#------------------------------------------------------------------------------ #$Date: 2026-06-04 18:00:53 +0100 (Thu, 04 Jun 2026) $ #$Revision: 306214 $ #$URL: svn://www.crystallography.net/cod/cif/7/72/10/7721089.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7721089 loop_ _publ_author_name 'Khalaniya, Roman A.' 'Lyssenko, Konstantin A.' 'Shakhmukhametova, Iasmin A.' 'Shuyev, Nikita' 'Mironov, Andrei V.' 'Kulchu, Aleksandr N.' 'Polevik, Alexey O.' 'Samarin, Alexander N.' 'Bogach, Alexey V.' 'Shevelkov, Andrei V.' _publ_section_title ; Completing the triad: synthesis, structure, and magnetic properties of kagome metals Ti3Mn3Sn4Ga and Hf3Mn3Sn4Ga. ; _journal_issue 20 _journal_name_full 'Dalton transactions (Cambridge, England : 2003)' _journal_page_first 8008 _journal_page_last 8015 _journal_paper_doi 10.1039/d6dt00557h _journal_volume 55 _journal_year 2026 _chemical_formula_moiety 'Hf3 Mn3 Sn4 Ga' _chemical_formula_sum 'Ga Hf3 Mn3 Sn4' _chemical_formula_weight 1244.77 _chemical_name_systematic Hf3Mn3Sn4Ga _space_group_crystal_system hexagonal _space_group_IT_number 194 _space_group_name_Hall '-P 6c 2c' _space_group_name_H-M_alt 'P 63/m m c' _audit_block_doi 10.25505/fiz.icsd.cc2r38v0 _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2026-03-05 deposited with the CCDC. 2026-05-20 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 2 _cell_length_a 9.1388(5) _cell_length_b 9.1388(5) _cell_length_c 5.5634(3) _cell_measurement_reflns_used 3027 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 60.853 _cell_measurement_theta_min 5.147 _cell_volume 402.39(4) _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Bruker D8 Quest with Photon III detector' _diffrn_measurement_method '\w and \f scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0573 _diffrn_reflns_av_unetI/netI 0.0243 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 7 _diffrn_reflns_limit_l_min -7 _diffrn_reflns_number 4173 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.427 _diffrn_reflns_theta_min 2.573 _diffrn_source 'microfocus sealed X-ray tube' _exptl_absorpt_coefficient_mu 58.401 _exptl_absorpt_correction_T_max 0.0398 _exptl_absorpt_correction_T_min 0.0113 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_crystal_colour grey _exptl_crystal_density_diffrn 10.274 _exptl_crystal_description 'truncated prism' _exptl_crystal_F_000 1044 _exptl_crystal_preparation 'Magnetic properties' _exptl_crystal_recrystallization_method 'From the Melt' _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.15 _refine_diff_density_max 1.885 _refine_diff_density_min -2.216 _refine_diff_density_rms 0.533 _refine_ls_extinction_coef 0.0039(3) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.339 _refine_ls_hydrogen_treatment undef _refine_ls_matrix_type full _refine_ls_number_parameters 18 _refine_ls_number_reflns 262 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.339 _refine_ls_R_factor_all 0.0241 _refine_ls_R_factor_gt 0.0237 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0031P)^2^+6.8591P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0459 _refine_ls_wR_factor_ref 0.0461 _reflns_Friedel_coverage 0.000 _reflns_number_gt 258 _reflns_number_total 262 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d6dt00557h2.cif _cod_data_source_block Hf3Mn3Sn4Ga _cod_original_cell_volume 402.39(5) _cod_database_code 7721089 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; TITL Hf3Mn3Sn4Ga_a.res in P6(3)/mmc Hf3Mn3Sn4Ga_a.res created by SHELXL-2018/3 at 18:21:26 on 14-Jan-2026 REM Old TITL Hf3Mn3Sn4Ga REM SHELXT solution in P6(3)/mmc: R1 0.084, Rweak 0.005, Alpha 0.013 REM 3.475 for 15 systematic absences, Orientation as input REM Formula found by SHELXT: Hf3 Ga4 Sn4 CELL 0.71073 9.1388 9.1388 5.5634 90.0000 90.0000 120.0000 ZERR 2.000 0.0005 0.0005 0.0003 0.0000 0.0000 0.0000 LATT 1 SYMM -Y, X-Y, Z SYMM -X+Y, -X, Z SYMM -X, -Y, 1/2+Z SYMM Y, -X+Y, 1/2+Z SYMM X-Y, X, 1/2+Z SYMM Y, X, -Z SYMM X-Y, -Y, -Z SYMM -X, -X+Y, -Z SYMM -Y, -X, 1/2-Z SYMM -X+Y, Y, 1/2-Z SYMM X, X-Y, 1/2-Z SFAC HF MN SN GA UNIT 6 6 8 2 LIST 4 TEMP -173.150 L.S. 10 BOND FMAP 2 acta PLAN 20 WGHT 0.003100 6.859100 EXTI 0.003867 FVAR 0.19708 HF 1 0.147540 0.295080 0.250000 10.25000 0.00592 0.00504 = 0.01470 0.00000 0.00000 0.00252 MN 2 0.500000 0.000000 0.000000 10.25000 0.00439 0.00536 = 0.01434 -0.00080 -0.00040 0.00268 SN1 3 0.789206 0.578413 0.250000 10.25000 0.00609 0.00713 = 0.01554 0.00000 0.00000 0.00357 SN2 3 0.333333 0.666667 0.250000 10.08333 0.00463 0.00463 = 0.01664 0.00000 0.00000 0.00231 GA 4 0.000000 0.000000 0.000000 10.08333 0.00472 0.00472 = 0.01588 0.00000 0.00000 0.00236 REM REM Hf3Mn3Sn4Ga_a.hkl REM HKLF 4 REM Hf3Mn3Sn4Ga_a.res in P6(3)/mmc REM wR2 = 0.046086, GooF = S = 1.33914, Restrained GooF = 1.33914 for all data REM R1 = 0.023671 for 258 Fo > 4sig(Fo) and 0.024069 for all 262 data REM 18 parameters refined using 0 restraints END WGHT 0.0032 6.8591 REM Highest difference peak 1.885, deepest hole -2.216, 1-sigma level 0.533 Q1 1 0.0000 0.0000 0.1373 10.16667 0.05 1.89 Q2 1 0.3333 0.6667 -0.1145 10.16667 0.05 1.65 Q3 1 0.5157 0.0314 0.1168 10.50000 0.05 1.62 Q4 1 0.1672 0.3344 0.1531 10.50000 0.05 1.51 Q5 1 0.1702 0.2763 0.1462 11.00000 0.05 1.29 Q6 1 0.3333 0.6667 0.0176 10.16667 0.05 1.25 Q7 1 0.8191 0.6381 0.1451 10.50000 0.05 1.13 Q8 1 0.8605 0.7209 0.0505 10.50000 0.05 1.05 Q9 1 0.7916 0.5832 -0.0193 10.50000 0.05 1.05 Q10 1 0.7584 0.5168 0.1292 10.50000 0.05 0.84 Q11 1 0.3059 0.3655 0.1046 11.00000 0.05 0.83 Q12 1 0.1930 0.0965 0.1282 10.50000 0.05 0.74 Q13 1 0.5827 0.1653 0.1433 10.50000 0.05 0.69 Q14 1 0.9436 0.6530 0.1387 11.00000 0.05 0.67 Q15 1 0.5465 -0.1022 0.1218 11.00000 0.05 0.67 Q16 1 -0.0600 -0.1199 0.2500 10.25000 0.05 0.57 Q17 1 0.0000 0.2195 0.0000 10.50000 0.05 0.54 Q18 1 0.7806 0.4740 0.1416 11.00000 0.05 0.49 Q19 1 0.4213 -0.1574 0.1260 10.50000 0.05 0.49 Q20 1 0.5853 0.0148 0.2500 10.50000 0.05 0.48 ; _shelx_res_checksum 98816 loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-x, -y, z+1/2' 'y, -x+y, z+1/2' 'x-y, x, z+1/2' 'y, x, -z' 'x-y, -y, -z' '-x, -x+y, -z' '-y, -x, -z+1/2' '-x+y, y, -z+1/2' 'x, x-y, -z+1/2' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' 'x, y, -z-1/2' '-y, x-y, -z-1/2' '-x+y, -x, -z-1/2' '-y, -x, z' '-x+y, y, z' 'x, x-y, z' 'y, x, z-1/2' 'x-y, -y, z-1/2' '-x, -x+y, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Hf Hf 0.14754(3) 0.29508(6) 0.250000 0.00865(18) Uani 1 4 d S T P . . Mn Mn 0.500000 0.000000 0.000000 0.0079(3) Uani 1 4 d S T P . . Sn1 Sn 0.78921(5) 0.57841(10) 0.250000 0.0095(2) Uani 1 4 d S T P . . Sn2 Sn 0.333333 0.666667 0.250000 0.0086(3) Uani 1 12 d S T P . . Ga Ga 0.000000 0.000000 0.000000 0.0084(4) Uani 1 12 d S T P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Hf 0.0059(2) 0.0050(2) 0.0147(3) 0.000 0.000 0.00252(12) Mn 0.0044(5) 0.0054(7) 0.0143(9) -0.0008(7) -0.0004(3) 0.0027(3) Sn1 0.0061(3) 0.0071(4) 0.0155(4) 0.000 0.000 0.00357(19) Sn2 0.0046(4) 0.0046(4) 0.0166(7) 0.000 0.000 0.00231(18) Ga 0.0047(6) 0.0047(6) 0.0159(11) 0.000 0.000 0.0024(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Hf Hf -0.5830 6.1852 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mn Mn 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ga Ga 0.2307 1.6083 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _citation_id _citation_doi _citation_year 1 10.1039/d6dt00557h 2026 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Ga Hf Ga 61.552(11) . 4 ? Ga Hf Sn2 149.224(6) . . ? Ga Hf Sn2 149.224(6) 4 . ? Ga Hf Sn1 140.57(2) . 13_666 ? Ga Hf Sn1 79.020(16) 4 13_666 ? Sn2 Hf Sn1 70.204(17) . 13_666 ? Ga Hf Sn1 79.020(16) . 13_665 ? Ga Hf Sn1 140.57(2) 4 13_665 ? Sn2 Hf Sn1 70.204(17) . 13_665 ? Sn1 Hf Sn1 140.41(3) 13_666 13_665 ? Ga Hf Sn1 78.857(12) . 3_565 ? Ga Hf Sn1 78.857(12) 4 3_565 ? Sn2 Hf Sn1 102.999(14) . 3_565 ? Sn1 Hf Sn1 94.369(2) 13_666 3_565 ? Sn1 Hf Sn1 94.369(1) 13_665 3_565 ? Ga Hf Sn1 78.857(12) . 2_655 ? Ga Hf Sn1 78.857(12) 4 2_655 ? Sn2 Hf Sn1 102.999(14) . 2_655 ? Sn1 Hf Sn1 94.369(1) 13_666 2_655 ? Sn1 Hf Sn1 94.369(1) 13_665 2_655 ? Sn1 Hf Sn1 154.00(3) 3_565 2_655 ? Ga Hf Mn 132.297(7) . 6 ? Ga Hf Mn 102.589(4) 4 6 ? Sn2 Hf Mn 58.770(8) . 6 ? Sn1 Hf Mn 53.562(8) 13_666 6 ? Sn1 Hf Mn 104.050(14) 13_665 6 ? Sn1 Hf Mn 145.925(11) 3_565 6 ? Sn1 Hf Mn 53.484(9) 2_655 6 ? Ga Hf Mn 102.589(4) . 3_665 ? Ga Hf Mn 132.297(7) 4 3_665 ? Sn2 Hf Mn 58.770(8) . 3_665 ? Sn1 Hf Mn 104.050(14) 13_666 3_665 ? Sn1 Hf Mn 53.562(7) 13_665 3_665 ? Sn1 Hf Mn 145.925(11) 3_565 3_665 ? Sn1 Hf Mn 53.484(9) 2_655 3_665 ? Mn Hf Mn 52.801(6) 6 3_665 ? Ga Hf Mn 132.297(7) . 5_565 ? Ga Hf Mn 102.589(4) 4 5_565 ? Sn2 Hf Mn 58.770(8) . 5_565 ? Sn1 Hf Mn 53.562(8) 13_666 5_565 ? Sn1 Hf Mn 104.050(14) 13_665 5_565 ? Sn1 Hf Mn 53.484(9) 3_565 5_565 ? Sn1 Hf Mn 145.925(11) 2_655 5_565 ? Mn Hf Mn 93.839(10) 6 5_565 ? Mn Hf Mn 117.539(15) 3_665 5_565 ? Ga Hf Mn 102.589(4) . 2 ? Ga Hf Mn 132.297(7) 4 2 ? Sn2 Hf Mn 58.770(8) . 2 ? Sn1 Hf Mn 104.050(14) 13_666 2 ? Sn1 Hf Mn 53.562(8) 13_665 2 ? Sn1 Hf Mn 53.484(9) 3_565 2 ? Sn1 Hf Mn 145.925(11) 2_655 2 ? Mn Hf Mn 117.539(15) 6 2 ? Mn Hf Mn 93.839(10) 3_665 2 ? Mn Hf Mn 52.801(6) 5_565 2 ? Sn1 Mn Sn1 180.000(16) 15_545 3_665 ? Sn1 Mn Sn1 75.43(3) 15_545 14 ? Sn1 Mn Sn1 104.57(3) 3_665 14 ? Sn1 Mn Sn1 104.57(3) 15_545 2_655 ? Sn1 Mn Sn1 75.43(3) 3_665 2_655 ? Sn1 Mn Sn1 180.00(4) 14 2_655 ? Sn1 Mn Mn 120.433(3) 15_545 4_655 ? Sn1 Mn Mn 59.567(3) 3_665 4_655 ? Sn1 Mn Mn 120.433(3) 14 4_655 ? Sn1 Mn Mn 59.567(3) 2_655 4_655 ? Sn1 Mn Mn 59.567(3) 15_545 4_654 ? Sn1 Mn Mn 120.433(3) 3_665 4_654 ? Sn1 Mn Mn 59.567(3) 14 4_654 ? Sn1 Mn Mn 120.433(3) 2_655 4_654 ? Mn Mn Mn 180.0 4_655 4_654 ? Sn1 Mn Sn2 107.532(10) 15_545 13_665 ? Sn1 Mn Sn2 72.468(10) 3_665 13_665 ? Sn1 Mn Sn2 107.533(10) 14 13_665 ? Sn1 Mn Sn2 72.467(10) 2_655 13_665 ? Mn Mn Sn2 117.798(2) 4_655 13_665 ? Mn Mn Sn2 62.202(2) 4_654 13_665 ? Sn1 Mn Sn2 72.468(10) 15_545 1_545 ? Sn1 Mn Sn2 107.532(10) 3_665 1_545 ? Sn1 Mn Sn2 72.468(10) 14 1_545 ? Sn1 Mn Sn2 107.533(10) 2_655 1_545 ? Mn Mn Sn2 62.202(2) 4_655 1_545 ? Mn Mn Sn2 117.798(2) 4_654 1_545 ? Sn2 Mn Sn2 180.0 13_665 1_545 ? Sn1 Mn Hf 119.770(16) 15_545 2_655 ? Sn1 Mn Hf 60.230(16) 3_665 2_655 ? Sn1 Mn Hf 60.021(9) 14 2_655 ? Sn1 Mn Hf 119.979(9) 2_655 2_655 ? Mn Mn Hf 63.599(3) 4_655 2_655 ? Mn Mn Hf 116.401(3) 4_654 2_655 ? Sn2 Mn Hf 122.520(8) 13_665 2_655 ? Sn2 Mn Hf 57.480(8) 1_545 2_655 ? Sn1 Mn Hf 60.230(16) 15_545 14 ? Sn1 Mn Hf 119.770(16) 3_665 14 ? Sn1 Mn Hf 119.979(9) 14 14 ? Sn1 Mn Hf 60.021(9) 2_655 14 ? Mn Mn Hf 116.401(3) 4_655 14 ? Mn Mn Hf 63.599(3) 4_654 14 ? Sn2 Mn Hf 57.480(8) 13_665 14 ? Sn2 Mn Hf 122.520(8) 1_545 14 ? Hf Mn Hf 180.0 2_655 14 ? Sn1 Mn Hf 119.980(9) 15_545 15_655 ? Sn1 Mn Hf 60.020(9) 3_665 15_655 ? Sn1 Mn Hf 60.229(16) 14 15_655 ? Sn1 Mn Hf 119.771(16) 2_655 15_655 ? Mn Mn Hf 116.400(3) 4_655 15_655 ? Mn Mn Hf 63.600(3) 4_654 15_655 ? Sn2 Mn Hf 57.482(8) 13_665 15_655 ? Sn2 Mn Hf 122.518(8) 1_545 15_655 ? Hf Mn Hf 70.980(14) 2_655 15_655 ? Hf Mn Hf 109.020(14) 14 15_655 ? Sn1 Mn Hf 60.020(9) 15_545 3 ? Sn1 Mn Hf 119.980(9) 3_665 3 ? Sn1 Mn Hf 119.771(16) 14 3 ? Sn1 Mn Hf 60.229(16) 2_655 3 ? Mn Mn Hf 63.600(3) 4_655 3 ? Mn Mn Hf 116.400(3) 4_654 3 ? Sn2 Mn Hf 122.518(8) 13_665 3 ? Sn2 Mn Hf 57.482(8) 1_545 3 ? Hf Mn Hf 109.020(14) 2_655 3 ? Hf Mn Hf 70.980(14) 14 3 ? Hf Mn Hf 180.000(10) 15_655 3 ? Mn Sn1 Mn 60.867(6) 5_665 2_655 ? Mn Sn1 Mn 153.87(3) 5_665 3_665 ? Mn Sn1 Mn 112.624(12) 2_655 3_665 ? Mn Sn1 Mn 112.624(12) 5_665 6 ? Mn Sn1 Mn 153.87(3) 2_655 6 ? Mn Sn1 Mn 60.867(6) 3_665 6 ? Mn Sn1 Hf 66.417(5) 5_665 13_666 ? Mn Sn1 Hf 123.582(4) 2_655 13_666 ? Mn Sn1 Hf 123.584(4) 3_665 13_666 ? Mn Sn1 Hf 66.419(5) 6 13_666 ? Mn Sn1 Hf 123.582(4) 5_665 13_665 ? Mn Sn1 Hf 66.417(5) 2_655 13_665 ? Mn Sn1 Hf 66.419(5) 3_665 13_665 ? Mn Sn1 Hf 123.584(4) 6 13_665 ? Hf Sn1 Hf 140.41(3) 13_666 13_665 ? Mn Sn1 Hf 66.287(10) 5_665 3_665 ? Mn Sn1 Hf 66.287(10) 2_655 3_665 ? Mn Sn1 Hf 137.12(2) 3_665 3_665 ? Mn Sn1 Hf 137.12(2) 6 3_665 ? Hf Sn1 Hf 75.659(16) 13_666 3_665 ? Hf Sn1 Hf 75.659(16) 13_665 3_665 ? Mn Sn1 Hf 137.12(2) 5_665 2_665 ? Mn Sn1 Hf 137.12(2) 2_655 2_665 ? Mn Sn1 Hf 66.286(10) 3_665 2_665 ? Mn Sn1 Hf 66.286(10) 6 2_665 ? Hf Sn1 Hf 75.660(16) 13_666 2_665 ? Hf Sn1 Hf 75.660(16) 13_665 2_665 ? Hf Sn1 Hf 86.00(3) 3_665 2_665 ? Hf Sn2 Hf 120.0 2_665 . ? Hf Sn2 Hf 120.0 2_665 3_565 ? Hf Sn2 Hf 120.0 . 3_565 ? Hf Sn2 Mn 63.749(1) 2_665 4_665 ? Hf Sn2 Mn 152.201(1) . 4_665 ? Hf Sn2 Mn 63.7 3_565 4_665 ? Hf Sn2 Mn 152.201(1) 2_665 2 ? Hf Sn2 Mn 63.750(1) . 2 ? Hf Sn2 Mn 63.7 3_565 2 ? Mn Sn2 Mn 127.499(1) 4_665 2 ? Hf Sn2 Mn 152.201(1) 2_665 5_565 ? Hf Sn2 Mn 63.750(1) . 5_565 ? Hf Sn2 Mn 63.7 3_565 5_565 ? Mn Sn2 Mn 100.006(3) 4_665 5_565 ? Mn Sn2 Mn 55.597(4) 2 5_565 ? Hf Sn2 Mn 63.749(1) 2_665 1_565 ? Hf Sn2 Mn 152.201(1) . 1_565 ? Hf Sn2 Mn 63.7 3_565 1_565 ? Mn Sn2 Mn 55.597(4) 4_665 1_565 ? Mn Sn2 Mn 100.006(3) 2 1_565 ? Mn Sn2 Mn 127.499(1) 5_565 1_565 ? Hf Sn2 Mn 63.750(1) 2_665 6 ? Hf Sn2 Mn 63.7 . 6 ? Hf Sn2 Mn 152.201(1) 3_565 6 ? Mn Sn2 Mn 100.006(2) 4_665 6 ? Mn Sn2 Mn 127.499(1) 2 6 ? Mn Sn2 Mn 100.006(2) 5_565 6 ? Mn Sn2 Mn 127.499(1) 1_565 6 ? Hf Sn2 Mn 63.750(1) 2_665 3_665 ? Hf Sn2 Mn 63.750(1) . 3_665 ? Hf Sn2 Mn 152.201(1) 3_565 3_665 ? Mn Sn2 Mn 127.499(1) 4_665 3_665 ? Mn Sn2 Mn 100.006(2) 2 3_665 ? Mn Sn2 Mn 127.499(1) 5_565 3_665 ? Mn Sn2 Mn 100.006(3) 1_565 3_665 ? Mn Sn2 Mn 55.597(4) 6 3_665 ? Hf Ga Hf 180.000(16) 15 3 ? Hf Ga Hf 83.842(7) 15 . ? Hf Ga Hf 96.158(7) 3 . ? Hf Ga Hf 96.158(7) 15 13 ? Hf Ga Hf 83.842(7) 3 13 ? Hf Ga Hf 180.0 . 13 ? Hf Ga Hf 83.842(7) 15 2 ? Hf Ga Hf 96.158(7) 3 2 ? Hf Ga Hf 96.158(7) . 2 ? Hf Ga Hf 83.843(7) 13 2 ? Hf Ga Hf 96.158(7) 15 14 ? Hf Ga Hf 83.842(7) 3 14 ? Hf Ga Hf 83.842(7) . 14 ? Hf Ga Hf 96.157(7) 13 14 ? Hf Ga Hf 180.000(16) 2 14 ? Hf Ga Ga 120.777(6) 15 4 ? Hf Ga Ga 59.223(6) 3 4 ? Hf Ga Ga 59.224(6) . 4 ? Hf Ga Ga 120.776(6) 13 4 ? Hf Ga Ga 59.224(6) 2 4 ? Hf Ga Ga 120.776(6) 14 4 ? Hf Ga Ga 59.223(6) 15 4_554 ? Hf Ga Ga 120.777(6) 3 4_554 ? Hf Ga Ga 120.776(5) . 4_554 ? Hf Ga Ga 59.224(6) 13 4_554 ? Hf Ga Ga 120.776(6) 2 4_554 ? Hf Ga Ga 59.224(6) 14 4_554 ? Ga Ga Ga 180.0 4 4_554 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Hf Ga 2.7182(4) . ? Hf Ga 2.7182(4) 4 ? Hf Sn2 2.9409(5) . ? Hf Sn1 2.9564(4) 13_666 ? Hf Sn1 2.9564(4) 13_665 ? Hf Sn1 2.9656(6) 3_565 ? Hf Sn1 2.9656(6) 2_655 ? Hf Mn 3.1280(3) 6 ? Hf Mn 3.1280(3) 3_665 ? Hf Mn 3.1280(3) 5_565 ? Hf Mn 3.1280(3) 2 ? Mn Sn1 2.7458(2) 15_545 ? Mn Sn1 2.7458(2) 3_665 ? Mn Sn1 2.7458(2) 14 ? Mn Sn1 2.7458(2) 2_655 ? Mn Mn 2.78170(15) 4_655 ? Mn Mn 2.78170(15) 4_654 ? Mn Sn2 2.98235(13) 13_665 ? Mn Sn2 2.98235(13) 1_545 ? Ga Ga 2.78170(15) 4 ? Ga Ga 2.78170(15) 4_554 ?