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Information card for entry 7108924
Preview
| Coordinates | 7108924.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C68 H106 Fe2 P10 Sm2 |
|---|---|
| Calculated formula | C68 H106 Fe2 P10 Sm2 |
| Title of publication | P-P bond formation via reductive dimerization of [Cp^*^Fe(η^5^-P~5~)] by divalent samarocenes |
| Authors of publication | Li, Tianshu; Gamer, Michael T.; Scheer, Manfred; Konchenko, Sergey N.; Roesky, Peter W. |
| Journal of publication | Chemical Communications (Cambridge, United Kingdom) |
| Year of publication | 2013 |
| Journal volume | 49 |
| Journal issue | 22 |
| Pages of publication | 2183 - 2185 |
| a | 14.357 ± 0.003 Å |
| b | 28.55 ± 0.006 Å |
| c | 17.985 ± 0.004 Å |
| α | 90° |
| β | 95.08 ± 0.03° |
| γ | 90° |
| Cell volume | 7343 ± 3 Å3 |
| Cell temperature | 200 ± 2 K |
| Ambient diffraction temperature | 200 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0434 |
| Residual factor for significantly intense reflections | 0.0337 |
| Weighted residual factors for significantly intense reflections | 0.0834 |
| Weighted residual factors for all reflections included in the refinement | 0.0868 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.968 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
Version history
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