#------------------------------------------------------------------------------ #$Date: 2025-08-21 23:24:23 +0100 (Thu, 21 Aug 2025) $ #$Revision: 301857 $ #$URL: svn://www.crystallography.net/cod/cif/7/11/21/7112105.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7112105 loop_ _publ_author_name 'Yan Li' 'Kartik Chandra Mondal' 'Peter Stollberg' 'Hongping Zhu' 'Herbert W. Roesky' 'Regine Herbst-Irmer' 'Dietmar Stalke' 'Heike Fliegl' _publ_section_title ; Unusual formation of a N-heterocyclic germylene via homolytic cleavage of a C-C bond ; _journal_name_full Chem.Commun. _journal_page_first 3356 _journal_paper_doi 10.1039/c4cc00251b _journal_volume 50 _journal_year 2014 _chemical_formula_moiety 'C18 H23 Cl3 N2 Si' _chemical_formula_sum 'C18 H23 Cl3 N2 Si' _chemical_formula_weight 401.82 _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2013 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 9.984(2) _cell_length_b 13.987(2) _cell_length_c 14.110(2) _cell_measurement_reflns_used 9906 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 28.986 _cell_measurement_theta_min 2.499 _cell_volume 1970.4(6) _computing_cell_refinement 'SAINT V7.68A' _computing_data_collection 'APEX2 v2012.2' _computing_data_reduction 'SAINT V7.68A' _computing_molecular_graphics 'XP Version 5.1' _computing_publication_material 'XSHELL in SHELXTL-97' _computing_structure_refinement 'SHELXL-2012 (Sheldrick, 2012)' _computing_structure_solution 'SHELXS-2012 (Sheldrick, 2012)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Smart APEX II Ultra' _diffrn_measurement_method 'omega scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0330 _diffrn_reflns_av_unetI/netI 0.0161 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 55923 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 29.134 _diffrn_reflns_theta_min 2.050 _diffrn_source 'rotating anode' _exptl_absorpt_coefficient_mu 0.529 _exptl_absorpt_correction_T_max 0.8621 _exptl_absorpt_correction_T_min 0.8083 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS-2012/1 _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.355 _exptl_crystal_description plate _exptl_crystal_F_000 840 _exptl_crystal_size_max 0.1 _exptl_crystal_size_mid 0.09 _exptl_crystal_size_min 0.05 _refine_diff_density_max 0.521 _refine_diff_density_min -0.187 _refine_diff_density_rms 0.071 _refine_ls_abs_structure_details ; Refined as an inversion twin. ; _refine_ls_abs_structure_Flack 0.34(6) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.080 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 222 _refine_ls_number_reflns 5318 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.080 _refine_ls_R_factor_all 0.0334 _refine_ls_R_factor_gt 0.0322 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0550P)^2^+0.4465P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0856 _refine_ls_wR_factor_ref 0.0864 _reflns_Friedel_coverage 0.774 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 1.000 _reflns_number_gt 5131 _reflns_number_total 5318 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file c4cc00251b2.cif _cod_data_source_block p2_a _cod_database_code 7112105 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelxl_version_number 2013-4 _shelx_res_file ; REM Solution 1 R1 0.109, Alpha = 0.0067 in P2(1)2(1)2(1) REM Flack x = 0.356 ( 0.010 ) from Parsons' quotients REM C18 N2 Si Cl3 TITL p2 in P2(1)2(1)2(1) CELL 0.71073 9.984 13.987 14.110 90.000 90.000 90.000 ZERR 4.00 0.002 0.002 0.002 0.000 0.000 0.000 LATT -1 SYMM 1/2-X, -Y, 1/2+Z SYMM -X, 1/2+Y, 1/2-Z SYMM 1/2+X, 1/2-Y, -Z SFAC C H N SI CL UNIT 72 92 8 4 12 TEMP -173.000 L.S. 10 LIST 4 ACTA CONF BOND $H omit 2 5 0 omit 0 9 6 omit 1 3 0 FMAP 2 PLAN 20 twin WGHT 0.055000 0.446500 BASF 0.34434 FVAR 0.41627 CL1 5 0.673507 0.869655 0.269622 11.00000 0.03335 0.03702 = 0.02351 -0.00829 0.00245 -0.00244 CL2 5 0.409556 0.965371 0.327027 11.00000 0.02321 0.04829 = 0.02264 0.00222 -0.00656 -0.00012 CL3 5 0.622527 1.114451 0.269469 11.00000 0.03525 0.04085 = 0.02972 0.01716 0.00046 0.00498 SI1 4 0.619504 0.989875 0.351045 11.00000 0.02074 0.02808 = 0.01435 0.00284 -0.00076 0.00074 N1 3 0.810821 1.009051 0.377114 11.00000 0.02180 0.02350 = 0.01784 0.00130 0.00152 -0.00037 N2 3 0.606547 0.990148 0.472421 11.00000 0.01489 0.02420 = 0.01474 0.00117 0.00015 -0.00122 C1 1 0.909009 1.015156 0.310892 11.00000 0.02770 0.03042 = 0.02192 0.00237 0.00590 -0.00107 AFIX 43 H1 2 0.885708 1.014111 0.245622 11.00000 -1.20000 AFIX 0 C2 1 1.040701 1.022776 0.336147 11.00000 0.02321 0.03239 = 0.03026 0.00163 0.00875 0.00003 AFIX 43 H2 2 1.108381 1.026610 0.288974 11.00000 -1.20000 AFIX 0 C3 1 1.074468 1.024850 0.431799 11.00000 0.01898 0.03172 = 0.03480 0.00160 0.00138 -0.00186 AFIX 43 H3 2 1.165693 1.028766 0.450544 11.00000 -1.20000 AFIX 0 C4 1 0.974729 1.021188 0.499088 11.00000 0.02137 0.02734 = 0.02602 0.00152 -0.00182 -0.00240 AFIX 43 H4 2 0.995704 1.024591 0.564673 11.00000 -1.20000 AFIX 0 C5 1 0.842910 1.012421 0.469098 11.00000 0.01887 0.01956 = 0.02046 0.00110 0.00123 -0.00029 C6 1 0.723965 1.002931 0.531812 11.00000 0.01731 0.02600 = 0.01570 0.00027 -0.00098 -0.00131 AFIX 23 H6A 2 0.734959 0.947238 0.574408 11.00000 -1.20000 H6B 2 0.713828 1.061015 0.571260 11.00000 -1.20000 AFIX 0 C7 1 0.487406 0.973499 0.527917 11.00000 0.01575 0.02490 = 0.01467 -0.00074 -0.00043 -0.00136 C8 1 0.452533 0.879338 0.551251 11.00000 0.01888 0.02138 = 0.01736 -0.00093 -0.00121 -0.00113 C9 1 0.335691 0.864207 0.603283 11.00000 0.02109 0.02753 = 0.02239 -0.00081 0.00121 -0.00605 AFIX 43 H9 2 0.308895 0.800721 0.617880 11.00000 -1.20000 AFIX 0 C10 1 0.258126 0.940103 0.634010 11.00000 0.01928 0.03702 = 0.02060 -0.00308 0.00321 -0.00351 AFIX 43 H10 2 0.178465 0.928659 0.669041 11.00000 -1.20000 AFIX 0 C11 1 0.297302 1.033167 0.613383 11.00000 0.02100 0.03208 = 0.02198 -0.00647 0.00145 0.00368 AFIX 43 H11 2 0.245183 1.085072 0.636311 11.00000 -1.20000 AFIX 0 C12 1 0.411731 1.051852 0.559636 11.00000 0.02184 0.02336 = 0.01948 -0.00099 -0.00310 0.00091 C13 1 0.450508 1.154649 0.536910 11.00000 0.02954 0.02053 = 0.03070 -0.00083 0.00081 0.00148 AFIX 13 H13 2 0.536628 1.152768 0.500771 11.00000 -1.20000 AFIX 0 C14 1 0.475737 1.211166 0.628266 11.00000 0.04722 0.03018 = 0.04031 -0.00926 0.00034 -0.00444 AFIX 137 H14A 2 0.511913 1.274306 0.612414 11.00000 -1.50000 H14B 2 0.540134 1.176582 0.667919 11.00000 -1.50000 H14C 2 0.391294 1.218742 0.662869 11.00000 -1.50000 AFIX 0 C15 1 0.345927 1.203959 0.473857 11.00000 0.04452 0.02934 = 0.05214 0.00700 -0.00971 0.00273 AFIX 137 H15A 2 0.379226 1.266962 0.454666 11.00000 -1.50000 H15B 2 0.262161 1.211524 0.509277 11.00000 -1.50000 H15C 2 0.329644 1.164866 0.417382 11.00000 -1.50000 AFIX 0 C16 1 0.536380 0.793942 0.521257 11.00000 0.02081 0.02066 = 0.02349 0.00032 0.00134 -0.00055 AFIX 13 H16 2 0.616296 0.818694 0.486283 11.00000 -1.20000 AFIX 0 C17 1 0.587016 0.737548 0.607007 11.00000 0.03103 0.02863 = 0.03356 0.00552 -0.00411 0.00276 AFIX 137 H17A 2 0.652481 0.689802 0.586077 11.00000 -1.50000 H17B 2 0.511491 0.705324 0.637792 11.00000 -1.50000 H17C 2 0.629502 0.781401 0.652067 11.00000 -1.50000 AFIX 0 C18 1 0.457580 0.728939 0.453281 11.00000 0.03123 0.02644 = 0.03358 -0.00837 -0.00248 0.00009 AFIX 137 H18A 2 0.428242 0.766153 0.398216 11.00000 -1.50000 H18B 2 0.379149 0.702921 0.486127 11.00000 -1.50000 H18C 2 0.515141 0.676326 0.432188 11.00000 -1.50000 AFIX 0 HKLF 4 REM p2 in P2(1)2(1)2(1) REM R1 = 0.0322 for 5131 Fo > 4sig(Fo) and 0.0334 for all 5318 data REM 222 parameters refined using 0 restraints END WGHT 0.0550 0.4466 REM Highest difference peak 0.521, deepest hole -0.187, 1-sigma level 0.071 Q1 1 0.6354 0.9168 0.2531 11.00000 0.05 0.52 Q2 1 0.6166 1.1656 0.3046 11.00000 0.05 0.50 Q3 1 0.7489 0.8772 0.2710 11.00000 0.05 0.43 Q4 1 0.4648 0.9221 0.5403 11.00000 0.05 0.39 Q5 1 0.4083 1.0253 0.3330 11.00000 0.05 0.39 Q6 1 0.3047 0.9003 0.6229 11.00000 0.05 0.37 Q7 1 0.6982 1.1193 0.2765 11.00000 0.05 0.36 Q8 1 0.4883 0.9771 0.3235 11.00000 0.05 0.35 Q9 1 0.4363 1.1022 0.5457 11.00000 0.05 0.35 Q10 1 0.3905 0.8763 0.5827 11.00000 0.05 0.34 Q11 1 0.9734 1.0294 0.3336 11.00000 0.05 0.34 Q12 1 0.8347 1.0167 0.4224 11.00000 0.05 0.33 Q13 1 0.7930 0.9995 0.5009 11.00000 0.05 0.33 Q14 1 0.4850 0.8335 0.5348 11.00000 0.05 0.33 Q15 1 0.6216 1.0561 0.3142 11.00000 0.05 0.32 Q16 1 0.9067 1.0143 0.4817 11.00000 0.05 0.32 Q17 1 0.4462 1.0042 0.5435 11.00000 0.05 0.31 Q18 1 1.0546 1.0265 0.3817 11.00000 0.05 0.31 Q19 1 0.8629 1.0078 0.3486 11.00000 0.05 0.31 Q20 1 0.6157 0.9988 0.4195 11.00000 0.05 0.29 ; _shelx_res_checksum 99592 _shelx_hkl_file ; 1 0 0 0.10 0.20 -1 0 0 0.30 0.10 -1 0 0 0.40 0.20 -1 0 0 0.50 0.10 -1 0 0 0.00 0.20 -1 0 0 0.30 0.30 1 0 0 0.40 0.10 1 0 0 0.10 0.20 1 0 0 0.10 0.20 1 0 0 0.40 0.10 1 0 0 0.50 0.20 -2 0 0 1562.44 50.69 2 0 0 1589.94 51.39 2 0 0 1620.24 51.69 2 0 0 1571.34 52.79 -2 0 0 1419.96 61.19 -2 0 0 1471.65 49.70 -2 0 0 1545.95 52.89 -2 0 0 1627.64 51.49 2 0 0 1474.15 49.80 -2 0 0 1593.34 51.79 2 0 0 1518.85 61.39 2 0 0 1551.34 52.89 3 0 0 0.00 0.40 3 0 0 0.00 0.50 -3 0 0 0.40 0.20 -3 0 0 0.00 0.40 -3 0 0 0.10 0.60 -3 0 0 0.00 0.40 3 0 0 0.80 0.30 3 0 0 0.00 0.40 3 0 0 0.10 0.60 3 0 0 0.50 0.40 3 0 0 2.20 0.40 -3 0 0 0.00 0.40 -3 0 0 0.50 0.30 -3 0 0 0.40 0.30 -4 0 0 1722.13 58.39 4 0 0 1711.63 57.29 4 0 0 1748.43 60.89 -4 0 0 1729.63 69.69 -4 0 0 1926.81 57.99 4 0 0 1687.73 70.69 4 0 0 1835.22 56.69 4 0 0 1796.92 60.39 -4 0 0 1701.23 56.59 -4 0 0 1837.32 60.89 -4 0 0 1756.72 59.09 4 0 0 1840.72 58.39 4 0 0 1740.33 59.09 -4 0 0 1740.73 83.89 5 0 0 0.40 0.40 -5 0 0 0.00 0.50 -5 0 0 0.50 0.40 -5 0 0 2.40 1.10 5 0 0 1.00 0.90 5 0 0 1.50 0.90 -5 0 0 2.30 0.70 5 0 0 1.40 0.40 5 0 0 0.90 0.70 5 0 0 1.70 0.70 -5 0 0 2.10 0.60 5 0 0 1.40 0.70 -5 0 0 1.30 0.70 -5 0 0 1.10 0.70 -6 0 0 38.30 2.50 -6 0 0 42.10 2.40 -6 0 0 39.00 3.20 -6 0 0 41.00 2.00 6 0 0 42.10 1.70 6 0 0 39.20 2.30 -6 0 0 40.30 1.90 6 0 0 44.30 3.20 6 0 0 39.10 1.90 6 0 0 38.90 2.40 6 0 0 39.20 2.40 -6 0 0 37.80 2.00 7 0 0 2.20 0.80 -7 0 0 0.90 0.60 7 0 0 2.50 0.50 -7 0 0 0.80 0.70 7 0 0 1.60 0.50 -7 0 0 1.80 1.10 -7 0 0 0.00 0.50 7 0 0 4.00 0.90 7 0 0 3.00 0.90 7 0 0 3.70 1.20 -8 0 0 12.60 1.30 8 0 0 10.30 2.00 -8 0 0 10.80 1.30 8 0 0 10.10 1.50 8 0 0 13.70 1.80 -8 0 0 11.30 2.30 8 0 0 9.20 1.40 -8 0 0 11.30 1.60 8 0 0 12.50 1.10 9 0 0 0.40 0.90 9 0 0 0.00 0.80 -9 0 0 0.00 0.70 -9 0 0 0.00 0.70 -9 0 0 0.00 0.60 9 0 0 0.40 0.90 9 0 0 0.40 1.10 10 0 0 62.09 5.00 10 0 0 57.29 3.70 -10 0 0 52.69 3.00 -10 0 0 59.89 3.20 -11 0 0 0.30 0.80 11 0 0 1.20 1.60 11 0 0 1.60 1.10 12 0 0 2.30 1.40 12 0 0 5.60 2.10 13 0 0 5.00 1.60 13 0 0 6.80 2.40 0 -1 0 0.60 0.20 0 1 0 0.50 0.10 0 -1 0 0.40 0.10 0 -1 0 0.30 0.10 0 1 0 0.30 0.10 0 1 0 0.20 0.10 0 -1 0 0.30 0.10 0 1 0 0.30 0.10 0 1 0 0.20 0.20 0 -1 0 0.20 0.10 -1 1 0 1003.30 49.70 1 1 0 1070.49 35.30 1 -1 0 1098.59 34.40 1 -1 0 1099.59 34.20 -1 1 0 1059.19 41.60 1 -1 0 1132.69 36.40 1 -1 0 996.60 35.70 1 -1 0 1108.19 33.80 -1 -1 0 1078.79 36.60 -1 -1 0 1045.20 35.10 1 1 0 1058.99 35.10 1 1 0 1043.80 36.00 1 1 0 1114.29 36.60 -1 1 0 1024.00 36.00 -1 1 0 953.40 34.80 -1 1 0 1023.60 34.40 -1 1 0 951.90 35.00 1 1 0 1035.90 33.60 1 1 0 1000.70 33.70 1 -1 0 1062.49 42.00 -1 1 0 1094.09 33.80 1 -1 0 1123.79 35.20 1 1 0 1092.19 34.30 -1 -1 0 965.10 35.10 1 -1 0 1136.69 50.49 -2 1 0 205.08 7.00 2 1 0 210.78 7.30 2 1 0 200.78 6.80 -2 1 0 203.78 6.90 2 -1 0 202.68 7.00 2 -1 0 211.28 7.40 2 -1 0 209.58 7.00 2 -1 0 205.48 6.90 -2 1 0 212.38 8.30 2 1 0 198.48 7.10 2 1 0 202.58 6.90 2 -1 0 206.98 8.30 -2 1 0 218.68 10.30 -2 -1 0 206.08 10.10 2 -1 0 202.48 10.20 2 1 0 204.08 7.10 -2 -1 0 207.78 7.30 -2 1 0 211.48 6.80 -2 1 0 198.18 7.40 -2 -1 0 182.78 7.00 2 -1 0 206.98 7.20 -2 -1 0 210.68 7.10 -2 1 0 200.58 7.20 2 -1 0 199.38 7.10 2 -1 0 203.18 8.60 2 1 0 207.18 6.80 -2 -1 0 206.68 7.00 3 -1 0 12.70 1.10 3 1 0 12.70 1.50 3 -1 0 15.80 1.50 -3 1 0 15.00 0.90 -3 1 0 15.60 1.60 3 1 0 14.40 1.00 3 -1 0 15.20 1.50 -3 1 0 13.70 1.10 -3 -1 0 16.20 1.10 -3 -1 0 13.00 0.90 -3 -1 0 13.10 0.90 -3 -1 0 14.20 1.00 -3 -1 0 16.70 1.50 -3 1 0 15.00 1.00 -3 1 0 15.90 0.90 3 -1 0 13.60 1.10 3 -1 0 15.10 1.10 3 1 0 14.30 0.80 3 1 0 14.20 1.10 3 1 0 13.30 1.00 3 1 0 13.00 1.00 -3 -1 0 15.40 0.90 3 -1 0 14.00 0.90 -3 1 0 13.60 1.10 3 1 0 14.80 0.90 3 1 0 15.30 0.90 -3 1 0 13.10 0.90 3 -1 0 13.60 0.90 3 -1 0 14.40 1.10 3 -1 0 14.90 0.80 4 -1 0 110.59 6.20 4 1 0 112.69 3.90 4 1 0 109.99 4.30 -4 1 0 109.29 4.90 4 1 0 106.49 5.30 -4 -1 0 114.39 4.50 4 -1 0 110.39 4.10 -4 1 0 104.79 4.00 -4 1 0 119.19 6.40 4 -1 0 108.99 4.30 4 -1 0 108.79 4.10 -4 -1 0 110.89 6.20 4 1 0 107.49 4.40 -4 1 0 110.89 4.60 -4 1 0 107.49 4.00 4 -1 0 108.49 4.40 4 1 0 108.39 4.10 -4 -1 0 103.79 4.10 4 1 0 109.49 4.30 4 -1 0 101.69 4.50 4 -1 0 110.59 5.40 -4 1 0 104.79 3.90 -4 -1 0 112.79 4.30 -4 1 0 108.69 4.40 -4 -1 0 106.09 4.00 5 -1 0 1925.21 63.69 -5 -1 0 1897.61 61.99 5 -1 0 1698.53 75.09 -5 1 0 2057.29 61.19 -5 1 0 1978.80 62.89 -5 1 0 1873.51 61.89 -5 -1 0 1928.61 60.09 5 -1 0 1881.21 60.99 5 1 0 1933.81 60.89 5 1 0 1789.62 64.59 5 -1 0 1792.02 64.69 -5 -1 0 1880.31 64.69 -5 1 0 1705.23 89.09 -5 1 0 1880.71 60.09 5 1 0 1914.61 62.69 5 1 0 1913.51 59.99 5 1 0 1880.11 63.69 5 -1 0 1897.01 62.79 -5 1 0 1901.21 73.99 -5 1 0 1945.61 64.79 5 1 0 1855.11 75.09 -5 -1 0 1950.60 62.79 5 -1 0 1633.74 88.89 6 1 0 69.79 4.40 6 1 0 68.99 3.00 -6 -1 0 61.99 4.80 -6 -1 0 74.99 3.50 6 -1 0 79.49 3.60 -6 -1 0 73.09 3.10 6 -1 0 72.19 3.50 6 -1 0 75.39 3.70 6 -1 0 71.59 3.00 -6 -1 0 72.79 3.80 6 -1 0 68.09 4.30 -6 -1 0 77.89 3.00 6 1 0 79.09 3.50 6 1 0 72.79 3.40 6 1 0 74.39 2.90 -6 1 0 77.49 3.60 6 1 0 73.39 3.60 -6 1 0 72.09 3.10 -6 -1 0 72.69 3.20 -6 1 0 74.79 3.10 -6 1 0 76.69 5.10 -6 1 0 72.59 3.80 -6 1 0 79.59 3.00 7 1 0 29.70 2.00 -7 -1 0 33.20 1.90 -7 1 0 31.10 1.90 7 -1 0 28.40 2.10 7 1 0 31.20 2.20 -7 -1 0 35.70 3.30 7 1 0 31.90 2.20 7 1 0 37.50 3.20 -7 1 0 32.00 2.20 -7 -1 0 37.20 2.00 7 1 0 32.50 1.60 7 -1 0 34.30 1.80 7 -1 0 31.00 2.30 7 -1 0 33.00 1.50 7 -1 0 29.20 3.00 -7 1 0 33.10 1.90 -7 1 0 35.20 3.40 -7 -1 0 36.50 2.40 7 1 0 35.50 1.80 7 -1 0 34.10 2.30 8 1 0 30.80 2.40 8 -1 0 35.10 2.60 -8 1 0 35.80 2.10 -8 1 0 38.20 2.20 -8 -1 0 35.50 2.60 8 -1 0 34.80 2.60 -8 1 0 39.80 3.80 8 1 0 32.50 3.20 -8 -1 0 37.50 2.10 8 -1 0 30.80 3.20 -8 -1 0 34.20 2.10 8 1 0 35.10 2.40 8 -1 0 35.10 2.40 8 -1 0 34.20 1.90 8 1 0 33.10 1.90 -8 -1 0 37.90 3.60 8 1 0 37.30 2.60 -8 1 0 35.00 2.50 -9 1 0 142.49 5.80 -9 1 0 141.89 7.00 -9 1 0 149.88 5.90 9 1 0 140.09 6.20 -9 -1 0 147.49 9.40 9 -1 0 134.09 6.30 -9 -1 0 151.28 5.90 9 1 0 146.69 6.40 9 1 0 135.29 8.00 9 -1 0 150.88 8.20 -9 -1 0 148.29 5.90 9 1 0 147.29 6.60 9 -1 0 141.09 6.40 9 -1 0 131.79 6.60 -9 -1 0 148.09 7.20 -10 -1 0 47.40 2.70 -10 -1 0 38.10 2.60 -10 1 0 42.90 2.60 10 1 0 41.60 3.10 10 -1 0 46.50 4.20 -10 -1 0 40.10 3.20 10 -1 0 41.30 3.20 10 1 0 42.90 4.30 10 1 0 49.90 3.30 11 1 0 131.39 7.90 -11 -1 0 124.09 5.50 11 -1 0 120.79 6.30 -11 1 0 121.49 5.50 11 1 0 131.39 6.30 11 -1 0 135.39 8.00 12 1 0 5.00 1.60 12 1 0 2.80 1.90 12 -1 0 8.20 2.40 12 -1 0 3.40 1.30 13 -1 0 2.90 2.00 13 1 0 9.20 2.70 13 1 0 6.70 1.80 13 -1 0 8.60 2.10 0 -2 0 8756.82 322.37 0 2 0 9556.24 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156.98 5.50 1 -3 0 150.18 5.20 -1 -3 0 129.89 5.60 1 3 0 154.18 5.30 2 3 0 635.84 21.20 2 -3 0 632.24 25.20 -2 -3 0 632.94 21.20 -2 -3 0 651.03 21.80 -2 3 0 643.44 22.10 2 3 0 619.44 20.60 -2 -3 0 605.54 30.20 2 3 0 630.04 20.50 -2 3 0 623.74 20.40 -2 3 0 633.74 25.20 2 3 0 631.84 20.50 2 -3 0 644.34 22.10 -2 3 0 642.84 21.10 2 -3 0 604.54 21.40 -2 -3 0 643.64 21.20 2 -3 0 642.54 21.10 2 -3 0 651.63 21.00 2 -3 0 624.44 20.70 2 -3 0 590.14 25.40 -2 3 0 634.04 21.50 2 3 0 596.94 21.80 2 -3 0 691.43 30.50 -2 -3 0 657.63 21.80 -2 3 0 641.04 30.40 -2 -3 0 612.04 21.20 2 -3 0 617.94 21.80 -2 -3 0 646.24 21.80 3 -3 0 28.90 1.50 3 3 0 32.10 1.50 3 3 0 33.80 1.70 -3 3 0 33.40 1.80 -3 -3 0 33.20 1.60 3 -3 0 34.10 2.60 3 -3 0 30.40 1.80 -3 3 0 33.20 1.50 3 3 0 32.40 1.60 -3 -3 0 32.70 1.50 3 3 0 37.00 2.10 -3 3 0 32.90 1.90 3 -3 0 32.70 1.60 3 3 0 30.80 1.50 3 3 0 33.20 1.70 -3 3 0 31.20 2.50 3 -3 0 34.90 2.20 3 -3 0 32.00 1.80 -3 -3 0 31.60 1.50 3 -3 0 34.80 1.70 -3 3 0 31.00 1.80 3 3 0 33.50 1.60 -3 3 0 31.50 1.50 3 -3 0 32.10 1.80 3 3 0 31.30 1.60 4 -3 0 531.95 18.70 4 3 0 528.15 18.30 4 -3 0 521.35 18.10 4 -3 0 510.05 17.50 -4 3 0 527.75 17.40 4 3 0 546.35 17.80 4 -3 0 534.25 18.10 4 -3 0 510.05 25.50 4 3 0 522.05 17.10 4 3 0 514.75 17.30 4 3 0 530.25 17.70 -4 -3 0 465.25 17.70 4 3 0 536.35 18.10 4 3 0 520.85 21.40 -4 3 0 449.46 25.50 -4 3 0 535.65 18.10 -4 3 0 530.65 17.50 4 -3 0 529.35 17.50 -4 3 0 536.55 17.10 -4 3 0 542.85 18.70 -4 3 0 520.15 21.00 -4 -3 0 536.15 18.40 4 -3 0 530.05 17.40 -4 -3 0 525.85 17.80 -4 -3 0 438.76 25.30 4 3 0 520.65 17.20 4 -3 0 522.15 21.60 4 -3 0 537.75 21.00 -5 -3 0 96.09 5.60 -5 3 0 86.39 4.30 5 -3 0 86.49 3.90 5 3 0 89.49 3.90 5 -3 0 93.19 4.30 5 -3 0 90.79 3.50 5 3 0 89.69 4.70 5 3 0 88.49 3.70 5 3 0 86.79 3.60 5 -3 0 89.09 4.00 5 3 0 88.29 3.70 5 -3 0 97.99 5.70 -5 3 0 87.09 4.00 -5 3 0 83.29 5.50 -5 -3 0 88.09 3.70 -5 -3 0 89.49 3.60 5 -3 0 87.19 4.80 5 -3 0 89.69 3.70 -5 3 0 88.09 3.50 -5 -3 0 87.49 3.90 5 3 0 88.19 3.50 -5 3 0 88.79 3.50 -5 -3 0 89.59 3.70 5 3 0 90.49 3.80 -5 3 0 87.69 3.50 6 -3 0 55.99 3.30 6 -3 0 66.99 3.30 6 -3 0 63.39 3.20 6 3 0 58.79 3.90 -6 3 0 64.79 3.40 6 -3 0 65.99 2.80 -6 -3 0 59.79 2.80 6 3 0 64.39 3.00 -6 3 0 66.39 2.80 -6 3 0 52.79 4.40 -6 3 0 61.19 2.80 -6 -3 0 60.89 2.90 -6 -3 0 66.59 3.10 6 3 0 59.69 2.90 6 -3 0 66.79 3.40 6 -3 0 59.29 3.90 6 3 0 63.09 2.70 6 3 0 64.39 2.90 -6 -3 0 63.59 3.20 -6 -3 0 72.29 4.60 6 3 0 60.39 3.10 6 -3 0 63.69 2.70 7 -3 0 12.10 1.10 7 3 0 11.00 1.10 7 3 0 13.00 2.00 -7 -3 0 13.20 1.40 -7 -3 0 10.40 1.30 -7 3 0 12.20 1.30 -7 3 0 9.10 1.90 7 -3 0 9.30 1.40 -7 3 0 10.10 1.30 7 -3 0 10.80 1.90 7 -3 0 11.50 1.50 -7 3 0 10.10 1.10 7 3 0 12.70 1.50 7 3 0 8.80 1.30 7 -3 0 10.60 1.50 7 3 0 12.40 1.10 -7 -3 0 11.00 2.10 -7 -3 0 8.40 1.10 7 3 0 9.90 1.30 8 3 0 28.30 2.00 -8 -3 0 25.40 2.20 8 -3 0 23.90 2.20 8 -3 0 27.40 3.00 8 -3 0 26.40 2.30 8 3 0 24.80 1.60 -8 3 0 26.00 1.80 8 3 0 23.70 2.80 -8 -3 0 30.20 3.20 8 3 0 26.70 2.10 8 3 0 27.00 2.00 -8 3 0 25.40 1.70 -8 3 0 25.80 2.10 -8 3 0 26.40 3.10 8 -3 0 28.40 2.20 8 -3 0 24.20 1.60 8 3 0 24.30 1.70 -8 -3 0 25.00 1.80 -8 -3 0 28.70 2.00 -9 3 0 93.89 4.00 9 3 0 89.39 4.60 -9 3 0 95.19 4.10 9 3 0 86.59 4.50 -9 -3 0 88.29 5.00 -9 -3 0 85.19 4.20 -9 3 0 94.09 4.90 9 3 0 88.79 4.30 -9 -3 0 88.29 4.10 9 -3 0 92.79 6.00 9 3 0 81.19 5.70 9 -3 0 93.69 5.00 9 -3 0 85.59 4.70 10 3 0 40.10 2.80 -10 -3 0 41.90 2.60 10 -3 0 41.70 4.10 10 3 0 40.00 2.90 10 -3 0 43.80 3.20 10 3 0 43.10 4.00 -10 -3 0 36.50 3.10 -10 -3 0 35.40 2.50 -10 3 0 38.10 2.50 10 3 0 37.20 2.90 11 3 0 29.10 2.60 11 3 0 27.20 3.80 -11 -3 0 18.80 2.00 11 -3 0 28.10 2.80 11 -3 0 22.90 3.60 12 3 0 0.20 1.60 12 -3 0 1.50 1.80 12 -3 0 0.70 1.20 12 3 0 3.60 1.40 13 -3 0 19.70 3.60 13 -3 0 17.20 2.80 13 3 0 18.40 2.60 13 3 0 16.30 3.40 0 -4 0 5745.93 189.38 0 4 0 5470.95 184.08 0 -4 0 5431.46 177.58 0 -4 0 5459.05 183.88 0 -4 0 5651.13 262.37 0 4 0 5564.54 183.68 0 4 0 5468.85 177.48 0 -4 0 5537.45 182.28 0 4 0 6038.50 189.58 0 -4 0 4719.73 187.38 0 4 0 5722.23 262.37 -1 -4 0 2176.98 70.59 -1 4 0 2116.69 66.69 1 4 0 2144.99 71.29 -1 4 0 1979.60 68.39 1 4 0 2010.40 68.39 1 4 0 1977.60 66.29 -1 -4 0 2191.28 71.49 1 -4 0 2211.18 71.59 1 -4 0 1894.91 81.59 1 4 0 2155.68 69.69 -1 4 0 2072.89 98.69 -1 -4 0 2063.99 66.79 -1 4 0 2044.20 68.99 -1 4 0 2078.89 70.99 1 -4 0 2014.70 70.49 1 -4 0 2033.70 68.99 1 4 0 2091.89 99.09 -1 -4 0 2042.90 98.49 1 -4 0 2017.40 66.69 1 -4 0 2094.19 68.39 1 -4 0 2141.69 98.69 -1 -4 0 2124.89 69.79 2 -4 0 953.20 36.50 2 -4 0 914.31 31.60 -2 -4 0 922.81 43.80 -2 4 0 947.61 31.00 -2 -4 0 924.01 31.60 2 -4 0 903.81 29.90 2 4 0 906.51 29.80 2 -4 0 875.11 43.90 2 -4 0 912.11 31.00 -2 4 0 902.31 30.60 -2 4 0 915.21 29.60 -2 4 0 936.51 31.90 -2 -4 0 923.31 30.70 2 -4 0 954.60 30.60 2 4 0 902.41 29.70 2 -4 0 935.81 30.40 2 4 0 905.01 30.70 -2 4 0 918.11 36.50 2 4 0 932.51 43.80 -2 -4 0 919.01 31.60 2 -4 0 965.10 31.90 2 4 0 897.01 31.60 -2 4 0 902.61 43.90 2 -4 0 891.51 36.80 2 4 0 919.71 30.70 -2 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0.50 4 -4 0 1.10 1.00 5 -4 0 52.59 3.90 -5 -4 0 50.89 2.40 -5 -4 0 50.69 3.70 5 -4 0 52.39 2.80 -5 4 0 53.69 2.90 -5 4 0 54.29 2.40 5 -4 0 51.39 2.90 -5 -4 0 57.69 2.60 -5 4 0 51.09 2.90 5 4 0 53.59 2.50 5 -4 0 47.00 2.40 -5 -4 0 58.39 2.60 5 4 0 47.20 3.20 5 4 0 52.99 2.40 5 -4 0 55.69 2.40 -5 4 0 53.09 2.40 5 4 0 51.79 2.50 -5 4 0 49.99 3.90 5 -4 0 48.30 2.80 5 4 0 52.79 2.40 5 4 0 56.59 2.60 5 4 0 54.19 2.60 5 -4 0 51.99 3.40 -5 -4 0 53.69 2.60 5 4 0 51.29 2.50 6 4 0 518.75 17.30 6 -4 0 505.05 18.10 6 4 0 519.15 18.40 -6 4 0 500.05 17.10 6 4 0 494.05 21.60 -6 4 0 513.85 17.50 6 4 0 516.75 18.10 6 4 0 504.75 17.40 -6 -4 0 502.85 17.80 -6 4 0 534.85 21.10 6 4 0 512.55 17.80 -6 4 0 514.55 26.10 6 4 0 483.35 17.10 -6 -4 0 512.15 25.70 6 -4 0 512.45 21.80 -6 -4 0 500.15 17.20 6 -4 0 509.05 18.30 6 -4 0 515.65 17.30 -6 -4 0 520.25 18.50 -6 -4 0 525.05 17.90 6 -4 0 510.25 17.80 6 -4 0 546.35 21.00 7 4 0 2.30 0.80 -7 -4 0 2.30 1.20 7 4 0 1.70 0.70 -7 4 0 2.90 0.90 7 4 0 4.30 0.90 -7 4 0 3.30 0.70 -7 4 0 4.00 0.80 7 -4 0 3.40 1.00 7 4 0 3.00 0.70 7 -4 0 2.70 1.00 7 -4 0 2.60 0.90 7 4 0 2.70 1.20 -7 -4 0 2.40 0.80 -7 -4 0 3.70 0.90 -7 4 0 3.90 1.50 7 -4 0 2.90 0.70 7 -4 0 4.70 1.00 7 -4 0 5.10 0.80 7 4 0 2.40 0.70 -7 -4 0 3.50 0.80 7 -4 0 0.30 1.00 8 4 0 45.70 2.40 8 4 0 41.50 2.30 8 -4 0 40.50 2.90 -8 4 0 48.30 4.40 -8 4 0 46.60 2.50 8 -4 0 45.80 3.80 -8 4 0 47.20 2.40 -8 4 0 44.00 2.90 8 4 0 48.30 3.70 -8 -4 0 43.90 2.60 8 -4 0 41.90 3.00 8 -4 0 43.40 2.40 -8 -4 0 45.50 4.10 8 4 0 44.90 2.70 8 -4 0 42.40 2.90 8 4 0 46.70 2.80 8 4 0 41.20 2.50 -8 -4 0 40.90 2.50 9 4 0 4.80 1.70 -9 -4 0 2.40 1.20 9 -4 0 0.20 1.40 9 4 0 3.20 1.00 9 -4 0 4.60 1.40 -9 -4 0 2.40 0.90 9 4 0 2.50 1.00 -9 4 0 3.10 1.00 9 -4 0 2.20 1.10 -9 -4 0 2.30 0.90 9 4 0 2.50 1.10 10 -4 0 188.28 9.90 -10 -4 0 165.08 7.30 -10 -4 0 173.08 8.80 10 4 0 183.48 9.70 10 -4 0 172.68 7.90 -10 4 0 181.68 7.10 10 4 0 175.68 7.50 -10 -4 0 177.18 7.20 10 4 0 182.68 7.80 11 4 0 6.00 2.10 11 4 0 5.50 1.50 -11 -4 0 4.80 1.20 11 -4 0 4.40 2.10 11 -4 0 3.40 1.50 12 -4 0 1.60 1.30 12 4 0 0.00 0.90 -12 -4 0 0.00 0.80 12 4 0 1.80 1.80 12 -4 0 1.70 1.80 13 -4 0 6.10 1.90 13 4 0 8.20 2.50 13 4 0 9.70 2.00 13 -4 0 7.10 2.50 -1 5 0 15.20 1.10 1 5 0 15.10 1.10 1 -5 0 14.20 0.90 1 -5 0 16.40 1.10 1 5 0 15.50 0.90 1 -5 0 12.80 1.20 -1 5 0 17.00 1.20 1 5 0 13.90 1.20 -1 5 0 15.60 1.10 -1 -5 0 15.40 1.00 1 5 0 14.20 0.90 1 -5 0 13.60 1.30 -1 -5 0 12.10 1.30 -1 -5 0 14.90 1.50 -1 5 0 16.80 1.50 1 5 0 15.80 1.50 -1 5 0 13.10 1.10 1 -5 0 15.90 1.60 1 -5 0 13.60 1.00 -1 -5 0 14.30 0.70 -1 -5 0 15.10 0.90 2 5 0 29.10 2.20 -2 -5 0 27.30 1.40 -2 -5 0 30.90 1.20 -2 5 0 32.20 2.00 -2 5 0 31.10 1.70 2 -5 0 30.60 1.80 2 5 0 29.40 1.40 2 -5 0 30.90 2.40 -2 -5 0 28.20 1.40 2 -5 0 27.80 1.70 2 -5 0 27.80 1.70 2 5 0 26.50 1.20 -2 -5 0 29.70 2.20 -2 5 0 28.10 1.50 2 5 0 29.30 1.40 2 5 0 27.10 1.60 2 -5 0 31.30 1.90 -2 -5 0 28.70 1.40 -2 5 0 28.80 1.60 -2 5 0 29.20 2.30 2 -5 0 28.10 1.50 2 -5 0 27.60 1.80 -2 5 0 27.90 1.70 -2 -5 0 32.10 1.80 -3 -5 0 8.90 0.80 -3 5 0 8.20 0.90 3 -5 0 8.40 1.60 3 -5 0 7.90 1.10 3 5 0 8.00 0.80 3 5 0 7.00 0.90 -3 5 0 9.80 1.00 -3 -5 0 9.10 0.80 3 -5 0 7.10 1.00 -3 -5 0 8.80 0.80 3 5 0 9.40 1.10 3 -5 0 8.90 1.10 3 -5 0 9.10 1.00 -3 -5 0 6.90 1.00 -3 5 0 9.90 1.20 -3 5 0 6.80 1.00 -3 5 0 6.60 1.00 3 -5 0 7.20 0.90 -3 -5 0 9.70 1.30 -3 -5 0 9.10 0.80 3 -5 0 7.40 1.00 3 5 0 9.30 1.10 3 5 0 8.50 1.00 3 -5 0 9.40 1.00 3 5 0 9.90 1.10 -3 5 0 9.90 1.60 4 -5 0 29.80 1.60 4 -5 0 24.10 1.80 4 5 0 24.60 1.70 -4 -5 0 26.40 2.30 -4 5 0 27.80 1.90 -4 -5 0 26.40 1.70 -4 -5 0 26.30 1.50 4 5 0 23.20 2.00 -4 5 0 25.30 2.40 -4 -5 0 28.00 1.50 4 5 0 24.40 1.60 -4 5 0 25.00 1.50 -4 5 0 25.50 1.50 4 5 0 23.10 1.60 4 -5 0 26.70 2.60 4 -5 0 22.80 1.60 -4 -5 0 26.80 1.40 4 -5 0 27.00 1.80 4 -5 0 28.00 1.80 4 5 0 25.90 1.70 -4 5 0 25.50 1.90 4 -5 0 26.00 2.20 4 -5 0 25.50 1.90 4 5 0 24.90 1.40 -4 5 0 28.40 1.90 -4 -5 0 25.30 1.50 5 -5 0 36.20 2.00 -5 -5 0 36.90 2.10 -5 -5 0 38.30 2.00 -5 -5 0 37.70 2.00 5 -5 0 33.70 2.70 -5 -5 0 40.80 2.10 5 -5 0 39.70 2.10 5 5 0 41.40 2.10 -5 -5 0 37.20 2.10 5 5 0 36.30 2.00 5 -5 0 39.70 2.40 5 -5 0 36.80 2.30 5 5 0 39.50 2.00 -5 5 0 38.10 3.20 -5 -5 0 37.10 1.90 5 -5 0 35.90 2.40 5 5 0 39.90 2.20 -5 5 0 35.40 2.30 -5 5 0 39.20 2.00 5 5 0 35.80 2.10 5 5 0 36.50 2.10 -5 5 0 40.30 2.00 5 -5 0 30.90 2.20 -5 -5 0 39.20 3.00 5 5 0 40.80 2.70 -6 -5 0 153.78 6.10 -6 -5 0 153.88 6.10 6 -5 0 154.28 7.00 6 -5 0 150.58 6.60 6 5 0 149.99 5.80 -6 -5 0 156.48 5.90 6 5 0 153.28 6.00 6 5 0 152.78 5.90 -6 -5 0 147.99 5.80 6 -5 0 153.38 6.20 6 -5 0 144.49 6.30 6 5 0 145.69 5.80 -6 -5 0 144.69 8.60 6 -5 0 146.49 6.00 -6 5 0 161.18 5.80 6 5 0 149.19 7.40 6 5 0 150.98 6.10 6 5 0 143.09 5.70 -6 5 0 154.78 7.00 6 -5 0 150.98 5.70 -6 -5 0 154.18 6.20 -6 5 0 145.19 8.90 -6 -5 0 150.78 5.90 6 -5 0 139.79 7.50 -6 5 0 158.38 5.80 7 -5 0 10.90 1.20 7 -5 0 10.70 2.00 -7 5 0 9.20 2.00 -7 -5 0 11.80 2.20 -7 5 0 10.90 1.20 7 5 0 11.80 1.40 -7 -5 0 13.60 1.50 -7 -5 0 12.30 1.20 -7 5 0 10.20 1.20 -7 -5 0 10.60 1.30 7 -5 0 10.80 1.40 7 -5 0 11.50 1.10 7 -5 0 9.80 1.50 7 5 0 12.90 1.50 7 5 0 11.60 1.80 -7 5 0 10.20 1.40 7 5 0 9.80 1.30 7 5 0 10.90 1.20 7 5 0 10.90 1.10 7 -5 0 6.50 1.40 7 -5 0 9.50 1.50 7 5 0 11.40 1.30 -7 -5 0 11.80 1.30 8 -5 0 0.00 0.80 8 -5 0 0.90 0.60 -8 -5 0 0.50 0.60 -8 5 0 0.00 0.70 8 5 0 0.30 1.00 -8 -5 0 1.60 1.20 -8 5 0 0.60 0.70 8 -5 0 0.00 0.50 8 -5 0 0.00 1.10 8 5 0 1.60 0.70 -8 -5 0 0.40 0.60 8 5 0 0.00 0.50 -8 5 0 0.30 1.20 -8 5 0 0.10 0.60 8 5 0 0.90 0.70 -8 -5 0 0.00 0.70 8 -5 0 0.00 0.80 8 5 0 0.70 0.60 8 -5 0 0.00 0.80 8 5 0 0.00 0.60 9 5 0 26.20 3.30 -9 -5 0 27.50 2.10 9 -5 0 29.60 3.60 9 -5 0 27.10 2.60 -9 -5 0 22.80 2.00 9 5 0 28.50 2.40 9 5 0 26.50 2.00 -9 5 0 27.80 2.10 9 5 0 24.60 2.10 -9 -5 0 28.70 2.10 -10 -5 0 71.79 3.90 10 -5 0 77.59 4.60 10 5 0 72.29 4.10 10 5 0 83.99 5.70 -10 -5 0 73.39 3.90 -10 5 0 73.89 3.80 10 -5 0 76.69 5.70 10 5 0 77.69 4.10 -11 -5 0 19.70 2.00 11 5 0 20.70 3.20 11 5 0 22.90 2.40 11 -5 0 17.50 2.60 -11 -5 0 21.10 2.00 11 -5 0 21.00 3.40 12 -5 0 0.00 1.10 12 5 0 0.00 1.00 12 5 0 0.00 1.30 12 -5 0 0.00 1.60 -12 -5 0 0.70 0.90 13 -5 0 0.00 1.50 13 -5 0 2.50 2.20 13 5 0 4.70 2.30 13 5 0 2.50 1.40 0 -6 0 3108.09 97.59 0 6 0 2985.40 97.39 0 6 0 2879.51 93.19 0 6 0 2810.72 99.59 0 -6 0 2860.81 99.29 0 6 0 2866.81 138.49 0 -6 0 2836.82 137.49 0 6 0 2875.81 96.29 0 -6 0 2918.31 94.09 0 -6 0 3059.69 100.59 -1 6 0 565.74 19.90 1 6 0 585.64 28.20 1 -6 0 568.04 20.40 1 6 0 590.44 19.20 1 -6 0 599.14 23.70 1 6 0 592.04 19.70 -1 -6 0 583.94 18.80 -1 6 0 576.94 19.80 1 -6 0 572.74 19.90 -1 -6 0 591.14 20.20 -1 6 0 589.34 20.40 1 6 0 578.24 19.90 -1 6 0 580.04 28.20 -1 -6 0 569.84 19.70 1 6 0 578.24 20.10 1 -6 0 635.54 28.30 1 -6 0 587.34 20.50 -1 -6 0 533.95 20.50 1 -6 0 588.04 19.00 -1 6 0 574.24 19.20 -1 -6 0 578.64 28.20 2 -6 0 10.30 1.20 2 -6 0 16.00 1.40 2 6 0 12.20 1.50 2 -6 0 12.60 1.40 2 6 0 13.10 1.20 2 6 0 15.80 1.00 -2 -6 0 13.60 1.50 -2 6 0 13.60 1.30 -2 6 0 11.90 1.30 2 -6 0 14.40 1.20 2 -6 0 13.00 1.70 -2 6 0 12.90 1.20 -2 -6 0 13.10 1.40 -2 -6 0 14.50 0.80 -2 6 0 12.90 1.10 2 6 0 13.00 1.20 -2 -6 0 12.90 0.90 2 -6 0 12.50 1.30 2 -6 0 12.90 1.20 -2 6 0 13.20 1.60 2 6 0 14.60 0.90 -2 -6 0 13.80 0.90 3 -6 0 146.29 6.00 -3 -6 0 152.78 5.50 -3 6 0 148.89 5.90 -3 6 0 148.19 6.80 3 6 0 146.29 6.50 3 -6 0 152.88 6.80 3 -6 0 161.98 8.60 3 6 0 149.29 5.20 -3 -6 0 153.48 8.10 -3 -6 0 151.48 5.60 3 -6 0 155.18 6.00 3 6 0 147.79 5.50 -3 6 0 134.49 8.20 3 6 0 142.79 5.80 3 6 0 146.79 5.60 3 -6 0 153.58 6.80 -3 6 0 148.89 5.60 -3 -6 0 144.89 5.50 3 -6 0 149.88 5.60 3 -6 0 152.18 6.10 -3 -6 0 152.78 5.60 -3 6 0 147.89 5.50 -3 -6 0 152.98 6.00 -3 6 0 162.38 6.10 3 -6 0 148.39 5.70 4 6 0 120.99 4.50 -4 6 0 123.59 5.20 -4 -6 0 130.09 5.10 -4 6 0 124.89 5.80 -4 -6 0 120.29 7.00 4 -6 0 126.19 5.10 4 6 0 123.79 5.10 -4 -6 0 121.99 4.70 4 -6 0 114.49 5.90 4 -6 0 119.29 5.30 -4 6 0 117.69 7.20 -4 -6 0 124.69 4.80 4 -6 0 118.49 5.20 4 -6 0 125.89 4.90 4 -6 0 134.29 7.40 -4 6 0 121.59 4.80 4 -6 0 121.59 4.90 -4 -6 0 126.39 4.80 -4 6 0 119.79 4.70 4 -6 0 122.89 5.70 4 6 0 124.29 5.70 4 6 0 119.09 5.10 -4 -6 0 118.49 4.60 4 6 0 119.39 4.80 5 -6 0 804.92 29.20 -5 -6 0 850.31 27.80 -5 -6 0 818.62 27.70 5 -6 0 817.82 28.40 -5 -6 0 859.71 28.60 5 -6 0 840.42 33.00 -5 6 0 801.82 40.00 5 6 0 818.52 27.90 5 6 0 817.02 26.90 5 -6 0 811.22 28.50 5 6 0 819.02 33.30 -5 -6 0 843.82 28.50 5 6 0 797.52 28.50 -5 6 0 814.72 27.50 5 6 0 803.22 26.90 -5 -6 0 838.82 28.60 -5 -6 0 818.72 27.90 -5 6 0 800.02 26.80 5 -6 0 801.72 27.40 -5 6 0 785.92 32.90 -5 -6 0 811.02 39.70 5 -6 0 807.32 27.40 5 -6 0 806.42 33.60 -6 6 0 26.10 1.70 -6 6 0 23.80 2.80 -6 -6 0 27.10 2.70 6 6 0 23.10 1.80 6 -6 0 27.30 1.70 6 -6 0 25.20 2.10 6 6 0 23.60 1.60 -6 -6 0 22.80 1.80 -6 6 0 24.00 2.00 -6 -6 0 24.90 1.70 -6 6 0 26.20 1.70 6 6 0 23.90 1.90 6 -6 0 27.20 2.60 6 -6 0 23.50 2.00 -6 -6 0 24.00 1.70 6 -6 0 23.70 2.00 6 -6 0 23.90 1.70 -6 -6 0 26.10 1.60 6 6 0 24.50 1.70 6 6 0 22.40 2.40 -6 -6 0 22.60 1.90 6 -6 0 21.80 2.00 -6 -6 0 23.70 1.80 6 6 0 25.70 1.80 -7 -6 0 0.80 0.60 7 -6 0 0.60 0.70 -7 6 0 0.00 1.00 7 6 0 0.00 0.50 7 -6 0 0.00 0.70 7 -6 0 0.00 0.80 7 -6 0 0.00 0.60 7 -6 0 0.10 0.50 -7 6 0 0.00 0.70 -7 -6 0 0.00 0.90 7 -6 0 0.00 0.90 -7 -6 0 0.30 0.70 -7 -6 0 0.00 0.50 -7 -6 0 0.00 0.50 -7 -6 0 0.50 0.60 7 6 0 1.40 1.00 7 6 0 0.00 0.50 7 6 0 0.90 0.70 7 -6 0 0.80 0.90 -7 6 0 0.40 0.60 7 6 0 0.00 0.50 -7 -6 0 0.00 0.50 -7 6 0 0.00 0.60 -8 -6 0 0.00 0.60 -8 6 0 1.10 0.90 8 6 0 0.00 0.60 8 -6 0 1.10 1.00 8 -6 0 0.60 1.20 -8 6 0 0.20 0.70 -8 -6 0 0.30 1.10 8 -6 0 0.30 1.00 -8 6 0 0.60 0.70 8 -6 0 0.50 0.60 8 6 0 0.40 1.00 8 6 0 0.00 0.70 -8 -6 0 0.60 0.70 -8 -6 0 1.40 0.70 8 6 0 0.50 0.70 8 6 0 0.40 0.70 -8 -6 0 0.20 0.70 -8 -6 0 1.60 0.80 8 -6 0 0.00 0.60 9 6 0 292.37 14.10 9 6 0 287.57 11.70 9 6 0 305.17 11.30 9 -6 0 310.07 11.90 -9 -6 0 315.17 11.90 -9 -6 0 312.07 11.60 -9 6 0 305.07 11.00 -9 -6 0 284.37 11.10 9 -6 0 311.57 14.60 10 -6 0 24.30 3.50 10 6 0 18.40 3.00 10 6 0 21.00 2.20 -10 -6 0 23.50 2.10 10 -6 0 19.00 2.50 -10 -6 0 22.50 2.10 11 -6 0 3.00 1.40 11 6 0 4.20 1.40 -11 -6 0 4.60 1.20 -11 -6 0 0.80 1.00 11 6 0 4.00 1.80 11 -6 0 0.00 1.50 12 6 0 3.20 1.90 12 6 0 1.30 1.20 12 -6 0 2.00 1.50 12 -6 0 1.20 1.80 -12 -6 0 0.00 0.80 1 7 0 1747.03 58.19 -1 -7 0 1726.73 59.89 1 7 0 1746.93 56.29 1 7 0 1782.02 58.29 -1 7 0 1788.22 60.09 -1 7 0 1717.53 56.29 1 -7 0 1780.62 83.09 1 -7 0 1765.52 60.09 1 7 0 1740.73 82.99 -1 7 0 1716.73 82.99 -1 -7 0 1761.32 82.89 1 -7 0 1710.43 59.99 1 -7 0 1734.73 58.49 1 -7 0 1786.02 69.39 -1 -7 0 1744.53 58.29 1 7 0 1799.02 59.89 1 -7 0 1723.63 56.39 -1 -7 0 1753.22 56.09 -1 7 0 1702.93 58.09 -1 7 0 1754.52 58.49 -2 -7 0 190.88 7.70 -2 7 0 193.48 7.40 2 -7 0 197.88 10.50 2 7 0 196.98 7.20 2 7 0 201.58 7.00 2 7 0 187.88 7.40 2 -7 0 188.68 7.50 -2 -7 0 199.88 7.10 2 -7 0 191.68 6.90 -2 7 0 199.68 7.30 -2 -7 0 202.48 7.20 -2 7 0 199.68 10.50 -2 7 0 199.58 7.10 2 -7 0 181.48 7.40 2 -7 0 214.88 8.80 2 7 0 199.68 10.40 2 7 0 200.98 7.10 -2 7 0 188.58 7.50 2 -7 0 185.88 8.30 2 -7 0 194.98 7.70 -2 -7 0 196.68 6.50 -2 -7 0 203.88 10.40 -3 7 0 15.00 1.40 3 7 0 11.40 1.60 3 -7 0 14.30 2.00 -3 7 0 13.10 1.20 3 -7 0 14.00 1.30 -3 -7 0 12.50 1.00 -3 -7 0 15.00 1.00 -3 7 0 14.50 1.40 -3 7 0 12.40 1.70 3 -7 0 13.10 1.20 3 7 0 16.60 1.50 -3 7 0 12.70 1.40 3 -7 0 12.80 1.50 3 -7 0 14.50 1.40 -3 -7 0 13.60 1.50 3 -7 0 15.20 1.60 3 7 0 12.60 1.20 -3 -7 0 13.70 0.90 3 -7 0 14.50 1.40 -3 -7 0 13.80 1.00 3 -7 0 12.60 1.40 -3 -7 0 11.80 1.60 -3 7 0 12.80 1.20 3 7 0 13.60 1.00 3 7 0 14.10 1.20 -3 -7 0 15.10 1.00 -4 7 0 16.00 1.30 -4 7 0 16.90 1.60 -4 -7 0 13.70 1.50 -4 -7 0 17.30 1.10 4 -7 0 14.10 1.50 4 7 0 15.90 1.10 -4 -7 0 17.10 1.20 4 -7 0 14.70 1.60 -4 -7 0 17.20 2.00 -4 7 0 16.20 1.30 4 -7 0 15.40 1.60 4 -7 0 16.30 1.50 4 -7 0 14.40 1.50 4 -7 0 13.20 1.40 -4 -7 0 18.20 1.20 4 7 0 16.80 1.40 4 7 0 15.30 1.50 4 7 0 15.60 1.50 -4 -7 0 16.80 1.10 -4 7 0 15.90 2.10 4 -7 0 13.50 1.70 5 -7 0 387.36 16.90 -5 -7 0 392.66 14.10 -5 -7 0 400.16 13.80 -5 7 0 398.26 16.60 -5 -7 0 326.57 14.30 5 7 0 396.26 13.30 -5 -7 0 389.06 13.70 5 -7 0 399.76 14.90 5 7 0 387.66 16.60 -5 -7 0 405.36 14.20 5 -7 0 394.76 16.50 5 -7 0 399.46 13.80 5 -7 0 393.86 14.50 5 -7 0 408.26 14.40 5 7 0 384.86 13.60 -5 7 0 390.26 20.40 5 7 0 383.76 14.10 5 -7 0 417.26 13.90 -5 7 0 404.46 13.50 -5 7 0 403.36 13.80 6 7 0 45.30 2.60 6 -7 0 52.19 3.70 -6 7 0 47.20 4.10 6 -7 0 49.90 3.00 -6 7 0 46.30 3.00 6 -7 0 51.99 3.20 6 -7 0 51.29 2.80 6 7 0 47.60 2.40 -6 -7 0 48.00 2.70 6 7 0 48.10 2.80 -6 7 0 49.50 2.50 6 -7 0 46.30 3.00 -6 -7 0 48.60 2.80 -6 -7 0 46.00 2.80 6 -7 0 49.20 3.10 6 7 0 48.40 3.30 -6 -7 0 49.00 2.40 6 7 0 47.30 2.80 -6 7 0 44.70 2.50 -6 -7 0 52.59 2.60 -6 -7 0 50.89 2.50 6 -7 0 50.79 2.60 -7 -7 0 126.49 5.30 -7 7 0 127.99 5.10 7 -7 0 124.89 5.90 -7 -7 0 129.09 7.90 7 -7 0 121.89 6.00 -7 7 0 125.49 8.20 7 7 0 112.49 5.20 7 -7 0 122.39 5.10 -7 7 0 122.19 6.20 7 -7 0 126.79 5.70 -7 -7 0 121.19 5.50 -7 7 0 126.59 5.20 7 7 0 127.79 5.10 7 -7 0 129.59 6.90 -7 -7 0 116.69 5.40 7 7 0 125.99 5.50 -7 -7 0 126.79 5.10 -7 -7 0 132.19 5.30 7 7 0 134.59 6.60 7 -7 0 125.09 5.40 -8 -7 0 35.00 2.50 -8 -7 0 35.40 2.30 8 -7 0 37.60 2.20 -8 7 0 34.80 2.30 8 7 0 36.70 2.60 8 -7 0 35.70 2.30 -8 -7 0 34.50 2.40 8 7 0 35.60 3.30 8 -7 0 38.90 3.00 -8 -7 0 32.90 2.40 8 7 0 38.50 2.40 8 -7 0 35.10 2.80 8 7 0 34.60 2.40 -8 -7 0 35.20 3.70 8 -7 0 36.20 3.50 -9 -7 0 0.80 0.90 -9 -7 0 2.70 1.10 9 7 0 3.20 1.10 9 -7 0 2.10 1.70 9 -7 0 0.00 1.00 -9 7 0 2.10 0.90 9 7 0 3.90 1.60 10 -7 0 163.08 9.40 10 7 0 177.88 9.20 -10 -7 0 156.78 6.90 10 -7 0 169.78 7.70 10 7 0 172.58 7.10 -10 -7 0 156.78 7.20 11 7 0 15.60 2.90 -11 -7 0 12.90 1.90 11 -7 0 14.10 2.30 11 -7 0 15.50 3.10 -11 -7 0 11.70 1.80 -12 -7 0 0.80 1.10 12 -7 0 1.90 1.50 12 7 0 1.90 1.60 12 -7 0 0.20 1.80 0 8 0 2709.33 88.09 0 -8 0 2833.92 108.59 0 8 0 2692.23 90.89 0 -8 0 2784.82 88.19 0 -8 0 2677.53 129.89 0 -8 0 2731.43 91.39 0 8 0 2774.92 93.89 0 8 0 2813.22 91.39 0 -8 0 2717.03 93.79 0 8 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4.10 -5 9 0 71.99 3.50 -5 -9 0 77.79 3.10 5 -9 0 75.29 4.00 5 -9 0 78.59 3.70 5 9 0 73.39 3.70 -5 -9 0 80.19 3.40 -5 9 0 78.19 3.60 5 -9 0 79.49 4.50 5 9 0 74.19 3.90 -5 -9 0 77.49 3.30 -5 -9 0 64.39 3.80 6 9 0 8.00 1.40 6 -9 0 6.60 1.20 -6 -9 0 9.30 1.40 6 -9 0 7.90 1.30 -6 9 0 7.40 1.10 -6 9 0 7.50 1.90 6 -9 0 7.20 1.40 -6 -9 0 5.80 1.20 -6 9 0 6.30 1.40 6 9 0 7.40 1.20 6 -9 0 6.80 1.40 6 -9 0 5.70 1.40 6 -9 0 7.10 1.40 -6 9 0 6.60 1.20 -7 -9 0 118.19 5.50 7 9 0 115.99 5.30 7 9 0 112.79 5.40 7 -9 0 121.89 6.70 -7 9 0 122.39 5.10 7 -9 0 115.59 5.90 -7 9 0 122.59 6.20 7 -9 0 111.89 5.10 -7 -9 0 116.89 5.50 7 -9 0 114.39 5.50 7 -9 0 122.39 5.40 -7 9 0 115.89 5.00 8 -9 0 0.40 0.80 -8 9 0 1.40 0.90 8 -9 0 2.00 1.20 -8 -9 0 0.90 0.90 8 9 0 1.50 1.00 -8 -9 0 0.50 0.90 8 -9 0 0.20 1.20 9 9 0 3.30 1.20 -9 -9 0 1.50 1.00 -9 9 0 2.50 1.00 -9 -9 0 2.30 1.10 9 -9 0 4.50 1.50 9 -9 0 3.50 1.70 -10 -9 0 0.00 0.90 10 -9 0 0.60 1.50 -10 -9 0 1.80 1.10 10 -9 0 0.90 1.10 -11 -9 0 39.10 2.90 11 -9 0 37.70 3.40 11 -9 0 38.50 4.20 12 -9 0 6.80 2.10 12 -9 0 11.80 2.90 -12 -9 0 12.40 2.00 0 -10 0 214.58 7.90 0 10 0 213.18 7.80 0 -10 0 207.28 7.00 0 10 0 197.98 8.00 0 -10 0 205.08 7.90 0 -10 0 203.48 8.40 0 10 0 210.08 7.80 0 10 0 205.78 7.80 0 10 0 203.58 11.20 -1 -10 0 634.34 22.40 -1 10 0 638.44 31.50 -1 -10 0 618.84 21.90 1 -10 0 638.84 21.00 1 10 0 630.34 31.40 1 10 0 657.83 21.90 -1 -10 0 618.84 23.00 1 10 0 635.14 21.50 -1 10 0 645.64 22.60 -1 10 0 656.63 22.20 1 -10 0 628.04 22.60 1 10 0 666.33 22.30 1 10 0 633.54 22.20 1 -10 0 619.44 23.00 -1 10 0 647.54 21.50 -1 10 0 636.94 22.10 1 -10 0 627.44 22.20 2 -10 0 0.00 0.50 2 -10 0 0.10 0.60 -2 -10 0 0.00 0.70 2 10 0 0.00 0.50 2 10 0 0.50 0.80 -2 10 0 0.40 0.90 2 10 0 0.00 0.40 2 10 0 0.30 0.50 2 -10 0 0.60 0.80 2 10 0 0.30 0.70 -2 -10 0 0.00 0.50 -2 -10 0 0.00 0.40 2 -10 0 0.00 0.60 -2 10 0 0.00 0.60 -2 10 0 0.70 0.70 -3 -10 0 27.00 1.50 3 10 0 29.80 2.80 3 -10 0 23.80 2.00 3 10 0 26.20 2.00 -3 -10 0 30.30 2.40 3 -10 0 25.80 2.00 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1.50 1.00 -7 10 0 2.50 0.90 7 -10 0 2.50 1.40 7 -10 0 0.00 0.70 -8 -10 0 116.99 5.50 -8 10 0 117.29 5.10 8 10 0 116.39 5.30 8 -10 0 107.49 6.60 8 -10 0 107.49 5.40 -8 -10 0 101.49 5.40 8 -10 0 106.89 5.20 -9 -10 0 27.60 2.40 -9 -10 0 35.50 2.80 9 10 0 33.90 2.60 9 -10 0 32.70 3.70 9 -10 0 32.60 2.90 10 10 0 0.00 0.90 -10 -10 0 0.00 0.80 10 -10 0 0.90 1.70 10 -10 0 0.00 1.20 -10 -10 0 1.20 1.20 11 -10 0 68.79 5.70 11 -10 0 70.49 4.60 -11 -10 0 62.39 4.00 0 11 0 3.20 0.80 0 11 0 2.00 0.60 0 11 0 4.80 1.00 0 11 0 2.40 1.20 0 11 0 5.00 1.10 0 -11 0 4.50 1.20 -1 -11 0 194.88 7.60 1 11 0 192.48 8.00 -1 11 0 201.68 7.90 -1 11 0 210.38 7.80 1 11 0 188.48 10.90 -1 -11 0 197.18 8.40 1 -11 0 200.88 8.40 1 11 0 208.28 7.80 -1 11 0 203.98 7.70 1 11 0 209.48 7.60 1 -11 0 197.58 7.80 1 -11 0 191.68 7.80 -1 -11 0 203.48 7.60 -1 11 0 191.78 11.00 2 -11 0 0.00 0.60 -2 11 0 0.00 0.60 -2 -11 0 0.70 0.60 2 11 0 1.20 0.80 -2 11 0 0.00 0.90 2 -11 0 0.00 0.70 -2 -11 0 1.10 0.50 2 -11 0 0.00 0.50 -2 -11 0 0.50 0.90 2 11 0 0.60 1.00 2 11 0 0.00 0.50 2 11 0 0.00 0.60 -2 11 0 0.90 0.80 2 -11 0 0.00 0.90 3 11 0 199.68 8.00 3 11 0 209.48 11.50 -3 11 0 218.08 8.00 -3 11 0 207.38 8.20 -3 -11 0 194.98 7.70 3 -11 0 213.38 7.60 3 -11 0 207.88 8.40 3 11 0 196.78 8.30 -3 11 0 213.08 11.70 3 -11 0 211.48 8.30 3 -11 0 220.08 8.80 -3 -11 0 198.18 8.60 3 -11 0 201.98 8.40 4 11 0 177.48 7.70 -4 11 0 189.98 7.30 -4 11 0 183.48 10.80 -4 11 0 196.88 7.50 4 -11 0 177.98 7.80 4 11 0 178.78 7.40 4 -11 0 194.98 7.70 4 -11 0 192.08 7.20 4 -11 0 182.38 7.80 -4 -11 0 166.58 7.80 4 -11 0 194.58 8.00 -5 -11 0 13.80 2.00 -5 11 0 11.90 1.50 5 -11 0 10.00 1.60 5 11 0 11.50 1.70 5 -11 0 12.50 1.60 5 11 0 11.00 1.60 -5 11 0 12.30 1.50 -5 11 0 12.50 2.50 5 -11 0 9.70 1.70 5 -11 0 12.10 1.70 5 -11 0 13.00 1.80 6 -11 0 2.40 1.00 -6 -11 0 4.30 1.30 6 -11 0 2.20 1.20 6 11 0 2.00 1.10 -6 11 0 3.30 1.00 6 11 0 2.90 1.00 6 -11 0 0.00 0.80 -6 11 0 2.60 1.00 6 -11 0 0.90 1.00 6 -11 0 0.30 1.00 -7 -11 0 160.68 7.30 7 -11 0 178.38 7.40 7 11 0 171.18 7.40 7 -11 0 159.38 6.90 -7 11 0 160.78 6.80 -7 -11 0 133.19 7.20 7 11 0 177.28 7.10 7 -11 0 178.38 8.70 7 -11 0 170.38 7.20 8 -11 0 38.10 2.80 -8 -11 0 34.20 2.80 -8 -11 0 34.80 2.90 8 11 0 39.30 2.80 8 -11 0 36.60 3.60 -8 11 0 33.30 2.50 8 -11 0 35.50 2.80 -9 -11 0 12.40 2.10 9 11 0 15.00 2.00 9 -11 0 11.20 2.40 9 -11 0 12.40 2.10 -9 -11 0 13.00 2.00 10 11 0 2.40 1.20 10 -11 0 3.90 1.50 10 -11 0 3.00 1.80 -10 -11 0 0.10 1.10 -11 -11 0 12.50 2.10 11 -11 0 15.80 3.10 11 -11 0 14.30 2.50 0 -12 0 271.57 10.20 0 -12 0 275.17 10.20 0 -12 0 275.27 11.00 0 12 0 265.17 14.50 0 12 0 266.67 10.50 0 12 0 272.97 10.20 1 12 0 377.76 19.40 1 12 0 368.16 13.40 1 12 0 354.76 13.80 -1 12 0 360.16 13.70 -1 12 0 379.36 13.40 1 -12 0 370.96 13.70 1 -12 0 371.06 14.40 -1 -12 0 385.56 13.50 1 -12 0 379.26 13.90 -1 -12 0 371.96 14.40 -1 12 0 379.66 19.40 -2 12 0 13.30 2.30 2 12 0 11.70 1.70 2 12 0 13.10 1.70 2 -12 0 14.50 1.90 -2 12 0 16.40 1.80 2 12 0 14.30 2.10 2 -12 0 16.00 1.60 -2 12 0 12.50 1.60 2 -12 0 16.60 1.70 -2 -12 0 13.60 1.40 -2 -12 0 10.40 1.80 -3 12 0 84.69 4.20 3 12 0 84.49 5.90 3 12 0 84.29 4.50 3 12 0 85.69 4.30 3 -12 0 85.89 4.70 -3 12 0 87.09 4.20 3 -12 0 89.69 4.50 3 -12 0 85.89 4.30 3 -12 0 84.69 4.40 -3 -12 0 93.09 4.80 -3 12 0 89.09 6.10 4 -12 0 1.10 1.00 4 -12 0 0.80 1.00 -4 12 0 0.40 1.20 4 -12 0 2.40 1.10 4 12 0 1.70 0.90 4 -12 0 1.40 1.00 4 12 0 2.70 1.10 -4 12 0 1.90 0.90 -4 12 0 3.70 1.00 4 -12 0 2.00 0.80 -4 -12 0 0.20 1.00 5 -12 0 53.69 3.00 -5 12 0 55.59 3.20 5 -12 0 48.90 3.30 5 -12 0 59.39 3.60 5 -12 0 56.49 3.40 5 12 0 51.89 3.20 -5 12 0 53.39 3.10 5 12 0 49.20 3.30 -5 -12 0 48.40 3.40 -6 12 0 23.80 2.00 -6 -12 0 22.90 2.50 6 12 0 25.50 2.30 6 -12 0 23.90 2.50 6 -12 0 25.10 2.30 6 12 0 22.70 2.30 6 -12 0 29.10 2.30 -6 12 0 29.60 2.30 6 -12 0 27.10 2.50 -7 12 0 20.30 1.90 7 12 0 14.90 2.00 7 -12 0 14.00 2.00 7 -12 0 20.00 2.30 -7 -12 0 19.20 2.40 7 -12 0 15.20 2.00 7 12 0 16.70 2.20 -7 -12 0 22.00 2.30 -8 -12 0 25.90 2.60 8 12 0 25.80 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105.79 5.00 -7 -2 -9 102.69 5.10 7 -2 9 102.29 5.20 7 2 -9 98.29 5.10 -7 2 9 102.09 6.10 7 -2 9 106.69 5.00 -7 2 9 100.59 5.20 7 -2 9 101.59 6.60 7 2 9 105.49 5.00 -7 -2 9 107.89 5.00 -7 2 -9 105.49 7.20 -7 2 -9 93.59 5.00 -7 -2 9 102.69 6.10 7 -2 -9 110.29 5.10 7 2 9 123.69 6.70 7 -2 -9 115.29 6.50 7 -2 -9 111.49 5.30 7 2 9 100.09 5.00 8 2 -9 78.19 4.10 8 -2 9 72.09 4.30 -8 -2 -9 75.49 4.10 8 -2 9 76.39 4.20 8 -2 9 81.09 5.70 8 2 -9 76.29 4.30 -8 -2 -9 69.29 4.10 8 2 -9 72.59 4.10 8 2 -9 78.49 5.40 -8 2 9 76.39 5.20 -8 -2 9 68.79 5.00 8 2 9 77.59 4.20 8 2 9 75.89 5.50 -8 -2 9 74.59 4.10 -8 2 -9 74.49 4.20 8 -2 -9 73.89 4.10 -8 2 -9 73.09 4.10 8 -2 -9 83.99 5.40 8 -2 -9 74.89 4.20 9 -2 9 74.59 5.80 9 2 -9 70.69 4.20 -9 -2 -9 75.19 4.20 -9 -2 -9 71.29 4.30 9 -2 9 74.19 4.50 9 2 -9 77.49 4.20 -9 2 9 78.59 5.40 9 2 -9 77.79 4.40 9 2 -9 83.39 5.60 9 -2 -9 69.09 4.30 9 -2 -9 80.29 5.60 9 2 9 76.89 5.80 -9 2 -9 74.69 4.40 9 2 9 81.39 4.50 -9 2 -9 79.89 4.30 9 -2 -9 76.89 4.30 -9 -2 9 74.69 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385.76 16.50 1 3 9 390.36 13.70 -1 3 -9 382.56 19.00 1 -3 -9 411.96 19.90 -1 3 -9 398.56 14.10 1 -3 -9 381.96 13.80 1 3 9 378.86 16.90 1 3 9 393.36 13.70 -1 3 -9 384.46 13.50 -1 3 -9 416.76 19.00 -1 3 -9 388.66 14.20 -1 3 -9 391.16 16.70 2 3 -9 90.59 4.40 -2 -3 -9 87.89 3.70 2 -3 9 83.09 4.20 2 -3 9 93.79 4.20 2 -3 9 95.49 5.20 2 3 -9 89.29 3.90 2 -3 9 91.99 4.10 -2 -3 -9 86.79 3.80 -2 -3 -9 97.79 4.10 2 3 -9 82.79 4.50 2 3 -9 89.19 4.10 2 3 -9 89.99 3.50 -2 3 9 89.79 4.00 -2 3 9 89.39 3.90 -2 3 9 90.59 4.00 -2 -3 -9 89.49 3.80 -2 -3 -9 87.69 3.70 -2 3 9 86.09 5.40 -2 -3 -9 84.49 3.50 -2 3 9 87.59 4.90 -2 -3 -9 88.19 4.70 -2 3 9 83.99 3.80 -2 -3 9 84.89 4.40 2 3 9 93.09 5.10 -2 3 -9 86.89 3.80 -2 -3 9 80.29 4.80 -2 3 -9 80.39 4.00 -2 -3 9 89.49 4.30 2 -3 -9 86.69 3.40 -2 3 -9 82.39 3.80 2 -3 -9 85.79 4.00 2 -3 -9 88.29 3.20 -2 -3 9 86.69 4.10 -2 -3 9 89.89 4.40 2 -3 -9 89.89 4.20 -2 3 -9 91.29 4.90 -2 3 -9 86.19 3.70 2 3 9 88.69 5.60 -2 3 -9 86.29 4.90 2 -3 -9 98.89 5.70 2 3 9 85.79 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31.30 2.50 7 3 -10 34.40 2.60 7 -3 -10 34.20 2.60 7 -3 -10 38.70 2.80 -7 3 -10 34.10 2.70 7 3 10 34.90 2.60 -7 3 -10 28.20 3.40 -7 -3 10 35.00 2.70 7 3 10 40.40 3.90 -7 -3 10 47.30 3.60 -7 3 -10 34.30 2.60 8 3 -10 1.20 1.10 8 3 -10 1.00 1.10 8 -3 10 0.90 1.60 -8 3 10 1.90 1.00 8 -3 10 2.20 1.20 -8 3 10 1.80 1.40 -8 -3 -10 2.00 1.10 -8 -3 -10 0.60 1.00 -8 -3 10 0.60 1.30 -8 3 -10 0.40 1.10 -8 -3 10 2.80 1.20 8 3 10 0.30 1.40 8 3 10 0.80 1.10 8 -3 -10 2.00 1.00 -8 3 -10 1.70 1.10 8 -3 -10 0.00 1.20 8 -3 -10 0.30 1.00 9 -3 10 79.89 4.90 9 -3 10 87.29 6.40 -9 3 10 76.89 4.40 9 3 -10 80.69 4.70 9 3 -10 81.09 4.50 -9 -3 -10 76.29 4.60 -9 -3 -10 83.49 4.60 -9 3 10 78.99 5.60 -9 3 -10 82.79 4.60 9 3 10 87.59 4.70 9 3 10 94.19 6.40 -9 3 -10 74.99 4.60 -9 -3 10 79.69 4.50 9 -3 -10 89.39 4.80 9 -3 -10 81.49 4.60 9 -3 -10 79.39 5.80 -9 -3 10 90.89 5.80 10 3 -10 29.30 2.80 10 -3 10 33.90 3.20 10 -3 10 40.50 4.40 -10 3 10 37.60 3.90 10 3 -10 30.30 2.90 10 3 -10 28.70 3.80 -10 -3 -10 33.60 2.90 10 3 -10 32.50 2.80 10 3 10 34.10 3.00 -10 3 -10 33.80 3.00 -10 -3 10 32.50 2.90 -10 -3 10 35.00 3.80 10 -3 -10 37.50 3.10 10 -3 -10 34.60 3.00 10 -3 -10 29.30 3.70 10 3 10 32.90 4.30 11 3 -10 11.80 2.20 11 -3 10 15.80 2.60 -11 3 10 16.20 3.00 11 3 -10 16.80 3.10 -11 -3 -10 13.20 2.30 11 -3 10 12.00 3.20 11 3 -10 14.70 2.40 -11 -3 10 17.10 2.40 11 -3 -10 17.50 2.40 11 -3 -10 12.10 2.20 11 3 10 15.00 3.30 -11 3 -10 16.20 2.50 11 -3 -10 14.50 3.20 11 3 10 15.50 2.40 -11 -3 10 15.40 2.80 0 4 10 13.00 1.10 0 -4 -10 9.90 1.20 0 4 -10 10.70 1.40 0 4 10 12.60 1.40 0 4 10 11.80 1.20 0 -4 10 12.90 1.90 0 -4 -10 13.20 1.40 0 -4 -10 10.70 1.40 0 4 10 10.90 1.20 0 4 10 13.00 1.80 0 4 -10 13.40 1.50 0 -4 10 11.10 1.50 0 4 10 12.30 1.30 0 4 -10 13.70 1.70 0 -4 10 9.00 1.40 0 -4 -10 10.10 1.20 0 4 -10 12.90 1.30 0 -4 10 10.10 1.40 0 4 -10 10.00 1.40 0 -4 -10 12.30 1.40 0 4 10 12.50 1.90 0 -4 -10 13.40 1.10 -1 4 10 57.59 3.80 -1 4 10 65.89 3.00 -1 -4 -10 55.19 2.90 1 4 -10 59.69 3.10 1 -4 10 56.89 3.20 -1 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10 57.39 2.80 2 4 -10 52.89 3.10 2 4 -10 56.29 3.40 2 4 -10 50.69 2.90 2 -4 10 43.90 3.10 2 4 10 53.39 2.40 -2 -4 10 54.09 3.10 2 -4 -10 51.99 2.90 2 4 10 53.89 4.10 2 4 10 54.19 3.70 -2 -4 10 51.79 3.70 -2 4 -10 52.89 3.00 -2 -4 10 52.69 3.20 -2 4 -10 54.29 2.70 -2 4 -10 57.99 2.90 -2 4 -10 53.29 2.90 -2 4 -10 51.29 3.60 -2 -4 10 53.79 3.10 2 -4 -10 53.99 2.40 2 4 10 55.19 2.70 2 4 10 54.39 2.80 2 -4 -10 53.59 3.10 3 4 -10 10.80 1.40 3 4 -10 11.40 1.60 -3 -4 -10 12.80 1.60 3 -4 10 11.40 1.60 -3 -4 -10 15.60 1.40 -3 -4 -10 14.40 1.50 -3 -4 -10 10.10 1.70 -3 4 10 13.60 2.00 3 -4 10 12.80 1.80 -3 4 10 13.90 2.00 -3 4 10 14.10 1.40 3 4 -10 14.00 1.70 3 4 -10 12.90 1.20 3 -4 10 13.10 2.10 -3 -4 -10 12.30 1.20 3 -4 10 12.50 1.70 -3 -4 -10 14.10 1.30 -3 4 10 11.50 1.40 -3 4 10 12.30 1.50 -3 -4 10 11.80 1.90 -3 4 -10 11.30 1.90 -3 4 -10 13.70 1.60 3 4 10 15.50 1.60 -3 -4 10 13.90 1.70 -3 -4 10 11.40 1.60 -3 4 -10 15.70 1.50 3 4 10 11.40 1.90 -3 4 -10 12.90 1.60 -3 -4 10 15.00 1.70 3 -4 -10 13.80 1.70 3 4 10 13.60 1.30 -3 4 -10 12.90 1.30 -3 -4 10 13.30 1.60 -4 4 10 203.68 8.00 -4 4 10 188.88 7.70 4 4 -10 206.08 7.70 4 -4 10 204.78 10.10 -4 4 10 197.28 11.20 4 4 -10 206.18 8.40 4 -4 10 192.28 8.10 4 -4 10 198.48 8.60 -4 4 10 194.98 8.20 4 -4 10 201.38 8.20 -4 -4 -10 210.68 8.10 -4 -4 -10 174.48 9.40 -4 4 10 185.88 9.50 -4 -4 -10 201.78 7.70 4 4 -10 197.58 7.90 -4 4 -10 192.98 7.80 -4 -4 10 210.38 9.70 4 -4 -10 198.18 8.30 -4 -4 10 202.68 8.00 -4 4 -10 204.88 7.30 -4 -4 10 208.68 8.50 4 4 10 198.88 7.70 -4 -4 10 199.68 8.20 4 4 10 201.08 9.80 -4 4 -10 213.08 9.90 -4 4 -10 191.88 8.10 -5 4 10 84.59 4.30 5 -4 10 87.29 4.80 -5 4 10 86.49 4.20 5 -4 10 94.99 5.90 5 4 -10 92.49 4.40 5 -4 10 88.39 4.50 -5 4 10 81.29 6.00 -5 4 10 88.79 4.50 -5 -4 -10 91.69 4.30 -5 -4 -10 84.09 4.40 5 -4 10 94.39 4.70 -5 4 10 97.99 5.50 5 4 -10 94.69 4.70 -5 -4 10 95.19 4.50 -5 4 -10 85.69 4.30 -5 -4 10 82.29 5.20 5 4 10 86.79 4.20 5 -4 -10 91.99 4.40 -5 -4 10 85.19 4.60 5 4 10 92.89 5.60 -5 4 -10 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13.80 0 5 -10 390.06 14.10 0 -5 10 388.36 16.60 0 -5 -10 354.46 13.30 0 5 10 395.46 13.30 0 -5 10 398.06 13.70 0 5 -10 377.96 13.20 0 -5 10 371.96 14.00 0 5 10 361.56 19.40 0 5 10 378.16 13.20 0 5 10 369.56 16.40 0 -5 -10 379.36 14.00 0 -5 -10 344.37 15.80 0 -5 10 359.06 14.40 0 5 10 386.76 13.30 -1 -5 -10 172.98 6.70 -1 -5 -10 173.28 7.00 -1 5 10 177.88 8.80 1 5 -10 175.38 8.60 -1 -5 -10 187.48 8.40 -1 5 10 189.58 7.20 1 -5 10 166.78 7.70 -1 5 10 174.78 6.90 1 5 -10 188.28 7.30 -1 -5 -10 181.48 7.00 -1 5 10 181.98 10.20 1 -5 10 188.68 9.00 1 -5 10 181.08 7.50 -1 5 10 185.78 7.00 1 5 -10 176.18 7.10 -1 -5 -10 170.58 7.00 1 5 -10 180.68 7.50 1 -5 10 190.08 7.40 1 5 -10 176.98 6.80 -1 5 10 180.68 6.90 -1 -5 -10 183.48 7.30 1 -5 -10 172.68 7.10 1 -5 -10 185.68 6.40 -1 -5 10 172.48 7.70 1 5 10 178.78 6.80 -1 5 -10 179.98 7.30 -1 5 -10 186.78 7.00 -1 5 -10 175.68 7.30 1 5 10 176.68 8.70 1 -5 -10 190.68 6.80 -1 5 -10 186.28 8.90 -1 -5 10 182.08 7.50 1 5 10 176.28 7.00 1 -5 -10 195.18 8.10 -1 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7.60 1.70 -5 5 10 7.40 2.00 5 5 -10 6.60 1.40 5 -5 10 6.10 1.40 -5 -5 -10 5.90 1.30 5 -5 10 7.70 1.90 5 -5 10 4.80 1.30 -5 -5 -10 8.70 1.40 5 5 -10 8.80 1.30 -5 5 10 5.40 1.20 5 5 -10 7.10 1.40 -5 -5 10 7.90 1.50 -5 5 -10 8.70 1.50 -5 5 -10 7.00 1.40 5 5 10 8.30 1.80 5 -5 -10 7.40 1.30 5 5 10 7.80 1.30 -5 -5 10 6.90 1.40 5 -5 -10 9.10 1.60 -5 -5 10 5.20 1.50 6 -5 10 44.10 3.30 -6 5 10 49.70 3.80 6 -5 10 54.89 4.40 6 5 -10 41.10 2.90 -6 -5 -10 47.00 3.00 -6 5 10 41.20 2.80 -6 -5 -10 43.00 3.00 -6 5 10 45.40 3.00 6 5 -10 47.60 3.20 6 -5 -10 41.20 3.10 -6 5 -10 42.40 3.00 6 5 10 36.60 3.70 6 5 10 47.30 2.90 6 -5 -10 50.69 3.00 -6 -5 10 56.79 3.20 -6 -5 10 50.69 3.90 -6 5 -10 46.70 3.10 -7 5 10 74.79 4.00 7 5 -10 72.59 4.10 -7 -5 -10 74.39 4.10 -7 5 10 85.39 5.20 7 -5 10 69.29 4.40 -7 -5 -10 74.89 4.30 7 5 -10 69.39 4.40 7 -5 10 75.99 5.60 -7 -5 10 75.89 5.10 -7 5 -10 77.69 4.30 -7 5 -10 74.59 4.30 7 -5 -10 65.49 4.20 7 -5 -10 75.29 4.10 -7 -5 10 75.29 4.10 7 5 10 73.39 3.90 7 5 10 94.69 5.70 8 5 -10 8.30 1.80 8 -5 10 7.60 1.70 -8 -5 -10 5.90 1.50 8 5 -10 6.80 1.50 8 -5 10 8.50 2.30 -8 5 10 6.40 1.40 -8 -5 -10 4.60 1.40 -8 5 10 5.80 1.80 -8 -5 10 5.00 1.70 8 5 10 6.30 2.10 8 -5 -10 7.60 1.60 -8 5 -10 6.40 1.60 -8 -5 10 5.50 1.40 -8 5 -10 4.80 1.50 8 -5 -10 6.60 1.60 9 -5 10 15.80 3.10 9 5 -10 17.40 2.30 9 -5 10 11.90 2.20 -9 5 10 12.10 2.40 9 5 -10 11.90 2.10 -9 -5 -10 15.90 2.30 9 5 10 16.70 3.10 9 -5 -10 12.10 2.10 -9 5 -10 8.60 1.90 9 -5 -10 15.20 2.10 -9 -5 10 12.50 2.00 -9 5 -10 10.90 2.00 9 -5 -10 12.10 2.60 -9 -5 10 13.80 2.50 10 5 -10 7.20 1.80 10 5 -10 2.70 1.40 10 -5 10 3.40 2.10 10 -5 10 5.90 1.90 -10 5 10 3.70 1.70 -10 -5 -10 3.00 1.40 -10 -5 10 4.90 1.90 10 -5 -10 4.50 2.00 10 -5 -10 2.40 1.40 10 5 10 5.70 2.30 -10 5 -10 3.80 1.50 -10 -5 10 0.70 1.00 10 -5 -10 3.70 1.50 11 -5 10 57.89 5.60 11 5 -10 56.49 4.10 -11 5 10 55.79 4.80 11 5 -10 50.49 3.70 11 -5 10 51.39 4.20 -11 -5 10 47.80 3.70 11 -5 -10 53.19 3.90 11 5 10 57.49 5.40 11 -5 -10 48.60 3.70 -11 -5 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5 14 92.09 5.80 -4 -5 14 81.39 5.60 5 5 -14 66.49 4.30 5 -5 14 68.09 5.50 5 -5 14 65.49 4.30 5 5 -14 64.89 4.10 -5 5 14 61.79 3.80 -5 -5 -14 68.09 4.10 -5 -5 -14 61.69 3.70 -5 5 14 65.59 5.00 -5 5 -14 62.09 4.10 5 5 14 68.89 5.30 -5 -5 14 71.19 5.20 5 -5 -14 65.59 4.20 -5 5 -14 68.89 4.00 -5 -5 14 59.19 4.00 6 -5 14 10.70 2.70 6 -5 14 14.10 2.30 -6 5 14 16.10 2.80 6 5 -14 16.40 2.30 6 5 -14 9.10 2.00 -6 -5 -14 11.60 1.90 -6 5 14 14.60 2.00 -6 5 -14 9.60 1.90 -6 -5 14 14.40 2.70 6 5 14 12.10 2.70 6 -5 -14 13.40 2.20 -6 -5 14 17.00 2.40 7 5 -14 13.50 2.30 7 -5 14 15.10 2.60 -7 -5 -14 11.60 2.00 -7 5 14 15.20 2.20 7 5 -14 11.80 2.20 -7 5 14 20.40 3.10 7 -5 14 10.60 2.80 -7 -5 14 13.50 2.70 -7 -5 14 14.10 2.10 7 -5 -14 13.60 2.20 7 5 14 19.20 3.40 -7 5 -14 11.70 2.10 8 5 -14 7.30 1.90 -8 -5 -14 6.80 1.70 -8 5 14 8.90 1.80 8 -5 14 1.40 1.40 -8 5 14 7.20 2.30 8 -5 14 3.80 2.30 8 5 -14 6.60 1.80 -8 5 -14 7.30 1.80 8 -5 -14 5.50 1.70 -8 -5 14 8.90 1.90 8 5 14 7.30 2.30 -8 -5 14 8.30 2.30 0 6 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3.10 -1 3 18 107.99 5.90 1 3 -18 114.39 5.90 1 -3 18 109.29 6.20 -1 3 18 115.39 7.70 1 -3 18 109.09 7.60 1 3 -18 118.49 6.10 1 -3 -18 121.79 6.10 -1 -3 18 108.89 6.20 1 3 18 120.29 6.10 -1 3 -18 120.59 5.80 -1 -3 18 118.69 7.70 1 3 18 121.19 7.80 2 -3 18 11.30 2.80 2 3 -18 16.50 2.50 2 3 -18 13.20 2.20 -2 3 18 11.80 2.80 2 -3 18 8.60 2.10 -2 3 18 17.40 2.40 2 -3 -18 11.40 2.10 2 3 18 8.60 1.90 2 3 18 15.40 3.10 -2 -3 18 12.50 2.90 -2 -3 18 10.50 2.10 -3 3 18 45.80 3.60 3 -3 18 42.50 3.70 -3 3 18 48.00 4.60 3 3 -18 51.29 3.90 3 -3 18 45.90 4.80 3 3 -18 46.50 3.60 3 -3 -18 45.20 3.60 3 3 18 51.29 3.70 -3 -3 18 41.00 4.60 3 3 18 49.00 4.80 -3 -3 18 42.00 3.60 4 3 -18 41.50 3.50 4 -3 18 36.20 3.60 4 -3 18 36.80 4.40 -4 3 18 39.10 4.30 -4 3 18 39.90 3.40 4 3 -18 40.90 3.70 4 3 18 44.30 3.50 4 -3 -18 43.60 3.70 -4 -3 18 47.60 3.70 4 3 18 35.20 4.40 -4 -3 18 45.60 4.60 0 4 18 76.59 4.60 0 4 18 84.19 6.20 0 -4 18 84.19 6.20 0 -4 18 75.19 4.90 0 4 -18 81.69 4.70 0 4 -18 75.39 4.70 1 -4 18 33.00 4.20 1 -4 18 35.50 3.40 -1 4 18 41.10 3.20 1 4 -18 38.70 3.20 1 4 -18 36.30 3.20 -1 4 18 38.30 4.20 1 4 18 35.50 3.10 -1 4 -18 33.60 2.90 1 -4 -18 33.40 3.10 -1 -4 18 33.10 4.00 1 4 18 41.10 4.30 -1 -4 18 33.60 3.20 -2 4 18 34.70 3.00 2 -4 18 33.00 3.20 2 -4 18 26.40 4.10 2 4 -18 30.60 3.10 -2 4 18 29.60 4.20 2 4 -18 31.10 3.10 2 -4 -18 32.80 3.00 -2 -4 18 37.30 4.10 -2 -4 18 34.30 3.20 2 4 18 30.10 4.20 -3 4 18 44.20 4.60 3 4 -18 43.50 3.60 3 -4 18 46.80 3.90 -3 4 18 52.79 3.70 3 -4 18 48.30 4.80 3 4 -18 44.80 3.80 -3 -4 18 48.40 4.80 3 4 18 47.70 4.80 3 -4 -18 42.80 3.70 -3 -4 18 49.99 3.90 -4 4 18 24.00 3.80 4 4 -18 24.20 3.00 4 -4 18 25.00 4.00 4 4 -18 20.80 3.00 4 -4 18 20.90 3.00 -4 4 18 23.80 2.90 -4 -4 18 32.40 4.10 4 4 18 23.50 3.80 4 -4 -18 23.10 3.00 -4 -4 18 26.30 3.10 0 -5 18 61.39 4.30 0 5 18 67.39 5.40 0 -5 18 54.39 5.20 0 5 -18 56.99 4.00 -1 5 18 71.89 5.70 1 -5 18 69.69 5.70 1 -5 18 70.99 4.70 1 5 -18 72.29 4.60 1 5 -18 67.59 4.40 1 5 18 75.89 5.80 1 -5 -18 70.59 4.40 -1 -5 18 62.39 5.70 -1 -5 18 62.09 4.60 -2 5 18 1.50 1.20 2 -5 18 6.10 1.90 2 -5 18 4.60 2.10 -2 5 18 0.00 1.60 2 5 -18 4.70 1.60 2 5 -18 4.60 1.70 2 -5 -18 2.60 1.50 -2 -5 18 2.40 1.60 2 5 18 1.20 1.80 -2 -5 18 2.00 2.00 3 5 -18 30.00 3.10 3 -5 18 31.70 3.60 -3 5 18 26.30 3.90 3 5 -18 29.30 3.20 3 -5 18 23.80 3.90 -3 5 18 27.10 3.00 3 5 18 29.50 4.20 3 -5 -18 29.00 3.00 -3 -5 18 24.80 3.10 -3 -5 18 32.10 4.10 0 6 18 16.70 3.20 0 -6 18 14.10 2.50 0 6 -18 18.60 2.50 0 -6 18 18.60 3.50 1 6 -18 11.50 2.20 1 -6 18 10.70 2.80 -1 6 18 13.70 3.00 1 -6 18 13.80 2.50 1 6 -18 13.80 2.40 1 -6 -18 11.80 2.10 1 6 18 9.50 2.70 -1 -6 18 12.60 2.40 -1 -6 18 13.10 2.90 2 6 -18 29.50 3.00 2 -6 18 31.50 4.40 -2 6 18 28.40 4.00 2 -6 18 27.30 3.30 2 6 -18 22.70 3.00 -2 -6 18 28.70 4.10 2 -6 -18 24.70 2.70 2 6 18 32.80 4.10 -2 -6 18 23.90 3.10 0 0 19 0.00 1.50 0 0 19 0.00 1.30 1 0 19 6.30 2.30 -1 0 19 5.20 2.10 1 0 19 6.00 1.90 1 0 -19 4.10 1.50 -1 0 19 2.20 1.40 2 0 19 10.60 2.20 2 0 19 14.10 3.10 2 0 -19 12.10 2.20 -2 0 19 10.40 2.80 -2 0 19 16.30 2.60 0 1 19 2.50 1.80 0 1 19 0.00 1.10 0 -1 19 1.90 2.00 0 -1 19 4.00 1.60 1 1 -19 12.10 2.10 -1 1 19 6.40 2.30 1 -1 19 9.40 2.10 1 -1 19 8.60 2.60 -1 1 19 6.00 1.80 1 1 19 9.50 2.10 1 1 19 8.50 2.70 -1 -1 19 9.30 2.10 1 -1 -19 11.20 2.00 -1 -1 19 13.10 2.90 2 -1 19 11.90 3.00 -2 1 19 17.60 2.60 -2 1 19 8.60 2.50 2 -1 19 13.10 2.30 2 1 -19 15.90 2.40 -2 -1 19 9.30 2.10 2 1 19 15.90 3.30 2 1 19 13.00 2.40 2 -1 -19 12.30 2.30 -2 -1 19 10.40 2.80 0 -2 19 5.70 2.30 0 -2 19 4.90 1.70 0 2 19 5.70 2.30 0 2 19 5.90 1.70 -1 2 19 1.00 1.70 1 2 -19 0.20 1.20 -1 2 19 2.10 1.40 1 -2 19 1.50 1.80 1 -2 19 0.90 1.30 -1 -2 19 0.70 1.30 1 2 19 1.50 1.30 1 -2 -19 2.10 1.30 -1 -2 19 0.50 1.60 1 2 19 1.20 1.80 -2 2 19 3.50 2.00 2 2 -19 5.60 1.80 2 -2 19 9.50 2.60 -2 2 19 8.60 2.00 2 -2 19 8.70 2.00 -2 -2 19 6.10 1.90 2 2 19 3.90 2.20 2 2 19 6.70 1.80 2 -2 -19 3.10 1.60 -2 -2 19 5.50 2.30 0 -3 19 7.00 2.40 0 -3 19 6.00 1.90 0 3 -19 6.20 1.80 0 3 19 4.40 2.30 0 3 19 9.90 2.10 -1 3 19 9.90 2.00 -1 3 19 7.50 2.40 1 3 -19 13.60 2.40 1 -3 19 10.50 2.80 1 -3 19 6.30 1.90 1 3 -19 10.30 2.10 -1 -3 19 3.70 1.60 1 3 19 7.20 2.40 1 3 19 9.10 2.00 1 -3 -19 9.70 1.90 -1 -3 19 7.90 2.60 ; _shelx_hkl_checksum 55050 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp Cl1 Cl 0.67351(6) 0.86966(5) 0.26962(4) 0.03129(14) Uani 1 1 d . . Cl2 Cl 0.40956(6) 0.96537(5) 0.32703(4) 0.03138(14) Uani 1 1 d . . Cl3 Cl 0.62253(7) 1.11445(5) 0.26947(4) 0.03527(15) Uani 1 1 d . . Si1 Si 0.61950(6) 0.98988(4) 0.35104(4) 0.02106(13) Uani 1 1 d . . N1 N 0.81082(19) 1.00905(13) 0.37711(12) 0.0210(4) Uani 1 1 d . . N2 N 0.60655(18) 0.99015(13) 0.47242(11) 0.0179(3) Uani 1 1 d . . C1 C 0.9090(2) 1.01516(17) 0.31089(16) 0.0267(4) Uani 1 1 d . . H1 H 0.8857 1.0141 0.2456 0.032 Uiso 1 1 calc R U C2 C 1.0407(2) 1.02278(18) 0.33615(18) 0.0286(5) Uani 1 1 d . . H2 H 1.1084 1.0266 0.2890 0.034 Uiso 1 1 calc R U C3 C 1.0745(2) 1.02485(18) 0.43180(18) 0.0285(5) Uani 1 1 d . . H3 H 1.1657 1.0288 0.4505 0.034 Uiso 1 1 calc R U C4 C 0.9747(2) 1.02119(17) 0.49909(17) 0.0249(4) Uani 1 1 d . . H4 H 0.9957 1.0246 0.5647 0.030 Uiso 1 1 calc R U C5 C 0.8429(2) 1.01242(15) 0.46910(15) 0.0196(4) Uani 1 1 d . . C6 C 0.7240(2) 1.00293(16) 0.53181(14) 0.0197(4) Uani 1 1 d . . H6A H 0.7350 0.9472 0.5744 0.024 Uiso 1 1 calc R U H6B H 0.7138 1.0610 0.5713 0.024 Uiso 1 1 calc R U C7 C 0.4874(2) 0.97350(15) 0.52792(14) 0.0184(4) Uani 1 1 d . . C8 C 0.4525(2) 0.87934(15) 0.55125(14) 0.0192(4) Uani 1 1 d . . C9 C 0.3357(2) 0.86421(17) 0.60328(15) 0.0237(4) Uani 1 1 d . . H9 H 0.3089 0.8007 0.6179 0.028 Uiso 1 1 calc R U C10 C 0.2581(2) 0.94010(18) 0.63401(16) 0.0256(4) Uani 1 1 d . . H10 H 0.1785 0.9287 0.6690 0.031 Uiso 1 1 calc R U C11 C 0.2973(2) 1.03317(18) 0.61338(16) 0.0250(4) Uani 1 1 d . . H11 H 0.2452 1.0851 0.6363 0.030 Uiso 1 1 calc R U C12 C 0.4117(2) 1.05185(16) 0.55964(14) 0.0216(4) Uani 1 1 d . . C13 C 0.4505(3) 1.15465(17) 0.53691(18) 0.0269(5) Uani 1 1 d . . H13 H 0.5366 1.1528 0.5008 0.032 Uiso 1 1 calc R U C14 C 0.4757(3) 1.2112(2) 0.6283(2) 0.0392(6) Uani 1 1 d . . H14A H 0.5119 1.2743 0.6124 0.059 Uiso 1 1 calc R U H14B H 0.5401 1.1766 0.6679 0.059 Uiso 1 1 calc R U H14C H 0.3913 1.2187 0.6629 0.059 Uiso 1 1 calc R U C15 C 0.3459(3) 1.2040(2) 0.4739(2) 0.0420(7) Uani 1 1 d . . H15A H 0.3792 1.2670 0.4547 0.063 Uiso 1 1 calc R U H15B H 0.2622 1.2115 0.5093 0.063 Uiso 1 1 calc R U H15C H 0.3296 1.1649 0.4174 0.063 Uiso 1 1 calc R U C16 C 0.5364(2) 0.79394(16) 0.52126(16) 0.0217(4) Uani 1 1 d . . H16 H 0.6163 0.8187 0.4863 0.026 Uiso 1 1 calc R U C17 C 0.5870(3) 0.73755(18) 0.60701(18) 0.0311(5) Uani 1 1 d . . H17A H 0.6525 0.6898 0.5861 0.047 Uiso 1 1 calc R U H17B H 0.5115 0.7053 0.6378 0.047 Uiso 1 1 calc R U H17C H 0.6295 0.7814 0.6521 0.047 Uiso 1 1 calc R U C18 C 0.4576(3) 0.72894(18) 0.45328(19) 0.0304(5) Uani 1 1 d . . H18A H 0.4282 0.7662 0.3982 0.046 Uiso 1 1 calc R U H18B H 0.3791 0.7029 0.4861 0.046 Uiso 1 1 calc R U H18C H 0.5151 0.6763 0.4322 0.046 Uiso 1 1 calc R U loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.0334(3) 0.0370(3) 0.0235(2) -0.0083(2) 0.0024(2) -0.0024(2) Cl2 0.0232(3) 0.0483(3) 0.0226(2) 0.0022(2) -0.00656(19) -0.0001(2) Cl3 0.0353(3) 0.0409(3) 0.0297(3) 0.0172(2) 0.0005(2) 0.0050(3) Si1 0.0207(3) 0.0281(3) 0.0143(2) 0.0028(2) -0.0008(2) 0.0007(2) N1 0.0218(8) 0.0235(9) 0.0178(8) 0.0013(6) 0.0015(7) -0.0004(7) N2 0.0149(8) 0.0242(8) 0.0147(7) 0.0012(6) 0.0002(6) -0.0012(7) C1 0.0277(11) 0.0304(11) 0.0219(9) 0.0024(8) 0.0059(9) -0.0011(9) C2 0.0232(10) 0.0324(12) 0.0303(11) 0.0016(10) 0.0087(9) 0.0000(9) C3 0.0190(10) 0.0317(12) 0.0348(12) 0.0016(9) 0.0014(9) -0.0019(9) C4 0.0214(10) 0.0273(11) 0.0260(10) 0.0015(9) -0.0018(8) -0.0024(8) C5 0.0189(9) 0.0196(9) 0.0205(9) 0.0011(7) 0.0012(7) -0.0003(7) C6 0.0173(9) 0.0260(10) 0.0157(8) 0.0003(7) -0.0010(7) -0.0013(8) C7 0.0158(9) 0.0249(10) 0.0147(8) -0.0007(7) -0.0004(7) -0.0014(8) C8 0.0189(9) 0.0214(10) 0.0174(9) -0.0009(7) -0.0012(7) -0.0011(8) C9 0.0211(9) 0.0275(10) 0.0224(9) -0.0008(8) 0.0012(8) -0.0060(8) C10 0.0193(10) 0.0370(12) 0.0206(10) -0.0031(9) 0.0032(8) -0.0035(9) C11 0.0210(10) 0.0321(11) 0.0220(9) -0.0065(9) 0.0015(8) 0.0037(9) C12 0.0218(10) 0.0234(10) 0.0195(9) -0.0010(7) -0.0031(8) 0.0009(8) C13 0.0295(11) 0.0205(10) 0.0307(11) -0.0008(8) 0.0008(9) 0.0015(9) C14 0.0472(16) 0.0302(12) 0.0403(15) -0.0093(11) 0.0003(12) -0.0044(11) C15 0.0445(16) 0.0293(13) 0.0521(17) 0.0070(12) -0.0097(13) 0.0027(11) C16 0.0208(10) 0.0207(9) 0.0235(10) 0.0003(8) 0.0013(8) -0.0005(8) C17 0.0310(12) 0.0286(11) 0.0336(12) 0.0055(9) -0.0041(10) 0.0028(10) C18 0.0312(12) 0.0264(12) 0.0336(12) -0.0084(9) -0.0025(10) 0.0001(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle N2 Si1 N1 83.46(8) N2 Si1 Cl3 123.28(7) N1 Si1 Cl3 88.58(6) N2 Si1 Cl1 124.39(7) N1 Si1 Cl1 87.84(6) Cl3 Si1 Cl1 111.20(4) N2 Si1 Cl2 94.82(7) N1 Si1 Cl2 177.85(6) Cl3 Si1 Cl2 93.45(3) Cl1 Si1 Cl2 92.08(3) C5 N1 C1 119.5(2) C5 N1 Si1 114.81(15) C1 N1 Si1 125.62(15) C7 N2 C6 111.85(15) C7 N2 Si1 127.07(14) C6 N2 Si1 120.99(14) N1 C1 C2 121.4(2) N1 C1 H1 119.3 C2 C1 H1 119.3 C1 C2 C3 119.2(2) C1 C2 H2 120.4 C3 C2 H2 120.4 C4 C3 C2 119.5(2) C4 C3 H3 120.2 C2 C3 H3 120.2 C3 C4 C5 118.6(2) C3 C4 H4 120.7 C5 C4 H4 120.7 N1 C5 C4 121.7(2) N1 C5 C6 112.52(18) C4 C5 C6 125.72(19) N2 C6 C5 108.20(16) N2 C6 H6A 110.1 C5 C6 H6A 110.1 N2 C6 H6B 110.1 C5 C6 H6B 110.1 H6A C6 H6B 108.4 C8 C7 C12 121.66(19) C8 C7 N2 118.94(18) C12 C7 N2 119.37(19) C9 C8 C7 118.3(2) C9 C8 C16 119.2(2) C7 C8 C16 122.46(19) C10 C9 C8 121.1(2) C10 C9 H9 119.4 C8 C9 H9 119.4 C9 C10 C11 119.7(2) C9 C10 H10 120.2 C11 C10 H10 120.2 C10 C11 C12 121.3(2) C10 C11 H11 119.4 C12 C11 H11 119.4 C11 C12 C7 117.9(2) C11 C12 C13 119.9(2) C7 C12 C13 122.2(2) C12 C13 C14 110.6(2) C12 C13 C15 111.9(2) C14 C13 C15 111.6(2) C12 C13 H13 107.5 C14 C13 H13 107.5 C15 C13 H13 107.5 C13 C14 H14A 109.5 C13 C14 H14B 109.5 H14A C14 H14B 109.5 C13 C14 H14C 109.5 H14A C14 H14C 109.5 H14B C14 H14C 109.5 C13 C15 H15A 109.5 C13 C15 H15B 109.5 H15A C15 H15B 109.5 C13 C15 H15C 109.5 H15A C15 H15C 109.5 H15B C15 H15C 109.5 C8 C16 C17 111.54(19) C8 C16 C18 110.90(19) C17 C16 C18 110.9(2) C8 C16 H16 107.8 C17 C16 H16 107.8 C18 C16 H16 107.8 C16 C17 H17A 109.5 C16 C17 H17B 109.5 H17A C17 H17B 109.5 C16 C17 H17C 109.5 H17A C17 H17C 109.5 H17B C17 H17C 109.5 C16 C18 H18A 109.5 C16 C18 H18B 109.5 H18A C18 H18B 109.5 C16 C18 H18C 109.5 H18A C18 H18C 109.5 H18B C18 H18C 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Cl1 Si1 2.1067(9) Cl2 Si1 2.1508(9) Cl3 Si1 2.0885(8) Si1 N2 1.7175(17) Si1 N1 1.964(2) N1 C5 1.338(3) N1 C1 1.357(3) N2 C7 1.443(3) N2 C6 1.452(3) C1 C2 1.366(4) C1 H1 0.9500 C2 C3 1.391(4) C2 H2 0.9500 C3 C4 1.377(3) C3 H3 0.9500 C4 C5 1.388(3) C4 H4 0.9500 C5 C6 1.487(3) C6 H6A 0.9900 C6 H6B 0.9900 C7 C8 1.402(3) C7 C12 1.404(3) C8 C9 1.395(3) C8 C16 1.519(3) C9 C10 1.384(3) C9 H9 0.9500 C10 C11 1.390(4) C10 H10 0.9500 C11 C12 1.396(3) C11 H11 0.9500 C12 C13 1.523(3) C13 C14 1.533(4) C13 C15 1.535(4) C13 H13 1.0000 C14 H14A 0.9800 C14 H14B 0.9800 C14 H14C 0.9800 C15 H15A 0.9800 C15 H15B 0.9800 C15 H15C 0.9800 C16 C17 1.530(3) C16 C18 1.538(3) C16 H16 1.0000 C17 H17A 0.9800 C17 H17B 0.9800 C17 H17C 0.9800 C18 H18A 0.9800 C18 H18B 0.9800 C18 H18C 0.9800 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion N1 Si1 N2 C7 -176.12(19) Cl3 Si1 N2 C7 99.91(18) Cl1 Si1 N2 C7 -93.27(18) Cl2 Si1 N2 C7 2.58(18) N1 Si1 N2 C6 0.29(17) Cl3 Si1 N2 C6 -83.68(17) Cl1 Si1 N2 C6 83.14(17) Cl2 Si1 N2 C6 178.99(16) C5 N1 C1 C2 1.3(3) Si1 N1 C1 C2 -175.97(18) N1 C1 C2 C3 -0.4(4) C1 C2 C3 C4 -1.3(4) C2 C3 C4 C5 2.0(4) C1 N1 C5 C4 -0.6(3) Si1 N1 C5 C4 177.00(17) C1 N1 C5 C6 -178.9(2) Si1 N1 C5 C6 -1.3(2) C3 C4 C5 N1 -1.1(3) C3 C4 C5 C6 177.0(2) C7 N2 C6 C5 175.88(17) Si1 N2 C6 C5 -1.0(2) N1 C5 C6 N2 1.5(3) C4 C5 C6 N2 -176.8(2) C6 N2 C7 C8 -90.0(2) Si1 N2 C7 C8 86.6(2) C6 N2 C7 C12 88.0(2) Si1 N2 C7 C12 -95.3(2) C12 C7 C8 C9 3.3(3) N2 C7 C8 C9 -178.73(18) C12 C7 C8 C16 -177.28(19) N2 C7 C8 C16 0.7(3) C7 C8 C9 C10 -2.1(3) C16 C8 C9 C10 178.4(2) C8 C9 C10 C11 -0.4(3) C9 C10 C11 C12 1.9(3) C10 C11 C12 C7 -0.8(3) C10 C11 C12 C13 179.0(2) C8 C7 C12 C11 -1.8(3) N2 C7 C12 C11 -179.81(18) C8 C7 C12 C13 178.4(2) N2 C7 C12 C13 0.4(3) C11 C12 C13 C14 60.4(3) C7 C12 C13 C14 -119.9(2) C11 C12 C13 C15 -64.7(3) C7 C12 C13 C15 115.1(3) C9 C8 C16 C17 -60.7(3) C7 C8 C16 C17 119.9(2) C9 C8 C16 C18 63.5(3) C7 C8 C16 C18 -115.9(2) loop_ _cod_related_entry_id _cod_related_entry_database _cod_related_entry_code 1 PubChem 139184375