14.40 1 6 31 138.39 20.10 2 6 -31 216.58 19.50 -2 6 31 177.98 14.00 -2 -6 -31 165.48 29.20 2 6 31 141.79 13.00 2 6 31 204.38 21.60 2 -6 -31 220.18 23.40 -2 6 -31 151.88 16.60 -3 -6 -31 56.09 18.10 3 -6 -31 8.70 13.60 3 6 31 10.50 7.20 0 7 31 10.00 7.80 0 7 -31 17.10 9.40 0 -7 -31 40.50 14.10 0 7 31 17.10 6.00 1 7 -31 72.69 12.60 -1 -7 -31 59.99 17.70 -1 7 31 69.89 10.40 1 7 31 63.99 13.60 -1 7 -31 96.69 13.00 -1 7 -31 78.59 12.60 1 7 31 72.39 9.50 1 -7 -31 80.09 18.40 -2 -7 -31 74.99 20.60 2 7 -31 51.19 11.80 -2 7 31 62.69 9.60 -2 7 -31 39.50 10.70 2 -7 -31 100.69 19.80 2 7 31 70.69 10.40 2 7 31 69.89 14.40 -2 7 -31 64.59 11.40 0 8 31 28.80 10.90 0 0 -32 79.89 14.00 -1 0 -32 6.60 8.60 -2 0 -32 172.88 23.60 0 1 -32 6.30 8.10 0 -1 -32 9.60 8.80 -1 -1 -32 143.89 21.30 -1 1 -32 97.89 17.00 1 -1 -32 152.08 26.80 1 1 32 107.69 10.70 -2 -1 -32 17.00 11.20 2 1 32 24.20 6.30 -2 1 -32 20.80 10.10 0 2 -32 3.60 7.00 0 -2 -32 17.10 9.90 0 2 32 10.00 5.30 -1 2 32 16.70 5.10 -1 -2 -32 17.20 9.00 -1 2 -32 13.70 8.70 1 2 32 3.60 4.60 1 -2 -32 2.90 8.10 -2 2 32 22.80 6.00 2 2 32 19.40 6.50 -2 2 -32 17.60 8.30 -2 2 -32 44.10 12.20 0 3 -32 31.40 10.30 0 3 32 46.30 8.70 0 -3 -32 52.39 13.80 -1 3 32 60.29 8.70 -1 -3 -32 72.69 15.70 -1 3 -32 72.49 13.10 1 3 32 59.29 9.10 1 -3 -32 87.29 15.60 -1 3 -32 75.49 13.50 -2 -3 -32 38.50 13.40 -2 3 -32 30.90 9.30 2 3 32 29.90 10.30 -2 3 -32 37.80 10.60 0 4 -32 195.68 19.10 0 4 32 156.18 13.30 0 -4 -32 186.68 24.90 -1 -4 -32 -8.50 9.20 1 4 -32 -13.50 6.10 -1 4 32 -1.20 4.30 -1 4 -32 -0.10 6.30 1 -4 -32 17.60 10.40 -1 4 -32 7.60 7.10 1 4 32 -1.60 4.10 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 13563 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pd1 Pd 0.28105(2) 0.61351(2) 0.28054(2) 0.01006(4) Uani 1 1 d . . . . . Cl1 Cl 0.31683(6) 0.72486(3) 0.30069(3) 0.01847(14) Uani 1 1 d . . . . . Cl2 Cl 0.24802(6) 0.50306(3) 0.25489(3) 0.01730(13) Uani 1 1 d . . . . . Fe1 Fe 0.51315(3) 0.60156(2) 0.42531(2) 0.01253(8) Uani 1 1 d . . . . . Fe2 Fe 0.04058(3) 0.62993(2) 0.14167(2) 0.01166(8) Uani 1 1 d . . . . . P1 P 0.48627(5) 0.60241(3) 0.28265(3) 0.01104(12) Uani 1 1 d . . . . . P2 P 0.07535(5) 0.62682(3) 0.28237(3) 0.01096(12) Uani 1 1 d . . . . . O1 O 0.45047(18) 0.40939(10) 0.41323(9) 0.0196(4) Uani 1 1 d . . . . . O2 O 0.08794(19) 0.81767(10) 0.15492(9) 0.0204(4) Uani 1 1 d . . . . . N1 N 0.6685(2) 0.45695(12) 0.51198(10) 0.0186(5) Uani 1 1 d . . . . . N2 N 0.6626(2) 0.36284(12) 0.46207(10) 0.0175(5) Uani 1 1 d . . . . . N3 N -0.0360(2) 0.79672(12) 0.02413(10) 0.0202(5) Uani 1 1 d . . . . . N4 N -0.1184(2) 0.85550(12) 0.09191(10) 0.0174(5) Uani 1 1 d . . . . . C1 C 0.4529(2) 0.51379(13) 0.45890(11) 0.0149(5) Uani 1 1 d . . . . . C2 C 0.3622(2) 0.54520(14) 0.42649(13) 0.0170(6) Uani 1 1 d . . . . . H2 H 0.323601 0.525868 0.395764 0.020 Uiso 1 1 calc R U . . . C3 C 0.3410(2) 0.61035(15) 0.44881(12) 0.0200(6) Uani 1 1 d . . . . . H3 H 0.285884 0.642318 0.435341 0.024 Uiso 1 1 calc R U . . . C4 C 0.4162(2) 0.61961(14) 0.49464(12) 0.0191(6) Uani 1 1 d . . . . . H4 H 0.419253 0.658649 0.517196 0.023 Uiso 1 1 calc R U . . . C5 C 0.4861(3) 0.56061(13) 0.50106(12) 0.0181(6) Uani 1 1 d . . . . . H5 H 0.544364 0.553441 0.528331 0.022 Uiso 1 1 calc R U . . . C6 C 0.5597(2) 0.62314(12) 0.34613(11) 0.0129(5) Uani 1 1 d . . . . . C7 C 0.5485(3) 0.68384(13) 0.37795(11) 0.0153(5) Uani 1 1 d . . . . . H7 H 0.495925 0.720060 0.370727 0.018 Uiso 1 1 calc R U . . . C8 C 0.6298(3) 0.68023(14) 0.42215(12) 0.0182(6) Uani 1 1 d . . . . . H8 H 0.641190 0.713777 0.449438 0.022 Uiso 1 1 calc R U . . . C9 C 0.6909(2) 0.61782(14) 0.41844(12) 0.0172(5) Uani 1 1 d . . . . . H9 H 0.750111 0.602403 0.442864 0.021 Uiso 1 1 calc R U . . . C10 C 0.6481(2) 0.58239(14) 0.37182(12) 0.0153(5) Uani 1 1 d . . . . . H10 H 0.673781 0.539211 0.359790 0.018 Uiso 1 1 calc R U . . . C11 C 0.5476(2) 0.66078(12) 0.23268(11) 0.0126(5) Uani 1 1 d . . . . . C12 C 0.6176(2) 0.71552(13) 0.24714(12) 0.0165(5) Uani 1 1 d . . . . . H12 H 0.638911 0.722409 0.284333 0.020 Uiso 1 1 calc R U . . . C13 C 0.6563(3) 0.76012(14) 0.20713(13) 0.0204(6) Uani 1 1 d . . . . . H13 H 0.702758 0.797964 0.217340 0.024 Uiso 1 1 calc R U . . . C14 C 0.6283(3) 0.75022(14) 0.15273(13) 0.0207(6) Uani 1 1 d . . . . . H14 H 0.655785 0.780866 0.125690 0.025 Uiso 1 1 calc R U . . . C15 C 0.5594(3) 0.69505(14) 0.13766(13) 0.0194(6) Uani 1 1 d . . . . . H15 H 0.540881 0.687567 0.100229 0.023 Uiso 1 1 calc R U . . . C16 C 0.5180(2) 0.65108(13) 0.17747(12) 0.0166(5) Uani 1 1 d . . . . . H16 H 0.469226 0.614202 0.167279 0.020 Uiso 1 1 calc R U . . . C17 C 0.5541(2) 0.52152(12) 0.26624(11) 0.0127(5) Uani 1 1 d . . . . . C18 C 0.5129(2) 0.46333(13) 0.29253(11) 0.0148(5) Uani 1 1 d . . . . . H18 H 0.445460 0.465692 0.315440 0.018 Uiso 1 1 calc R U . . . C19 C 0.5705(2) 0.40209(13) 0.28511(13) 0.0189(6) Uani 1 1 d . . . . . H19 H 0.542248 0.362604 0.302846 0.023 Uiso 1 1 calc R U . . . C20 C 0.6692(3) 0.39853(14) 0.25189(13) 0.0209(6) Uani 1 1 d . . . . . H20 H 0.708335 0.356602 0.246820 0.025 Uiso 1 1 calc R U . . . C21 C 0.7109(3) 0.45609(13) 0.22607(13) 0.0202(6) Uani 1 1 d . . . . . H21 H 0.778628 0.453656 0.203401 0.024 Uiso 1 1 calc R U . . . C22 C 0.6534(2) 0.51734(14) 0.23337(12) 0.0161(6) Uani 1 1 d . . . . . H22 H 0.682351 0.556712 0.215710 0.019 Uiso 1 1 calc R U . . . C23 C 0.5011(3) 0.44637(13) 0.44577(12) 0.0157(5) Uani 1 1 d . . . . . C24 C 0.6105(3) 0.42385(13) 0.47305(12) 0.0159(5) Uani 1 1 d . . . . . C25 C 0.7596(3) 0.41566(14) 0.52614(12) 0.0203(6) Uani 1 1 d . . . . . H25 H 0.816692 0.425835 0.553308 0.024 Uiso 1 1 calc R U . . . C26 C 0.7574(2) 0.35767(15) 0.49585(12) 0.0202(6) Uani 1 1 d . . . . . H26 H 0.811170 0.321071 0.497956 0.024 Uiso 1 1 calc R U . . . C27 C 0.6282(3) 0.31150(15) 0.42222(14) 0.0266(7) Uani 1 1 d . . . . . H27A H 0.682081 0.273019 0.424643 0.040 Uiso 1 1 calc R U . . . H27B H 0.631451 0.330698 0.385273 0.040 Uiso 1 1 calc R U . . . H27C H 0.547824 0.296360 0.430017 0.040 Uiso 1 1 calc R U . . . C31 C 0.1055(2) 0.71589(14) 0.10573(12) 0.0150(5) Uani 1 1 d . . . . . C32 C 0.1929(2) 0.68492(13) 0.14078(12) 0.0149(5) Uani 1 1 d . . . . . H32 H 0.229845 0.705253 0.171538 0.018 Uiso 1 1 calc R U . . . C33 C 0.2135(2) 0.61869(14) 0.12083(11) 0.0166(5) Uani 1 1 d . . . . . H33 H 0.266998 0.586958 0.135977 0.020 Uiso 1 1 calc R U . . . C34 C 0.1406(2) 0.60769(14) 0.07439(12) 0.0177(5) Uani 1 1 d . . . . . H34 H 0.137363 0.567510 0.053189 0.021 Uiso 1 1 calc R U . . . C35 C 0.0732(2) 0.66716(13) 0.06508(12) 0.0160(5) Uani 1 1 d . . . . . H35 H 0.016685 0.673432 0.036869 0.019 Uiso 1 1 calc R U . . . C36 C -0.0054(2) 0.60766(13) 0.22068(11) 0.0133(5) Uani 1 1 d . . . . . C37 C 0.0008(3) 0.54756(13) 0.18787(11) 0.0153(5) Uani 1 1 d . . . . . H37 H 0.050926 0.510000 0.194267 0.018 Uiso 1 1 calc R U . . . C38 C -0.0810(2) 0.55403(13) 0.14417(12) 0.0173(6) Uani 1 1 d . . . . . H38 H -0.095344 0.521454 0.116416 0.021 Uiso 1 1 calc R U . . . C39 C -0.1377(2) 0.61790(15) 0.14924(12) 0.0178(5) Uani 1 1 d . . . . . H39 H -0.196103 0.635330 0.125255 0.021 Uiso 1 1 calc R U . . . C40 C -0.0925(2) 0.65089(14) 0.19599(12) 0.0149(5) Uani 1 1 d . . . . . H40 H -0.115437 0.694160 0.208922 0.018 Uiso 1 1 calc R U . . . C41 C 0.0164(2) 0.57049(13) 0.33411(11) 0.0135(5) Uani 1 1 d . . . . . C42 C 0.0605(3) 0.57681(16) 0.38718(13) 0.0219(6) Uani 1 1 d . . . . . H42 H 0.118816 0.609827 0.394866 0.026 Uiso 1 1 calc R U . . . C43 C 0.0198(3) 0.53517(17) 0.42889(14) 0.0296(7) Uani 1 1 d . . . . . H43 H 0.050123 0.539708 0.464935 0.035 Uiso 1 1 calc R U . . . C44 C -0.0652(3) 0.48707(16) 0.41769(15) 0.0301(8) Uani 1 1 d . . . . . H44 H -0.093635 0.458747 0.446161 0.036 Uiso 1 1 calc R U . . . C45 C -0.1087(3) 0.48020(14) 0.36534(15) 0.0253(7) Uani 1 1 d . . . . . H45 H -0.166176 0.446602 0.357904 0.030 Uiso 1 1 calc R U . . . C46 C -0.0695(2) 0.52191(13) 0.32312(13) 0.0179(6) Uani 1 1 d . . . . . H46 H -0.100909 0.517340 0.287269 0.022 Uiso 1 1 calc R U . . . C47 C 0.0127(2) 0.70877(13) 0.30012(11) 0.0128(5) Uani 1 1 d . . . . . C48 C -0.0798(3) 0.71453(14) 0.33750(13) 0.0181(6) Uani 1 1 d . . . . . H48 H -0.107177 0.675873 0.356670 0.022 Uiso 1 1 calc R U . . . C49 C -0.1317(3) 0.77742(15) 0.34651(14) 0.0245(7) Uani 1 1 d . . . . . H49 H -0.194167 0.781592 0.372094 0.029 Uiso 1 1 calc R U . . . C50 C -0.0924(3) 0.83395(15) 0.31825(14) 0.0261(7) Uani 1 1 d . . . . . H50 H -0.127939 0.876650 0.324576 0.031 Uiso 1 1 calc R U . . . C51 C -0.0018(3) 0.82814(13) 0.28103(13) 0.0206(6) Uani 1 1 d . . . . . H51 H 0.024316 0.866815 0.261505 0.025 Uiso 1 1 calc R U . . . C52 C 0.0516(2) 0.76573(13) 0.27188(12) 0.0159(5) Uani 1 1 d . . . . . H52 H 0.114465 0.762055 0.246425 0.019 Uiso 1 1 calc R U . . . C53 C 0.0555(2) 0.78321(13) 0.11605(12) 0.0152(5) Uani 1 1 d . . . . . C54 C -0.0336(2) 0.80952(13) 0.07733(12) 0.0155(5) Uani 1 1 d . . . . . C55 C -0.1241(3) 0.83628(16) 0.00392(13) 0.0247(7) Uani 1 1 d . . . . . H55 H -0.146229 0.838488 -0.033543 0.030 Uiso 1 1 calc R U . . . C56 C -0.1762(3) 0.87223(15) 0.04499(13) 0.0232(6) Uani 1 1 d . . . . . H56 H -0.240129 0.902844 0.041524 0.028 Uiso 1 1 calc R U . . . C57 C -0.1470(3) 0.88295(15) 0.14585(12) 0.0221(6) Uani 1 1 d . . . . . H57A H -0.120278 0.851559 0.174256 0.033 Uiso 1 1 calc R U . . . H57B H -0.232286 0.889123 0.148827 0.033 Uiso 1 1 calc R U . . . H57C H -0.107617 0.926569 0.150612 0.033 Uiso 1 1 calc R U . . . C1S C 0.1178(3) 0.55705(15) 0.62990(14) 0.0241(6) Uani 1 1 d . . . . . H1S H 0.148583 0.532873 0.662870 0.029 Uiso 1 1 calc R U . . . Cl1S Cl 0.05952(8) 0.63493(4) 0.65099(4) 0.0363(2) Uani 1 1 d . . . . . Cl2S Cl 0.01027(8) 0.50618(5) 0.59888(4) 0.0407(2) Uani 1 1 d . . . . . Cl3S Cl 0.23431(8) 0.56877(5) 0.58384(4) 0.0407(2) Uani 1 1 d . . . . . C2S C 0.7740(3) 0.68518(16) 0.57922(15) 0.0332(8) Uani 1 1 d D . . . . H2S H 0.809894 0.697249 0.615285 0.040 Uiso 1 1 calc R U . A 1 Cl4S Cl 0.64355(8) 0.73123(5) 0.57066(4) 0.0413(2) Uani 1 1 d . . . . . Cl5S Cl 0.74642(16) 0.59618(7) 0.57761(10) 0.0454(5) Uani 0.852(5) 1 d . . P B 1 Cl5D Cl 0.7111(9) 0.6091(4) 0.6001(5) 0.0454(5) Uani 0.148(5) 1 d D . P B 2 Cl6S Cl 0.87466(9) 0.70219(5) 0.52736(4) 0.0372(2) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pd1 0.00855(8) 0.01013(8) 0.01149(9) 0.00074(7) 0.00155(7) 0.00024(7) Cl1 0.0140(3) 0.0120(3) 0.0295(4) -0.0036(2) -0.0009(3) 0.0007(2) Cl2 0.0145(3) 0.0124(3) 0.0250(4) -0.0021(2) -0.0008(3) 0.0000(2) Fe1 0.01119(17) 0.01278(17) 0.01361(19) 0.00096(14) 0.00091(14) 0.00032(13) Fe2 0.01003(17) 0.01275(17) 0.01220(19) 0.00089(14) 0.00014(14) -0.00020(13) P1 0.0094(3) 0.0106(3) 0.0131(3) 0.0008(3) 0.0018(3) 0.0003(2) P2 0.0092(3) 0.0115(3) 0.0122(3) 0.0003(3) 0.0017(3) -0.0002(2) O1 0.0182(10) 0.0177(9) 0.0229(11) -0.0008(8) -0.0018(8) -0.0024(8) O2 0.0248(11) 0.0180(9) 0.0184(11) 0.0015(8) -0.0046(9) -0.0026(8) N1 0.0166(12) 0.0200(12) 0.0191(13) 0.0022(10) -0.0005(10) -0.0038(9) N2 0.0169(12) 0.0171(11) 0.0185(12) 0.0014(9) 0.0027(10) 0.0028(9) N3 0.0180(12) 0.0232(12) 0.0194(13) 0.0013(10) -0.0036(10) 0.0054(10) N4 0.0145(11) 0.0170(11) 0.0208(13) -0.0001(9) 0.0008(10) -0.0003(9) C1 0.0162(13) 0.0134(12) 0.0152(14) 0.0016(10) 0.0036(11) -0.0012(10) C2 0.0104(12) 0.0181(13) 0.0225(15) 0.0013(11) 0.0027(11) -0.0012(10) C3 0.0129(13) 0.0192(13) 0.0279(16) 0.0003(12) 0.0054(11) 0.0016(11) C4 0.0205(14) 0.0183(13) 0.0184(14) -0.0022(11) 0.0067(11) 0.0006(11) C5 0.0231(15) 0.0173(12) 0.0140(14) 0.0023(10) 0.0030(12) 0.0000(11) C6 0.0114(12) 0.0133(12) 0.0140(13) 0.0019(10) 0.0013(10) -0.0002(9) C7 0.0177(13) 0.0121(11) 0.0160(14) 0.0010(10) 0.0011(11) -0.0012(10) C8 0.0192(14) 0.0186(13) 0.0166(14) -0.0007(11) -0.0005(12) -0.0062(11) C9 0.0104(12) 0.0224(13) 0.0186(14) 0.0011(11) -0.0014(10) -0.0020(10) C10 0.0093(12) 0.0183(12) 0.0184(14) 0.0003(10) 0.0029(10) 0.0013(10) C11 0.0089(11) 0.0125(11) 0.0165(14) 0.0026(9) 0.0027(10) 0.0028(9) C12 0.0138(13) 0.0185(13) 0.0171(15) 0.0015(11) 0.0029(11) -0.0013(10) C13 0.0189(14) 0.0170(12) 0.0252(17) 0.0039(11) 0.0042(12) -0.0043(11) C14 0.0177(14) 0.0196(13) 0.0248(16) 0.0105(12) 0.0045(12) 0.0001(11) C15 0.0188(14) 0.0244(14) 0.0151(14) 0.0053(11) -0.0002(11) 0.0044(11) C16 0.0147(13) 0.0163(12) 0.0188(14) 0.0019(11) -0.0009(11) -0.0006(10) C17 0.0104(12) 0.0124(11) 0.0154(14) -0.0011(9) -0.0006(10) 0.0011(9) C18 0.0129(12) 0.0167(12) 0.0147(14) 0.0005(10) 0.0005(10) -0.0007(10) C19 0.0210(13) 0.0125(11) 0.0232(15) 0.0019(11) -0.0043(12) -0.0024(10) C20 0.0202(14) 0.0135(12) 0.0290(16) -0.0049(11) -0.0041(12) 0.0030(11) C21 0.0153(13) 0.0210(12) 0.0242(16) -0.0048(11) 0.0041(12) 0.0020(11) C22 0.0134(13) 0.0158(12) 0.0191(15) 0.0011(10) 0.0007(10) -0.0014(10) C23 0.0165(13) 0.0156(12) 0.0150(14) 0.0032(10) 0.0052(11) -0.0014(10) C24 0.0167(13) 0.0151(12) 0.0158(14) 0.0027(10) 0.0038(11) -0.0006(10) C25 0.0168(14) 0.0257(14) 0.0184(15) 0.0068(11) -0.0004(11) -0.0016(11) C26 0.0143(13) 0.0246(14) 0.0217(15) 0.0081(11) 0.0029(11) 0.0019(11) C27 0.0336(18) 0.0223(15) 0.0239(17) -0.0064(12) -0.0016(14) 0.0073(13) C31 0.0122(12) 0.0181(13) 0.0147(14) 0.0051(10) 0.0020(11) -0.0016(10) C32 0.0109(12) 0.0199(12) 0.0139(13) 0.0028(10) 0.0005(10) -0.0024(9) C33 0.0120(12) 0.0212(13) 0.0166(13) 0.0033(10) 0.0037(10) 0.0025(11) C34 0.0185(13) 0.0186(13) 0.0161(13) 0.0001(11) 0.0057(11) 0.0016(11) C35 0.0164(13) 0.0178(13) 0.0139(14) 0.0023(10) 0.0016(10) -0.0002(10) C36 0.0102(11) 0.0161(11) 0.0135(12) 0.0015(11) 0.0022(10) -0.0013(9) C37 0.0179(13) 0.0130(11) 0.0150(14) 0.0012(10) -0.0008(11) -0.0029(10) C38 0.0182(13) 0.0167(12) 0.0171(15) 0.0010(11) -0.0011(11) -0.0063(10) C39 0.0101(11) 0.0246(14) 0.0186(14) 0.0012(12) 0.0006(10) -0.0011(11) C40 0.0100(12) 0.0196(13) 0.0153(14) 0.0002(11) 0.0014(10) 0.0000(10) C41 0.0098(12) 0.0141(11) 0.0165(14) 0.0038(10) 0.0044(10) 0.0037(9) C42 0.0207(15) 0.0262(15) 0.0189(15) 0.0039(12) 0.0012(12) 0.0025(12) C43 0.0363(19) 0.0348(17) 0.0176(16) 0.0082(13) 0.0064(14) 0.0102(14) C44 0.0312(18) 0.0268(16) 0.0322(19) 0.0166(14) 0.0201(15) 0.0122(13) C45 0.0184(14) 0.0144(13) 0.043(2) 0.0078(13) 0.0138(14) 0.0026(11) C46 0.0124(13) 0.0143(12) 0.0271(16) 0.0041(11) 0.0027(11) 0.0027(10) C47 0.0096(12) 0.0136(11) 0.0151(13) -0.0015(9) -0.0002(10) 0.0001(9) C48 0.0164(13) 0.0168(13) 0.0212(15) -0.0010(11) 0.0037(11) 0.0003(10) C49 0.0191(14) 0.0251(15) 0.0293(18) -0.0057(13) 0.0086(13) 0.0047(12) C50 0.0238(16) 0.0178(14) 0.0365(19) -0.0043(13) 0.0019(14) 0.0060(12) C51 0.0210(14) 0.0150(12) 0.0256(15) 0.0010(12) 0.0001(13) 0.0021(10) C52 0.0131(12) 0.0176(12) 0.0169(15) 0.0007(10) 0.0004(11) 0.0006(10) C53 0.0158(13) 0.0152(12) 0.0146(14) 0.0045(10) 0.0004(11) -0.0031(10) C54 0.0140(12) 0.0148(12) 0.0178(14) 0.0016(10) -0.0001(11) -0.0010(10) C55 0.0236(16) 0.0300(16) 0.0207(16) 0.0004(13) -0.0060(13) 0.0096(13) C56 0.0187(14) 0.0234(14) 0.0275(16) 0.0002(12) -0.0066(12) 0.0036(11) C57 0.0212(14) 0.0220(13) 0.0231(15) -0.0042(12) 0.0073(12) -0.0052(11) C1S 0.0243(16) 0.0245(15) 0.0235(17) 0.0034(12) -0.0001(13) -0.0025(12) Cl1S 0.0345(5) 0.0323(4) 0.0423(5) -0.0047(4) 0.0050(4) 0.0062(3) Cl2S 0.0357(5) 0.0349(4) 0.0514(6) 0.0060(4) -0.0062(4) -0.0166(4) Cl3S 0.0331(5) 0.0456(5) 0.0434(5) -0.0178(4) 0.0160(4) -0.0135(4) C2S 0.0343(19) 0.0369(18) 0.0284(18) -0.0034(14) -0.0055(16) -0.0140(16) Cl4S 0.0342(5) 0.0463(5) 0.0435(5) -0.0206(4) 0.0020(4) -0.0045(4) Cl5S 0.0352(8) 0.0341(5) 0.0670(12) 0.0201(6) -0.0128(8) -0.0113(5) Cl5D 0.0352(8) 0.0341(5) 0.0670(12) 0.0201(6) -0.0128(8) -0.0113(5) Cl6S 0.0368(5) 0.0367(4) 0.0383(5) -0.0021(4) 0.0041(4) -0.0051(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Pd Pd -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cl1 Pd1 Cl2 176.54(3) . . ? Cl1 Pd1 P1 84.78(2) . . ? Cl2 Pd1 P1 94.54(2) . . ? Cl1 Pd1 P2 93.70(2) . . ? Cl2 Pd1 P2 87.11(2) . . ? P1 Pd1 P2 177.43(3) . . ? C7 Fe1 C1 167.24(12) . . ? C7 Fe1 C5 149.41(11) . . ? C1 Fe1 C5 41.18(11) . . ? C7 Fe1 C3 106.23(12) . . ? C1 Fe1 C3 68.81(12) . . ? C5 Fe1 C3 68.65(12) . . ? C7 Fe1 C8 40.77(11) . . ? C1 Fe1 C8 151.75(12) . . ? C5 Fe1 C8 115.69(12) . . ? C3 Fe1 C8 124.40(12) . . ? C7 Fe1 C2 127.51(12) . . ? C1 Fe1 C2 41.28(11) . . ? C5 Fe1 C2 69.19(12) . . ? C3 Fe1 C2 40.62(11) . . ? C8 Fe1 C2 163.38(11) . . ? C7 Fe1 C6 41.16(10) . . ? C1 Fe1 C6 130.06(11) . . ? C5 Fe1 C6 167.36(11) . . ? C3 Fe1 C6 119.57(11) . . ? C8 Fe1 C6 68.82(11) . . ? C2 Fe1 C6 110.07(11) . . ? C7 Fe1 C10 68.84(11) . . ? C1 Fe1 C10 110.48(11) . . ? C5 Fe1 C10 128.02(11) . . ? C3 Fe1 C10 155.49(12) . . ? C8 Fe1 C10 68.43(11) . . ? C2 Fe1 C10 122.36(11) . . ? C6 Fe1 C10 40.94(10) . . ? C7 Fe1 C4 115.78(11) . . ? C1 Fe1 C4 68.66(11) . . ? C5 Fe1 C4 40.63(11) . . ? C3 Fe1 C4 40.55(12) . . ? C8 Fe1 C4 104.26(12) . . ? C2 Fe1 C4 68.47(12) . . ? C6 Fe1 C4 151.74(11) . . ? C10 Fe1 C4 163.73(12) . . ? C7 Fe1 C9 68.56(11) . . ? C1 Fe1 C9 119.81(11) . . ? C5 Fe1 C9 106.52(12) . . ? C3 Fe1 C9 161.91(12) . . ? C8 Fe1 C9 40.55(11) . . ? C2 Fe1 C9 155.74(11) . . ? C6 Fe1 C9 68.67(11) . . ? C10 Fe1 C9 40.58(11) . . ? C4 Fe1 C9 124.67(12) . . ? C37 Fe2 C33 105.35(11) . . ? C37 Fe2 C38 40.81(11) . . ? C33 Fe2 C38 125.33(11) . . ? C37 Fe2 C35 146.81(11) . . ? C33 Fe2 C35 68.71(11) . . ? C38 Fe2 C35 114.53(12) . . ? C37 Fe2 C34 113.35(11) . . ? C33 Fe2 C34 40.70(11) . . ? C38 Fe2 C34 103.97(12) . . ? C35 Fe2 C34 40.72(11) . . ? C37 Fe2 C32 128.37(11) . . ? C33 Fe2 C32 40.60(11) . . ? C38 Fe2 C32 164.72(11) . . ? C35 Fe2 C32 69.21(11) . . ? C34 Fe2 C32 68.64(11) . . ? C37 Fe2 C36 41.21(10) . . ? C33 Fe2 C36 117.21(10) . . ? C38 Fe2 C36 68.93(11) . . ? C35 Fe2 C36 170.51(11) . . ? C34 Fe2 C36 148.49(11) . . ? C32 Fe2 C36 109.93(11) . . ? C37 Fe2 C39 68.71(12) . . ? C33 Fe2 C39 164.07(11) . . ? C38 Fe2 C39 40.76(11) . . ? C35 Fe2 C39 107.67(12) . . ? C34 Fe2 C39 126.64(12) . . ? C32 Fe2 C39 154.18(11) . . ? C36 Fe2 C39 68.74(11) . . ? C37 Fe2 C31 169.15(11) . . ? C33 Fe2 C31 68.77(11) . . ? C38 Fe2 C31 150.02(12) . . ? C35 Fe2 C31 40.93(11) . . ? C34 Fe2 C31 68.61(11) . . ? C32 Fe2 C31 41.39(10) . . ? C36 Fe2 C31 132.34(11) . . ? C39 Fe2 C31 119.38(11) . . ? C37 Fe2 C40 68.91(11) . . ? C33 Fe2 C40 153.06(11) . . ? C38 Fe2 C40 68.36(11) . . ? C35 Fe2 C40 130.65(11) . . ? C34 Fe2 C40 166.21(11) . . ? C32 Fe2 C40 121.51(11) . . ? C36 Fe2 C40 41.13(10) . . ? C39 Fe2 C40 40.27(11) . . ? C31 Fe2 C40 111.92(11) . . ? C6 P1 C11 104.72(12) . . ? C6 P1 C17 101.12(12) . . ? C11 P1 C17 104.39(12) . . ? C6 P1 Pd1 117.19(9) . . ? C11 P1 Pd1 107.89(9) . . ? C17 P1 Pd1 119.93(9) . . ? C36 P2 C41 105.33(12) . . ? C36 P2 C47 100.76(12) . . ? C41 P2 C47 103.72(12) . . ? C36 P2 Pd1 117.79(9) . . ? C41 P2 Pd1 108.14(9) . . ? C47 P2 Pd1 119.47(9) . . ? C24 N1 C25 105.2(2) . . ? C26 N2 C24 106.8(2) . . ? C26 N2 C27 124.3(2) . . ? C24 N2 C27 128.9(3) . . ? C54 N3 C55 105.1(3) . . ? C56 N4 C54 106.4(2) . . ? C56 N4 C57 124.1(2) . . ? C54 N4 C57 129.5(3) . . ? C5 C1 C2 107.7(2) . . ? C5 C1 C23 129.9(3) . . ? C2 C1 C23 122.4(3) . . ? C5 C1 Fe1 69.51(15) . . ? C2 C1 Fe1 69.61(15) . . ? C23 C1 Fe1 123.88(19) . . ? C3 C2 C1 107.6(3) . . ? C3 C2 Fe1 69.66(16) . . ? C1 C2 Fe1 69.12(15) . . ? C3 C2 H2 126.2 . . ? C1 C2 H2 126.2 . . ? Fe1 C2 H2 126.6 . . ? C4 C3 C2 108.5(3) . . ? C4 C3 Fe1 69.93(16) . . ? C2 C3 Fe1 69.71(16) . . ? C4 C3 H3 125.7 . . ? C2 C3 H3 125.7 . . ? Fe1 C3 H3 126.2 . . ? C3 C4 C5 108.5(3) . . ? C3 C4 Fe1 69.53(16) . . ? C5 C4 Fe1 69.36(16) . . ? C3 C4 H4 125.8 . . ? C5 C4 H4 125.8 . . ? Fe1 C4 H4 126.9 . . ? C4 C5 C1 107.7(3) . . ? C4 C5 Fe1 70.01(16) . . ? C1 C5 Fe1 69.31(16) . . ? C4 C5 H5 126.1 . . ? C1 C5 H5 126.1 . . ? Fe1 C5 H5 126.1 . . ? C10 C6 C7 107.2(2) . . ? C10 C6 P1 124.8(2) . . ? C7 C6 P1 127.8(2) . . ? C10 C6 Fe1 69.57(15) . . ? C7 C6 Fe1 68.98(15) . . ? P1 C6 Fe1 129.99(14) . . ? C8 C7 C6 108.1(2) . . ? C8 C7 Fe1 69.95(16) . . ? C6 C7 Fe1 69.86(15) . . ? C8 C7 H7 125.9 . . ? C6 C7 H7 125.9 . . ? Fe1 C7 H7 125.8 . . ? C9 C8 C7 108.2(2) . . ? C9 C8 Fe1 69.95(15) . . ? C7 C8 Fe1 69.27(15) . . ? C9 C8 H8 125.9 . . ? C7 C8 H8 125.9 . . ? Fe1 C8 H8 126.5 . . ? C8 C9 C10 108.2(2) . . ? C8 C9 Fe1 69.50(16) . . ? C10 C9 Fe1 69.63(15) . . ? C8 C9 H9 125.9 . . ? C10 C9 H9 125.9 . . ? Fe1 C9 H9 126.6 . . ? C9 C10 C6 108.2(2) . . ? C9 C10 Fe1 69.80(15) . . ? C6 C10 Fe1 69.49(15) . . ? C9 C10 H10 125.9 . . ? C6 C10 H10 125.9 . . ? Fe1 C10 H10 126.4 . . ? C12 C11 C16 119.2(2) . . ? C12 C11 P1 123.0(2) . . ? C16 C11 P1 117.7(2) . . ? C13 C12 C11 119.9(3) . . ? C13 C12 H12 120.1 . . ? C11 C12 H12 120.1 . . ? C14 C13 C12 120.9(3) . . ? C14 C13 H13 119.5 . . ? C12 C13 H13 119.5 . . ? C13 C14 C15 119.7(3) . . ? C13 C14 H14 120.2 . . ? C15 C14 H14 120.2 . . ? C16 C15 C14 119.9(3) . . ? C16 C15 H15 120.1 . . ? C14 C15 H15 120.1 . . ? C15 C16 C11 120.4(3) . . ? C15 C16 H16 119.8 . . ? C11 C16 H16 119.8 . . ? C22 C17 C18 119.3(2) . . ? C22 C17 P1 121.6(2) . . ? C18 C17 P1 118.7(2) . . ? C19 C18 C17 120.0(3) . . ? C19 C18 H18 120.0 . . ? C17 C18 H18 120.0 . . ? C20 C19 C18 120.1(3) . . ? C20 C19 H19 119.9 . . ? C18 C19 H19 119.9 . . ? C21 C20 C19 120.1(3) . . ? C21 C20 H20 120.0 . . ? C19 C20 H20 120.0 . . ? C20 C21 C22 119.9(3) . . ? C20 C21 H21 120.0 . . ? C22 C21 H21 120.0 . . ? C17 C22 C21 120.6(3) . . ? C17 C22 H22 119.7 . . ? C21 C22 H22 119.7 . . ? O1 C23 C1 120.5(3) . . ? O1 C23 C24 120.5(2) . . ? C1 C23 C24 119.1(2) . . ? N1 C24 N2 111.1(3) . . ? N1 C24 C23 126.2(3) . . ? N2 C24 C23 122.7(3) . . ? N1 C25 C26 110.6(3) . . ? N1 C25 H25 124.7 . . ? C26 C25 H25 124.7 . . ? N2 C26 C25 106.2(3) . . ? N2 C26 H26 126.9 . . ? C25 C26 H26 126.9 . . ? N2 C27 H27A 109.5 . . ? N2 C27 H27B 109.5 . . ? H27A C27 H27B 109.5 . . ? N2 C27 H27C 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? C35 C31 C32 107.5(2) . . ? C35 C31 C53 129.1(3) . . ? C32 C31 C53 123.2(3) . . ? C35 C31 Fe2 69.24(15) . . ? C32 C31 Fe2 69.07(15) . . ? C53 C31 Fe2 122.64(19) . . ? C33 C32 C31 107.5(2) . . ? C33 C32 Fe2 69.56(15) . . ? C31 C32 Fe2 69.54(15) . . ? C33 C32 H32 126.2 . . ? C31 C32 H32 126.2 . . ? Fe2 C32 H32 126.2 . . ? C32 C33 C34 108.7(2) . . ? C32 C33 Fe2 69.84(15) . . ? C34 C33 Fe2 69.79(16) . . ? C32 C33 H33 125.7 . . ? C34 C33 H33 125.7 . . ? Fe2 C33 H33 126.3 . . ? C33 C34 C35 108.3(2) . . ? C33 C34 Fe2 69.51(16) . . ? C35 C34 Fe2 69.58(16) . . ? C33 C34 H34 125.8 . . ? C35 C34 H34 125.8 . . ? Fe2 C34 H34 126.6 . . ? C34 C35 C31 108.0(3) . . ? C34 C35 Fe2 69.70(16) . . ? C31 C35 Fe2 69.83(16) . . ? C34 C35 H35 126.0 . . ? C31 C35 H35 126.0 . . ? Fe2 C35 H35 126.0 . . ? C37 C36 C40 107.0(2) . . ? C37 C36 P2 127.9(2) . . ? C40 C36 P2 125.0(2) . . ? C37 C36 Fe2 68.90(15) . . ? C40 C36 Fe2 69.68(15) . . ? P2 C36 Fe2 127.70(13) . . ? C38 C37 C36 108.2(2) . . ? C38 C37 Fe2 69.92(15) . . ? C36 C37 Fe2 69.89(15) . . ? C38 C37 H37 125.9 . . ? C36 C37 H37 125.9 . . ? Fe2 C37 H37 125.9 . . ? C37 C38 C39 108.1(2) . . ? C37 C38 Fe2 69.27(15) . . ? C39 C38 Fe2 69.88(15) . . ? C37 C38 H38 125.9 . . ? C39 C38 H38 125.9 . . ? Fe2 C38 H38 126.5 . . ? C40 C39 C38 108.4(3) . . ? C40 C39 Fe2 70.04(15) . . ? C38 C39 Fe2 69.36(15) . . ? C40 C39 H39 125.8 . . ? C38 C39 H39 125.8 . . ? Fe2 C39 H39 126.4 . . ? C39 C40 C36 108.3(2) . . ? C39 C40 Fe2 69.69(16) . . ? C36 C40 Fe2 69.19(15) . . ? C39 C40 H40 125.8 . . ? C36 C40 H40 125.8 . . ? Fe2 C40 H40 126.8 . . ? C42 C41 C46 119.4(3) . . ? C42 C41 P2 117.3(2) . . ? C46 C41 P2 123.2(2) . . ? C43 C42 C41 120.5(3) . . ? C43 C42 H42 119.7 . . ? C41 C42 H42 119.7 . . ? C44 C43 C42 119.7(3) . . ? C44 C43 H43 120.1 . . ? C42 C43 H43 120.1 . . ? C45 C44 C43 120.1(3) . . ? C45 C44 H44 119.9 . . ? C43 C44 H44 119.9 . . ? C44 C45 C46 120.9(3) . . ? C44 C45 H45 119.6 . . ? C46 C45 H45 119.6 . . ? C45 C46 C41 119.3(3) . . ? C45 C46 H46 120.4 . . ? C41 C46 H46 120.4 . . ? C52 C47 C48 119.7(2) . . ? C52 C47 P2 118.6(2) . . ? C48 C47 P2 121.5(2) . . ? C49 C48 C47 119.6(3) . . ? C49 C48 H48 120.2 . . ? C47 C48 H48 120.2 . . ? C50 C49 C48 120.3(3) . . ? C50 C49 H49 119.8 . . ? C48 C49 H49 119.8 . . ? C51 C50 C49 120.0(3) . . ? C51 C50 H50 120.0 . . ? C49 C50 H50 120.0 . . ? C50 C51 C52 120.3(3) . . ? C50 C51 H51 119.8 . . ? C52 C51 H51 119.8 . . ? C47 C52 C51 119.9(3) . . ? C47 C52 H52 120.0 . . ? C51 C52 H52 120.0 . . ? O2 C53 C31 121.4(3) . . ? O2 C53 C54 120.3(2) . . ? C31 C53 C54 118.3(2) . . ? N3 C54 N4 111.6(3) . . ? N3 C54 C53 125.0(3) . . ? N4 C54 C53 123.2(3) . . ? N3 C55 C56 110.6(3) . . ? N3 C55 H55 124.7 . . ? C56 C55 H55 124.7 . . ? N4 C56 C55 106.4(3) . . ? N4 C56 H56 126.8 . . ? C55 C56 H56 126.8 . . ? N4 C57 H57A 109.5 . . ? N4 C57 H57B 109.5 . . ? H57A C57 H57B 109.5 . . ? N4 C57 H57C 109.5 . . ? H57A C57 H57C 109.5 . . ? H57B C57 H57C 109.5 . . ? Cl3S C1S Cl1S 110.93(17) . . ? Cl3S C1S Cl2S 108.98(18) . . ? Cl1S C1S Cl2S 111.55(19) . . ? Cl3S C1S H1S 108.4 . . ? Cl1S C1S H1S 108.4 . . ? Cl2S C1S H1S 108.4 . . ? Cl6S C2S Cl5D 130.5(6) . . ? Cl6S C2S Cl4S 111.6(2) . . ? Cl5D C2S Cl4S 97.9(4) . . ? Cl6S C2S Cl5S 106.8(2) . . ? Cl4S C2S Cl5S 111.19(19) . . ? Cl6S C2S H2S 109.0 . . ? Cl4S C2S H2S 109.0 . . ? Cl5S C2S H2S 109.0 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pd1 Cl1 2.2957(7) . ? Pd1 Cl2 2.3062(6) . ? Pd1 P1 2.3442(7) . ? Pd1 P2 2.3540(7) . ? Fe1 C7 2.038(3) . ? Fe1 C1 2.041(3) . ? Fe1 C5 2.044(3) . ? Fe1 C3 2.047(3) . ? Fe1 C8 2.047(3) . ? Fe1 C2 2.047(3) . ? Fe1 C6 2.050(3) . ? Fe1 C10 2.051(3) . ? Fe1 C4 2.052(3) . ? Fe1 C9 2.053(3) . ? Fe2 C37 2.034(3) . ? Fe2 C33 2.043(3) . ? Fe2 C38 2.043(3) . ? Fe2 C35 2.045(3) . ? Fe2 C34 2.046(3) . ? Fe2 C32 2.046(3) . ? Fe2 C36 2.048(3) . ? Fe2 C39 2.050(3) . ? Fe2 C31 2.053(3) . ? Fe2 C40 2.054(3) . ? P1 C6 1.808(3) . ? P1 C11 1.820(3) . ? P1 C17 1.823(3) . ? P2 C36 1.805(3) . ? P2 C41 1.814(3) . ? P2 C47 1.825(3) . ? O1 C23 1.224(3) . ? O2 C53 1.226(3) . ? N1 C24 1.330(4) . ? N1 C25 1.364(4) . ? N2 C26 1.361(4) . ? N2 C24 1.372(3) . ? N2 C27 1.461(4) . ? N3 C54 1.324(4) . ? N3 C55 1.365(4) . ? N4 C56 1.362(4) . ? N4 C54 1.373(4) . ? N4 C57 1.462(4) . ? C1 C5 1.436(4) . ? C1 C2 1.441(4) . ? C1 C23 1.479(4) . ? C2 C3 1.421(4) . ? C2 H2 0.9500 . ? C3 C4 1.420(4) . ? C3 H3 0.9500 . ? C4 C5 1.422(4) . ? C4 H4 0.9500 . ? C5 H5 0.9500 . ? C6 C10 1.434(4) . ? C6 C7 1.437(4) . ? C7 C8 1.423(4) . ? C7 H7 0.9500 . ? C8 C9 1.421(4) . ? C8 H8 0.9500 . ? C9 C10 1.423(4) . ? C9 H9 0.9500 . ? C10 H10 0.9500 . ? C11 C12 1.390(4) . ? C11 C16 1.403(4) . ? C12 C13 1.389(4) . ? C12 H12 0.9500 . ? C13 C14 1.381(4) . ? C13 H13 0.9500 . ? C14 C15 1.394(4) . ? C14 H14 0.9500 . ? C15 C16 1.388(4) . ? C15 H15 0.9500 . ? C16 H16 0.9500 . ? C17 C22 1.388(4) . ? C17 C18 1.400(4) . ? C18 C19 1.391(4) . ? C18 H18 0.9500 . ? C19 C20 1.387(4) . ? C19 H19 0.9500 . ? C20 C21 1.386(4) . ? C20 H20 0.9500 . ? C21 C22 1.389(4) . ? C21 H21 0.9500 . ? C22 H22 0.9500 . ? C23 C24 1.480(4) . ? C25 C26 1.366(4) . ? C25 H25 0.9500 . ? C26 H26 0.9500 . ? C27 H27A 0.9800 . ? C27 H27B 0.9800 . ? C27 H27C 0.9800 . ? C31 C35 1.433(4) . ? C31 C32 1.448(4) . ? C31 C53 1.471(4) . ? C32 C33 1.419(4) . ? C32 H32 0.9500 . ? C33 C34 1.422(4) . ? C33 H33 0.9500 . ? C34 C35 1.423(4) . ? C34 H34 0.9500 . ? C35 H35 0.9500 . ? C36 C37 1.437(4) . ? C36 C40 1.441(4) . ? C37 C38 1.422(4) . ? C37 H37 0.9500 . ? C38 C39 1.425(4) . ? C38 H38 0.9500 . ? C39 C40 1.413(4) . ? C39 H39 0.9500 . ? C40 H40 0.9500 . ? C41 C42 1.395(4) . ? C41 C46 1.397(4) . ? C42 C43 1.390(4) . ? C42 H42 0.9500 . ? C43 C44 1.384(5) . ? C43 H43 0.9500 . ? C44 C45 1.378(5) . ? C44 H44 0.9500 . ? C45 C46 1.394(4) . ? C45 H45 0.9500 . ? C46 H46 0.9500 . ? C47 C52 1.395(4) . ? C47 C48 1.397(4) . ? C48 C49 1.396(4) . ? C48 H48 0.9500 . ? C49 C50 1.389(5) . ? C49 H49 0.9500 . ? C50 C51 1.378(4) . ? C50 H50 0.9500 . ? C51 C52 1.395(4) . ? C51 H51 0.9500 . ? C52 H52 0.9500 . ? C53 C54 1.481(4) . ? C55 C56 1.365(4) . ? C55 H55 0.9500 . ? C56 H56 0.9500 . ? C57 H57A 0.9800 . ? C57 H57B 0.9800 . ? C57 H57C 0.9800 . ? C1S Cl3S 1.753(3) . ? C1S Cl1S 1.756(3) . ? C1S Cl2S 1.756(3) . ? C1S H1S 1.0000 . ? C2S Cl6S 1.740(4) . ? C2S Cl5D 1.744(3) . ? C2S Cl4S 1.753(4) . ? C2S Cl5S 1.790(4) . ? C2S H2S 1.0000 . ?