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Information card for entry 7112293
Preview
| Coordinates | 7112293.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C26 H23 N3 O3 |
|---|---|
| Calculated formula | C26 H23 N3 O3 |
| SMILES | N(C(=O)C1=C(N(C(C(=O)Nc2ccccc2)(C1=O)C)c1ccccc1)C)c1ccccc1 |
| Title of publication | Cu(II)-catalyzed cyclization of α-diazo-β-oxoamides with amines leading to pyrrol-3(2H)-ones |
| Authors of publication | Wang, Zikun; Bi, Xihe; Liao, Peiqiu; Liu, Xu; Dong, Dewen |
| Journal of publication | Chemical Communications (Cambridge, United Kingdom) |
| Year of publication | 2013 |
| Journal volume | 49 |
| Journal issue | 13 |
| Pages of publication | 1309 - 1311 |
| a | 11.1712 ± 0.0011 Å |
| b | 12.066 ± 0.0012 Å |
| c | 17.6929 ± 0.0018 Å |
| α | 70.489 ± 0.002° |
| β | 83.942 ± 0.002° |
| γ | 86.093 ± 0.002° |
| Cell volume | 2234 ± 0.4 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0878 |
| Residual factor for significantly intense reflections | 0.0613 |
| Weighted residual factors for significantly intense reflections | 0.1574 |
| Weighted residual factors for all reflections included in the refinement | 0.1748 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.031 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Duplicate of | 7108835 |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|
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Users of the data should acknowledge the original authors of the
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